CN103468380B - A kind of aluminium wiredrawing lubricating grease - Google Patents

Abstract

A kind of aluminium wiredrawing lubricating grease, is made up of the raw material of following weight part: SN150 base oil 40-50, stearic acid 2-3, molybdenumdisulphide 2-3, polyisobutene 2-3, nano-graphite 0.3-0.5, defoamer are T901 1-2, propylene glycol 5-8, Viscotrol C potash soap 1-2, sulfuration haco oil 2-3, tertbutyl peroxide 1-2, modification aluminium nitride powder 2-3, water 1000.

Description

A kind of aluminium wiredrawing lubricating grease

Technical field

The present invention relates to metal wire drawing lubrication technical field, is a kind of aluminium wiredrawing lubricating grease and preparation method thereof.

Background technology

In existing drawing process, the lubricating oil that adopts as wire drawing medium more, and the conductive line surfaces that drawing goes out is mellow and full, fine and smooth, smooth, bright, no-sundries is detained, and wire broken rate reduces, and quality product improves greatly.But lubricating oil heat radiation is slow, damage mould, affect quality product, while high temperature easily to ignite oil product or oil evaporation is smoldered cause site environment to worsen.

Summary of the invention

The object of this invention is to provide a kind of aluminium wiredrawing lubricating grease and preparation method thereof, have that film forming properties is good, lubricant effect is good, stability is high, heat transfer rate is fast, the feature of good cooling results, easy cleaning.

Technical scheme of the present invention is as follows:

A kind of aluminium wiredrawing lubricating grease, is characterized in that being made up of the raw material of following weight part: SN150 base oil 40-50, stearic acid 2-3, molybdenumdisulphide 2-3, polyisobutene 2-3, nano-graphite 0.3-0.5, defoamer are T901 1-2, propylene glycol 5-8, Viscotrol C potash soap 1-2, sulfuration haco oil 2-3, tertbutyl peroxide 1-2, modification aluminium nitride powder 2-3, water 1000;

Modification aluminium nitride powder is made up of the raw material of following weight part:

Tea-polyphenol 0.3-0.5, ammonium persulphate 0.8-1.2, polyvinyl alcohol 2.3-2.5, Sodium dodecylbenzene sulfonate 1.0-1.2, silane coupling agent KH560 1.2-1.5, ammonium molybdate 2.3-2.5, morpholine 1.4-1.6, jasmin quintessence oil 0.4-0.7, nano aluminum nitride 4.5-5.0, nano silicon 1.2-1.4, methylolurea 1.0-1.5, magnesium hydroxide 0.8-1.2, water 60-65;

The preparation method of described modification aluminium nitride powder is as follows: polyvinyl alcohol, tea-polyphenol are dissolved in the water, are heated to 80-85 DEG C, then add ammonium persulphate, stirring reaction 15-20 minute, then, then adds jasmin quintessence oil, 45-50 DEG C is stirred 10-20 minute, then, add other surplus stock, be warming up to 90-95 DEG C, stirring reaction 30-40 minute, dry, abrasive dust, to obtain final product.

Described aluminium wiredrawing lubricating grease, is characterized in that, preparation method comprises the following steps:

Preparation method is as follows: first SN150 base oil, sulfuration haco oil are added to the water, be heated to 40-45 DEG C, 500-800 rev/min of stirring reaction 10-20 minute, then, then add stearic acid, molybdenumdisulphide, 800-900 rev/min is stirred after 20-25 minute, add other surplus stock again, be warming up to 50-60 DEG C, 700-800 rev/min is continued stirring reaction 1-2 hour, to obtain final product.

Beneficial effect of the present invention is:

The present invention solves the problem that aluminium draws the easy oxidation and rusting of wire surface, the present invention have never degenerate, not dry and cracked, improve the advantages such as wire surface quality.

Embodiment

A kind of aluminium wiredrawing lubricating grease, is characterized in that being made up of the raw material of following weight part (kg): SN150 base oil 45, stearic acid 3, molybdenumdisulphide 3, polyisobutene 2, nano-graphite 0.5, defoamer are T901 2, propylene glycol 5, Viscotrol C potash soap 2, sulfuration haco oil 3, tertbutyl peroxide 2, modification aluminium nitride powder 3, water 1000;

Modification aluminium nitride powder is made up of the raw material of following weight part:

Tea-polyphenol 0.3, ammonium persulphate 1.2, polyvinyl alcohol 2.5, Sodium dodecylbenzene sulfonate 1.0, silane coupling agent KH560 1.5, ammonium molybdate 2.5, morpholine 1.4, jasmin quintessence oil 0.6, nano aluminum nitride 4.5, nano silicon 1.4, methylolurea 1.5, magnesium hydroxide 0.8, water 65;

The preparation method of described modification aluminium nitride powder is as follows: polyvinyl alcohol, tea-polyphenol are dissolved in the water, be heated to 80-85 DEG C, then add ammonium persulphate, stirring reaction 15-20 minute, then, add jasmin quintessence oil again, 45-50 DEG C is stirred 10-20 minute, then, add other surplus stock, be warming up to 90-95 DEG C, stirring reaction 30-40 minute, to obtain final product.

Described aluminium wiredrawing lubricating grease, is characterized in that, preparation method comprises the following steps:

Preparation method is as follows: first SN150 base oil, sulfuration haco oil are added to the water, be heated to 40-45 DEG C, 500-800 rev/min of stirring reaction 10-20 minute, then, add stearic acid, molybdenumdisulphide again, 800-900 rev/min is stirred after 20-25 minute, then adds other surplus stock, be warming up to 50-60 DEG C, 700-800 rev/min is continued stirring reaction 1-2 hour, dry, abrasive dust, to obtain final product.

Use the present embodiment, the highest drawing speed can reach 21m/sec.The copper wire rust prevention during manufacture time of producing is more than 6 days; Concentrate the oil sump drain period to be 3 years, the unit oil sump drain period is 9 months, decreases liquid waste disposal and discharge, protects environment.

Claims (2)

1. an aluminium wiredrawing lubricating grease, is characterized in that being made up of the raw material of following weight part: SN150 base oil 40-50, stearic acid 2-3, molybdenumdisulphide 2-3, polyisobutene 2-3, nano-graphite 0.3-0.5, defoamer are T901 1-2, propylene glycol 5-8, Viscotrol C potash soap 1-2, sulfuration haco oil 2-3, tertbutyl peroxide 1-2, modification aluminium nitride powder 2-3, water 1000;

Modification aluminium nitride powder is made up of the raw material of following weight part:

Tea-polyphenol 0.3-0.5, ammonium persulphate 0.8-1.2, polyvinyl alcohol 2.3-2.5, Sodium dodecylbenzene sulfonate 1.0-1.2, silane coupling agent KH560 1.2-1.5, ammonium molybdate 2.3-2.5, morpholine 1.4-1.6, jasmin quintessence oil 0.4-0.7, nano aluminum nitride 4.5-5.0, nano silicon 1.2-1.4, methylolurea 1.0-1.5, magnesium hydroxide 0.8-1.2, water 60-65;

The preparation method of described modification aluminium nitride powder is as follows: polyvinyl alcohol, tea-polyphenol are dissolved in the water, are heated to 80-85 DEG C, then add ammonium persulphate, stirring reaction 15-20 minute, then, then adds jasmin quintessence oil, 45-50 DEG C is stirred 10-20 minute, then, add other surplus stock, be warming up to 90-95 DEG C, stirring reaction 30-40 minute, dry, abrasive dust, to obtain final product.

2. aluminium wiredrawing lubricating grease according to claim 1, is characterized in that,

Preparation method is as follows: first SN150 base oil, sulfuration haco oil are added to the water, be heated to 40-45 DEG C, 500-800 rev/min of stirring reaction 10-20 minute, then, then add stearic acid, molybdenumdisulphide, 800-900 rev/min is stirred after 20-25 minute, add other surplus stock again, be warming up to 50-60 DEG C, 700-800 rev/min is continued stirring reaction 1-2 hour, to obtain final product.