CN105969491A - Oily eco-friendly drawing lubricant replacing wire drawing powder and preparation technology thereof - Google Patents
Oily eco-friendly drawing lubricant replacing wire drawing powder and preparation technology thereof Download PDFInfo
- Publication number
- CN105969491A CN105969491A CN201610292875.2A CN201610292875A CN105969491A CN 105969491 A CN105969491 A CN 105969491A CN 201610292875 A CN201610292875 A CN 201610292875A CN 105969491 A CN105969491 A CN 105969491A
- Authority
- CN
- China
- Prior art keywords
- eco
- friendly
- oily
- base oil
- mineral base
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/1006—Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/026—Butene
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
- C10M2219/024—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of esters, e.g. fats
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/64—Environmental friendly compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Metal Extraction Processes (AREA)
- Lubricants (AREA)
Abstract
The invention discloses an oily eco-friendly drawing lubricant replacing wire drawing powder and a preparation technology thereof. The oily eco-friendly drawing lubricant comprises mineral base oil, sulfuretted fat and additives. The additives comprise, by mass, 55-65% of sulfuretted fat, 3-8% of triazole fatty amine salt, 3-8% of polyisobutene and the balance mineral base oil. The oily eco-friendly drawing lubricant does not produce dust pollution in a work environment and dust damage to an operator, reduces friction and wear, prolongs a grinding tool service life by one time, improves product quality, realizes energy saving, and is convenient for eco-friendly product later treatment. The traditional drawing process is carried out at a high temperature under high pressure so that metal wire bonding is produced and labor, water and time consumption is large. The product treated by the drawing lubricant solves the above problem and only needs to be washed once.
Description
Technical field
The present invention relates to metal drawing shaping assistant technical field, be specifically related to a kind of oiliness environmental protection replacing wire drawing powder and draw
Pull out lubricant and preparation technology thereof.
Background technology
There is a class to be belonging to bar, wire rod or tubing in metal working process and reach technological requirement by drawing molding
Required shape or size, this technique is widely used in the wide spectrums such as industry, civilian and building, in actual production, for a long time
Use powder to use as lubricant (drawing powder), be nearly all especially to use powder class lubrication in bar, wire drawing.Its
Advantage is low cost, and effect is obvious, and shortcoming is owing to producing in the high-speed motion of wire rod and alternative process in drawing process
Heat and electrostatic make to fill the air everywhere as the powder of Lubrication Composition, pollute environment, also the health of operator are caused wound simultaneously
Evil, the anthraco-silicosis incidence rate of the personnel being engaged in this work post in this industry for a long time is the highest.
Therefore metal drawing industry is in the urgent need to a kind of products substitution safe and environment-friendly, efficient existing drawing powder, and I am public
Department studies discovery by inquiry, and due to the particularity of its drawing process, a kind of substitute products difficulty of invention is very big, because drawing is raw
In product, material modification amount is big, and speed is fast, and general oil product in use, all can not meet technique needs.
Summary of the invention
The invention provides a kind of oiliness environmental protection drawing compound replacing wire drawing powder and preparation technology thereof, existing to solve
The problem that the metal drawing molding that technology exists can not use lubricating oil.
The technical solution adopted for the present invention to solve the technical problems is:
A kind of oiliness environmental protection drawing compound replacing wire drawing powder, is made up of mineral base oil, sulfurized fatty and additive, adds
Adding agent and include fatty amine triazole and polyisobutylene, the mass percent that described each component uses is: sulfurized fatty 55% ~ 65%;
Fatty amine triazole 3% ~ 8%;Polyisobutylene 3% ~ 8%;Surplus is mineral base oil.
The preparation technology of the oiliness environmental protection drawing compound of above-mentioned replacement wire drawing powder is: add mineral base in reactor
Plinth oil is warming up to 60 DEG C, is subsequently adding sulfurized fatty and fatty amine triazole under agitation, finally adds polyisobutylene,
Treat after stirring one hour that it all dissolves and become stable, thickness, limpid state.
Adding fatty amine triazole in oiliness environmental protection drawing lubrication agent prescription of the present invention, fatty amine triazole is powder,
Use as metallic reducing agent, the fretting wear between metal can be prevented effectively from.
The drawing compound of the present invention is oil preparation product, and working environment no dust pollution, operator are without dust harzard;Fall
Low friction wear, grinding tool extends one times service life, and product quality is improved, and energy-saving effect is obvious simultaneously;At the product later stage
Reason facilitates environmental protection, and the drawing in past is many under High Temperature High Pressure effect, has pinning phenomenon with metal wire rod, and later stage process is taken a lot of work, expense
Water, time-consuming, with the product of drawing oil then without this phenomenon, only need to clean once.
Detailed description of the invention
A kind of oiliness environmental protection drawing compound replacing wire drawing powder, by mineral base oil, sulfurized fatty and additive group
Becoming, additive includes fatty amine triazole and polyisobutylene, and the mass percent that described each component uses is: sulfurized fatty 55% ~
65%;Fatty amine triazole 3% ~ 8%;Polyisobutylene 3% ~ 8%;Surplus is mineral base oil.The oiliness environmental protection replacing wire drawing powder draws
The preparation technology pulling out lubricant is: adds mineral base oil in reactor and is warming up to 60 DEG C, the most then adds
Enter sulfurized fatty and fatty amine triazole, finally add polyisobutylene, treat after stirring one hour its all dissolve become stable,
Thickness, limpid state.
This lubricant is tried out in Duo Jia drawing enterprise, achieves positive effect, and comparing tradition drawing powder has following several
Big advantage:
Working environment no dust pollution, operator are without dust harzard
Reducing friction wear, grinding tool extends one times service life, and product quality is improved, simultaneously energy-saving effect substantially (joint
Electricity 10%)
The process of product later stage facilitates environmental protection, and the drawing in past is many under High Temperature High Pressure effect, has bonding existing with metal wire rod
As, later stage process take a lot of work, water wasting, time-consuming, with the product of drawing oil then without this phenomenon, only need to clean once.
Claims (2)
1. replace an oiliness environmental protection drawing compound for wire drawing powder, it is characterized in that by mineral base oil, sulfurized fatty and add
Adding agent composition, additive includes fatty amine triazole and polyisobutylene, and the mass percent that described each component uses is: sulfurized fat
Fat 55% ~ 65%;Fatty amine triazole 3% ~ 8%;Polyisobutylene 3% ~ 8%;Surplus is mineral base oil.
2. the preparation technology of the oiliness environmental protection drawing compound replacing wire drawing powder described in claim 1, is characterized in that in reaction
Add mineral base oil in still and be warming up to 60 DEG C, be subsequently adding sulfurized fatty and fatty amine triazole under agitation,
After add polyisobutylene, treating after stirring one hour that it all dissolves becomes stable, thickness, limpid state.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201610292875.2A CN105969491A (en) | 2016-05-06 | 2016-05-06 | Oily eco-friendly drawing lubricant replacing wire drawing powder and preparation technology thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610292875.2A CN105969491A (en) | 2016-05-06 | 2016-05-06 | Oily eco-friendly drawing lubricant replacing wire drawing powder and preparation technology thereof |
Publications (1)
Publication Number | Publication Date |
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CN105969491A true CN105969491A (en) | 2016-09-28 |
Family
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Family Applications (1)
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CN201610292875.2A Pending CN105969491A (en) | 2016-05-06 | 2016-05-06 | Oily eco-friendly drawing lubricant replacing wire drawing powder and preparation technology thereof |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106867648A (en) * | 2016-12-22 | 2017-06-20 | 当涂县宏宇金属炉料有限责任公司 | A kind of waste lubricating oil makes wire drawing powder method |
CN106867642A (en) * | 2017-01-19 | 2017-06-20 | 南京百丝胜新材料科技有限公司 | A kind of metal wire rod wire drawing powder and preparation method thereof |
CN111876222A (en) * | 2020-07-16 | 2020-11-03 | 常州市九鑫铜业有限公司 | Crystallizer copper pipe drawing oil containing sulfuration modified swill-cooked dirty oil |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH1150080A (en) * | 1997-08-06 | 1999-02-23 | Sumitomo Metal Ind Ltd | Pre-die lubricant for wire drawing and lubrication treatment of base material for high strength bolt |
CN103374452A (en) * | 2012-04-27 | 2013-10-30 | 中国石油化工股份有限公司 | Manual transmission lubricating oil composition |
CN103695126A (en) * | 2013-12-18 | 2014-04-02 | 广西大学 | Lubricating agent for drawing of permalloy stainless steel plate |
CN104974834A (en) * | 2015-07-20 | 2015-10-14 | 广西大学 | Rhenium filament drawing lubricant composition |
-
2016
- 2016-05-06 CN CN201610292875.2A patent/CN105969491A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH1150080A (en) * | 1997-08-06 | 1999-02-23 | Sumitomo Metal Ind Ltd | Pre-die lubricant for wire drawing and lubrication treatment of base material for high strength bolt |
CN103374452A (en) * | 2012-04-27 | 2013-10-30 | 中国石油化工股份有限公司 | Manual transmission lubricating oil composition |
CN103695126A (en) * | 2013-12-18 | 2014-04-02 | 广西大学 | Lubricating agent for drawing of permalloy stainless steel plate |
CN104974834A (en) * | 2015-07-20 | 2015-10-14 | 广西大学 | Rhenium filament drawing lubricant composition |
Non-Patent Citations (1)
Title |
---|
沈萌红等: "《机械设计》", 30 September 2012, 华中科技大学出版社 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106867648A (en) * | 2016-12-22 | 2017-06-20 | 当涂县宏宇金属炉料有限责任公司 | A kind of waste lubricating oil makes wire drawing powder method |
CN106867648B (en) * | 2016-12-22 | 2020-04-21 | 当涂县宏宇金属炉料有限责任公司 | Method for preparing wire drawing powder from waste lubricating oil |
CN106867642A (en) * | 2017-01-19 | 2017-06-20 | 南京百丝胜新材料科技有限公司 | A kind of metal wire rod wire drawing powder and preparation method thereof |
CN111876222A (en) * | 2020-07-16 | 2020-11-03 | 常州市九鑫铜业有限公司 | Crystallizer copper pipe drawing oil containing sulfuration modified swill-cooked dirty oil |
CN111876222B (en) * | 2020-07-16 | 2022-08-12 | 常州市九鑫铜业有限公司 | Crystallizer copper pipe drawing oil containing sulfuration modified swill-cooked dirty oil |
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Application publication date: 20160928 |