CN103614219A - High-temperature wire drawing lubricant and preparation method thereof - Google Patents
High-temperature wire drawing lubricant and preparation method thereof Download PDFInfo
- Publication number
- CN103614219A CN103614219A CN201310494278.4A CN201310494278A CN103614219A CN 103614219 A CN103614219 A CN 103614219A CN 201310494278 A CN201310494278 A CN 201310494278A CN 103614219 A CN103614219 A CN 103614219A
- Authority
- CN
- China
- Prior art keywords
- parts
- lubricant
- preparation
- wire drawing
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Lubricants (AREA)
Abstract
The invention discloses a high-temperature wire drawing lubricant and a preparation method thereof. The lubricant and the preparation method are characterized in that: the lubricant is prepared from following raw materials by weight: 2-3 parts of sodium dodecyl benzene sulfonate, 1-2 parts of boric acid, 2-3 parts of triethanolamine borate, 1-2 parts of ricinoleic acid polyester, 12-15 parts of ricinus oil, 1-2 parts of a polyoxyethylene alkyl ether, 10-12 parts of glycol, 1-2 parts of citric acid, 1-2 parts of triethanolamine oleate soap, 10-14 parts of an antiwear agent and 1000 parts of water; nano aluminium nitride powder is added into the antiwear agent, thus promoting heat dissipation so that cooling effects are good, enhancing the film-forming property and prolonging the service lifetime of a wire drawing die; the lubricant can resolve issues of extreme-pressure wear resistance, resistance to high-temperature oxidation, surface rust protection, and the like of metal wires at high-temperature environments; the method is simple and the cost is reduced; problems of failure at high temperature, etc. of conventional lubricants are solved; and the lubricant is suitable for wire drawing processes of various metals and alloys.
Description
Technical field
The present invention relates to metal manufacture field, particularly a kind of high-temperature fiber drawing consistent agent and preparation method thereof.
Background technology
Metal wire-drawing is repeatedly with sand paper, aluminium sheet to be scraped to the manufacturing processed of lines, and the main flow process of its technique is divided into de-ester, sand mill, 3 parts of washing.In wire drawing processing procedure, the special epithelium technology after anodizing, can make metallic surface generate a kind of skin membrane that contains this metal ingredient, clearly manifests the trickle sleek of each root, thereby makes to glow in metal dumb light fine and closely woven hair gloss.In recent years, the metal shell of increasing product has all been used metal wire-drawing technique, attractive in appearance to play, erosion-resistant effect.Make product have both fashion and scientific and technological element.This is also one of reason of enjoying great popularity of this technique.
In stress metal processing. make under external force metal pass through by force mould, metal cross section is long-pending compressed, and the technology working method that obtains desired cross-sectional area shape and size is called metal wire-drawing technique. and make it change shape. the instrument of size is called wortle
In existing drawing process, the lubricating oil that adopts is as wire drawing medium more, and conductive line surfaces that drawing goes out is mellow and full, fine and smooth, smooth, bright, no-sundries is detained, wire broken rate reduction, and quality product improves greatly.But lubricating oil heat radiation is slow, damage mould, affect quality product, simultaneously easily ignite oil product or oil evaporation is smoldered cause site environment deterioration of high temperature.
Summary of the invention
For the problems referred to above, the present invention proposes a kind of good heat dissipation, and lubricity is good, high-temperature fiber drawing consistent agent of improving the quality of products and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
A kind of high-temperature fiber drawing consistent agent and preparation method thereof, is made by the raw material of following weight part: Sodium dodecylbenzene sulfonate 2-3, boric acid 1-2, trolamine boric acid ester 2-3, ricinolic acid polyester 1-2, Viscotrol C 12-15, fatty alcohol-polyoxyethylene ether 1-2, ethylene glycol 10-12, citric acid 1-2, triethanolamine oleate 1-2, anti-wear agent 10-14, water 1000;
Described anti-wear agent is made by the raw material of following weight part: diatomite 2.4-2.7, jade 1.2-1.4, urotropine 2.0-2.3, urea 0.4-0.7, silane resin acceptor kh-550 1.0-1.2, Sodium dodecylbenzene sulfonate 0.1-0.2, xitix 1-2, SULPHUR POWDER 1-2, nano aluminum nitride powder 1.2-1.4, water 60; Preparation method is that just jade, diatomite are sent in 540-570 ℃ of calcining furnace, calcining 2-3 hour, cooling rear pulverizing is put into 10-15% hydrochloric acid soln and is soaked 2-3 hour, take out, washes clean, dries and grinds 250-400 order powder, mixes with other remaining component, be heated to 70-75 ℃, under 1200-1500 rev/min, stir 45-60 minute.
High-temperature fiber drawing consistent agent of the present invention, is made by following concrete steps: Sodium dodecylbenzene sulfonate, Viscotrol C, triethanolamine oleate are added to water, be heated to 65-70 ℃; Add again trolamine boric acid ester, ricinolic acid polyester, stirring reaction 30-45 minute; Finally add anti-wear agent and other remaining component, 800-1000 rev/min of lower stirring reaction 60-90 minute, obtains.
Anti-wear agent of the present invention adds nano aluminum nitride powder and plays promotion thermolysis, and good cooling results, has increased film-forming properties, and has extended the work-ing life of wortle; The problem such as the invention solves that the extreme pressure of wire under hot environment is wear-resisting, resistance to high temperature oxidation, surface are antirust; While side sends out simple, and cost lowers, and efficiently solves the problems such as high temperature failure of traditional lubrication agent, is applicable to the drawing process of various metals and alloy.
Specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of high-temperature fiber drawing consistent agent and preparation method thereof, by following weight part (kilogram) raw material make: Sodium dodecylbenzene sulfonate 2, boric acid 1, trolamine boric acid ester 2, ricinolic acid polyester 1, Viscotrol C 12, fatty alcohol-polyoxyethylene ether 1, ethylene glycol 10, citric acid 1, triethanolamine oleate 1, anti-wear agent 10, water 1000;
Described anti-wear agent by following weight part (kilogram) raw material make: diatomite 2.4, jade 1.2, urotropine 2.0, urea 0.4, silane resin acceptor kh-550 1.0, Sodium dodecylbenzene sulfonate 0.1, xitix 1, SULPHUR POWDER 1, nano aluminum nitride powder 1.2, water 60; Preparation method is that just jade, diatomite are sent in 540-570 ℃ of calcining furnace, calcining 2-3 hour, cooling rear pulverizing is put into 10-15% hydrochloric acid soln and is soaked 2-3 hour, take out, washes clean, dries and grinds 250-400 order powder, mixes with other remaining component, be heated to 70-75 ℃, under 1200-1500 rev/min, stir 45-60 minute.
High-temperature fiber drawing consistent agent of the present invention, is made by following concrete steps: Sodium dodecylbenzene sulfonate, Viscotrol C, triethanolamine oleate are added to water, be heated to 65-70 ℃; Add again trolamine boric acid ester, ricinolic acid polyester, stirring reaction 30-45 minute; Finally add anti-wear agent and other remaining component, 800-1000 rev/min of lower stirring reaction 60-90 minute, obtains.
Use wire drawing liquid of the present invention, the highest drawing speed can reach 19m/sec.The copper wire rust prevention during manufacture time of producing is more than 5 days; Concentrating the oil sump drain period is 3 years, and the unit oil sump drain period is 8 months, has reduced liquid waste disposal and discharge, has protected environment.
Claims (2)
1. high-temperature fiber drawing consistent agent and preparation method thereof, is characterized in that, by the raw material of following weight part, is made:
Sodium dodecylbenzene sulfonate 2-3, boric acid 1-2, trolamine boric acid ester 2-3, ricinolic acid polyester 1-2, Viscotrol C 12-15, fatty alcohol-polyoxyethylene ether 1-2, ethylene glycol 10-12, citric acid 1-2, triethanolamine oleate 1-2, anti-wear agent 10-14, water 1000;
Described anti-wear agent is made by the raw material of following weight part: diatomite 2.4-2.7, jade 1.2-1.4, urotropine 2.0-2.3, urea 0.4-0.7, silane resin acceptor kh-550 1.0-1.2, Sodium dodecylbenzene sulfonate 0.1-0.2, xitix 1-2, SULPHUR POWDER 1-2, nano aluminum nitride powder 1.2-1.4, water 60; Preparation method is that just jade, diatomite are sent in 540-570 ℃ of calcining furnace, calcining 2-3 hour, cooling rear pulverizing is put into 10-15% hydrochloric acid soln and is soaked 2-3 hour, take out, washes clean, dries and grinds 250-400 order powder, mixes with other remaining component, be heated to 70-75 ℃, under 1200-1500 rev/min, stir 45-60 minute.
2. according to high-temperature fiber drawing consistent agent described in claims 1, it is characterized in that, by following concrete steps, made: Sodium dodecylbenzene sulfonate, Viscotrol C, triethanolamine oleate are added to water, be heated to 65-70 ℃; Add again trolamine boric acid ester, ricinolic acid polyester, stirring reaction 30-45 minute; Finally add anti-wear agent and other remaining component, 800-1000 rev/min of lower stirring reaction 60-90 minute, obtains.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310494278.4A CN103614219A (en) | 2013-10-21 | 2013-10-21 | High-temperature wire drawing lubricant and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310494278.4A CN103614219A (en) | 2013-10-21 | 2013-10-21 | High-temperature wire drawing lubricant and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103614219A true CN103614219A (en) | 2014-03-05 |
Family
ID=50164939
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310494278.4A Pending CN103614219A (en) | 2013-10-21 | 2013-10-21 | High-temperature wire drawing lubricant and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103614219A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104450120A (en) * | 2014-10-30 | 2015-03-25 | 苏州禾川化学技术服务有限公司 | Semi-synthetic metal wire drawing lubricant liquid and preparation method thereof |
| CN105441168A (en) * | 2015-11-30 | 2016-03-30 | 蚌埠市华科机电有限责任公司 | Friction improved lubricating oil |
| CN105969502A (en) * | 2016-05-10 | 2016-09-28 | 安徽九华金润铜业有限公司 | Drawing oil for quick drawing of enameled wire |
| CN106398821A (en) * | 2016-08-30 | 2017-02-15 | 宝捷润滑油镇江有限公司 | Preparation method of plant oil-based lubricating oil |
| CN106479623A (en) * | 2016-08-30 | 2017-03-08 | 宝捷润滑油镇江有限公司 | The preparation method of the lubricating oil based on plant base artificial oil |
| CN108913308A (en) * | 2018-08-06 | 2018-11-30 | 蒙城县望槐信息科技有限责任公司 | A kind of Novel material lubricant processing flow and its formula |
| CN111411009A (en) * | 2019-12-13 | 2020-07-14 | 贵州水钢同鑫晟金属制品有限公司 | Metal drawing lubricant and preparation method thereof |
| CN111530951A (en) * | 2020-04-03 | 2020-08-14 | 贵州水钢同鑫晟金属制品有限公司 | Steel wire drawing method |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101240217A (en) * | 2008-02-29 | 2008-08-13 | 益田润石（北京）化工有限公司 | Micro-emulsion type metal cutting liquor composition |
| CN101531946A (en) * | 2009-04-22 | 2009-09-16 | 上海应用技术学院 | Metal cutting solution of green semi-synthesis double-base oil and preparation method thereof |
| WO2012166615A1 (en) * | 2011-05-27 | 2012-12-06 | Howard University | Hybrid nanolubricant |
-
2013
- 2013-10-21 CN CN201310494278.4A patent/CN103614219A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101240217A (en) * | 2008-02-29 | 2008-08-13 | 益田润石（北京）化工有限公司 | Micro-emulsion type metal cutting liquor composition |
| CN101531946A (en) * | 2009-04-22 | 2009-09-16 | 上海应用技术学院 | Metal cutting solution of green semi-synthesis double-base oil and preparation method thereof |
| WO2012166615A1 (en) * | 2011-05-27 | 2012-12-06 | Howard University | Hybrid nanolubricant |
Non-Patent Citations (1)
| Title |
|---|
| 周雍鑫，周俊: "《金属加工液使用指南》", 31 May 2000 * |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104450120A (en) * | 2014-10-30 | 2015-03-25 | 苏州禾川化学技术服务有限公司 | Semi-synthetic metal wire drawing lubricant liquid and preparation method thereof |
| CN105441168A (en) * | 2015-11-30 | 2016-03-30 | 蚌埠市华科机电有限责任公司 | Friction improved lubricating oil |
| CN105969502A (en) * | 2016-05-10 | 2016-09-28 | 安徽九华金润铜业有限公司 | Drawing oil for quick drawing of enameled wire |
| CN106398821A (en) * | 2016-08-30 | 2017-02-15 | 宝捷润滑油镇江有限公司 | Preparation method of plant oil-based lubricating oil |
| CN106479623A (en) * | 2016-08-30 | 2017-03-08 | 宝捷润滑油镇江有限公司 | The preparation method of the lubricating oil based on plant base artificial oil |
| CN108913308A (en) * | 2018-08-06 | 2018-11-30 | 蒙城县望槐信息科技有限责任公司 | A kind of Novel material lubricant processing flow and its formula |
| CN111411009A (en) * | 2019-12-13 | 2020-07-14 | 贵州水钢同鑫晟金属制品有限公司 | Metal drawing lubricant and preparation method thereof |
| CN111411009B (en) * | 2019-12-13 | 2021-11-23 | 贵州水钢同鑫晟金属制品有限公司 | Metal drawing lubricant and preparation method thereof |
| CN111530951A (en) * | 2020-04-03 | 2020-08-14 | 贵州水钢同鑫晟金属制品有限公司 | Steel wire drawing method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103614219A (en) | High-temperature wire drawing lubricant and preparation method thereof | |
| CN103614221A (en) | Copper wire drawing lubricating fluid and preparation method thereof | |
| CN103614204A (en) | Metal drawing oil and preparation method thereof | |
| CN103351916A (en) | Aluminium wiredrawing lubricant and preparation method thereof | |
| CN102094146B (en) | Novel high-temperature resistant self-lubricating sliding bearing material and preparation method thereof | |
| CN103614214A (en) | Alloy wire drawing lubricant and preparation method thereof | |
| CN103614226A (en) | Aluminium-alloy wire drawing lubricating fluid and preparation method thereof | |
| CN106367172A (en) | Wire drawing lubricant used in copper wire and preparing method of lubricant | |
| CN103614203A (en) | Aluminium drawing fluid and preparation method thereof | |
| CN105647631A (en) | A lubricating fluid for high-speed fine wire drawing of copper wires and a preparing method thereof | |
| CN102052450B (en) | Technology for casting transfer case casing of concrete pump truck through aluminum alloy | |
| CN103695087B (en) | Lubricant for cold die forging of copper and copper alloy metal plates | |
| CN103614206A (en) | Metal drawing lubricating fluid and preparation method thereof | |
| CN105312559A (en) | Abrasion resistant oil-containing bearing and manufacturing method thereof | |
| CN104450070A (en) | Warm forging lubricant composition of tungsten and tungsten alloy | |
| CN103614227A (en) | High-grade high-speed copper wire drawing lubricant and preparation method thereof | |
| CN103614212A (en) | A wire drawing lubricant and a preparation method thereof | |
| CN104450074A (en) | Stainless steel hot-forging lubricant composition | |
| CN103614213A (en) | High-speed wire drawing lubricant used for drawing metal wires and preparation method of the lubricant | |
| CN103614201A (en) | Copper wire drawing fluid added with anti-grinding agent and preparation method thereof | |
| CN103614208A (en) | Copper drawing fluid and preparation method thereof | |
| CN104479819A (en) | Composition of aluminum and aluminum alloy hot forging lubricant | |
| CN103468380B (en) | A kind of aluminium wiredrawing lubricating grease | |
| CN103614215A (en) | Aluminium-wire high-speed fine wire drawing lubricating fluid and preparation method thereof | |
| CN103614228A (en) | Stainless steel wire drawing liquid lubricant and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20140305 |