CN104263487A - Water-based aluminum product wire drawing solution with bactericidal action and preparation method thereof - Google Patents
Water-based aluminum product wire drawing solution with bactericidal action and preparation method thereof Download PDFInfo
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- CN104263487A CN104263487A CN201410454679.1A CN201410454679A CN104263487A CN 104263487 A CN104263487 A CN 104263487A CN 201410454679 A CN201410454679 A CN 201410454679A CN 104263487 A CN104263487 A CN 104263487A
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Abstract
The invention discloses a water-based aluminum product wire drawing solution with bactericidal action. The invention is characterized in that the wire drawing solution is prepared from the following raw materials in parts by weight: 3.5-4.5 parts of sodium paraxylene sulfonate, 2-3 parts of mercaptobenzothiazole, 3-4 parts of triethanolamine, 2.5-3.5 parts of borate, 2-3 parts of phytate, 4.5-6 parts of palm oil, 6.5-8 parts of vulcanized lard, 1-2 parts of sulfur suspending agent, 1.5-2 parts of sodium citrate, 1-2 parts of sodium sulfite, 3-5 parts of nano silicon carbide, 5-7 parts of assistant and 900-950 parts of deionized water. The wire drawing solution has reasonable formula; by adopting the water-based formula, the wire drawing solution has favorable cooling property; the added sulfur suspending agent has certain bactericidal effect, prevents the wire drawing solution from fouling or deterioration, and prolongs the service time; and the added assistant has favorable wear resistance, dispersity, lubricating property and film formation property, and has the slow-release and protective actions when being matched with the surfactant. The aluminum wire drawn by the product has the advantages of uniform line shape and bright surface.
Description
Technical field
The present invention relates to wire-drawing technology field, particularly a kind of water base aluminium wire drawing liquid with germicidal action and preparation method thereof.
Background technology
In existing drawing process, the lubricating oil that adopts as wire drawing medium more, and the conductive line surfaces that drawing goes out is mellow and full, fine and smooth, smooth, bright, no-sundries is detained, and wire broken rate reduces, and quality product improves greatly.But lubricating oil heat radiation is slow, damage mould, affects quality product.Being determined by the processing characteristics of aluminum metal itself, aluminium Wire Drawing is very high to the requirement of wire drawing liquid.First require that the oilness of wire drawing liquid is very high, only have oilness to meet processing request, the aluminium wire pulled out smoothly could not have cut, could carry out the processing of postorder to aluminium wire; Its two, aluminium wire, after Uniform Tension, through the flushing of high velocity flow, will be rinsed the wire drawing liquid on aluminium wire surface well, in order to carrying out the processing of next process, therefore, requires that wire drawing liquid has excellent cleaning; Certainly, for aluminum metal, etching problem no less important, this just requires that wire drawing liquid has excellent aluminium barrier propterty, even if still have good protection function to aluminium wire under high strength processing conditions.Wire drawing liquid for aluminium has multiple, and use properties differs greatly, and some wire drawing lubricants in use can go bad, blackening, smelly, and this just requires that wire drawing liquid has sterilization effect, extends the duration of service of wire drawing liquid.The present invention adopts water prescription, has good cooling performance.
Summary of the invention
The object of this invention is to provide a kind of water base aluminium wire drawing liquid with germicidal action and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
There is a water base aluminium wire drawing liquid for germicidal action, be made up of the raw material of following weight part: p-Xylol sodium sulfonate 3.5-4.5, mercaptobenzothiazole 2-3, trolamine 3-4, boric acid ester 2.5-3.5, myo-Inositol hexaphosphate 2-3, plam oil 4.5-6, sulfurized lard 6.5-8, sulphur suspends 1-2, Trisodium Citrate 1.5-2, S-WAT 1-2, nanometer silicon carbide 3-5, auxiliary agent 5-7, deionized water 900-950;
Described auxiliary agent is made up of the raw material of following weight part: granular graphite 2-4, nano diatomite 2.5-3.5, bisphenol a dimethacrylate 1-2, sulfuration Oleum Gossypii semen 2-2.5, Lauryl Alcohol ester 2-3, anilinomethyl triethoxysilane 1-1.5, Oleum Bupleuri 1-2, pull open powder 3-4, water 90-94; Preparation method be first by granular graphite, nano diatomite, Oleum Bupleuri, pull open powder and add in the water of half amount, grinding 1-2 hour, then slowly adds all the other remaining components, is slowly heated to 70 DEG C-80 DEG C, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
A kind of water base aluminium wire drawing liquid with germicidal action of the present invention, be made up of following concrete steps:
(1) p-Xylol sodium sulfonate, plam oil, sulfurized lard, nanometer silicon carbide are mixed, add appropriate deionized water, be heated to 30 DEG C-35 DEG C, stir 30-40 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 55 DEG C-65 DEG C, insulation 1-1.5 hour, obtain mixing B material;
(3) slowly joined while stirring in mixing A material by the mixing B of insulation material, add auxiliary agent after fully stirring, 600-800 rev/min of lower stirring reaction 40-60 minute, is cooled to room temperature and get final product.
Excellent effect of the present invention is: the present invention fills a prescription rationally, adopt water prescription, there is good cooling, add sulphur suspends, there is certain sterilization effect, prevent wire drawing liquid from going bad, extending duration of service, add auxiliary agent, there is good wear-resistant, dispersion, lubrication, film-forming properties, coordinate with tensio-active agent, play slowly-releasing and provide protection; The aluminium wire adopting this product to draw is evenly linear, surface-brightening.
Embodiment
Below by specific examples, the present invention is described in detail.
There is a water base aluminium wire drawing liquid for germicidal action, be made up of the raw material of following weight part (kilogram): p-Xylol sodium sulfonate 3.5, mercaptobenzothiazole 2, trolamine 3, boric acid ester 2.5, myo-Inositol hexaphosphate 2, plam oil 4.5, sulfurized lard 6.5, sulphur suspends 1, Trisodium Citrate 1.5, S-WAT 1, nanometer silicon carbide 3, auxiliary agent 5, deionized water 900;
Described auxiliary agent is made up of the raw material of following weight part (kilogram): granular graphite 2, nano diatomite 2.5, bisphenol a dimethacrylate 1, sulfuration Oleum Gossypii semen 2, Lauryl Alcohol ester 2, anilinomethyl triethoxysilane 1, Oleum Bupleuri 1, pull open powder 3, water 90; Preparation method be first by granular graphite, nano diatomite, Oleum Bupleuri, pull open powder and add in the water of half amount, grinding 1-2 hour, then slowly adds all the other remaining components, is slowly heated to 70 DEG C-80 DEG C, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
A kind of water base aluminium wire drawing liquid with germicidal action of the present invention, be made up of following concrete steps:
(1) p-Xylol sodium sulfonate, plam oil, sulfurized lard, nanometer silicon carbide are mixed, add appropriate deionized water, be heated to 30 DEG C-35 DEG C, stir 30-40 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 55 DEG C-65 DEG C, insulation 1-1.5 hour, obtain mixing B material;
(3) slowly joined while stirring in mixing A material by the mixing B of insulation material, add auxiliary agent after fully stirring, 600-800 rev/min of lower stirring reaction 40-60 minute, is cooled to room temperature and get final product.
Use the present embodiment wire drawing liquid, the highest drawing speed can reach 20m/sec.Concentrate the oil sump drain period to be 3 years, the unit oil sump drain period is 8 months, decreases liquid waste disposal and discharge, protects environment.
Claims (2)
1. one kind has the water base aluminium wire drawing liquid of germicidal action, it is characterized in that, be made up of the raw material of following weight part: p-Xylol sodium sulfonate 3.5-4.5, mercaptobenzothiazole 2-3, trolamine 3-4, boric acid ester 2.5-3.5, myo-Inositol hexaphosphate 2-3, plam oil 4.5-6, sulfurized lard 6.5-8, sulphur suspends 1-2, Trisodium Citrate 1.5-2, S-WAT 1-2, nanometer silicon carbide 3-5, auxiliary agent 5-7, deionized water 900-950;
Described auxiliary agent is made up of the raw material of following weight part: granular graphite 2-4, nano diatomite 2.5-3.5, bisphenol a dimethacrylate 1-2, sulfuration Oleum Gossypii semen 2-2.5, Lauryl Alcohol ester 2-3, anilinomethyl triethoxysilane 1-1.5, Oleum Bupleuri 1-2, pull open powder 3-4, water 90-94; Preparation method be first by granular graphite, nano diatomite, Oleum Bupleuri, pull open powder and add in the water of half amount, grinding 1-2 hour, then slowly adds all the other remaining components, is slowly heated to 70 DEG C-80 DEG C, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
2. a kind of water base aluminium wire drawing liquid with germicidal action according to claim 1, is characterized in that, be made up of following concrete steps:
(1) p-Xylol sodium sulfonate, plam oil, sulfurized lard, nanometer silicon carbide are mixed, add appropriate deionized water, be heated to 30 DEG C-35 DEG C, stir 30-40 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 55 DEG C-65 DEG C, insulation 1-1.5 hour, obtain mixing B material;
(3) slowly joined while stirring in mixing A material by the mixing B of insulation material, add auxiliary agent after fully stirring, 600-800 rev/min of lower stirring reaction 40-60 minute, is cooled to room temperature and get final product.
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CN201410454679.1A CN104263487A (en) | 2014-09-09 | 2014-09-09 | Water-based aluminum product wire drawing solution with bactericidal action and preparation method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111180136A (en) * | 2019-12-07 | 2020-05-19 | 安徽瑞之星电缆集团有限公司 | Flexible stranded conductor manufacturing process and stranded conductor |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1197108A (en) * | 1997-04-18 | 1998-10-28 | 郭紫鸣 | Aluminium wiredrawing lubricating grease |
CN101747988A (en) * | 2009-12-21 | 2010-06-23 | 克拉玛依市金山石油化工有限公司 | Copper and aluminum wire drawing oil and preparation method and use method thereof |
CN101747987A (en) * | 2009-12-21 | 2010-06-23 | 克拉玛依市金山石油化工有限公司 | Water-based copper and aluminum wiredrawing oil composite and preparation method thereof |
CN101812363A (en) * | 2009-12-18 | 2010-08-25 | 益田润石(北京)化工有限公司 | Full synthetic aluminum drawing fluid composition |
-
2014
- 2014-09-09 CN CN201410454679.1A patent/CN104263487A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1197108A (en) * | 1997-04-18 | 1998-10-28 | 郭紫鸣 | Aluminium wiredrawing lubricating grease |
CN101812363A (en) * | 2009-12-18 | 2010-08-25 | 益田润石(北京)化工有限公司 | Full synthetic aluminum drawing fluid composition |
CN101747988A (en) * | 2009-12-21 | 2010-06-23 | 克拉玛依市金山石油化工有限公司 | Copper and aluminum wire drawing oil and preparation method and use method thereof |
CN101747987A (en) * | 2009-12-21 | 2010-06-23 | 克拉玛依市金山石油化工有限公司 | Water-based copper and aluminum wiredrawing oil composite and preparation method thereof |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111180136A (en) * | 2019-12-07 | 2020-05-19 | 安徽瑞之星电缆集团有限公司 | Flexible stranded conductor manufacturing process and stranded conductor |
CN111180136B (en) * | 2019-12-07 | 2021-11-09 | 安徽瑞之星电缆集团有限公司 | Flexible stranded conductor manufacturing process and stranded conductor |
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