CN103992856B - The anti-oxidant efficient wire drawing oil of a kind of spacetabs type - Google Patents
The anti-oxidant efficient wire drawing oil of a kind of spacetabs type Download PDFInfo
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- CN103992856B CN103992856B CN201410170024.1A CN201410170024A CN103992856B CN 103992856 B CN103992856 B CN 103992856B CN 201410170024 A CN201410170024 A CN 201410170024A CN 103992856 B CN103992856 B CN 103992856B
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Abstract
The present invention relates to a kind of wire drawing oil, be specifically related to the anti-oxidant efficient wire drawing oil of a kind of spacetabs type, wire drawing oil of the present invention is made up of the raw material of following weight portion: isooctyl oleate 30-40, silicone emulsion 20-30, soybean oil 60-80, lanonol 4-6, APES 12-14, Calcium Disodium Versenate 1-2, triphenyl phosphate 1-2, starch Sodium Octenyl Succinate 2-3, lipoic acid 1-2, molybdenum dialkyl-dithiophosphate 0.5-1, deionized water are appropriate, auxiliary agent 2-3; The present invention utilizes starch Sodium Octenyl Succinate to make the aqueous solution of easy film forming, also be dispersed in uniformly in base oil coated high-efficiency anti-oxidant lipoic acid, make the antioxidant that discharges that it slowly continues, extend the service life of wire drawing oil, wire drawing oil prepared by the present invention has good greasy property, wire-drawing effect is good, is difficult for blackout and bubbles, environment-friendly high-efficiency.
Description
Technical field
The present invention relates to a kind of wire drawing oil, be specifically related to the anti-oxidant efficient wire drawing oil of a kind of spacetabs type and preparation technology thereof.
Background technology
Wire drawing oil is the important industrial auxiliary agent of a class, in wire drawing, drawing process process, does efficient lubricant oil use, has lubricated, cleaning, the effect such as cooling, antirust, assists metal flow, avoids mould to drag colored bracing wire, improves yield rate, reduces production loss. Existing wire drawing oil is mainly divided into oiliness wire drawing oil and water-based wire drawing oil, this two classes wire drawing oil cuts both ways in the time that reality is used, as oiliness wire drawing oil exists heat dispersion poor, cleaning chip removal difficulty, the problems such as waste liquid difficult degradation, and although the wire drawing oil heat dispersion of water-based is good compared with oiliness wire drawing oil, but lubricant effect is not fully up to expectations, the wire drawing that is difficult to meet various metals line is drawn and is dialled technological requirement, therefore for improve enterprise machined level, reduce production costs, need to improve wire drawing oil formula and technique, make it reach good serviceability.
Summary of the invention
The object of the invention is to, provide a kind of spacetabs type anti-oxidant efficient wire drawing oil, to achieve these goals, the technical solution used in the present invention is as follows:
The anti-oxidant efficient wire drawing oil of a kind of spacetabs type, it is characterized in that, material of the present invention is made up of the raw material of following weight portion: isooctyl oleate 30-40, silicone emulsion 20-30, soybean oil 60-80, lanonol 4-6, APES 12-14, Calcium Disodium Versenate 1-2, triphenyl phosphate 1-2, starch Sodium Octenyl Succinate 2-3, lipoic acid 1-2, molybdenum dialkyl-dithiophosphate 0.5-1, deionized water are appropriate, auxiliary agent 2-3; Described auxiliary agent is made up of the raw material of following weight portion: Graphene 1-2, silane coupler KH5600.1-0.2, isostearic acid 15-18, xanthans 10-12, sorbester p17 4-5, deionized water are appropriate; Preparation method is: first by Graphene and silane coupler mixed grinding 10-15min, the powder obtaining mixes with isostearic acid, sorbester p17, under the rotating speed of 1000-1500 rev/min, stir 20-30min, make emulsion for subsequent use, then xanthans is mixed with appropriate deionized water, be mixed with the xanthan gum solution that mass concentration is 60-70%, finally the aqueous solution, emulsion are mixed, continue to stir 15-20min with 1000-1500 rev/min of rotating speed, stir and finish rear standing 2-4h, to obtain final product.
The anti-oxidant efficient wire drawing oil of described a kind of spacetabs type, its preparation technology is:
(1) first starch Sodium Octenyl Succinate is dissolved in appropriate deionized water, being made into mass concentration is the starch Sodium Octenyl Succinate aqueous solution of 70-80%, adds subsequently lipoic acid, mix and blend 20-30min, solution for standby;
(2) isooctyl oleate, silicone emulsion, soybean oil are mixed, be heated to 50-60 DEG C, add APES, lanonol, mix and blend 30-40min, add subsequently step (1) gained solution and other leftover materials, continue to stir 40-50min, after stirring finishes, through naturally cooling to room temperature, get product.
The wire drawing oil advantage that the present invention prepares is: lipoic acid is the high-efficiency antioxidant agent of a class safety, can effectively prevent lipid oxidation, in order more to fully play its antioxidation, the present invention utilizes starch Sodium Octenyl Succinate to make the aqueous solution of easy film forming, the lipoic acid dissolving is wherein coated, this solution can form film at oil-water interfaces, thereby the particulate that contains lipoic acid is dispersed in base oil uniformly, what make that the product oil of preparation can slowly continue discharges antioxidant, increase the service life, again in conjunction with other class additive, wire drawing oil prepared by the present invention has good greasy property, wire-drawing effect is good, being difficult for blackout bubbles, environment-friendly high-efficiency.
Detailed description of the invention
Embodiment
The present embodiment wire drawing oil by following weight portion (kilogram) raw material make: isooctyl oleate 40, silicone emulsion 20, soybean oil 80, lanonol 4, APES 14, Calcium Disodium Versenate 1, triphenyl phosphate 2, starch Sodium Octenyl Succinate 2, lipoic acid 2, molybdenum dialkyl-dithiophosphate 0.5, deionized water are appropriate, auxiliary agent 3; Described auxiliary agent is made up of the raw material of following weight portion: Graphene 1, silane coupler KH5600.2, isostearic acid 15, xanthans 10, sorbester p17 4, deionized water are appropriate; Preparation method is: first by Graphene and silane coupler mixed grinding 15min, the powder obtaining mixes with isostearic acid, sorbester p17, under the rotating speed of 1500 revs/min, stir 20min, make emulsion for subsequent use, then xanthans is mixed with appropriate deionized water, be mixed with mass concentration and be 60% xanthan gum solution, finally the aqueous solution, emulsion are mixed, continue to stir 15min with 1500 revs/min of rotating speeds, stir and finish rear standing 2h, to obtain final product.
The anti-oxidant efficient wire drawing oil of described a kind of spacetabs type, its preparation technology is:
(1) first starch Sodium Octenyl Succinate is dissolved in appropriate deionized water, being made into mass concentration is the starch Sodium Octenyl Succinate aqueous solution of 70-80%, adds subsequently lipoic acid, mix and blend 30min, solution for standby;
(2) isooctyl oleate, silicone emulsion, soybean oil are mixed, be heated to 50-60 DEG C, add APES, lanonol, mix and blend 40min, add subsequently step (1) gained solution and other leftover materials, continue to stir 50min, after stirring finishes, through naturally cooling to room temperature, get product.
Wire drawing oil of the present invention can stablize at ambient temperature deposit at least one year, during this time without precipitating, lamination; Concrete each performance indications are as follows:
| Project | Index |
| Kinematic viscosity (100 DEG C) | 15-18mm2/s |
| Condensation point | ≤-5℃ |
| Flash-point (opening) | ≥240℃ |
| 5% emulsion pH value | 6.8 |
| 5% emulsion corrosion (55 ± 2) DEG C, soaks copper sheet 24h entirely | Corrosion-free |
| Rust-preventing characteristic (35 ± 2) DEG C, copper scale 2h | Qualified |
| 5% emulsion stability (15-35 DEG C) 4h | Without layering, without precipitation, separate out without soap, oil |
| PBValue/N | 580 |
Claims (2)
1. the anti-oxidant efficient wire drawing oil of spacetabs type, it is characterized in that, this wire drawing oil is made up of the raw material of following weight portion: isooctyl oleate 30-40, silicone emulsion 20-30, soybean oil 60-80, lanonol 4-6, APES 12-14, Calcium Disodium Versenate 1-2, triphenyl phosphate 1-2, starch Sodium Octenyl Succinate 2-3, lipoic acid 1-2, molybdenum dialkyl-dithiophosphate 0.5-1, deionized water are appropriate, auxiliary agent 2-3; Described auxiliary agent is made up of the raw material of following weight portion: Graphene 1-2, silane coupler KH5600.1-0.2, isostearic acid 15-18, xanthans 10-12, sorbester p17 4-5, deionized water are appropriate; Preparation method is: first by Graphene and silane coupler mixed grinding 10-15min, the powder obtaining mixes with isostearic acid, sorbester p17, under the rotating speed of 1000-1500 rev/min, stir 20-30min, make emulsion for subsequent use, then xanthans is mixed with appropriate deionized water, be mixed with the xanthan gum solution that mass concentration is 60-70%, finally the aqueous solution, emulsion are mixed, continue to stir 15-20min with 1000-1500 rev/min of rotating speed, stir and finish rear standing 2-4h, to obtain final product.
2. the anti-oxidant efficient wire drawing oil of a kind of spacetabs type as claimed in claim 1, its preparation technology is as follows:
(1) first starch Sodium Octenyl Succinate is dissolved in appropriate deionized water, being made into mass concentration is the starch Sodium Octenyl Succinate aqueous solution of 70-80%, adds subsequently lipoic acid, mix and blend 20-30min, solution for standby;
(2) isooctyl oleate, silicone emulsion, soybean oil are mixed, be heated to 50-60 DEG C, add APES, lanonol, mix and blend 30-40min, add subsequently step (1) gained solution and other leftover materials, continue to stir 40-50min, after stirring finishes, through naturally cooling to room temperature, get product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410170024.1A CN103992856B (en) | 2014-04-25 | 2014-04-25 | The anti-oxidant efficient wire drawing oil of a kind of spacetabs type |
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| CN201410170024.1A CN103992856B (en) | 2014-04-25 | 2014-04-25 | The anti-oxidant efficient wire drawing oil of a kind of spacetabs type |
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| CN103992856A CN103992856A (en) | 2014-08-20 |
| CN103992856B true CN103992856B (en) | 2016-05-11 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018138246A1 (en) * | 2017-01-27 | 2018-08-02 | Oleon Nv | Dimer diol dilipoate and use thereof as an additive |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104277899B (en) * | 2014-09-25 | 2016-08-24 | 苏州长盛机电有限公司 | Environment-friendly metal cutting fluid and preparation method thereof |
| CN106867645B (en) * | 2017-02-04 | 2020-01-31 | 北京康普锡威科技有限公司 | graphene-containing drawing fluid and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1197108A (en) * | 1997-04-18 | 1998-10-28 | 郭紫鸣 | Aluminium wiredrawing lubricating grease |
| CN1319649A (en) * | 2001-02-23 | 2001-10-31 | 华南理工大学 | Method for making high-effiicent environment protection energy-saving metal wire-drawing solution |
| CN101838579A (en) * | 2010-03-31 | 2010-09-22 | 江西圣达威电工材料有限公司 | Special aluminum wire drawing oil used for aluminum wires and production method thereof |
| CN103614218A (en) * | 2013-10-21 | 2014-03-05 | 全威（铜陵）铜业科技有限公司 | Synthetic base wire drawing liquid and preparation method thereof |
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2014
- 2014-04-25 CN CN201410170024.1A patent/CN103992856B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1197108A (en) * | 1997-04-18 | 1998-10-28 | 郭紫鸣 | Aluminium wiredrawing lubricating grease |
| CN1319649A (en) * | 2001-02-23 | 2001-10-31 | 华南理工大学 | Method for making high-effiicent environment protection energy-saving metal wire-drawing solution |
| CN101838579A (en) * | 2010-03-31 | 2010-09-22 | 江西圣达威电工材料有限公司 | Special aluminum wire drawing oil used for aluminum wires and production method thereof |
| CN103614218A (en) * | 2013-10-21 | 2014-03-05 | 全威（铜陵）铜业科技有限公司 | Synthetic base wire drawing liquid and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018138246A1 (en) * | 2017-01-27 | 2018-08-02 | Oleon Nv | Dimer diol dilipoate and use thereof as an additive |
| FR3062387A1 (en) * | 2017-01-27 | 2018-08-03 | Oleon Nv | DILIPOATE OF DIMERE (S) DIOL AND USE THEREOF AS ADDITIVE |
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| Publication number | Publication date |
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| CN103992856A (en) | 2014-08-20 |
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Inventor after: Li Yanguo Inventor before: Zhu Xingtang Inventor before: Zhu Liangliang Inventor before: Chen Junyan |
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Effective date of registration: 20170717 Address after: 300000 Tianjin City Jizhou District of Tianjin Special Automobile Industrial Park East Golden Street on the north side (500KV Corridor West) Patentee after: Shengbaolu oil chemical (Tianjin) Limited by Share Ltd Address before: 233010 Bengbu high tech Development Zone, Anhui Province Road No. 555 Patentee before: Bengbu Times Electronics Co., Ltd. |
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