CN109608928A - A kind of inner wall putty powder and preparation method thereof containing organic cementitious material - Google Patents

A kind of inner wall putty powder and preparation method thereof containing organic cementitious material Download PDF

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Publication number
CN109608928A
CN109608928A CN201811623896.3A CN201811623896A CN109608928A CN 109608928 A CN109608928 A CN 109608928A CN 201811623896 A CN201811623896 A CN 201811623896A CN 109608928 A CN109608928 A CN 109608928A
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parts
powder
wall putty
cementitious material
starch
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CN201811623896.3A
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CN109608928B (en
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汪建平
余欢
屈哲辉
陈耀根
莫小萍
谭曦
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GUANGZHOU GLORYSTAR CHEMICAL CO Ltd
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GUANGZHOU GLORYSTAR CHEMICAL CO Ltd
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/34Filling pastes

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)
  • Sealing Material Composition (AREA)

Abstract

The present invention provides a kind of inner wall putty powder and preparation method thereof containing organic cementitious material, is related to building material technical field.The inner wall putty powder containing organic cementitious material, the raw material including following parts by weight: 55~75 parts of heavy calcium carbonate, 15~35 parts of talcum powder, 1~15 part of organic cementitious material and 1~5 part of additive.Inner wall putty powder of the invention, is free of inorganic coagulation material, and chemical property stability has both moisture-proof, alkaline-resisting, cracking resistance performance characteristics.

Description

A kind of inner wall putty powder and preparation method thereof containing organic cementitious material
Technical field
The present invention relates to building material technical field, more particularly, to a kind of inner wall putty powder containing organic cementitious material and Preparation method.
Background technique
In recent years, as the rapid development of building trade, various building coatings emerge one after another, meet it is various not Same consumption demand.With the continuous improvement of people's living standards, people require coating quality also higher and higher.Putty is to build The a part for building decorations is that a kind of pretreated surface packing material is carried out to construction surface, and main purpose is filling construction The hole in face and the curve deviation for correcting construction surface, the lacquer painting to obtain uniform, smooth are laid a solid foundation.Inner wall putty composite index Preferably, health environment-friendly is increasingly got the favour of people.
However, existing inner wall putty is usually gypsum or cement base.Wherein, gypsum has certain hygroscopicity, no Suitable for wet environment, it be easy to cause level to fall off after moisture absorption;Sierozem power, white cement do cementing material with from a wealth of sources, valence The advantages that lattice are cheap, but they belong to overbased materials, tensile strength and crack resistance are poor, scrape metope meeting with the painting of such material Because shrinking it is big due to occurs cracking, coating rockets and other issues.
Summary of the invention
Based on this, it is necessary to the technical issues of moisture-proof, cracking resistance cannot be had both for existing inner wall putty powder, provide A kind of inner wall putty powder and preparation method thereof containing organic cementitious material.
A kind of inner wall putty powder containing organic cementitious material, is made of the raw material of following parts by weight: heavy calcium carbonate 55 ~75 parts, 15~35 parts of talcum powder, 1~15 part of organic cementitious material and 1~5 part of additive.
Above-mentioned inner wall putty powder, is free of inorganic gel, and it is special to have both moisture-proof, alkaline-resisting, cracking resistance performance for chemical property stability Point.
The inner wall putty powder is made of the raw material of following parts by weight in one of the embodiments: heavy calcium carbonate 65~70 parts, 20~22 parts of talcum powder, 6~10 parts of organic cementitious material and 2~5 parts of additive.
The inner wall putty powder is made of the raw material of following parts by weight in one of the embodiments: heavy calcium carbonate 68 parts, 21 parts of talcum powder, 8 parts of organic cementitious material and 3 parts of additive.
The fineness partial size of the heavy calcium carbonate is 200~400 mesh in one of the embodiments,;The talcum powder Fineness partial size be 200~400 mesh.
The organic cementitious material is selected from one of the embodiments: pre-gelatinized starch, dialdehyde starch, crosslinked starch, Carboxymethyl starch, cross-linking carboxymethyl composite modified starch, crosslinking-hydroxypropyl-carboxymethyl composite modified starch, hydroxyethyl starch, Hydroxypropul starch, carboxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, hydroxyethylmethylcellulose, hydroxypropyl methyl In cellulose, guar gum, hydroxypropyl guar gum, xanthan gum, redispersible latex powder, resin rubber powder and polyvinyl alcohol extremely Few one kind.
The organic cementitious material is selected from one of the embodiments: pre-gelatinized starch, dialdehyde starch, carboxymethyl form sediment Powder, cross-linking carboxymethyl composite modified starch, hydroxypropul starch, hydroxyethylmethylcellulose, guar gum, redispersible cream It is at least three kinds of in rubber powder and polyvinyl alcohol.
The organic cementitious material is selected from the raw material of following parts by weight in one of the embodiments:
The redispersable latex powder in one of the embodiments, are as follows: ethylene-vinyl acetate copolymer, wherein ethylene Content be higher than vinyl acetate content;The polyvinyl alcohol is are as follows: PVA1788, fineness partial size are greater than 100 mesh.
The additive includes the raw material of following parts by weight in one of the embodiments: mould inhibitor 0.3~1.5 part, point 0.3~2.5 part of powder, 0.2~2.5 part of water-reducing agent, 0.2~1.5 part of defoaming agent.
The additive is made of the raw material of following parts by weight in one of the embodiments: 0.6 part of mould inhibitor, dispersion 0.9 part of agent, 0.9 part of water-reducing agent, 0.6 part of defoaming agent.
The invention also includes the preparation methods of the above-mentioned inner wall putty powder containing organic cementitious material, comprising the following steps: mixed It closes: heavy calcium carbonate, talcum powder, organic cementitious material and additive is mixed according to the ratio to get containing organic gelling material The inner wall putty powder of material.
Above-mentioned preparation method, obtained inner wall putty powder are free of inorganic gel, and chemical property stability has both moisture-proof, resistance to The performance characteristics of alkali, cracking resistance;And preparation method is simple, it is convenient to operate, and is suitble to large-scale production.
The mixing step includes: in one of the embodiments,
Step 1: premixing, by 15%~25% heavy calcium carbonate and 15%~25% talcum powder and organic Cementitious material and additive are added to WLD-6U type mixing machine, are pre-mixed, temperature be 13~35 DEG C, speed of agitator be 25~ 50rpm, incorporation time are 15~25min;
Step 2: mixing again, and remaining heavy calcium carbonate and talcum powder are added in the mixture of step 1, into Row mixes again, and incorporation time is 35~45min to get the inner wall putty powder containing organic cementitious material.
Compared with prior art, the invention has the following advantages:
Inner wall putty powder of the invention is free of inorganic coagulation material, has moisture-proof, cracking resistance, corrosion resistant performance;With good Well levelling is used, and is easy to polish, and feel is good, is not cracked, is particularly suitable for using the demanding internal wall finishing of whiteness;Product Quality is stablized, and is readily produced, is easy to construct.
Specific embodiment
To facilitate the understanding of the present invention, below in conjunction with preferred embodiment to invention is more fully described.But It is that the invention can be realized in many different forms, however it is not limited to embodiment described herein.On the contrary, providing this The purpose of a little embodiments is to make the disclosure of the present invention more thorough and comprehensive.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool The purpose of the embodiment of body, it is not intended that in the limitation present invention.
Embodiment 1
A kind of inner wall putty powder containing organic cementitious material, is prepared by the following method to obtain:
1) it stocks up: weighing raw material according to following parts by weight: 55 parts of heavy calcium carbonate, 35 parts of talcum powder, organic gelling material 7.5 parts and 2.5 parts of additive of material;
The organic cementitious material is made of the raw material of following parts by weight:
The additive are as follows: 0.5 part of mould inhibitor, 1 part of dispersing agent, 0.5 part of water-reducing agent, 0.5 part of defoaming agent;
2) it is pre-mixed: by 20% heavy calcium carbonate (i.e. 11 parts), 20% talcum powder (i.e. 7 parts), organic gelling material Material and additive are mixed, and 20min is mixed, and obtain premix material;
3) it mixes again: the heavy calcium carbonate and talcum powder of remainder being added into premix material, is mixed again Close, be mixed 40min to get.
Embodiment 2
A kind of inner wall putty powder containing organic cementitious material, substantially the same manner as Example 1, difference is:
Stock: raw material is weighed according to following parts by weight: 75 parts of heavy calcium carbonate, 15 parts of talcum powder, organic cementitious material 5 Part and 5 parts of additive;
The organic cementitious material is made of the raw material of following parts by weight:
The additive are as follows: 1.5 parts of mould inhibitor, 2.5 parts of dispersing agent, 0.5 part of water-reducing agent, 0.5 part of defoaming agent.
Embodiment 3
A kind of inner wall putty powder containing organic cementitious material, substantially the same manner as Example 1, difference is:
Stock: raw material is weighed according to following parts by weight: 70 parts of heavy calcium carbonate, 24 parts of talcum powder, organic cementitious material 1 Part and 5 parts of additive;
The organic cementitious material is made of the raw material of following parts by weight:
0.5 part of carboxymethyl starch,
0.25 part of redispersible latex powder,
0.25 part of polyvinyl alcohol;
The additive are as follows: 0.5 part of mould inhibitor, 0.5 part of dispersing agent, 2.5 parts of water-reducing agent, 1.5 parts of defoaming agent.
Embodiment 4
A kind of inner wall putty powder containing organic cementitious material, substantially the same manner as Example 1, difference is:
Stock: raw material is weighed according to following parts by weight: 68 parts of heavy calcium carbonate, 21 parts of talcum powder, organic cementitious material 8 Part and 3 parts of additive;
The organic cementitious material is made of the raw material of following parts by weight:
Additive are as follows: 0.6 part of mould inhibitor, 0.9 part of dispersing agent, 0.9 part of water-reducing agent, 0.6 part of defoaming agent.
Embodiment 5
A kind of inner wall putty powder containing organic cementitious material, substantially the same manner as Example 1, difference is:
Stock: raw material is weighed according to following parts by weight: 66 parts of heavy calcium carbonate, 18 parts of talcum powder, organic cementitious material 15 parts and 1 part of additive;
The organic cementitious material is made of the raw material of following parts by weight:
The additive are as follows: 0.3 part of mould inhibitor, 0.3 part of dispersing agent, 0.2 part of water-reducing agent, 0.2 part of defoaming agent.
Embodiment 6
A kind of inner wall putty powder containing organic cementitious material, substantially the same manner as Example 1, difference is:
Stock: raw material is weighed according to following parts by weight: 61 parts of heavy calcium carbonate, 32 parts of talcum powder, 3 parts of organic gelling agent With 4 parts of additive;
The organic cementitious material is made of the raw material of following parts by weight:
The additive are as follows: 1.2 parts of mould inhibitor, 0.8 part of dispersing agent, 0.8 part of water-reducing agent, 1.2 parts of defoaming agent.
Embodiment 7
A kind of inner wall putty powder containing organic cementitious material, substantially the same manner as Example 1, difference is:
Stock: raw material is weighed according to following parts by weight: 64 parts of heavy calcium carbonate, 25 parts of talcum powder, 9 parts of organic gelling agent With 2 parts of additive;
The organic cementitious material is made of the raw material of following parts by weight:
The additive are as follows: mould dose 0.5 part, 0.7 part of dispersing agent, water-reducing agent 0.2,0.6 part of defoaming agent.
Embodiment 8
A kind of inner wall putty powder containing organic cementitious material, substantially the same manner as Example 1, difference is:
Stock: raw material is weighed according to following parts by weight: 57 parts of heavy calcium carbonate, 27 parts of talcum powder, organic gelling agent 12.5 parts and 3.5 parts of additive;
The organic cementitious material is made of the raw material of following parts by weight:
The additive are as follows: 0.7 part of mould inhibitor, 1.1 parts of dispersing agent, water-reducing agent 0.6,1.1 parts of defoaming agent.
To be contrasted with the above inner wall putty powder, following comparative example is set and is compareed.
Comparative example 1
A kind of gypsum base inner wall putty powder, is prepared by the following method to obtain:
1) stock up: weigh raw material according to following parts by weight: 56 parts of heavy calcium carbonate, 20 parts of talcum powder, 20 parts of land plaster, 1 part and 3 parts of additive of hydroxyethylmethylcellulose;Wherein, additive are as follows: 0.6 part of mould inhibitor, 0.9 part of dispersing agent, water-reducing agent 0.9 part, 0.6 part of defoaming agent.
2) it is pre-mixed: by 20% heavy calcium carbonate (i.e. 11.2 parts), 20% talcum powder (i.e. 4 parts), 20% stone Cream powder (i.e. 4 parts), hydroxyethylmethylcellulose and additive are mixed, and 20min is mixed, and obtain premix material;
3) it mixes again: heavy calcium carbonate, talcum powder and the land plaster of remainder being added into premix material, into Row mix again, be mixed 40min to get.
Comparative example 2
A kind of cement base inner wall putty powder, is prepared by the following method to obtain:
1) stock up: weigh raw material according to following parts by weight: 56 parts of heavy calcium carbonate, 20 parts of talcum powder, 15 parts of white cement, 5 parts of sierozem power, 1 part of hydroxyethylmethylcellulose and 3 parts of additive;Wherein, additive are as follows: 0.6 part of mould inhibitor, dispersing agent 0.9 Part, 0.9 part of water-reducing agent, 0.6 part of defoaming agent;
2) be pre-mixed: by 20% heavy calcium carbonate (i.e. 11.2 parts), 20% talcum powder (i.e. 4 parts), 20% it is white Cement (i.e. 4 parts), sierozem power, hydroxyethylmethylcellulose and additive are mixed, and 20min is mixed, obtains pre-composition Material;
3) it mixes again: heavy calcium carbonate, talcum powder and the white cement of remainder being added into premix material, carries out Mix again, be mixed 40min to get.
The inner wall putty powder of above embodiments and comparative example is tested for the property.
Experimental example
Performance detection, testing standard are carried out to the inner wall putty powder that embodiment 1-8 and comparative example 1-2 are obtained are as follows:
(1) surface drying time: according to JG/T 298-2010 " architecture indoor putty ";
(2) initial dry cracking resistance: according to JG/T 298-2010 " architecture indoor putty ";
(3) water resistance: according to JG/T 298-2010 " architecture indoor putty ";
(4) alkali resistance: according to GB/T9265-2009 " measurement of building coating coating alkali resistance ";
(5) adhesion strength: according to JG/T 298-2010 " architecture indoor putty ";
(6) condition in container, application property, grinability are according to JG/T 298-2010 " architecture indoor putty ".
Test result is as shown in table 1-2:
1 drying time of table and adhesion strength test result
Other performance parameter test results of table 2
Under equal conditions have by the inner wall putty that above-mentioned experiment can be seen that preparation of the embodiment of the present invention excellent The performances such as cracking resistance, water-fast, acidproof, and cohesive force is strong, is easy to polish, and feel is good, and internal wall finishing is suitble to use;In addition, choosing It takes pre-gelatinized starch, dialdehyde starch, carboxymethyl starch, melon bean gum, hydroxypropul starch, hydroxyethylmethylcellulose, can divide again When dissipating the raw material of property latex powder and polyvinyl alcohol as organic cementitious material, comprehensive performance is best.
Each technical characteristic of embodiment described above can be combined arbitrarily, for simplicity of description, not to above-mentioned reality It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited In contradiction, all should be considered as described in this specification.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention Range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.

Claims (10)

1. a kind of inner wall putty powder containing organic cementitious material, which is characterized in that be made of the raw material of following parts by weight: heavy carbon 55~75 parts of sour calcium powder, 15~35 parts of talcum powder, 1~15 part of organic cementitious material and 1~5 part of additive.
2. inner wall putty powder according to claim 1, which is characterized in that be made of the raw material of following parts by weight: heavy carbon 65~70 parts of sour calcium powder, 20~22 parts of talcum powder, 6~10 parts of organic cementitious material and 2~5 parts of additive.
3. inner wall putty powder according to claim 1, which is characterized in that the fineness partial size of the heavy calcium carbonate is 200~400 mesh;The fineness partial size of the talcum powder is 200~400 mesh.
4. inner wall putty powder according to claim 1-3, which is characterized in that the organic cementitious material is selected from: Pre-gelatinized starch, dialdehyde starch, crosslinked starch, carboxymethyl starch, cross-linking carboxymethyl composite modified starch, crosslinking-hydroxypropyl- Carboxymethyl composite modified starch, hydroxyethyl starch, hydroxypropul starch, carboxymethyl cellulose, hydroxyethyl cellulose, hydroxy propyl cellulose Element, hydroxyethylmethylcellulose, hydroxypropyl methyl cellulose, guar gum, hydroxypropyl guar gum, xanthan gum, redispersible At least one of latex powder, resin rubber powder and polyvinyl alcohol.
5. inner wall putty powder according to claim 4, which is characterized in that the organic cementitious material is selected from: pre-gelatinized is formed sediment Powder, dialdehyde starch, carboxymethyl starch, cross-linking carboxymethyl composite modified starch, hydroxypropul starch, hydroxyethylmethylcellulose, melon It is at least three kinds of in your bean gum, redispersible latex powder and polyvinyl alcohol.
6. inner wall putty powder according to claim 4, which is characterized in that the organic cementitious material is selected from following parts by weight Raw material:
7. inner wall putty powder according to claim 4, which is characterized in that the redispersable latex powder are as follows: ethyl vinyl acetate Ethylene copolymer, wherein the content of ethylene is higher than the content of vinyl acetate;The polyvinyl alcohol is are as follows: PVA1788, fineness grain Diameter is greater than 100 mesh.
8. inner wall putty powder according to claim 1, which is characterized in that the additive includes the original of following parts by weight Material: 0.3~1.5 part of mould inhibitor, 0.3~2.5 part of dispersing agent, 0.2~2.5 part of water-reducing agent, 0.2~1.5 part of defoaming agent.
9. a kind of preparation method of the described in any item inner wall putty powders containing organic cementitious material of claim 1-8, feature It is, comprising the following steps:
Mixing: heavy calcium carbonate, talcum powder, organic cementitious material and additive are mixed according to the ratio to get containing organic The inner wall putty powder of cementitious material.
10. preparation method according to claim 9, which is characterized in that the mixing step includes:
Step 1: premixing, by 15%~25% heavy calcium carbonate and 15%~25% talcum powder and organic gelling Material and additive are added to WLD-6U type mixing machine, are pre-mixed, temperature be 13~35 DEG C, speed of agitator be 25~ 50rpm, incorporation time are 15~25min;
Step 2: mixing again, and remaining heavy calcium carbonate and talcum powder are added in the mixture of step 1, carries out again Secondary mixing, incorporation time are 35~45min to get the inner wall putty powder containing organic cementitious material.
CN201811623896.3A 2018-12-28 2018-12-28 Interior wall putty powder containing organic cementing material and preparation method thereof Active CN109608928B (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110183894A (en) * 2019-07-03 2019-08-30 北京生态家园科技集团有限公司 A kind of neutrality mildew-proof putty
CN110305517A (en) * 2019-08-12 2019-10-08 中山爱因新材料有限公司 A kind of interior wall naturally plants this putty
CN110527345A (en) * 2019-09-18 2019-12-03 重庆兴渝涂料股份有限公司 Colorful flame-retardant inner wall of building powder of lacquer putty for use on and preparation method thereof
CN110845894A (en) * 2019-11-29 2020-02-28 重庆贝亨源节能建材有限公司 Interior wall putty powder
CN114806257A (en) * 2022-05-31 2022-07-29 贵州翰匠装饰建材有限公司 Environment-friendly putty powder and preparation method thereof
CN116731550A (en) * 2022-03-04 2023-09-12 庄继昌 Multifunctional wall material

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Publication number Priority date Publication date Assignee Title
CN103450732A (en) * 2013-08-18 2013-12-18 邹建波 Natural vegetable glue putty
CN105949864A (en) * 2016-05-24 2016-09-21 西昌市蓝鼎环保科技有限公司 Method for preparing interior wall putty powder from semi-dry desulfurization ash

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103450732A (en) * 2013-08-18 2013-12-18 邹建波 Natural vegetable glue putty
CN105949864A (en) * 2016-05-24 2016-09-21 西昌市蓝鼎环保科技有限公司 Method for preparing interior wall putty powder from semi-dry desulfurization ash

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110183894A (en) * 2019-07-03 2019-08-30 北京生态家园科技集团有限公司 A kind of neutrality mildew-proof putty
CN110305517A (en) * 2019-08-12 2019-10-08 中山爱因新材料有限公司 A kind of interior wall naturally plants this putty
CN110527345A (en) * 2019-09-18 2019-12-03 重庆兴渝涂料股份有限公司 Colorful flame-retardant inner wall of building powder of lacquer putty for use on and preparation method thereof
CN110845894A (en) * 2019-11-29 2020-02-28 重庆贝亨源节能建材有限公司 Interior wall putty powder
CN116731550A (en) * 2022-03-04 2023-09-12 庄继昌 Multifunctional wall material
CN114806257A (en) * 2022-05-31 2022-07-29 贵州翰匠装饰建材有限公司 Environment-friendly putty powder and preparation method thereof

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