CN105967582A - Leaking stoppage waterproof paint and preparation method thereof - Google Patents

Leaking stoppage waterproof paint and preparation method thereof Download PDF

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Publication number
CN105967582A
CN105967582A CN201610292848.5A CN201610292848A CN105967582A CN 105967582 A CN105967582 A CN 105967582A CN 201610292848 A CN201610292848 A CN 201610292848A CN 105967582 A CN105967582 A CN 105967582A
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CN
China
Prior art keywords
leakage
blocking water
proof paint
retarder
cement
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Granted
Application number
CN201610292848.5A
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Chinese (zh)
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CN105967582B (en
Inventor
潘巨峰
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Shanghai Zhonghui Waterproof Engineering Co Ltd
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Shanghai Zhonghui Waterproof Engineering Co Ltd
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Priority to CN201610292848.5A priority Critical patent/CN105967582B/en
Publication of CN105967582A publication Critical patent/CN105967582A/en
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00482Coating or impregnation materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/20Resistance against chemical, physical or biological attack
    • C04B2111/27Water resistance, i.e. waterproof or water-repellent materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/72Repairing or restoring existing buildings or building materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Sealing Material Composition (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention discloses leaking stoppage waterproof paint and a preparation method thereof. The leaking stoppage waterproof paint is prepared from 95-105 parts by weight of cement, 10-20 parts by weight of an accelerator, 1-5 parts by weight of glass fibers, 3-7 parts by weight of redispersible glue powder, 0.01-0.03 parts by weight of hydroxyethyl cellulose, 0.02-0.03 parts by weight of a retarder and 0.2-0.6 parts by weight of a filler. Through a reasonable formula and selection of appropriate types and amounts of the waterproof paint accelerator and retarder, water resistance, weather resistance, fire resistance, corrosion resistance and stability are improved, bonding strength is high, safety is obtained, toxicity is avoided, curing time is shortened, construction is convenient and efficiency is high.

Description

Leakage-blocking water-proof paint and preparation method thereof
Technical field
The present invention relates to technical field of coatings, particularly relate to a kind of leakage-blocking water-proof paint and preparation method thereof.
Background technology
Paint finishing can very well bond with matrix material in body surface and form complete and tough and tensile protecting film Material, referred to as coating.Coating and paint are the identicals concept.Paint is people's custom used for a long time titles, After introducing China, utilize in building trade the most always.The effect of coating may be summarized to be three aspects: protects Protect effect, decoration function, specific function effect.The general composition of coating: comprise film forming matter, face is filled out Material, solvent, auxiliary agent.
Building coating has decoration functions, defencive function and livability and improves function.Shared by various functions Proportion is not quite similar because application target is different.Decoration functions is to improve its by beautifying of building The function of appearance value.Mainly include the concept in terms of plane color, pattern and gloss and stereo-flower The concept of stricture of vagina.But to match with the size and shape of the moulding of building itself and base material itself, Just can fully play out.
The invention provides a kind of leakage-blocking water-proof paint, there is the heat reflection cooling-down effect of excellence.
Summary of the invention
For above-mentioned deficiency present in prior art, one of the technical problem to be solved is to carry For a kind of leakage-blocking water-proof paint.
The two of the technical problem to be solved are to provide the preparation method of a kind of leakage-blocking water-proof paint.
The present invention seeks to be achieved through the following technical solutions:
A kind of leakage-blocking water-proof paint, is prepared from by the raw material of following weight parts:
Cement 95-105 part, accelerator 10-20 part, glass fibre 1-5 part, redispersible rubber powder 3-7 Part, hydroxyethyl cellulose 0.01-0.03 part, retarder 0.02-0.05 part, inserts 0.2-0.6 part.
Preferably, described cement is high-mark cement, described high-mark cement selected from being numbered 62.5, 52.5, in 52.5R, 62.5R one or more.
Preferably, described accelerator is a kind of or many in lithium carbonate, sodium aluminate, zinc oxide, aluminum sulfate The mixture planted.
It is highly preferred that described accelerator is mixed by lithium carbonate, sodium aluminate, zinc oxide, described carbon Acid lithium, sodium aluminate, the mass ratio of zinc oxide are (1-3): (1-3): (1-3).
Preferably, described redispersible rubber powder can be bought or prepare, it is also possible to reference to patent Application number: in 201110240131.3 prepared by the method for embodiment 1.
Preferably, described retarder is one or more in sodium humate, calcium citrate, magnesium stearate Mixture.
It is highly preferred that described retarder is mixed by sodium humate, calcium citrate, magnesium stearate, Described sodium humate, calcium citrate, the mass ratio of magnesium stearate are (1-3): (1-3): (1-3).
Preferably, described inserts is one or more in titanium dioxide, silicon dioxide, Kaolin Mixture.
Present invention also offers the preparation method of above-mentioned leakage-blocking water-proof paint: by cement, accelerator, glass Fiber, redispersible rubber powder, hydroxyethyl cellulose, retarder, inserts mix homogeneously and get final product.
Leakage-blocking water-proof paint that the present invention provides and preparation method thereof, by rational proportioning, preferably goes out suitable Close water-repellent paint accelerator, the kind of retarder and consumption, improve resistance to water, weatherability, fire resistance, Corrosion resistance and excellent in stability, adhesion strength is high, safety non-toxic, and hardening time is short, easy construction, Efficiency is high.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further, the following stated, only to the present invention Preferred embodiment, not does the restriction of other forms, any technology being familiar with this specialty to the present invention Personnel are changed to the Equivalent embodiments changed on an equal basis possibly also with the technology contents of the disclosure above.Every Without departing from the present invention program content, any letter following example done according to the technical spirit of the present invention Single amendment or equivalent variations, all fall within protection scope of the present invention.
Each raw material introduction in embodiment:
Cement, use Tangshan Polar Bear Building Material Co., Ltd.'s offer is numbered 52.5 cement.
Glass fibre, No. CAS: 65997-17-3, use Nanjing Xing Xing fiberglass products company limited The fiberglas chopped strand provided, length 2mm.
Redispersible rubber powder, with reference to number of patent application: the method for embodiment 1 in 201110240131.3 Preparation.
Hydroxyethyl cellulose, No. CAS: 9004-62-0, use Feicheng Yu Tian Chemical Co., Ltd. to provide Rain field board hydroxyethyl cellulose.
Lithium carbonate, No. CAS: 554-13-2, particle diameter 30-40 μm.
Sodium aluminate, No. CAS: 1302-42-7, particle diameter 30-40 μm.
Zinc oxide, No. CAS: 1314-13-2, particle diameter 30-40nm.
Sodium humate, No. CAS: 68131-04-4.
Calcium citrate, No. CAS: 813-94-5.
Magnesium stearate, No. CAS: 557-04-0.
Titanium dioxide, No. CAS: 13463-67-7, use Du Pont, model is the rutile-type of R-960 Titanium dioxide.
Embodiment 1
Leakage-blocking water-proof paint raw material (weight portion):
No. 52.5 cement 100 parts, accelerator 15 parts, glass fibre 3 parts, redispersible rubber powder 5 Part, hydroxyethyl cellulose 0.02 part, retarder 0.03 part, titanium dioxide 0.4 part.
Described accelerator is mixed for 1:1:1 stirring in mass ratio by lithium carbonate, sodium aluminate, zinc oxide Uniformly obtain.
Described retarder is stirred for 1:1:1 in mass ratio by sodium humate, calcium citrate, magnesium stearate Mix mix homogeneously to obtain.
The preparation method of leakage-blocking water-proof paint: by No. 52.5 cement, accelerator, glass fibre, can divide again Scattered property rubber powder, hydroxyethyl cellulose, retarder, titanium dioxide use cantilever double-spiral conical mixer to stir Mix 15 minutes mix homogeneously and get final product.
Embodiment 2
Substantially the same manner as Example 1, differ only in: described accelerator is pressed by sodium aluminate, zinc oxide Mass ratio is that 1:1 is uniformly mixed and obtains.Obtain the leakage-blocking water-proof paint of embodiment 2.
Embodiment 3
Substantially the same manner as Example 1, differ only in: described accelerator is pressed by lithium carbonate, zinc oxide Mass ratio is that 1:1 is uniformly mixed and obtains.Obtain the leakage-blocking water-proof paint of embodiment 3.
Embodiment 4
Substantially the same manner as Example 1, differ only in: described accelerator is pressed by lithium carbonate, sodium aluminate Mass ratio is that 1:1 is uniformly mixed and obtains.Obtain the leakage-blocking water-proof paint of embodiment 4.
Embodiment 5
Substantially the same manner as Example 1, differ only in: described retarder is by calcium citrate, stearic acid Magnesium is uniformly mixed for 1:1 in mass ratio and obtains.Obtain the leakage-blocking water-proof paint of embodiment 5.
Embodiment 6
Substantially the same manner as Example 1, differ only in: described retarder is by sodium humate, stearic acid Magnesium is uniformly mixed for 1:1 in mass ratio and obtains.Obtain the leakage-blocking water-proof paint of embodiment 6.
Embodiment 7
Substantially the same manner as Example 1, differ only in: described retarder is by sodium humate, citric acid Calcium is uniformly mixed for 1:1 in mass ratio and obtains.Obtain the leakage-blocking water-proof paint of embodiment 7.
Test case 1
The leakage-blocking water-proof paint preparing embodiment 1-7, takes the leak stopping that 1-7 prepares respectively and prevents Water paint 10kg and 6kg water is uniformly mixed i.e. to obtain and can be used for constructing, and builds according to the People's Republic of China (PRC) Material industry standard JC/T894-2001 is tested.Concrete outcome is shown in Table 1.
Table 1: coating property test result table
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (lithium carbonate, sodium aluminate, zinc oxide are compounding) Coating property is substantially better than embodiment 2-4 (in lithium carbonate, sodium aluminate, zinc oxide, arbitrarily the two is compounding).
Comparing embodiment 1 and embodiment 5-7, embodiment 1 (sodium humate, calcium citrate, magnesium stearate Compounding) coating property is substantially better than embodiment 5-7 and (appoints in sodium humate, calcium citrate, magnesium stearate The two is compounding for meaning).
Test case 2
The leakage-blocking water-proof paint preparing embodiment 1-7, takes the leak stopping that 1-7 prepares respectively and prevents Water paint 10kg and 6kg water is uniformly mixed i.e. to obtain and can be used for constructing, and anti-microbial property is pressed GB/T21866-2008 antibiotic paint anti-microbial property assay method and antibacterial effect, HG/T 3980-2007 Antibiotic paint measures.Concrete outcome is shown in Table 2.
Table 2: anti-microbial property test result is shown in Table
Sample Antibiotic rate, %
Embodiment 1 99.99
Embodiment 2 99.34
Embodiment 3 99.53
Embodiment 4 99.23
Embodiment 5 99.04
Embodiment 6 99.11
Embodiment 7 99.05
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (lithium carbonate, sodium aluminate, zinc oxide are compounding) Anti-microbial property is substantially better than embodiment 2-4 (in lithium carbonate, sodium aluminate, zinc oxide, arbitrarily the two is compounding).
Comparing embodiment 1 and embodiment 5-7, embodiment 1 (sodium humate, calcium citrate, magnesium stearate Compounding) anti-microbial property is substantially better than embodiment 5-7 and (appoints in sodium humate, calcium citrate, magnesium stearate The two is compounding for meaning).

Claims (8)

1. a leakage-blocking water-proof paint, it is characterised in that be prepared from by the raw material of following weight parts: by The raw material of following weight parts is prepared from: cement 95-105 part, accelerator 10-20 part, glass fibre 1-5 Part, redispersible rubber powder 3-7 part, hydroxyethyl cellulose 0.01-0.03 part, retarder 0.02-0.05 Part, inserts 0.2-0.6 part.
2. leakage-blocking water-proof paint as claimed in claim 1, it is characterised in that: described accelerator is carbon The mixture of one or more in acid lithium, sodium aluminate, zinc oxide, aluminum sulfate.
3. leakage-blocking water-proof paint as claimed in claim 2, it is characterised in that: described accelerator is by carbon Acid lithium, sodium aluminate, zinc oxide mix, and described lithium carbonate, sodium aluminate, the mass ratio of zinc oxide are (1-3): (1-3): (1-3).
4. the leakage-blocking water-proof paint as according to any one of claim 1-3, it is characterised in that: described Retarder is the mixture of one or more in sodium humate, calcium citrate, magnesium stearate.
5. leakage-blocking water-proof paint as claimed in claim 4, it is characterised in that: described retarder is by corruption Sodium phytate, calcium citrate, magnesium stearate mix, described sodium humate, calcium citrate, stearic acid The mass ratio of magnesium is (1-3): (1-3): (1-3).
6. leakage-blocking water-proof paint as claimed in claim 1, it is characterised in that: described cement is high standard Number cement, described high-mark cement selected from being numbered 62.5,52.5, in 52.5R, 62.5R a kind of or Multiple.
7. leakage-blocking water-proof paint as claimed in claim 1, it is characterised in that: described inserts is two The mixture of one or more in titanium oxide, silicon dioxide, Kaolin.
8. the preparation method of the leakage-blocking water-proof paint as described in any one of claim 1-7, it is characterised in that By cement, accelerator, glass fibre, redispersible rubber powder, hydroxyethyl cellulose, retarder, fill out Charge mix homogeneously and get final product.
CN201610292848.5A 2016-05-05 2016-05-05 Leakage-blocking water-proof paint and preparation method thereof Active CN105967582B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108395809A (en) * 2018-03-21 2018-08-14 合肥广民建材有限公司 A kind of indoor wall environment-friendly waterproof paint and preparation method thereof
CN110256964A (en) * 2019-07-12 2019-09-20 江苏澄筑建筑科技有限公司 A kind of concrete negative sense slow setting coating and preparation method thereof
CN111607261A (en) * 2020-07-04 2020-09-01 富华防水科技股份有限公司 Efficient and rapid leaking stoppage waterproof coating and preparation method thereof
CN112608091A (en) * 2021-02-05 2021-04-06 新京喜(唐山)建材有限公司 Polymer cement-based waterproof coating and construction method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103274647A (en) * 2013-06-20 2013-09-04 厦门力嘉诚防水工程有限公司 Leakage-stopping and water-proofing paint
CN103601442A (en) * 2013-10-31 2014-02-26 德高(广州)建材有限公司 Waterproof slurry with sterilization function for toilet bath room decoration surfaces

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103274647A (en) * 2013-06-20 2013-09-04 厦门力嘉诚防水工程有限公司 Leakage-stopping and water-proofing paint
CN103601442A (en) * 2013-10-31 2014-02-26 德高(广州)建材有限公司 Waterproof slurry with sterilization function for toilet bath room decoration surfaces

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108395809A (en) * 2018-03-21 2018-08-14 合肥广民建材有限公司 A kind of indoor wall environment-friendly waterproof paint and preparation method thereof
CN110256964A (en) * 2019-07-12 2019-09-20 江苏澄筑建筑科技有限公司 A kind of concrete negative sense slow setting coating and preparation method thereof
CN110256964B (en) * 2019-07-12 2021-06-29 南通达海澄筑建筑科技有限公司 Negative-direction slow-setting coating for concrete and preparation method thereof
CN111607261A (en) * 2020-07-04 2020-09-01 富华防水科技股份有限公司 Efficient and rapid leaking stoppage waterproof coating and preparation method thereof
CN112608091A (en) * 2021-02-05 2021-04-06 新京喜(唐山)建材有限公司 Polymer cement-based waterproof coating and construction method thereof

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