CN104327929A - High-abrasion resistance water-based cutting fluid and preparation method thereof - Google Patents
High-abrasion resistance water-based cutting fluid and preparation method thereof Download PDFInfo
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Abstract
The invention provides a high-abrasion resistance water-based cutting fluid and a preparation method thereof, the water-based cutting fluid comprises the following raw materials: oleic acid, organic alkylol amine, boric acid, molybdenum disulfide, a composite emulsifier, a composite antirust agent, a composite bactericide, an organosilicon antifoaming agent and deionized water, the preparation method comprises the following steps: a)preparing a component A product, b)preparing a component B product, and c)mixing the component A and the component B to prepare the finished product. The invention reveals the high-abrasion resistance water-based cutting fluid and the preparation method. The water-based cutting fluid has the advantages of low production cost, safety, no toxicity, good lubricity, anlirust property, anticorrosion performance and stability, and the antifriction and abrasion resistance performances can be obviously better than that of the same kind products.
Description
Technical field
The present invention relates to a kind of cutting fluid, particularly relate to a kind of high-wearing feature water-base cutting fluid and preparation method thereof, belong to cutting fluid technical field.
Background technology
Cutting fluid is that one is used in metal cutting, the mill course of processing, is used for the industrial type fluid of Cooling and Lubricator cutter and workpiece, and it is formed through science compound compatibility by several functions auxiliary agent.As a kind of important complementary supplementary material of metal cutting process, metal working fluid can extend the work-ing life of cutter and grinding tool, improves the smooth finish of workpiece, reduces cutting, grinding force, and its Main Function comprises cooling, lubrication, antirust and cleaning four aspects.Cutting fluid mainly oil base and water base two classes of general use, in recent years, water-base cutting fluid has outstanding feature and is able to apply more and more widely in cooling, cleaning, rust-preventing characteristic, oilness etc., and water-base cutting fluid can be divided into micro-emulsion type, oil-in-water type and complete synthesis type.Along with the requirement of harsh new complete processing and novel material in mechanized equipment manufacture, add continually developing of new type water-solubility additive, water-base cutting fluid is developed rapidly.
At present, water-base cutting fluid is just towards environmental protection, energy-conservation, efficient, general future development.Abroad, many processing characteristicies of water-base cutting fluid can compare favourably with oil base cutting fluid, can meet multiple material and kinds of processes processing request, can meet environmental requirement again; But domestic many water-base cutting fluids not only have a long way to go with external product, and also very large with the Practical Performance gap of oil base cutting fluid, and main Problems existing has: anti-attrition resistance to abrasion is slightly poor, and rust-preventing characteristic is slightly poor, is subject to bacteria effect and corrosion etc. occurs.Current, along with the development of nanotechnology and lubrication technology, micro Nano material being combined with water-base cutting fluid, providing extraordinary approach for preparing high-wearing feature water-base cutting fluid.
Summary of the invention
For the demand, the invention provides a kind of high-wearing feature water-base cutting fluid and preparation method thereof, this water-base cutting fluid production cost is low, safety non-toxic, and have good oilness, rust-preventing characteristic, corrosion-resistant and stability, its anti-wear and wear-resistant performance is obviously better than like product.
The present invention is a kind of high-wearing feature water-base cutting fluid and preparation method thereof, described water-base cutting fluid is prepared from by following raw material: oleic acid, organic alcohol amine, boric acid, molybdenumdisulphide, compound emulsifying agent, composite antirust agent, compound disinfectant, silicone antifoam agent, deionized water, described preparation method comprises the steps: a) to prepare component A product, b) prepare B component product, c) mix A, B component preparing finished articles.
In a preferred embodiment of the present invention, 1:1 is composite in mass ratio forms by cats product Gemini quaternary ammonium salt and nonionogenic tenside alkyl glycoside for described compound emulsifying agent.
In a preferred embodiment of the present invention, by alkenyl succinic acid ester and benzotriazole, 2:3 is composite in mass ratio forms in described composite antirust agent.
In a preferred embodiment of the present invention, 2:1 is composite in mass ratio forms by polyquaternium and isothiazolinone for described compound disinfectant.
In a preferred embodiment of the present invention, in described step a), the raw material that preparation component A product is selected and weight percentage are: oleic acid 18 ~ 20%, organic alcohol amine 12 ~ 14%, boric acid 8 ~ 10%, molybdenumdisulphide 2 ~ 3%, deionized water 53 ~ 60%.
In a preferred embodiment of the present invention, the processing condition of described preparation component A product are: whipping temp 55 DEG C, stirring velocity 60r/min, churning time 25min.
In a preferred embodiment of the present invention, in described step b), the raw material that preparation B component product is selected and weight percentage are: compound emulsifying agent 20 ~ 22%, composite antirust agent 10 ~ 12%, compound disinfectant 6 ~ 8%, silicone antifoam agent 2 ~ 4%, deionized water 54 ~ 62%.
In a preferred embodiment of the present invention, the processing condition of described preparation B component product are: whipping temp 40 DEG C, stirring velocity 40r/min, churning time 15min.
In a preferred embodiment of the present invention, in described step c), the processing condition of mixing A, B component preparing finished articles are: whipping temp 60 DEG C, stirring velocity 80r/min, churning time 20min.
Present invention is disclosed a kind of high-wearing feature water-base cutting fluid and preparation method thereof, this water-base cutting fluid production cost be low, safety non-toxic, have good oilness, rust-preventing characteristic, corrosion-resistant and stability, its anti-wear and wear-resistant performance is obviously better than like product.
Accompanying drawing explanation
Below in conjunction with the drawings and specific embodiments, the present invention is further detailed explanation:
Fig. 1 is the process figure of embodiment of the present invention high-wearing feature water-base cutting fluid preparation method.
Embodiment
Below in conjunction with accompanying drawing, preferred embodiment of the present invention is described in detail, can be easier to make advantages and features of the invention be readily appreciated by one skilled in the art, thus more explicit defining is made to protection scope of the present invention.
Fig. 1 is the process figure of embodiment of the present invention high-wearing feature water-base cutting fluid preparation method; This water-base cutting fluid is prepared from by following raw material: oleic acid, organic alcohol amine, boric acid, molybdenumdisulphide, compound emulsifying agent, composite antirust agent, compound disinfectant, silicone antifoam agent, deionized water, described preparation method comprises the steps: a) to prepare component A product, b) prepare B component product, c) mix A, B component preparing finished articles.
The high-wearing feature water-base cutting fluid that the present invention mentions adopts the method for brand-new lubricant, emulsifying agent and additive compatibility to be prepared, wherein, lubricant is a kind of oleic acid organic alcohol amine boron ester, it is formulated by oleic acid, organic alcohol amine and boric acid, this lubricant oxidation good stability, low-temperature fluidity are good, have good oilness, sticky warm nature and the extreme pressure property that resistance to wears.1:1 is composite in mass ratio forms by cats product Gemini quaternary ammonium salt and nonionogenic tenside alkyl glycoside for emulsifying agent; Wherein, cats product Gemini quaternary ammonium salt is the tensio-active agent containing 2 hydrophilic groups and 2 oleophilic groups in a kind of molecule, this structure enhances the hydrophobic interaction of hydrocarbon chain on the one hand, make the repulsive interaction between hydrophilic group because greatly weakening by chemical bond restriction on the other hand, therefore tensio-active agent can be made to possess more excellent physics-chem characteristic; Nontoxic, non-stimulated, the low bubble of this cats product, itself and nontoxic, readily biodegradable, high surface the composite use of nonionogenic tenside alkyl glycoside, can significantly improve the oilness of metal working fluid, cleaning and cooling.The additive that this high-wearing feature water-base cutting fluid is selected comprises molybdenumdisulphide, composite antirust agent, compound disinfectant and silicone antifoam agent; Wherein, molybdenumdisulphide adds in cutting fluid as a kind of micro Nano material of frictional behaviour excellence, substantially increases the anti-wear and wear-resistant performance of cutting fluid; By alkenyl succinic acid ester and benzotriazole, 2:3 is composite in mass ratio forms in composite antirust agent, and this composite antirust agent is nontoxic, can significantly improve antirust, the Corrosion Protection of cutting fluid to metal; 2:1 is composite in mass ratio forms by polyquaternium and isothiazolinone for compound disinfectant, wherein, polyquaternium good water solubility, germicidal action is gentle, there is certain dispersion, osmosis, there is certain deodorizing and corrosion inhibition simultaneously, itself and the composite use of universal bactericide of iso-thiazolinone, the Antimicrobial preservative of the cutting fluid that can significantly improve.
Embodiment 1
Concrete preparation method is as follows:
A) component A product is prepared, concrete preparation process is: weight percentage, first get the oleic acid of 18%, the organic alcohol amine of 12%, boric acid, the molybdenumdisulphide of 2%, the deionized water of 60% of 8%, they are put into thermostat water bath, then 55 DEG C are heated to, with 60r/min rotating speed stirring reaction 25min, obtain component A product.
B) B component product is prepared, concrete preparation process is: weight percentage, first get the compound emulsifying agent of 20%, the composite antirust agent of 10%, compound disinfectant, the silicone antifoam agent of 2%, the deionized water of 62% of 6%, they are put into thermostat water bath, then 40 DEG C are heated to, with 40r/min rotating speed stirring reaction 15min, obtain B component product.
C) A, B component preparing finished articles is mixed, B component product prepared by the component A product first step a) prepared and step b) puts into thermostat water bath, be heated to 60 DEG C, with 80r/min rotating speed stirring reaction 20min, be then cooled to room temperature and can obtain high-wearing feature water-base cutting fluid finished product.
Embodiment 2
Concrete preparation method is as follows:
A) component A product is prepared, concrete preparation process is: weight percentage, first get the oleic acid of 20%, the organic alcohol amine of 14%, boric acid, the molybdenumdisulphide of 3%, the deionized water of 53% of 10%, they are put into thermostat water bath, then 55 DEG C are heated to, with 60r/min rotating speed stirring reaction 25min, obtain component A product.
B) B component product is prepared, concrete preparation process is: weight percentage, first get the compound emulsifying agent of 22%, the composite antirust agent of 12%, compound disinfectant, the silicone antifoam agent of 4%, the deionized water of 54% of 8%, they are put into thermostat water bath, then 40 DEG C are heated to, with 40r/min rotating speed stirring reaction 15min, obtain B component product.
C) A, B component preparing finished articles is mixed, B component product prepared by the component A product first step a) prepared and step b) puts into thermostat water bath, be heated to 60 DEG C, with 80r/min rotating speed stirring reaction 20min, be then cooled to room temperature and can obtain high-wearing feature water-base cutting fluid finished product.
Present invention is disclosed a kind of high-wearing feature water-base cutting fluid and preparation method thereof, this water-base cutting fluid production cost be low, safety non-toxic, have good oilness, rust-preventing characteristic, corrosion-resistant and stability, its anti-wear and wear-resistant performance is obviously better than like product.
The above; be only the specific embodiment of the present invention; but protection scope of the present invention is not limited thereto; any those of ordinary skill in the art are in the technical scope disclosed by the present invention; the change can expected without creative work or replacement, all should be encompassed within protection scope of the present invention.Therefore, the protection domain that protection scope of the present invention should limit with claims is as the criterion.
Claims (9)
1. high-wearing feature water-base cutting fluid and preparation method thereof, it is characterized in that, described water-base cutting fluid is prepared from by following raw material: oleic acid, organic alcohol amine, boric acid, molybdenumdisulphide, compound emulsifying agent, composite antirust agent, compound disinfectant, silicone antifoam agent, deionized water, described preparation method comprises the steps: a) to prepare component A product, b) prepare B component product, c) mix A, B component preparing finished articles.
2. high-wearing feature water-base cutting fluid according to claim 1 and preparation method thereof, is characterized in that, 1:1 is composite in mass ratio forms by cats product Gemini quaternary ammonium salt and nonionogenic tenside alkyl glycoside for described compound emulsifying agent.
3. high-wearing feature water-base cutting fluid according to claim 1 and preparation method thereof, is characterized in that, by alkenyl succinic acid ester and benzotriazole, 2:3 is composite in mass ratio forms in described composite antirust agent.
4. high-wearing feature water-base cutting fluid according to claim 1 and preparation method thereof, is characterized in that, 2:1 is composite in mass ratio forms by polyquaternium and isothiazolinone for described compound disinfectant.
5. high-wearing feature water-base cutting fluid according to claim 1 and preparation method thereof, it is characterized in that, in described step a), the raw material that preparation component A product is selected and weight percentage are: oleic acid 18 ~ 20%, organic alcohol amine 12 ~ 14%, boric acid 8 ~ 10%, molybdenumdisulphide 2 ~ 3%, deionized water 53 ~ 60%.
6. high-wearing feature water-base cutting fluid according to claim 5 and preparation method thereof, is characterized in that, the processing condition of described preparation component A product are: whipping temp 55 DEG C, stirring velocity 60r/min, churning time 25min.
7. high-wearing feature water-base cutting fluid according to claim 1 and preparation method thereof, it is characterized in that, in described step b), the raw material that preparation B component product is selected and weight percentage are: compound emulsifying agent 20 ~ 22%, composite antirust agent 10 ~ 12%, compound disinfectant 6 ~ 8%, silicone antifoam agent 2 ~ 4%, deionized water 54 ~ 62%.
8. high-wearing feature water-base cutting fluid according to claim 7 and preparation method thereof, is characterized in that, the processing condition of described preparation B component product are: whipping temp 40 DEG C, stirring velocity 40r/min, churning time 15min.
9. high-wearing feature water-base cutting fluid according to claim 1 and preparation method thereof, is characterized in that, in described step c), the processing condition of mixing A, B component preparing finished articles are: whipping temp 60 DEG C, stirring velocity 80r/min, churning time 20min.
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| CN104745282A (en) * | 2015-04-10 | 2015-07-01 | 合肥环照高分子材料厂 | Raw silk highly-antirust cutting solution |
| CN105670762A (en) * | 2016-03-24 | 2016-06-15 | 北京科技大学 | Water-based metal-processing lubricating liquid containing nano molybdenum disulfide and preparation method of water-based metal-processing lubricating liquid |
| CN105985856A (en) * | 2015-02-27 | 2016-10-05 | 全椒县兴盛化工厂 | Monocrystal silicon cutting fluid |
| CN109913292A (en) * | 2019-04-04 | 2019-06-21 | 上海绿晟环保科技有限公司 | A kind of multifunction additive and its preparation method and application for cutting fluid |
| CN110982602A (en) * | 2019-12-23 | 2020-04-10 | 联泓(江苏)新材料研究院有限公司 | Biological stable low-oil-content microemulsion and preparation method and application thereof |
| CN114276863A (en) * | 2021-11-29 | 2022-04-05 | 常州巨石新能源科技有限公司 | Water-based cutting fluid and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109913292B (en) * | 2019-04-04 | 2022-04-15 | 上海绿晟环保科技有限公司 | Multifunctional additive for cutting fluid and preparation method and application thereof |
| CN110982602A (en) * | 2019-12-23 | 2020-04-10 | 联泓(江苏)新材料研究院有限公司 | Biological stable low-oil-content microemulsion and preparation method and application thereof |
| CN114276863A (en) * | 2021-11-29 | 2022-04-05 | 常州巨石新能源科技有限公司 | Water-based cutting fluid and preparation method thereof |
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Application publication date: 20150204 |