CN103468379B

CN103468379B - A kind of aluminum wire drawing lubricant

Info

Publication number: CN103468379B
Application number: CN201310372392.XA
Authority: CN
Inventors: 何康
Original assignee: TIANCHANG KANGHE METAL MATERIAL Co Ltd
Current assignee: TIANCHANG KANGHE METAL MATERIAL Co Ltd
Priority date: 2013-08-24
Filing date: 2013-08-24
Publication date: 2015-09-09
Anticipated expiration: 2033-08-24
Also published as: CN103468379A

Abstract

A kind of aluminum wire drawing lubricant, it is characterized in that being made up of the raw material of following weight part: rapeseed oil 20-24,2,5 di tert butyl hydroquinone 1-2,2-aminoethyl 17 alkenyl imidazoline 1-2, sulphur phosphorus fourth octyl group zinc salt 2-3, diisobutyl phthalate 1-2, aluminum stearate 2-3, diesel oil 30-34, two ten four carbon alcohols ester 12-14, petroleum sodium sulfonate 2-3, tertbutyl peroxide 1-2, modified silicon carbide powder 2-3, water 1000.

Description

A kind of aluminum wire drawing lubricant

Technical field

The present invention relates to copper, aluminium conductor wire-drawing technology field, is a kind of aluminum wire drawing lubricant and preparation method thereof.

Background technology

In existing drawing process, the lubricating oil that adopts as wire drawing medium more, and the conductive line surfaces that drawing goes out is mellow and full, fine and smooth, smooth, bright, no-sundries is detained, and wire broken rate reduces, and quality product improves greatly.But lubricating oil heat radiation is slow, damage mould, affect quality product, while high temperature easily to ignite oil product or oil evaporation is smoldered cause site environment to worsen.

Summary of the invention

The object of this invention is to provide a kind of aluminum wire drawing lubricant.

Technical scheme of the present invention is as follows:

A kind of aluminum wire drawing lubricant, it is characterized in that being made up of the raw material of following weight part: rapeseed oil 20-24,2,5 di tert butyl hydroquinone 1-2,2-aminoethyl 17 alkenyl imidazoline 1-2, sulphur phosphorus fourth octyl group zinc salt 2-3, diisobutyl phthalate 1-2, aluminum stearate 2-3, diesel oil 30-34, two ten four carbon alcohols ester 12-14, petroleum sodium sulfonate 2-3, tertbutyl peroxide 1-2, modified silicon carbide powder 2-3, water 1000;

Modified silicon carbide powder is made up of the raw material of following weight part: tripoly phosphate sodium STPP 2.3-2.5, chitosan 1.6-1.8, Sodium Persulfate 1.0-1.2,1-hydroxyethyl-2-oil-based imidazoline 2.0-2.3, nanometer silicon carbide 3.4-3.8, nanometer silicon carbide 1.2-1.4, Sodium dodecylbenzene sulfonate 0.4-0.7, silane resin acceptor kh-550 1.2-1.3, methylolurea 2.0-2.3, polyvinylpyrrolidone 2.4-2.8, water 50;

The preparation method of described modified silicon carbide powder is as follows: chitosan, tripoly phosphate sodium STPP are dissolved in the water, add Sodium Persulfate again, 35-45 DEG C is selected stirring reaction 35-40 minute, then, then adds silane resin acceptor kh-550, polyvinylpyrrolidone, 1000-1200 rev/min is stirred 30-45 minute, then, add other surplus stock, be warming up to 90-95 DEG C, 1200-1500 rev/min of stirring reaction 1-2 hour, to obtain final product.

Described aluminum wire drawing lubricant, is characterized in that, preparation method comprises the following steps:

Preparation method is as follows: first rapeseed oil, sulphur phosphorus fourth octyl group zinc salt are added to the water, be heated to 50-55 DEG C, stirring reaction 20-30 minute, then, then adds aluminum stearate, diesel oil, stir after 20-30 minute, add other raw material again, be warming up to 80-90 DEG C, 100-300 rev/min is continued stirring reaction 1-2 hour, oven dry, abrasive dust, to obtain final product.

Beneficial effect of the present invention is:

Cost of the present invention is lower, and oilness is good, and wire-drawing effect is good, and drawing speed is fast, is applicable to high-speed wire-drawing, the aluminum steel any surface finish of drawing, and greasy dirt and aluminium powder attachment less, need not through cleanings for the japanning of felt method.

Embodiment

A kind of aluminum wire drawing lubricant, it is characterized in that being made up of the raw material of following weight part (kg): rapeseed oil 24,2,5 di tert butyl hydroquinone 2,2-aminoethyl 17 alkenyl imidazoline 2, sulphur phosphorus fourth octyl group zinc salt 3, diisobutyl phthalate 2, aluminum stearate 2.3, diesel oil 34, two ten four carbon alcohols esters 14, petroleum sodium sulfonate 3, tertbutyl peroxide 2, modified silicon carbide powder 2, water 1000;

Modified silicon carbide powder is made up of the raw material of following weight part: tripoly phosphate sodium STPP 2.5, chitosan 1.8, Sodium Persulfate 1.0,1-hydroxyethyl-2-oil-based imidazoline 2.3, nanometer silicon carbide 3.4, nanometer silicon carbide 1.4, Sodium dodecylbenzene sulfonate 0.7, silane resin acceptor kh-550 1.3, methylolurea 2.0, polyvinylpyrrolidone 2.8, water 50;

The preparation method of described modified silicon carbide powder is as follows: chitosan, tripoly phosphate sodium STPP are dissolved in the water, add Sodium Persulfate again, 38 DEG C are selected stirring reaction 40 minutes, then, add silane resin acceptor kh-550, polyvinylpyrrolidone again, 1200 revs/min are stirred 45 minutes, then, add other surplus stock, be warming up to 95 DEG C, 1500 revs/min of stirring reactions 2 hours, dry, abrasive dust, to obtain final product.

Described aluminum wire drawing lubricant, preparation method comprises the following steps:

Preparation method is as follows: first rapeseed oil, sulphur phosphorus fourth octyl group zinc salt are added to the water, are heated to 55 DEG C, stirring reaction 30 minutes, then, add aluminum stearate, diesel oil again, stir after 30 minutes, then add other raw material, be warming up to 80 DEG C, 300 revs/min are continued stirring reaction 2 hours, to obtain final product.

Use the present embodiment, the highest drawing speed can reach 17m/sec.The copper wire rust prevention during manufacture time of producing is more than 5 days; Concentrate the oil sump drain period to be 3 years, the unit oil sump drain period is 10 months, decreases liquid waste disposal and discharge, protects environment.

Claims

1. an aluminum wire drawing lubricant, it is characterized in that being made up of the raw material of following weight part: rapeseed oil 20-24,2,5 di tert butyl hydroquinone 1-2,2-aminoethyl 17 alkenyl imidazoline 1-2, sulphur phosphorus fourth octyl group zinc salt 2-3, diisobutyl phthalate 1-2, aluminum stearate 2-3, diesel oil 30-34, two ten four carbon alcohols ester 12-14, petroleum sodium sulfonate 2-3, tertbutyl peroxide 1-2, modified silicon carbide powder 2-3, water 1000;

The preparation method of described modified silicon carbide powder is as follows: chitosan, tripoly phosphate sodium STPP are dissolved in the water, add Sodium Persulfate again, 35-45 DEG C of stirring reaction 35-40 minute, then, add silane resin acceptor kh-550, polyvinylpyrrolidone again, 1000-1200 rev/min is stirred 30-45 minute, then, adds other surplus stock, be warming up to 90-95 DEG C, 1200-1500 rev/min of stirring reaction 1-2 hour, oven dry, abrasive dust, to obtain final product.

2. aluminum wire drawing lubricant according to claim 1, is characterized in that, preparation method comprises the following steps:

Preparation method is as follows: first rapeseed oil, sulphur phosphorus fourth octyl group zinc salt are added to the water, be heated to 50-55 DEG C, stirring reaction 20-30 minute, then, then add aluminum stearate, diesel oil, stir after 20-30 minute, add other raw material again, be warming up to 80-90 DEG C, 100-300 rev/min is continued stirring reaction 1-2 hour, to obtain final product.