CN103992862B - A kind of oil of the wire drawing containing Yelkin TTS - Google Patents
A kind of oil of the wire drawing containing Yelkin TTS Download PDFInfo
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- CN103992862B CN103992862B CN201410172480.XA CN201410172480A CN103992862B CN 103992862 B CN103992862 B CN 103992862B CN 201410172480 A CN201410172480 A CN 201410172480A CN 103992862 B CN103992862 B CN 103992862B
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- oil
- wire drawing
- yelkin tts
- mixed
- present
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- 238000005491 wire drawing Methods 0.000 title claims abstract description 35
- LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 claims abstract description 22
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229940074391 gallic acid Drugs 0.000 claims abstract description 11
- 235000004515 gallic acid Nutrition 0.000 claims abstract description 11
- 229920002545 silicone oil Polymers 0.000 claims abstract description 9
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 8
- SAUIGQBKPDQYHL-QXMHVHEDSA-N 6-methylheptyl (z)-octadec-9-enoate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCCCCCC(C)C SAUIGQBKPDQYHL-QXMHVHEDSA-N 0.000 claims abstract description 7
- 235000011187 glycerol Nutrition 0.000 claims abstract description 7
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims abstract description 7
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims abstract description 7
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 6
- RNMDNPCBIKJCQP-UHFFFAOYSA-N 5-nonyl-7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-ol Chemical compound C(CCCCCCCC)C1=C2C(=C(C=C1)O)O2 RNMDNPCBIKJCQP-UHFFFAOYSA-N 0.000 claims abstract description 4
- -1 polyoxyethylene nonylphenol Polymers 0.000 claims abstract description 4
- WSFQLUVWDKCYSW-UHFFFAOYSA-M sodium;2-hydroxy-3-morpholin-4-ylpropane-1-sulfonate Chemical compound [Na+].[O-]S(=O)(=O)CC(O)CN1CCOCC1 WSFQLUVWDKCYSW-UHFFFAOYSA-M 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 18
- 235000010493 xanthan gum Nutrition 0.000 claims description 9
- 239000000230 xanthan gum Substances 0.000 claims description 9
- 229920001285 xanthan gum Polymers 0.000 claims description 9
- 229940082509 xanthan gum Drugs 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 238000002360 preparation method Methods 0.000 claims description 7
- QMMJWQMCMRUYTG-UHFFFAOYSA-N 1,2,4,5-tetrachloro-3-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=C(Cl)C(Cl)=CC(Cl)=C1Cl QMMJWQMCMRUYTG-UHFFFAOYSA-N 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical class CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 6
- 239000000839 emulsion Substances 0.000 claims description 6
- 229910021389 graphene Inorganic materials 0.000 claims description 6
- 238000005516 engineering process Methods 0.000 claims description 5
- 239000000243 solution Substances 0.000 claims description 4
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 3
- 239000003921 oil Substances 0.000 abstract description 29
- 238000000034 method Methods 0.000 abstract description 5
- 229910052751 metal Inorganic materials 0.000 abstract description 4
- 239000002184 metal Substances 0.000 abstract description 4
- 238000005461 lubrication Methods 0.000 abstract description 3
- 150000002739 metals Chemical class 0.000 abstract description 3
- 229910000831 Steel Inorganic materials 0.000 abstract description 2
- 239000000654 additive Substances 0.000 abstract description 2
- 230000003670 easy-to-clean Effects 0.000 abstract description 2
- 239000003995 emulsifying agent Substances 0.000 abstract description 2
- 230000001804 emulsifying effect Effects 0.000 abstract description 2
- 239000010959 steel Substances 0.000 abstract description 2
- 230000000996 additive effect Effects 0.000 abstract 1
- 239000002199 base oil Substances 0.000 abstract 1
- 231100000252 nontoxic Toxicity 0.000 abstract 1
- 230000003000 nontoxic effect Effects 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 3
- 239000000314 lubricant Substances 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Abstract
The present invention relates to a kind of wire drawing oil, be specifically related to a kind of wire drawing containing Yelkin TTS oil, wire drawing oil of the present invention is made up of the raw material of following weight part: Oleum Cocois 80-100, fluorinated silicone oil 60-80, polyvinylpyrrolidone 0.01-0.02, isooctyl oleate 10-12, Yelkin TTS 8-10, gallic acid 0.2-0.3, glycerine 2-3, zinc naphthenate 0.5-0.6, polyoxyethylene nonylphenol ether 0.4-0.5, clorafin 0.5-1, auxiliary agent 2-3; Wire drawing oil of the present invention with the addition of the fluorinated silicone oil of heatproof in base oil, and using nontoxic Yelkin TTS as emulsifying agent, obtain good emulsifying effect, again in conjunction with other additive, wire drawing of the present invention oil is made to have excellent extreme-pressure wear-resistant performance and high temperature lubrication property, and not corrode steel bar when using, modest viscosity, easy to clean, the wire drawing of various metals material can be applicable to, drawing process is used.
Description
Technical field
The present invention relates to a kind of wire drawing oil, be specifically related to a kind of wire drawing containing Yelkin TTS oil and preparation technology thereof.
Background technology
Wire drawing oil is the important commercial auxiliaries of a class, in wire drawing, drawing process process, do efficient lubricant oil use, has lubrication, cleaning, cooling, the effect such as antirust, assists metal flow, avoid mould to drag colored bracing wire, improve yield rate, reduce production loss.Existing wire drawing oil is mainly divided into oiliness wire drawing oil and water-based wire drawing oil, this two classes wire drawing oil cuts both ways when reality uses, as oiliness wire drawing oil exists heat dispersion difference, cleaning chip removal difficulty, the problems such as waste liquid difficult degradation, and although the wire drawing of water-based oil heat dispersion is excellent compared with oiliness wire drawing oil, but lubricant effect is not fully up to expectations, group processing requirement is drawn in the wire drawing being difficult to meet various metals line, therefore in order to improve machining level, the reduction production cost of enterprise, need to improve wire drawing oil formula and technique, make it reach good use properties.
Summary of the invention
The object of the invention is to, provide a kind of wire drawing containing Yelkin TTS oil, the technical solution used in the present invention is as follows:
A kind of oil of the wire drawing containing Yelkin TTS, it is characterized in that, material of the present invention is made up of the raw material of following weight part: Oleum Cocois 80-100, fluorinated silicone oil 60-80, polyvinylpyrrolidone 0.01-0.02, isooctyl oleate 10-12, Yelkin TTS 8-10, gallic acid 0.2-0.3, glycerine 2-3, zinc naphthenate 0.5-0.6, polyoxyethylene nonylphenol ether 0.4-0.5, clorafin 0.5-1, auxiliary agent 2-3; Described auxiliary agent is made up of the raw material of following weight part: butyl stearate 12-15, Graphene 1-2, Starso 1-2, xanthan gum 10-12, ethoxylated dodecyl alcohol 4-5, deionized water are appropriate; Preparation method is: first will add ethoxylated dodecyl alcohol, Graphene in butyl stearate, 20-30min is stirred under 1000-1500 rev/min, make emulsion for subsequent use, again xanthan gum is mixed with appropriate deionized water, be mixed with the xanthan gum solution that mass concentration is 60-70%, finally the aqueous solution, emulsion and other remaining component mixed, continue to stir 15-20min with 1000-1500 rev/min of rotating speed, stirring terminates rear standing 2-4h, to obtain final product.
Described a kind of oil of the wire drawing containing Yelkin TTS, its preparation technology is:
(1) first polyvinylpyrrolidone is mixed with isooctyl oleate, for subsequent use after fully stirring 20-25min;
(2) mixed with glycerine by gallic acid, be stirred well to gallic acid and dissolve completely, mixed solution is for subsequent use;
(3) Oleum Cocois, fluorinated silicone oil are mixed and heated to 50-60 DEG C, add Yelkin TTS, after stirring 30-40min, add step (1), step (2) gained material and other remaining component again, continue to stir 50-80min, naturally cool to room temperature after stirring terminates, get product.
The wire drawing oil that the present invention prepares, oil based on Oleum Cocois and fluorinated silicone oil mixing, impart the heat resistance that wire drawing of the present invention oil is excellent, environmentally friendly, and using Yelkin TTS as emulsifying agent, the lubricity of this wire drawing oil can not only be improved, and emulsifying effectiveness is stablized, lubricant effect is more lasting, again in conjunction with gallic acid, the additives such as clorafin, wire drawing of the present invention oil is made to have excellent extreme-pressure wear-resistant performance and high temperature lubrication property, not corrode steel bar during use, stable chemical performance, modest viscosity, easy to clean, the wire drawing of various metals material can be applicable to, drawing process is used.
Embodiment
Embodiment
The present embodiment wire drawing oil is made up of the raw material of following weight part (kilogram): Oleum Cocois 100, fluorinated silicone oil 60, polyvinylpyrrolidone 0.02, isooctyl oleate 10, Yelkin TTS 8, gallic acid 0.2, glycerine 2, zinc naphthenate 0.5, polyoxyethylene nonylphenol ether 0.5, clorafin 1, auxiliary agent 3; Described auxiliary agent is made up of the raw material of following weight part: butyl stearate 15, Graphene 1, Starso 2, xanthan gum 10, ethoxylated dodecyl alcohol 4, deionized water are appropriate; Preparation method is: first will add ethoxylated dodecyl alcohol, Graphene in butyl stearate, 20min is stirred under 1500 revs/min, make emulsion for subsequent use, again xanthan gum is mixed with appropriate deionized water, be mixed with the xanthan gum solution that mass concentration is 70%, finally the aqueous solution, emulsion and other remaining component mixed, continue to stir 15min with 1500 revs/min of rotating speeds, stirring terminates rear standing 3h, to obtain final product.
Described a kind of oil of the wire drawing containing Yelkin TTS, its preparation technology is:
(1) first polyvinylpyrrolidone is mixed with isooctyl oleate, for subsequent use after fully stirring 25min;
(2) mixed with glycerine by gallic acid, be stirred well to gallic acid and dissolve completely, mixed solution is for subsequent use;
(3) Oleum Cocois, fluorinated silicone oil are mixed and heated to 50-60 DEG C, add Yelkin TTS, after stirring 40min, add step (1), step (2) gained material and other remaining component again, continue to stir 60min, naturally cool to room temperature after stirring terminates, get product.
Wire drawing oil of the present invention can be stablized at ambient temperature and deposits at least one year, and period is without precipitation, demixing phenomenon; Concrete each performance index are as follows:
Claims (2)
1. the oil of the wire drawing containing Yelkin TTS, it is characterized in that, this wire drawing oil is made up of the raw material of following weight part: Oleum Cocois 80-100, fluorinated silicone oil 60-80, polyvinylpyrrolidone 0.01-0.02, isooctyl oleate 10-12, Yelkin TTS 8-10, gallic acid 0.2-0.3, glycerine 2-3, zinc naphthenate 0.5-0.6, polyoxyethylene nonylphenol ether 0.4-0.5, clorafin 0.5-1, auxiliary agent 2-3; Described auxiliary agent is made up of the raw material of following weight part: butyl stearate 12-15, Graphene 1-2, Starso 1-2, xanthan gum 10-12, ethoxylated dodecyl alcohol 4-5, deionized water are appropriate; The preparation method of described auxiliary agent is: first will add ethoxylated dodecyl alcohol, Graphene in butyl stearate, 20-30min is stirred under 1000-1500 rev/min, make emulsion for subsequent use, again xanthan gum is mixed with appropriate deionized water, be mixed with the xanthan gum solution that mass concentration is 60-70%, finally the aqueous solution, emulsion and other remaining component mixed, continue to stir 15-20min with 1000-1500 rev/min of rotating speed, stirring terminates rear standing 2-4h, to obtain final product.
2. a kind of wire drawing containing Yelkin TTS is oily as claimed in claim 1, and its preparation technology is as follows: polyvinylpyrrolidone first mixes with isooctyl oleate by (1), for subsequent use after fully stirring 20-25min; (2) mixed with glycerine by gallic acid, be stirred well to gallic acid and dissolve completely, mixed solution is for subsequent use; (3) Oleum Cocois, fluorinated silicone oil are mixed and heated to 50-60 DEG C, add Yelkin TTS, after stirring 30-40min, add step (1), step (2) gained material and other remaining component again, continue to stir 50-80min, stir after terminating and naturally cool to room temperature, get product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410172480.XA CN103992862B (en) | 2014-04-25 | 2014-04-25 | A kind of oil of the wire drawing containing Yelkin TTS |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410172480.XA CN103992862B (en) | 2014-04-25 | 2014-04-25 | A kind of oil of the wire drawing containing Yelkin TTS |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103992862A CN103992862A (en) | 2014-08-20 |
| CN103992862B true CN103992862B (en) | 2016-04-13 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410172480.XA Active CN103992862B (en) | 2014-04-25 | 2014-04-25 | A kind of oil of the wire drawing containing Yelkin TTS |
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| Country | Link |
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| CN (1) | CN103992862B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105695069A (en) * | 2016-02-25 | 2016-06-22 | 天津高盛钢丝绳有限公司 | Lubricant for wet-type wire-drawing technology for steel wire ropes |
| CN112048364A (en) * | 2020-09-16 | 2020-12-08 | 江苏赢新润滑科技有限公司 | Environment-friendly water-soluble stainless steel wire drawing liquid |
| CN115537259B (en) * | 2022-09-15 | 2023-11-03 | 湖北省化学工业研究设计院 | Water-based lubricant for stainless steel wire drawing and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1197108A (en) * | 1997-04-18 | 1998-10-28 | 郭紫鸣 | Aluminium wiredrawing lubricating grease |
| CN1319649A (en) * | 2001-02-23 | 2001-10-31 | 华南理工大学 | Method for making high-effiicent environment protection energy-saving metal wire-drawing solution |
| CN101838579A (en) * | 2010-03-31 | 2010-09-22 | 江西圣达威电工材料有限公司 | Special aluminum wire drawing oil used for aluminum wires and production method thereof |
-
2014
- 2014-04-25 CN CN201410172480.XA patent/CN103992862B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1197108A (en) * | 1997-04-18 | 1998-10-28 | 郭紫鸣 | Aluminium wiredrawing lubricating grease |
| CN1319649A (en) * | 2001-02-23 | 2001-10-31 | 华南理工大学 | Method for making high-effiicent environment protection energy-saving metal wire-drawing solution |
| CN101838579A (en) * | 2010-03-31 | 2010-09-22 | 江西圣达威电工材料有限公司 | Special aluminum wire drawing oil used for aluminum wires and production method thereof |
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| Publication number | Publication date |
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| CN103992862A (en) | 2014-08-20 |
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| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Drawing oil containing lecithin Effective date of registration: 20191206 Granted publication date: 20160413 Pledgee: Bengbu Science and Technology Financing Guarantee Co., Ltd. Pledgor: Bengbu Zhengyuan Electronic Technology Co., Ltd. Registration number: Y2019990000670 |
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Address after: 233000 No. 1259 Changqing South Road, hi tech Zone, Anhui, Bengbu Patentee after: Bengbu Zhengyuan Electronic Technology Co., Ltd Address before: 233000 No. 1259 Changqing South Road, hi tech Zone, Anhui, Bengbu Patentee before: BENGBU ZHENGYUAN ELECTRONIC TECHNOLOGY Co.,Ltd. |
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Date of cancellation: 20220107 Granted publication date: 20160413 Pledgee: Bengbu Science and Technology Financing Guarantee Co.,Ltd. Pledgor: BENGBU ZHENGYUAN ELECTRONIC TECHNOLOGY Co.,Ltd. Registration number: Y2019990000670 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
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Denomination of invention: A drawing oil containing lecithin Effective date of registration: 20220228 Granted publication date: 20160413 Pledgee: Bengbu Science and Technology Financing Guarantee Co.,Ltd. Pledgor: Bengbu Zhengyuan Electronic Technology Co.,Ltd. Registration number: Y2022980001890 |