CN104263485A - Antiwear-additive-added aluminum wire drawing solution with bactericidal action and preparation method thereof - Google Patents

Antiwear-additive-added aluminum wire drawing solution with bactericidal action and preparation method thereof Download PDF

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Publication number
CN104263485A
CN104263485A CN201410454616.6A CN201410454616A CN104263485A CN 104263485 A CN104263485 A CN 104263485A CN 201410454616 A CN201410454616 A CN 201410454616A CN 104263485 A CN104263485 A CN 104263485A
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China
Prior art keywords
parts
wire drawing
added
auxiliary agent
drawing solution
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Pending
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CN201410454616.6A
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Chinese (zh)
Inventor
周小刚
储刘生
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ANHUI WANGDA COPPER INDUSTRY DEVELOPMENT Co Ltd
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ANHUI WANGDA COPPER INDUSTRY DEVELOPMENT Co Ltd
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Priority to CN201410454616.6A priority Critical patent/CN104263485A/en
Publication of CN104263485A publication Critical patent/CN104263485A/en
Pending legal-status Critical Current

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Abstract

The invention discloses an antiwear-additive-added aluminum wire drawing solution with bactericidal action. The invention is characterized in that the aluminum wire drawing solution is prepared from the following raw materials in parts by weight: 3-5 parts of barium petroleum sulfonate, 1-2 parts of 2,6-benzoisothiazolinone, 2-3.5 parts of glycerin monostearate, 4-6 parts of vulcanized cotton oil, 3-4 parts of stearamidopropyl amine oxide, 2-4 parts of polyacrylamide, 3-5 parts of lauryl alcohol sodium sulfovinate, 1-2 parts of KATHON CG preservative, 3-5 parts of talcum powder, 4.5-5.5 parts of nano zirconium dioxide, 5-7 parts of assistant and 900-950 parts of deionized water. The added nano zirconium dioxide has favorable dispersity, wear resistance and corrosion resistance, and prevents the wire drawing die from damage; the added KATHON CG preservative with certain preservative effect prolongs the service life of the wire drawing solution; and the added assistant enhances the wear resistance, dispersity, lubricating property and film formation property. The aluminum wire drawing solution has the advantages of low cost, excellent film formation property, excellent heat stability, excellent corrosion resistance and excellent cooling effect.

Description

A kind ofly add aluminum drawing fluid with germicidal action of anti-wear agent and preparation method thereof
Technical field
The present invention relates to wire-drawing technology field, particularly a kind ofly add aluminum drawing fluid with germicidal action of anti-wear agent and preparation method thereof.
Background technology
Drawing process is a kind of metal working process.In metal-pressed machine. make metal be forced through mould under external force, metal cross-sectional area is compressed, and the technology working method of cross-sectional area shape and size required by obtaining is called metal wire-drawing technique.Make it change shape, the instrument of size is called wortle.
Being determined by the processing characteristics of aluminum metal itself, aluminium Wire Drawing is very high to the requirement of wire drawing liquid.First require that the oilness of wire drawing liquid is very high, only have oilness to meet processing request, the aluminium wire pulled out smoothly could not have cut, could carry out the processing of postorder to aluminium wire; Its two, aluminium wire, after Uniform Tension, through the flushing of high velocity flow, will be rinsed the wire drawing liquid on aluminium wire surface well, in order to carrying out the processing of next process, therefore, requires that wire drawing liquid has excellent cleaning; Certainly, for aluminum metal, etching problem no less important, this just requires that wire drawing liquid has excellent aluminium barrier propterty, even if still have good protection function to aluminium wire under high strength processing conditions.Lubricant for aluminium wire drawing has multiple, and use properties differs greatly, and some wire drawing lubricants in use can blackening, rotten, smelly, and this just requires that wire drawing liquid has certain sterilization effect, extends the duration of service of wire drawing liquid.
Summary of the invention
The object of this invention is to provide and a kind ofly add aluminum drawing fluid with germicidal action of anti-wear agent and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of aluminum drawing fluid with germicidal action adding anti-wear agent, be made up of the raw material of following weight part: barium mahogany sulfonate 3-5,2,6-BIT 1-2, single stearic acid glycerine lipoprotein 2-3.5, sulfuration Oleum Gossypii semen 4-6, stearylamide propyl group amine oxide 3-4, polyacrylamide 2-4, lauryl alcohol sodium sulfovinate 3-5, Kathon CG sanitas 1-2, talcum powder 3-5, nano zirconium dioxide 4.5-5.5, auxiliary agent 5-7, deionized water 900-950;
Described auxiliary agent is made up of the raw material of following weight part: granular graphite 2-4, nano diatomite 2.5-3.5, bisphenol a dimethacrylate 1-2, sulfuration Oleum Gossypii semen 2-2.5, Lauryl Alcohol ester 2-3, anilinomethyl triethoxysilane 1-1.5, Oleum Bupleuri 1-2, pull open powder 3-4, water 90-94; Preparation method be first by granular graphite, nano diatomite, Oleum Bupleuri, pull open powder and add in the water of half amount, grinding 1-2 hour, then slowly adds all the other remaining components, is slowly heated to 70 DEG C-80 DEG C, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
A kind of aluminum drawing fluid with germicidal action adding anti-wear agent of the present invention, be made up of following concrete steps:
(1) sulfuration Oleum Gossypii semen, stearylamide propyl group amine oxide, polyacrylamide, talcum powder, nano zirconium dioxide are mixed, add appropriate deionized water, be heated to 30 DEG C-35 DEG C, grinding 30-40 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 55 DEG C-65 DEG C, insulation 1-1.5 hour, obtain mixing B material;
(3) slowly joined while stirring in mixing A material by the mixing B of insulation material, add auxiliary agent after fully stirring, 600-800 rev/min of lower stirring reaction 40-60 minute, is cooled to room temperature and get final product.
Excellent effect of the present invention is: the present invention adds nano zirconium dioxide, there is good dispersiveness, wear-resisting, erosion resistance, prevent wortle from damaging, add Kathon CG sanitas, there is certain preservative effect, extend the work-ing life of wire drawing liquid, add auxiliary agent, enhance wear-resistant, dispersion, lubrication, film-forming properties; Aluminum drawing fluid cost of the present invention is low, possesses splendid film-forming properties, thermostability, non-corrosibility, cooling performance.
Embodiment
Below by specific examples, the present invention is described in detail.
A kind of aluminum drawing fluid with germicidal action adding anti-wear agent, be made up of the raw material of following weight part (kilogram): barium mahogany sulfonate 3,2,6-BIT 1, single stearic acid glycerine lipoprotein 2, sulfuration Oleum Gossypii semen 4, stearylamide propyl group amine oxide 3, polyacrylamide 2, lauryl alcohol sodium sulfovinate 3, Kathon CG sanitas 1, talcum powder 3, nano zirconium dioxide 4.5, auxiliary agent 5, deionized water 900;
Described auxiliary agent is made up of the raw material of following weight part (kilogram): granular graphite 2, nano diatomite 2.5, bisphenol a dimethacrylate 1, sulfuration Oleum Gossypii semen 2, Lauryl Alcohol ester 2, anilinomethyl triethoxysilane 1, Oleum Bupleuri 1, pull open powder 3, water 90; Preparation method be first by granular graphite, nano diatomite, Oleum Bupleuri, pull open powder and add in the water of half amount, grinding 1-2 hour, then slowly adds all the other remaining components, is slowly heated to 70 DEG C-80 DEG C, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
A kind of aluminum drawing fluid with germicidal action adding anti-wear agent of the present invention, be made up of following concrete steps:
(1) sulfuration Oleum Gossypii semen, stearylamide propyl group amine oxide, polyacrylamide, talcum powder, nano zirconium dioxide are mixed, add appropriate deionized water, be heated to 30 DEG C-35 DEG C, grinding 30-40 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 55 DEG C-65 DEG C, insulation 1-1.5 hour, obtain mixing B material;
(3) slowly joined while stirring in mixing A material by the mixing B of insulation material, add auxiliary agent after fully stirring, 600-800 rev/min of lower stirring reaction 40-60 minute, is cooled to room temperature and get final product.
Use the present embodiment wire drawing liquid, the highest drawing speed can reach 20m/sec.Concentrate the oil sump drain period to be 3 years, the unit oil sump drain period is 8 months, decreases liquid waste disposal and discharge, protects environment.

Claims (2)

1. one kind is added the aluminum drawing fluid with germicidal action of anti-wear agent, it is characterized in that, be made up of the raw material of following weight part: barium mahogany sulfonate 3-5,2,6-BIT 1-2, single stearic acid glycerine lipoprotein 2-3.5, sulfuration Oleum Gossypii semen 4-6, stearylamide propyl group amine oxide 3-4, polyacrylamide 2-4, lauryl alcohol sodium sulfovinate 3-5, Kathon CG sanitas 1-2, talcum powder 3-5, nano zirconium dioxide 4.5-5.5, auxiliary agent 5-7, deionized water 900-950;
Described auxiliary agent is made up of the raw material of following weight part: granular graphite 2-4, nano diatomite 2.5-3.5, bisphenol a dimethacrylate 1-2, sulfuration Oleum Gossypii semen 2-2.5, Lauryl Alcohol ester 2-3, anilinomethyl triethoxysilane 1-1.5, Oleum Bupleuri 1-2, pull open powder 3-4, water 90-94; Preparation method be first by granular graphite, nano diatomite, Oleum Bupleuri, pull open powder and add in the water of half amount, grinding 1-2 hour, then slowly adds all the other remaining components, is slowly heated to 70 DEG C-80 DEG C, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
2. a kind of aluminum drawing fluid with germicidal action adding anti-wear agent according to claim 1, is characterized in that, be made up of following concrete steps:
(1) sulfuration Oleum Gossypii semen, stearylamide propyl group amine oxide, polyacrylamide, talcum powder, nano zirconium dioxide are mixed, add appropriate deionized water, be heated to 30 DEG C-35 DEG C, grinding 30-40 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 55 DEG C-65 DEG C, insulation 1-1.5 hour, obtain mixing B material;
(3) slowly joined while stirring in mixing A material by the mixing B of insulation material, add auxiliary agent after fully stirring, 600-800 rev/min of lower stirring reaction 40-60 minute, is cooled to room temperature and get final product.
CN201410454616.6A 2014-09-09 2014-09-09 Antiwear-additive-added aluminum wire drawing solution with bactericidal action and preparation method thereof Pending CN104263485A (en)

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Application Number Priority Date Filing Date Title
CN201410454616.6A CN104263485A (en) 2014-09-09 2014-09-09 Antiwear-additive-added aluminum wire drawing solution with bactericidal action and preparation method thereof

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CN104263485A true CN104263485A (en) 2015-01-07

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104611106A (en) * 2015-01-10 2015-05-13 安徽旺达铜业发展有限公司 Water-based copper wire drawing liquid with excellent lubricity and preparation method of water-based copper wire drawing liquid
CN104611105A (en) * 2015-01-10 2015-05-13 安徽旺达铜业发展有限公司 Aluminum wiredrawing fluid with nanometer titanium dioxide, and preparation method for aluminum wiredrawing fluid
CN104611107A (en) * 2015-01-10 2015-05-13 安徽旺达铜业发展有限公司 Excellent-performance wiredrawing fluid added with nanometer graphite, and preparation method for wiredrawing fluid

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1197108A (en) * 1997-04-18 1998-10-28 郭紫鸣 Aluminium wiredrawing lubricating grease
CN101747987A (en) * 2009-12-21 2010-06-23 克拉玛依市金山石油化工有限公司 Water-based copper and aluminum wiredrawing oil composite and preparation method thereof
CN101812363A (en) * 2009-12-18 2010-08-25 益田润石(北京)化工有限公司 Full synthetic aluminum drawing fluid composition

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1197108A (en) * 1997-04-18 1998-10-28 郭紫鸣 Aluminium wiredrawing lubricating grease
CN101812363A (en) * 2009-12-18 2010-08-25 益田润石(北京)化工有限公司 Full synthetic aluminum drawing fluid composition
CN101747987A (en) * 2009-12-21 2010-06-23 克拉玛依市金山石油化工有限公司 Water-based copper and aluminum wiredrawing oil composite and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104611106A (en) * 2015-01-10 2015-05-13 安徽旺达铜业发展有限公司 Water-based copper wire drawing liquid with excellent lubricity and preparation method of water-based copper wire drawing liquid
CN104611105A (en) * 2015-01-10 2015-05-13 安徽旺达铜业发展有限公司 Aluminum wiredrawing fluid with nanometer titanium dioxide, and preparation method for aluminum wiredrawing fluid
CN104611107A (en) * 2015-01-10 2015-05-13 安徽旺达铜业发展有限公司 Excellent-performance wiredrawing fluid added with nanometer graphite, and preparation method for wiredrawing fluid

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Application publication date: 20150107