CN103351916B - A kind of aluminum wire drawing lubricant and preparation method thereof - Google Patents
A kind of aluminum wire drawing lubricant and preparation method thereof Download PDFInfo
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- CN103351916B CN103351916B CN201310243441.XA CN201310243441A CN103351916B CN 103351916 B CN103351916 B CN 103351916B CN 201310243441 A CN201310243441 A CN 201310243441A CN 103351916 B CN103351916 B CN 103351916B
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- wire drawing
- trolamine
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Abstract
A kind of aluminum wire drawing lubricant and preparation method thereof, is characterized in that being made up of the raw material of following weight part: monoethanolamine 0.3-0.4, trolamine 0.6-0.8, mercaptobenzimidazole 0.2-0.3, the acid of pungent certain herbaceous plants with big flowers 1-2, sodium lauryl sulphate 1-2, dibutyl tin laurate 1-2, zinc acetate 1-2, tung oil 1-2, methyltrimethoxy silane 2-3, film coalescence aid 3-4, water 150-160; The present invention adopts tung oil to promote lubricity, adopt and water basely play good thermolysis, increase trolamine and increase rust protection effect, methyltrimethoxy silane of the present invention is combined with mercaptobenzimidazole, the acid of pungent certain herbaceous plants with big flowers and membrane-forming agent, add film forming properties, extend the aluminium conductor rust protection time after wire drawing.
Description
Technical field
The present invention relates to copper, aluminium conductor wire-drawing technology field, is a kind of aluminum wire drawing lubricant and preparation method thereof.
Background technology
Copper cash (silk), aluminum steel (silk) are the prevailing transmission wires of power industry conveying electricity, usually obtained by drawing process, wire such as the steel wire larger by diameter passes through mould hole, and drawing under external force makes its reduced cross-sectional area form the wire rod of required diameter.
In existing drawing process, the lubricating oil that adopts as wire drawing medium more, and the conductive line surfaces that drawing goes out is mellow and full, fine and smooth, smooth, bright, no-sundries is detained, and wire broken rate reduces, and quality product improves greatly.But lubricating oil heat radiation is slow, damage mould, affect quality product, while high temperature easily to ignite oil product or oil evaporation is smoldered cause site environment to worsen.
Summary of the invention
The object of this invention is to provide a kind of aluminum wire drawing lubricant and preparation method thereof, have that film forming properties is good, lubricant effect is good, stability is high, heat transfer rate is fast, the feature of good cooling results, easy cleaning.
Technical scheme of the present invention is as follows:
A kind of aluminum wire drawing lubricant, is characterized in that being made up of the raw material of following weight part:
Monoethanolamine 0.3-0.4, trolamine 0.6-0.8, mercaptobenzimidazole 0.2-0.3, the acid of pungent certain herbaceous plants with big flowers 1-2, sodium lauryl sulphate 1-2, dibutyl tin laurate 1-2, zinc acetate 1-2, tung oil 1-2, methyltrimethoxy silane 2-3, film coalescence aid 3-4, water 150-160;
Described film coalescence aid is made up of the raw material of following weight part: benzoquinones 1-2, vinylbenzene 6-8, tertbutyl peroxide 0.1-0.2, dibutyl itaconate 3-4, Silane coupling agent KH550 1-2,1-hydroxyethyl-2-oil-based imidazoline 2-3; Preparation method is: mixed with itaconic ester by vinylbenzene, stir, add tertbutyl peroxide, benzoquinones, stirring reaction 45-60 minute, then, add 1-hydroxyethyl-2-oil-based imidazoline, stirring reaction, reacts after 2-3 hour, is warming up to 125-130 DEG C, add Silane coupling agent KH550, stirring reaction 2-3 hour; Obtain.
Preparation method is: monoethanolamine, trolamine, sodium lauryl sulphate, tung oil are added to the water, be heated to 90-98 DEG C, stir 40-50 minute, then adding methyltrimethoxy silane stirs after 20-30 minute, add film coalescence aid and stir 30-40 minute, add other remaining component again, reaction 1-2 hour, to obtain final product.
The present invention adopts tung oil to promote lubricity, adopt and water basely play good thermolysis, increase trolamine and increase rust protection effect, methyltrimethoxy silane of the present invention is combined with mercaptobenzimidazole, the acid of pungent certain herbaceous plants with big flowers and membrane-forming agent, add film forming properties, extend the aluminium conductor rust protection time after wire drawing.
The present invention has excellent lubricity, stability in storage, good cooling results, and heat transfer rate is fast, and in use procedure, temperature rise is little, nonflammable, easy cleaning, and the aluminium wire adopting this product to draw is evenly linear, surface-brightening, not easily corrosion.
Embodiment
A kind of aluminum wire drawing lubricant, be made up of the raw material (kilogram) of following weight part:
Monoethanolamine 0.3, trolamine 0.8, mercaptobenzimidazole 0.3, pungent certain herbaceous plants with big flowers acid 1, sodium lauryl sulphate 1, dibutyl tin laurate 2, zinc acetate 1, tung oil 2, methyltrimethoxy silane 2, film coalescence aid 3, water 160;
Preparation method is: monoethanolamine, trolamine, sodium lauryl sulphate, tung oil are added to the water, be heated to 90-98 DEG C, stir 40-50 minute, then adding methyltrimethoxy silane stirs after 20-30 minute, add film coalescence aid and stir 30-40 minute, add other remaining component again, reaction 1-2 hour, to obtain final product.
Described film coalescence aid is made up of the raw material of following weight part (kilogram): benzoquinones 1, vinylbenzene 6, tertbutyl peroxide 0.2, dibutyl itaconate 3, Silane coupling agent KH550 2,1-hydroxyethyl-2-oil-based imidazoline 2; Preparation method is: mixed with itaconic ester by vinylbenzene, stir, add tertbutyl peroxide, benzoquinones, stirring reaction 45-60 minute, then, add 1-hydroxyethyl-2-oil-based imidazoline, stirring reaction, reacts after 2-3 hour, is warming up to 125-130 DEG C, add Silane coupling agent KH550, stirring reaction 2-3 hour; Obtain.
Use wire drawing liquid of the present invention, the highest drawing speed can reach 19m/sec.The copper wire rust prevention during manufacture time of producing is more than 5 days; Concentrate the oil sump drain period to be 3 years, the unit oil sump drain period is 8 months, decreases liquid waste disposal and discharge, protects environment.
Claims (3)
1. an aluminum wire drawing lubricant, is characterized in that being made up of the raw material of following weight part: monoethanolamine 0.3-0.4, trolamine 0.6-0.8, mercaptobenzimidazole 0.2-0.3, pungent capric acid 1-2, sodium lauryl sulphate 1-2, dibutyl tin laurate 1-2, zinc acetate 1-2, tung oil 1-2, methyltrimethoxy silane 2-3, film coalescence aid 3-4, water 150-160;
Described film coalescence aid is made up of the raw material of following weight part: benzoquinones 1-2, vinylbenzene 6-8, tertbutyl peroxide 0.1-0.2, dibutyl itaconate 3-4, Silane coupling agent KH550 1-2,1-hydroxyethyl-2-oil-based imidazoline 2-3;
The preparation method of described film coalescence aid is: mixed with dibutyl itaconate by vinylbenzene, stir, add tertbutyl peroxide, benzoquinones, stirring reaction 45-60 minute, then, add 1-hydroxyethyl-2-oil-based imidazoline, stirring reaction, reacts after 2-3 hour, is warming up to 125-130 DEG C, add Silane coupling agent KH550, stirring reaction 2-3 hour; Obtain.
2. the preparation method of aluminum wire drawing lubricant according to claim 1, it is characterized in that comprising the following steps: monoethanolamine, trolamine, sodium lauryl sulphate, tung oil are added to the water, be heated to 90-98 DEG C, stir 40-50 minute, then add methyltrimethoxy silane to stir after 20-30 minute, add film coalescence aid and stir 30-40 minute, then add other remaining component, reaction 1-2 hour, to obtain final product.
3. aluminum wire drawing lubricant according to claim 1, is characterized in that being made up of the raw material of following weight part: monoethanolamine 0.3, trolamine 0.8, mercaptobenzimidazole 0.3, pungent capric acid 1, sodium lauryl sulphate 1, dibutyl tin laurate 2, zinc acetate 1, tung oil 2, methyltrimethoxy silane 2, film coalescence aid 3, water 160.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310243441.XA CN103351916B (en) | 2013-06-19 | 2013-06-19 | A kind of aluminum wire drawing lubricant and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201310243441.XA CN103351916B (en) | 2013-06-19 | 2013-06-19 | A kind of aluminum wire drawing lubricant and preparation method thereof |
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| Publication Number | Publication Date |
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| CN103351916A CN103351916A (en) | 2013-10-16 |
| CN103351916B true CN103351916B (en) | 2016-02-03 |
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| CN201310243441.XA Expired - Fee Related CN103351916B (en) | 2013-06-19 | 2013-06-19 | A kind of aluminum wire drawing lubricant and preparation method thereof |
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Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10993441B2 (en) | 2014-11-04 | 2021-05-04 | Allied Bioscience, Inc. | Antimicrobial coatings comprising organosilane homopolymers |
| US10980236B2 (en) | 2014-11-04 | 2021-04-20 | Allied Bioscience, Inc. | Broad spectrum antimicrobial coatings comprising combinations of organosilanes |
| US10258046B2 (en) | 2014-11-04 | 2019-04-16 | Allied Bioscience, Inc. | Antimicrobial coatings comprising quaternary silanes |
| EP3215553B1 (en) * | 2014-11-04 | 2021-06-02 | Allied Bioscience, Inc | Method to form a self decontaminating surface |
| CN105038908A (en) * | 2014-12-19 | 2015-11-11 | 李立群 | Degradable hydraulic oil and preparation method thereof |
| CA2972923C (en) | 2015-02-11 | 2019-04-30 | Allied Bioscience, Inc. | Anti-microbial coating and method to form same |
| CN107523378B (en) * | 2017-08-22 | 2020-02-04 | 山东莱克科技有限公司 | Stable benzimidazole antioxidant for lubricating oil and preparation method thereof |
| CN108977257A (en) * | 2018-09-04 | 2018-12-11 | 苏州襄行新材料有限公司 | It is a kind of without sliding microfilament drawing lubricating fluid and preparation method |
| CN112126489B (en) * | 2020-09-14 | 2022-10-11 | 苏州襄行新材料有限公司 | Aging lubricating fluid for wire drawing and rapid preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101747988A (en) * | 2009-12-21 | 2010-06-23 | 克拉玛依市金山石油化工有限公司 | Copper and aluminum wire drawing oil and preparation method and use method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003293797A (en) * | 2002-04-08 | 2003-10-15 | Minebea Co Ltd | Bearing for electronic controlled throttle motor |
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101747988A (en) * | 2009-12-21 | 2010-06-23 | 克拉玛依市金山石油化工有限公司 | Copper and aluminum wire drawing oil and preparation method and use method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 有色金属轧制工艺润滑技术研究;李德峰等;《轻金属》;20001231(第6期);58-60 * |
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