CN103614221A - Copper wire drawing lubricating fluid and preparation method thereof - Google Patents
Copper wire drawing lubricating fluid and preparation method thereof Download PDFInfo
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- CN103614221A CN103614221A CN201310494280.1A CN201310494280A CN103614221A CN 103614221 A CN103614221 A CN 103614221A CN 201310494280 A CN201310494280 A CN 201310494280A CN 103614221 A CN103614221 A CN 103614221A
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Abstract
The invention discloses a copper wire drawing lubricating fluid and a preparation method thereof. The lubricating fluid and the preparation method are characterized in that: the lubricating fluid is prepared from following raw materials by weight: 15-25 parts of palm oil, 2-3 parts of sodium petroleum sulfonate, 30-35 parts of polyethylene glycol, 1-2 parts of sulfurized calcium alkyl phenolate, 1-2 parts of a sodium naphthenate, 2-3 parts of a water soluble phosphate ester, 1-2 parts of sodium benzoate, 2-3 parts of triethanolamine oleate, 0.2-0.4 part of diamond nanoparticles, 10-14 parts of an antiwear agent and 1000 parts of water; nano aluminium nitride powder is added into the antiwear agent, thus promoting heat dissipation, enhancing cooling effects, enhancing film-forming property and prolonging the service lifetime; the service cycle of the lubricating fluid is long; and copper wires after wire drawing processes have significant characteristics of shining surfaces, capability of being stored for a long time, difficult surface oxidation, simple manufacturing technology, low technical requirements, and the like.
Description
Technical field
The present invention relates to metal manufacture field, particularly a kind of Copper Drawing Fluid and preparation method thereof.
Background technology
Drawing process is a kind of metal working process.In stress metal processing. make under external force metal by force by mould, metal cross section is long-pending compressed, and the technology working method that obtains desired cross-sectional area shape and size is called metal wire-drawing technique.Make it change shape. the instrument of size is called wortle.
At present, produce many producers suds class wire drawing oil that adopts when drawing core of electric wire more, mainly utilize the alkalescence of suds to play clean core, also have in addition lubricating function.But there is following shortcoming in it: because the lubrication of suds does not make by force and easily product and mould, do not damage; The alkalescence of suds is heavier, makes the product of drawing oxidizable rotten, affects the quality of finished product.And state's other places wire drawing oil production is expensive, greatly increased production cost.
Summary of the invention
The object of the invention is to propose a kind ofly provides a kind of lubricated and to clean cooling good, copper line surface light after wire drawing, and the shelf-time, long surface was not oxidizable, general on large, medium and small type drawing wire machine, and economical and practical Copper Drawing Fluid and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
A kind of Copper Drawing Fluid and preparation method thereof, is made by the raw material of following weight part: plam oil 15-25, petroleum sodium sulfonate 2-3, polyoxyethylene glycol 30-35, calcium sulfenyl phenolate 1-2, sodium napthionate 1-2, water-soluble phosphate 2-3, Sodium Benzoate 1-2, triethanolamine oleate 2-3, diamond nano particulate 0.2-0.4, anti-wear agent 10-14, water 1000;
Described anti-wear agent is made by the raw material of following weight part: diatomite 2.4-2.7, jade 1.2-1.4, urotropine 2.0-2.3, urea 0.4-0.7, silane resin acceptor kh-550 1.0-1.2, Sodium dodecylbenzene sulfonate 0.1-0.2, xitix 1-2, SULPHUR POWDER 1-2, nano aluminum nitride powder 1.2-1.4, water 60; Preparation method is that just jade, diatomite are sent in 540-570 ℃ of calcining furnace, calcining 2-3 hour, cooling rear pulverizing is put into 10-15% hydrochloric acid soln and is soaked 2-3 hour, take out, washes clean, dries and grinds 250-400 order powder, mixes with other remaining component, be heated to 70-75 ℃, under 1200-1500 rev/min, stir 45-60 minute.
Copper Drawing Fluid of the present invention, is made by following concrete steps: plam oil, petroleum sodium sulfonate, polyoxyethylene glycol, calcium sulfenyl phenolate are added to water, be heated to 65-70 ℃; Add again water-soluble phosphate, triethanolamine oleate, stirring reaction 30-45 minute; Finally add anti-wear agent and other remaining component, 800-1000 rev/min of lower stirring reaction 60-90 minute, obtains.
Anti-wear agent of the present invention adds nano aluminum nitride powder and plays promotion thermolysis, has promoted cooling performance, has increased film-forming properties, has extended the work-ing life of wortle; And life cycle of the present invention is long, copper line surface light after wire drawing, the shelf-time is long, and surface is not oxidizable and its manufacture craft is simple, the not high distinguishing feature of technical requirements.
Specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of Copper Drawing Fluid and preparation method thereof, is made by the raw material of following weight part: plam oil 15-25, petroleum sodium sulfonate 2-3, polyoxyethylene glycol 30-35, calcium sulfenyl phenolate 1-2, sodium napthionate 1-2, water-soluble phosphate 2-3, Sodium Benzoate 1-2, triethanolamine oleate 2-3, diamond nano particulate 0.2-0.4, anti-wear agent 10-14, water 1000;
Described anti-wear agent is made by the raw material of following weight part: diatomite 2.4-2.7, jade 1.2-1.4, urotropine 2.0-2.3, urea 0.4-0.7, silane resin acceptor kh-550 1.0-1.2, Sodium dodecylbenzene sulfonate 0.1-0.2, xitix 1-2, SULPHUR POWDER 1-2, nano aluminum nitride powder 1.2-1.4, water 60; Preparation method is that just jade, diatomite are sent in 540-570 ℃ of calcining furnace, calcining 2-3 hour, cooling rear pulverizing is put into 10-15% hydrochloric acid soln and is soaked 2-3 hour, take out, washes clean, dries and grinds 250-400 order powder, mixes with other remaining component, be heated to 70-75 ℃, under 1200-1500 rev/min, stir 45-60 minute.
Copper Drawing Fluid of the present invention, is made by following concrete steps: plam oil, petroleum sodium sulfonate, polyoxyethylene glycol, calcium sulfenyl phenolate are added to water, be heated to 65-70 ℃; Add again water-soluble phosphate, triethanolamine oleate, stirring reaction 30-45 minute; Finally add anti-wear agent and other remaining component, 800-1000 rev/min of lower stirring reaction 60-90 minute, obtains.
Use wire drawing liquid of the present invention, the highest drawing speed can reach 19m/sec.The copper wire rust prevention during manufacture time of producing is more than 5 days; Concentrating the oil sump drain period is 3 years, and the unit oil sump drain period is 8 months, has reduced liquid waste disposal and discharge, has protected environment.
Claims (2)
1. Copper Drawing Fluid and preparation method thereof, it is characterized in that, by the raw material of following weight part, made: plam oil 15-25, petroleum sodium sulfonate 2-3, polyoxyethylene glycol 30-35, calcium sulfenyl phenolate 1-2, sodium napthionate 1-2, water-soluble phosphate 2-3, Sodium Benzoate 1-2, triethanolamine oleate 2-3, diamond nano particulate 0.2-0.4, anti-wear agent 10-14, water 1000;
Described anti-wear agent is made by the raw material of following weight part: diatomite 2.4-2.7, jade 1.2-1.4, urotropine 2.0-2.3, urea 0.4-0.7, silane resin acceptor kh-550 1.0-1.2, Sodium dodecylbenzene sulfonate 0.1-0.2, xitix 1-2, SULPHUR POWDER 1-2, nano aluminum nitride powder 1.2-1.4, water 60; Preparation method is that just jade, diatomite are sent in 540-570 ℃ of calcining furnace, calcining 2-3 hour, cooling rear pulverizing is put into 10-15% hydrochloric acid soln and is soaked 2-3 hour, take out, washes clean, dries and grinds 250-400 order powder, mixes with other remaining component, be heated to 70-75 ℃, under 1200-1500 rev/min, stir 45-60 minute.
2. according to Copper Drawing Fluid described in claims 1, it is characterized in that, by following concrete steps, made: plam oil, petroleum sodium sulfonate, polyoxyethylene glycol, calcium sulfenyl phenolate are added to water, be heated to 65-70 ℃; Add again water-soluble phosphate, triethanolamine oleate, stirring reaction 30-45 minute; Finally add anti-wear agent and other remaining component, 800-1000 rev/min of lower stirring reaction 60-90 minute, obtains.
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| CN201310494280.1A CN103614221A (en) | 2013-10-21 | 2013-10-21 | Copper wire drawing lubricating fluid and preparation method thereof |
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| CN201310494280.1A CN103614221A (en) | 2013-10-21 | 2013-10-21 | Copper wire drawing lubricating fluid and preparation method thereof |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103966002A (en) * | 2014-03-28 | 2014-08-06 | 安徽龙杨铜业有限公司 | Efficient scale-inhibition clean water-based wire drawing fluid |
| CN103966000A (en) * | 2014-03-28 | 2014-08-06 | 安徽九华金润铜业有限公司 | Long-acting semi-emulsion copper drawing fluid |
| CN103966001A (en) * | 2014-03-28 | 2014-08-06 | 安徽九华金润铜业有限公司 | Copper wire drawing fluid containing nano activated carbon |
| CN103966005A (en) * | 2014-03-28 | 2014-08-06 | 安徽九华金润铜业有限公司 | Drawing fluid for rapidly drawing copper wire |
| CN103966006A (en) * | 2014-03-28 | 2014-08-06 | 安徽龙杨铜业有限公司 | Water-based wire drawing liquid for nonferrous metal |
| CN103966008A (en) * | 2014-03-28 | 2014-08-06 | 安徽龙杨铜业有限公司 | Water-based wire drawing liquid with waste liquor easy to treat |
| CN103966007A (en) * | 2014-03-28 | 2014-08-06 | 安徽联硕实业有限公司 | Antifriction and extreme-pressure-resistant water-based wire drawing liquid |
| CN104293459A (en) * | 2014-08-29 | 2015-01-21 | 安徽乐达精密合金有限公司 | High-efficiency copper wire drawing liquid with long usage life and preparation method thereof |
| CN104293461A (en) * | 2014-08-29 | 2015-01-21 | 安徽乐达精密合金有限公司 | High-efficiency environmental-protection wire drawing liquid with good antiwear effect and preparation method thereof |
| CN104450127A (en) * | 2014-11-14 | 2015-03-25 | 无锡贺邦金属制品有限公司 | Water-based copper wire drawing lubricant |
| CN104450125A (en) * | 2014-11-14 | 2015-03-25 | 无锡贺邦金属制品有限公司 | Wire drawing lubricant |
| CN105695069A (en) * | 2016-02-25 | 2016-06-22 | 天津高盛钢丝绳有限公司 | Lubricant for wet-type wire-drawing technology for steel wire ropes |
| CN106367172A (en) * | 2016-08-29 | 2017-02-01 | 芜湖楚江合金铜材有限公司 | Wire drawing lubricant used in copper wire and preparing method of lubricant |
| CN115637190A (en) * | 2022-09-22 | 2023-01-24 | 陕西耀威铜业有限公司 | Precise copper wire drawing lubricating fluid and preparation method thereof |
| CN115851352A (en) * | 2022-11-29 | 2023-03-28 | 宁波金田铜业(集团)股份有限公司 | Lubricant for preparing copper and copper alloy and using method thereof |
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Cited By (19)
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| CN103966000B (en) * | 2014-03-28 | 2016-01-27 | 安徽九华金润铜业有限公司 | A kind of long-acting semi-emulsifying copper drawing fluid |
| CN103966002B (en) * | 2014-03-28 | 2016-04-06 | 安徽龙杨铜业有限公司 | The peace and quiet water base wire drawing liquid of a kind of efficient scale |
| CN103966001B (en) * | 2014-03-28 | 2016-04-20 | 安徽九华金润铜业有限公司 | A kind of copper drawing fluid containing active carbon nanoparticles |
| CN103966005A (en) * | 2014-03-28 | 2014-08-06 | 安徽九华金润铜业有限公司 | Drawing fluid for rapidly drawing copper wire |
| CN103966006A (en) * | 2014-03-28 | 2014-08-06 | 安徽龙杨铜业有限公司 | Water-based wire drawing liquid for nonferrous metal |
| CN103966008A (en) * | 2014-03-28 | 2014-08-06 | 安徽龙杨铜业有限公司 | Water-based wire drawing liquid with waste liquor easy to treat |
| CN103966007A (en) * | 2014-03-28 | 2014-08-06 | 安徽联硕实业有限公司 | Antifriction and extreme-pressure-resistant water-based wire drawing liquid |
| CN103966000A (en) * | 2014-03-28 | 2014-08-06 | 安徽九华金润铜业有限公司 | Long-acting semi-emulsion copper drawing fluid |
| CN103966001A (en) * | 2014-03-28 | 2014-08-06 | 安徽九华金润铜业有限公司 | Copper wire drawing fluid containing nano activated carbon |
| CN103966002A (en) * | 2014-03-28 | 2014-08-06 | 安徽龙杨铜业有限公司 | Efficient scale-inhibition clean water-based wire drawing fluid |
| CN103966005B (en) * | 2014-03-28 | 2016-01-27 | 安徽九华金润铜业有限公司 | The quick drawing wire drawing liquid of a kind of copper cash |
| CN104293459A (en) * | 2014-08-29 | 2015-01-21 | 安徽乐达精密合金有限公司 | High-efficiency copper wire drawing liquid with long usage life and preparation method thereof |
| CN104293461A (en) * | 2014-08-29 | 2015-01-21 | 安徽乐达精密合金有限公司 | High-efficiency environmental-protection wire drawing liquid with good antiwear effect and preparation method thereof |
| CN104450125A (en) * | 2014-11-14 | 2015-03-25 | 无锡贺邦金属制品有限公司 | Wire drawing lubricant |
| CN104450127A (en) * | 2014-11-14 | 2015-03-25 | 无锡贺邦金属制品有限公司 | Water-based copper wire drawing lubricant |
| CN105695069A (en) * | 2016-02-25 | 2016-06-22 | 天津高盛钢丝绳有限公司 | Lubricant for wet-type wire-drawing technology for steel wire ropes |
| CN106367172A (en) * | 2016-08-29 | 2017-02-01 | 芜湖楚江合金铜材有限公司 | Wire drawing lubricant used in copper wire and preparing method of lubricant |
| CN115637190A (en) * | 2022-09-22 | 2023-01-24 | 陕西耀威铜业有限公司 | Precise copper wire drawing lubricating fluid and preparation method thereof |
| CN115851352A (en) * | 2022-11-29 | 2023-03-28 | 宁波金田铜业(集团)股份有限公司 | Lubricant for preparing copper and copper alloy and using method thereof |
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Application publication date: 20140305 |