CN103468379A

CN103468379A - Aluminum wire drawing lubricant

Info

Publication number: CN103468379A
Application number: CN201310372392XA
Authority: CN
Inventors: 何康
Original assignee: TIANCHANG KANGHE METAL MATERIAL Co Ltd
Current assignee: TIANCHANG KANGHE METAL MATERIAL Co Ltd
Priority date: 2013-08-24
Filing date: 2013-08-24
Publication date: 2013-12-25
Anticipated expiration: 2033-08-24
Also published as: CN103468379B

Abstract

The invention provides an aluminum wire drawing lubricant which is characterized by being prepared from the following raw materials in parts by weight: 20 to 24 parts of rapeseed oil, 1 to 2 parts of 2,5-di-tert-butylhydroquinone, 1 to 2 parts of 2-aminoethyl seventeen alkenyl imidazoline, 2 to 3 parts of sulfurphosphorousbutyloctyl zinc salt, 1 to 2 parts of diisobutyl phthalate, 2 to 3 parts of aluminium stearate, 30 to 40 parts of diesel oil, 12 to 14 parts of double fourteen carbon alcohol ester, 2 to 3 parts of petroleum sodium sulfonate, 1 to 2 parts of tert-butyl hydroperoxide, 2 to 3 parts of modified silicon carbide powder and 1000 parts of water.

Description

A kind of aluminum wire drawing lubricant

Technical field

The present invention relates to copper, aluminium conductor wire-drawing technology field, is a kind of aluminum wire drawing lubricant and preparation method thereof.

Background technology

In existing drawing process, the lubricating oil that adopts as the wire drawing medium more, and the conductive line surfaces that drawing goes out is mellow and full, fine and smooth, smooth, bright, no-sundries is detained, and wire broken rate reduces, and quality product improves greatly.But lubricating oil heat radiation is slow, the damage mould, affect quality product, simultaneously easily ignite oil product or oil evaporation is smoldered cause the site environment deterioration of high temperature.

Summary of the invention

The purpose of this invention is to provide a kind of aluminum wire drawing lubricant.

Technical scheme of the present invention is as follows:

A kind of aluminum wire drawing lubricant, it is characterized in that being made by the raw material of following weight part: rapeseed oil 20-24,2,5 di tert butyl hydroquinone 1-2,2-aminoethyl 17 alkenyl imidazoline 1-2, sulphur phosphorus fourth octyl group zinc salt 2-3, diisobutyl phthalate 1-2, aluminum stearate 2-3, diesel oil 30-34, two ten four carbon alcohols ester 12-14, petroleum sodium sulfonate 2-3, tertbutyl peroxide 1-2, modified silicon carbide powder 2-3, water 1000;

Modified silicon carbide powder is made by the raw material of following weight part: tripoly phosphate sodium STPP 2.3-2.5, chitosan 1.6-1.8, Sodium Persulfate 1.0-1.2,1-hydroxyethyl-2-oil-based imidazoline 2.0-2.3, nanometer silicon carbide 3.4-3.8, nanometer silicon carbide 1.2-1.4, Sodium dodecylbenzene sulfonate 0.4-0.7, silane resin acceptor kh-550 1.2-1.3, methylolurea 2.0-2.3, polyvinylpyrrolidone 2.4-2.8, water 50;

The preparation method of described modified silicon carbide powder is as follows: chitosan, tripoly phosphate sodium STPP are dissolved in the water, add again Sodium Persulfate, 35-45 ℃ is selected stirring reaction 35-40 minute, then, then adds silane resin acceptor kh-550, polyvinylpyrrolidone, 1000-1200 rev/min is stirred 30-45 minute, then, add other surplus stock, be warming up to 90-95 ℃, 1200-1500 rev/min of stirring reaction 1-2 hour, obtain.

Described aluminum wire drawing lubricant, is characterized in that, the preparation method comprises the following steps:

The preparation method is as follows: first rapeseed oil, sulphur phosphorus fourth octyl group zinc salt are added to the water, be heated to 50-55 ℃, stirring reaction 20-30 minute, then, then add aluminum stearate, diesel oil, stir after 20-30 minute, add other raw material again, be warming up to 80-90 ℃, 100-300 rev/min is continued stirring reaction 1-2 hour, oven dry, abrasive dust, obtain.

Beneficial effect of the present invention is:

Cost of the present invention is lower, and oilness is good, and wire-drawing effect is good, and drawing speed is fast, is applicable to high-speed wire-drawing, the aluminum steel any surface finish of drawing, and greasy dirt and aluminium powder adhere to few, need not be through cleaning for the japanning of felt method.

Embodiment

A kind of aluminum wire drawing lubricant, it is characterized in that being made by the raw material of following weight part (kg): rapeseed oil 24,2,5 di tert butyl hydroquinone 2,2-aminoethyl 17 alkenyl imidazolines 2, sulphur phosphorus fourth octyl group zinc salt 3, diisobutyl phthalate 2, aluminum stearate 2.3, diesel oil 34, two ten four carbon alcohols esters 14, petroleum sodium sulfonate 3, tertbutyl peroxide 2, modified silicon carbide powder 2, water 1000;

Modified silicon carbide powder is made by the raw material of following weight part: tripoly phosphate sodium STPP 2.5, chitosan 1.8, Sodium Persulfate 1.0,1-hydroxyethyl-2-oil-based imidazoline 2.3, nanometer silicon carbide 3.4, nanometer silicon carbide 1.4, Sodium dodecylbenzene sulfonate 0.7, silane resin acceptor kh-550 1.3, methylolurea 2.0, polyvinylpyrrolidone 2.8, water 50;

The preparation method of described modified silicon carbide powder is as follows: chitosan, tripoly phosphate sodium STPP are dissolved in the water, add Sodium Persulfate, 38 ℃ are selected stirring reaction 40 minutes, then again, add again silane resin acceptor kh-550, polyvinylpyrrolidone, 1200 rev/mins are stirred 45 minutes, then, add other surplus stock, be warming up to 95 ℃, 1500 rev/mins of stirring reactions 2 hours, dry, abrasive dust, obtains.

Described aluminum wire drawing lubricant, the preparation method comprises the following steps:

The preparation method is as follows: first rapeseed oil, sulphur phosphorus fourth octyl group zinc salt is added to the water, is heated to 55 ℃, and stirring reaction 30 minutes, then, add again aluminum stearate, diesel oil, after stirring 30 minutes, then add other raw material, be warming up to 80 ℃, 300 rev/mins are continued stirring reaction 2 hours, obtain.

Use the present embodiment, the highest drawing speed can reach 17m/sec.The copper wire rust prevention during manufacture time of producing is more than 5 days; Concentrating the oil sump drain period is 3 years, and the unit oil sump drain period is 10 months, has reduced liquid waste disposal and discharge, has protected environment.

Claims

1. an aluminum wire drawing lubricant, it is characterized in that being made by the raw material of following weight part: rapeseed oil 20-24,2,5 di tert butyl hydroquinone 1-2,2-aminoethyl 17 alkenyl imidazoline 1-2, sulphur phosphorus fourth octyl group zinc salt 2-3, diisobutyl phthalate 1-2, aluminum stearate 2-3, diesel oil 30-34, two ten four carbon alcohols ester 12-14, petroleum sodium sulfonate 2-3, tertbutyl peroxide 1-2, modified silicon carbide powder 2-3, water 1000;

The preparation method of described modified silicon carbide powder is as follows: chitosan, tripoly phosphate sodium STPP are dissolved in the water, add Sodium Persulfate, 35-45 ℃ is selected stirring reaction 35-40 minute, then again, add again silane resin acceptor kh-550, polyvinylpyrrolidone, 1000-1200 rev/min is stirred 30-45 minute, then, adds other surplus stock, be warming up to 90-95 ℃, 1200-1500 rev/min of stirring reaction 1-2 hour, oven dry, abrasive dust, obtain.

2. aluminum wire drawing lubricant according to claim 1, is characterized in that, the preparation method comprises the following steps:

The preparation method is as follows: first rapeseed oil, sulphur phosphorus fourth octyl group zinc salt are added to the water, be heated to 50-55 ℃, stirring reaction 20-30 minute, then, then add aluminum stearate, diesel oil, stir after 20-30 minute, add again other raw material, be warming up to 80-90 ℃, 100-300 rev/min is continued stirring reaction 1-2 hour, obtains.