CN103992868A - High temperature resistant high speed wire drawing oil - Google Patents
High temperature resistant high speed wire drawing oil Download PDFInfo
- Publication number
- CN103992868A CN103992868A CN201410174126.0A CN201410174126A CN103992868A CN 103992868 A CN103992868 A CN 103992868A CN 201410174126 A CN201410174126 A CN 201410174126A CN 103992868 A CN103992868 A CN 103992868A
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- Prior art keywords
- wire drawing
- oil
- parts
- drawing oil
- high temperature
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- 238000005491 wire drawing Methods 0.000 title claims abstract description 40
- 239000003921 oil Substances 0.000 claims abstract description 35
- QIQXTHQIDYTFRH-UHFFFAOYSA-N Stearic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 16
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 claims abstract description 9
- ZWYAVGUHWPLBGT-UHFFFAOYSA-N bis(6-methylheptyl) decanedioate Chemical compound CC(C)CCCCCOC(=O)CCCCCCCCC(=O)OCCCCCC(C)C ZWYAVGUHWPLBGT-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000004359 castor oil Substances 0.000 claims abstract description 9
- 235000019438 castor oil Nutrition 0.000 claims abstract description 9
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 8
- 239000008117 stearic acid Substances 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 7
- -1 polydecylene Polymers 0.000 claims abstract description 6
- 235000019387 fatty acid methyl ester Nutrition 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 21
- 229920001285 xanthan gum Polymers 0.000 claims description 9
- 239000000230 xanthan gum Substances 0.000 claims description 9
- 229940082509 xanthan gum Drugs 0.000 claims description 9
- 235000010493 xanthan gum Nutrition 0.000 claims description 9
- 238000002360 preparation method Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 210000000582 Semen Anatomy 0.000 claims description 7
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 7
- IGWHDMPTQKSDTL-JXOAFFINSA-N [(2R,3S,4R,5R)-3,4-dihydroxy-5-(5-methyl-2,4-dioxopyrimidin-1-yl)oxolan-2-yl]methyl dihydrogen phosphate Chemical compound O=C1NC(=O)C(C)=CN1[C@H]1[C@H](O)[C@H](O)[C@@H](COP(O)(O)=O)O1 IGWHDMPTQKSDTL-JXOAFFINSA-N 0.000 claims description 7
- 150000001336 alkenes Chemical class 0.000 claims description 7
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 238000005984 hydrogenation reaction Methods 0.000 claims description 7
- 238000005987 sulfurization reaction Methods 0.000 claims description 7
- ULBTUVJTXULMLP-UHFFFAOYSA-N butyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCCC ULBTUVJTXULMLP-UHFFFAOYSA-N 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 6
- 239000000839 emulsion Substances 0.000 claims description 6
- SFNALCNOMXIBKG-UHFFFAOYSA-N ethylene glycol monododecyl ether Chemical compound CCCCCCCCCCCCOCCO SFNALCNOMXIBKG-UHFFFAOYSA-N 0.000 claims description 6
- 229910021389 graphene Inorganic materials 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 238000005516 engineering process Methods 0.000 claims description 5
- MGIYRDNGCNKGJU-UHFFFAOYSA-N Isothiazolinone Chemical compound O=C1C=CSN1 MGIYRDNGCNKGJU-UHFFFAOYSA-N 0.000 claims description 4
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 4
- 239000000243 solution Substances 0.000 claims description 4
- 229940043253 Butylated Hydroxyanisole Drugs 0.000 claims description 3
- CZBZUDVBLSSABA-UHFFFAOYSA-N Butylated hydroxyanisole Chemical compound COC1=CC=C(O)C(C(C)(C)C)=C1.COC1=CC=C(O)C=C1C(C)(C)C CZBZUDVBLSSABA-UHFFFAOYSA-N 0.000 claims description 3
- 239000004255 Butylated hydroxyanisole Substances 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 235000019282 butylated hydroxyanisole Nutrition 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 6
- 239000000654 additive Substances 0.000 abstract description 2
- 239000002199 base oil Substances 0.000 abstract description 2
- 150000001875 compounds Chemical class 0.000 abstract description 2
- 238000003860 storage Methods 0.000 abstract description 2
- 235000019198 oils Nutrition 0.000 abstract 7
- PILWLJVFXLZGMS-UHFFFAOYSA-N 3-octyl-1,2-thiazol-4-one Chemical compound CCCCCCCCC1=NSCC1=O PILWLJVFXLZGMS-UHFFFAOYSA-N 0.000 abstract 2
- 235000012343 cottonseed oil Nutrition 0.000 abstract 2
- 239000002385 cottonseed oil Substances 0.000 abstract 2
- LEACJMVNYZDSKR-UHFFFAOYSA-N 2-octyldodecan-1-ol Chemical compound CCCCCCCCCCC(CO)CCCCCCCC LEACJMVNYZDSKR-UHFFFAOYSA-N 0.000 abstract 1
- 230000000844 anti-bacterial Effects 0.000 abstract 1
- 238000005260 corrosion Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 3
- 239000000314 lubricant Substances 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000004059 degradation Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000001376 precipitating Effects 0.000 description 1
- 230000001954 sterilising Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Abstract
The invention relates to a wire drawing oil, and in particular relates to a high temperature resistant high speed wire drawing oil; the high temperature resistant high speed wire drawing oil comprises the following raw materials by weight: 2-3 parts of stearic acid, 10-12 parts of 2-octyldodecanol, 2-4 parts of trimethylolpropane, 60-80 parts of di-iso-octyl sebacate, 65-70 parts of hydrogenated polydecylene, 5-6 parts of hydrogenated castor oil, 5-8 parts of sulfurized cottonseed oil, 1-2 parts of fatty acid methyl ester, 0.2-0.5 part of octyl isothiazolinone, 1-2 parts of butyl hydroxy anisd and 2-3 parts of an assistant; the high temperature resistant high speed wire drawing oil uses the di-iso-octyl sebacate and the hydrogenated polydecylene as base oil, by combination with the hydrogenated castor oil, sulfurized cottonseed oil, the trimethylolpropane and other additives, extreme pressure antiwear performance of the wire drawing oil can be greatly improved, the octyl isothiazolinone is a green bactericidal anti-corrosion compound, and makes the wire drawing oil more resistant to storage, the prepared wire drawing oil is particularly prominent in thermal stability, and is especially suitable for high speed wire drawing and drawing process needs.
Description
Technical field
The present invention relates to a kind of wire drawing oil, be specifically related to a kind of high temperature-resistant high-speed wire drawing oil and preparation technology thereof.
Background technology
Wire drawing oil is the important industrial auxiliary agent of a class, in wire drawing, drawing process process, does efficient lubricant oil use, has lubricated, cleaning, the effect such as cooling, antirust, assists metal flow, avoids mould to drag colored bracing wire, improves yield rate, reduces production loss.Existing wire drawing oil is mainly divided into oiliness wire drawing oil and water-based wire drawing oil, this two classes wire drawing oil cuts both ways in the time that reality is used, as oiliness wire drawing oil exists heat dispersion poor, cleaning chip removal difficulty, the problems such as waste liquid difficult degradation, and although the wire drawing oil heat dispersion of water-based is good compared with oiliness wire drawing oil, but lubricant effect is not fully up to expectations, the wire drawing that is difficult to meet various metals line is drawn and is dialled processing requirement, therefore for improve enterprise machining level, reduce production costs, need to improve wire drawing oil formula and technique, make it reach good use properties.
Summary of the invention
The object of the invention is to, a kind of high temperature-resistant high-speed wire drawing oil is provided, to improve the resistance toheat of wire drawing oil, improve drawing speed, to achieve these goals, the technical solution used in the present invention is as follows:
A kind of high temperature-resistant high-speed wire drawing oil, it is characterized in that, material of the present invention is made up of the raw material of following weight part: stearic acid 2-3,2-Standamul G 10-12, TriMethylolPropane(TMP) 2-4, diisooctyl sebacate 60-80, hydrogenation poly-certain herbaceous plants with big flowers alkene 65-70, hydrogenated castor oil 5-6, sulfuration Oleum Gossypii semen 5-8, fatty acid methyl ester 1-2, octyl group isothiazolinone 0.2-0.5, butylated hydroxy anisole 1-2, auxiliary agent 2-3; Described auxiliary agent is made up of the raw material of following weight part: butyl stearate 12-15, Graphene 1-2, Starso 1-2, xanthan gum 10-12, ethoxylated dodecyl alcohol 4-5, deionized water are appropriate; Preparation method is: first will in butyl stearate, add ethoxylated dodecyl alcohol, Graphene, under 1000-1500 rev/min, stir 20-30min, make emulsion for subsequent use, again xanthan gum is mixed with appropriate deionized water, be mixed with the xanthan gum solution that mass concentration is 60-70%, finally the aqueous solution, emulsion and other remaining component mixed, continue to stir 15-20min with 1000-1500 rev/min of rotating speed, stirring finishes rear standing 2-4h, to obtain final product.
Described a kind of high temperature-resistant high-speed wire drawing oil, its preparation technology is:
(1) first stearic acid, 2-Standamul G, TriMethylolPropane(TMP) are mixed, fully stir 20-30min, mixture is for subsequent use;
(2) hydrogenated castor oil is heated to 75-85 DEG C, add the mixture of diisooctyl sebacate, the poly-certain herbaceous plants with big flowers alkene of hydrogenation, sulfuration Oleum Gossypii semen and step (1) gained, stir 20-30min, leave standstill after 10-15min, add again other remaining component, continue to stir 50-60min, after stirring finishes, naturally cool to room temperature, get product.
Wire drawing oil advantage prepared by the present invention is: use the poly-certain herbaceous plants with big flowers alkene of resistant to elevated temperatures diisooctyl sebacate and hydrogenation as base oil, give wire drawing oil good resistance to elevated temperatures, go back cost economical rationality simultaneously, lubricant effect is good, coordinate again hydrogenated castor oil, sulfuration Oleum Gossypii semen and stearic acid, the additives such as TriMethylolPropane(TMP), improve greatly the extreme pressure and antiwear behavior of wire drawing oil, not oxidizable, good heat stability, octyl group isothiazolinone is a kind of sterilization and anticorrosion compound of green, make the more resistance to storage of wire drawing oil of preparation, in sum, wire drawing oil of the present invention shows particularly outstanding on thermal stability, can be applicable to the wire drawing of various metals wire rod, drawing process is used, especially can meet high-speed wire-drawing, the demand of drawing process.
Embodiment
Embodiment
The present embodiment wire drawing oil by following weight part (kilogram) raw material make: the poly-certain herbaceous plants with big flowers alkene 70 of stearic acid 2,2-Standamul G 12, TriMethylolPropane(TMP) 4, diisooctyl sebacate 80, hydrogenation, hydrogenated castor oil 5, sulfuration Oleum Gossypii semen 8, fatty acid methyl ester 1, octyl group isothiazolinone 0.5, butylated hydroxy anisole 1, auxiliary agent 3; Described auxiliary agent is made up of the raw material of following weight part: butyl stearate 15, Graphene 1, Starso 2, xanthan gum 10, ethoxylated dodecyl alcohol 4, deionized water are appropriate; Preparation method is: first will in butyl stearate, add ethoxylated dodecyl alcohol, Graphene, under 1500 revs/min, stir 20min, make emulsion for subsequent use, again xanthan gum is mixed with appropriate deionized water, be mixed with mass concentration and be 70% xanthan gum solution, finally the aqueous solution, emulsion and other remaining component are mixed, continue to stir 15min with 1500 revs/min of rotating speeds, stirring finishes rear standing 3h, to obtain final product.
Described a kind of high temperature-resistant high-speed wire drawing oil, its preparation technology is:
(1) first stearic acid, 2-Standamul G, TriMethylolPropane(TMP) are mixed, fully stir 30min, mixture is for subsequent use;
(2) hydrogenated castor oil is heated to 75-85 DEG C, add the mixture of diisooctyl sebacate, the poly-certain herbaceous plants with big flowers alkene of hydrogenation, sulfuration Oleum Gossypii semen and step (1) gained, stir 30min, leave standstill after 10min, add again other remaining component, continue to stir 60min, after stirring finishes, naturally cool to room temperature, get product.
Wire drawing oil of the present invention can stablize at ambient temperature deposit at least one year, during this time without precipitating, demixing phenomenon; Concrete each performance index are as follows:
Claims (2)
1. a high temperature-resistant high-speed wire drawing oil, it is characterized in that, this wire drawing oil is made up of the raw material of following weight part: stearic acid 2-3,2-Standamul G 10-12, TriMethylolPropane(TMP) 2-4, diisooctyl sebacate 60-80, hydrogenation poly-certain herbaceous plants with big flowers alkene 65-70, hydrogenated castor oil 5-6, sulfuration Oleum Gossypii semen 5-8, fatty acid methyl ester 1-2, octyl group isothiazolinone 0.2-0.5, butylated hydroxy anisole 1-2, auxiliary agent 2-3; Described auxiliary agent is made up of the raw material of following weight part: butyl stearate 12-15, Graphene 1-2, Starso 1-2, xanthan gum 10-12, ethoxylated dodecyl alcohol 4-5, deionized water are appropriate; Preparation method is: first will in butyl stearate, add ethoxylated dodecyl alcohol, Graphene, under 1000-1500 rev/min, stir 20-30min, make emulsion for subsequent use, again xanthan gum is mixed with appropriate deionized water, be mixed with the xanthan gum solution that mass concentration is 60-70%, finally the aqueous solution, emulsion and other remaining component mixed, continue to stir 15-20min with 1000-1500 rev/min of rotating speed, stirring finishes rear standing 2-4h, to obtain final product.
2. a kind of high temperature-resistant high-speed wire drawing oil as claimed in claim 1, its preparation technology is as follows:
(1) first stearic acid, 2-Standamul G, TriMethylolPropane(TMP) are mixed, fully stir 20-30min, mixture is for subsequent use;
(2) hydrogenated castor oil is heated to 75-85 DEG C, add the mixture of diisooctyl sebacate, the poly-certain herbaceous plants with big flowers alkene of hydrogenation, sulfuration Oleum Gossypii semen and step (1) gained, stir 20-30min, leave standstill after 10-15min, add again other remaining component, continue to stir 50-60min, after stirring finishes, naturally cool to room temperature, get product.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201410174126.0A CN103992868A (en) | 2014-04-25 | 2014-04-25 | High temperature resistant high speed wire drawing oil |
Applications Claiming Priority (1)
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CN201410174126.0A CN103992868A (en) | 2014-04-25 | 2014-04-25 | High temperature resistant high speed wire drawing oil |
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CN103992868A true CN103992868A (en) | 2014-08-20 |
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Family Applications (1)
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CN201410174126.0A Pending CN103992868A (en) | 2014-04-25 | 2014-04-25 | High temperature resistant high speed wire drawing oil |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105886095A (en) * | 2016-05-10 | 2016-08-24 | 安徽九华金润铜业有限公司 | Drawing oil for enamelled wire |
CN105925357A (en) * | 2016-05-10 | 2016-09-07 | 安徽九华金润铜业有限公司 | Low-density drawing oil used for red copper tube |
CN105969502A (en) * | 2016-05-10 | 2016-09-28 | 安徽九华金润铜业有限公司 | Drawing oil for quick drawing of enameled wire |
CN112980555A (en) * | 2021-03-04 | 2021-06-18 | 天津市弘亚润滑粉制造有限公司 | Wire drawing soap for dry wire drawing |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20080318820A1 (en) * | 2004-11-01 | 2008-12-25 | Nippon Oil Corporation | Oil Composition for Use in Trace Oil Supply Cutting/Grinding Work |
CN101386804A (en) * | 2008-10-11 | 2009-03-18 | 佛山市威奇电工材料有限公司 | Drawing oil special for aluminum wire and production process thereof |
CN101838579A (en) * | 2010-03-31 | 2010-09-22 | 江西圣达威电工材料有限公司 | Special aluminum wire drawing oil used for aluminum wires and production method thereof |
-
2014
- 2014-04-25 CN CN201410174126.0A patent/CN103992868A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20080318820A1 (en) * | 2004-11-01 | 2008-12-25 | Nippon Oil Corporation | Oil Composition for Use in Trace Oil Supply Cutting/Grinding Work |
CN101386804A (en) * | 2008-10-11 | 2009-03-18 | 佛山市威奇电工材料有限公司 | Drawing oil special for aluminum wire and production process thereof |
CN101838579A (en) * | 2010-03-31 | 2010-09-22 | 江西圣达威电工材料有限公司 | Special aluminum wire drawing oil used for aluminum wires and production method thereof |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105886095A (en) * | 2016-05-10 | 2016-08-24 | 安徽九华金润铜业有限公司 | Drawing oil for enamelled wire |
CN105925357A (en) * | 2016-05-10 | 2016-09-07 | 安徽九华金润铜业有限公司 | Low-density drawing oil used for red copper tube |
CN105969502A (en) * | 2016-05-10 | 2016-09-28 | 安徽九华金润铜业有限公司 | Drawing oil for quick drawing of enameled wire |
CN112980555A (en) * | 2021-03-04 | 2021-06-18 | 天津市弘亚润滑粉制造有限公司 | Wire drawing soap for dry wire drawing |
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Effective date of abandoning: 20170201 |
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