CN105942513A - Peony plant edible gum preparing method - Google Patents
Peony plant edible gum preparing method Download PDFInfo
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- CN105942513A CN105942513A CN201610385113.7A CN201610385113A CN105942513A CN 105942513 A CN105942513 A CN 105942513A CN 201610385113 A CN201610385113 A CN 201610385113A CN 105942513 A CN105942513 A CN 105942513A
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- Prior art keywords
- branch
- seed
- paeonia suffruticosa
- fructus gleditsia
- glue
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- 238000000034 method Methods 0.000 title abstract description 5
- 244000170916 Paeonia officinalis Species 0.000 title abstract 2
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 53
- 239000007788 liquid Substances 0.000 claims abstract description 23
- 238000000227 grinding Methods 0.000 claims abstract description 19
- 238000000605 extraction Methods 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 15
- 241000533849 Gleditsia Species 0.000 claims description 62
- 240000005001 Paeonia suffruticosa Species 0.000 claims description 55
- 235000003889 Paeonia suffruticosa Nutrition 0.000 claims description 41
- 239000003292 glue Substances 0.000 claims description 34
- 239000000203 mixture Substances 0.000 claims description 25
- 230000007062 hydrolysis Effects 0.000 claims description 14
- 238000006460 hydrolysis reaction Methods 0.000 claims description 14
- 235000013305 food Nutrition 0.000 claims description 13
- 238000002360 preparation method Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 229930003935 flavonoid Natural products 0.000 claims description 7
- 235000017173 flavonoids Nutrition 0.000 claims description 7
- 150000002215 flavonoids Chemical class 0.000 claims description 7
- 239000000047 product Substances 0.000 claims description 6
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 5
- 239000011347 resin Substances 0.000 claims description 5
- 229920005989 resin Polymers 0.000 claims description 5
- 238000001179 sorption measurement Methods 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- 239000004677 Nylon Substances 0.000 claims description 4
- 238000010828 elution Methods 0.000 claims description 4
- 239000000706 filtrate Substances 0.000 claims description 4
- 235000015203 fruit juice Nutrition 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000011068 loading method Methods 0.000 claims description 4
- 229920001778 nylon Polymers 0.000 claims description 4
- 239000002244 precipitate Substances 0.000 claims description 4
- 238000009461 vacuum packaging Methods 0.000 claims description 4
- 241001093152 Mangifera Species 0.000 claims description 3
- 241000220324 Pyrus Species 0.000 claims description 2
- 235000021017 pears Nutrition 0.000 claims description 2
- 238000000197 pyrolysis Methods 0.000 claims 1
- 210000002421 cell wall Anatomy 0.000 abstract description 8
- 208000030507 AIDS Diseases 0.000 abstract description 5
- 210000004027 cell Anatomy 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 5
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- 208000026435 phlegm Diseases 0.000 abstract description 4
- 239000000843 powder Substances 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 4
- 206010010774 Constipation Diseases 0.000 abstract description 3
- 230000036039 immunity Effects 0.000 abstract description 3
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- 235000010987 pectin Nutrition 0.000 abstract description 3
- 239000001814 pectin Substances 0.000 abstract description 3
- 239000013543 active substance Substances 0.000 abstract description 2
- 241000931143 Gleditsia sinensis Species 0.000 abstract 3
- 230000009286 beneficial effect Effects 0.000 abstract 2
- 206010012504 Dermatophytosis Diseases 0.000 abstract 1
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- 235000013813 Gleditsia triacanthos Nutrition 0.000 description 4
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- 239000004615 ingredient Substances 0.000 description 4
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- 230000000694 effects Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- OMDQUFIYNPYJFM-XKDAHURESA-N (2r,3r,4s,5r,6s)-2-(hydroxymethyl)-6-[[(2r,3s,4r,5s,6r)-4,5,6-trihydroxy-3-[(2s,3s,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-2-yl]methoxy]oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O[C@H]2[C@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)[C@H](O)[C@H](O)[C@H](O)O1 OMDQUFIYNPYJFM-XKDAHURESA-N 0.000 description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- 229920000926 Galactomannan Polymers 0.000 description 2
- 230000001093 anti-cancer Effects 0.000 description 2
- LGJMUZUPVCAVPU-UHFFFAOYSA-N beta-Sitostanol Natural products C1CC2CC(O)CCC2(C)C2C1C1CCC(C(C)CCC(CC)C(C)C)C1(C)CC2 LGJMUZUPVCAVPU-UHFFFAOYSA-N 0.000 description 2
- IRHTZOCLLONTOC-UHFFFAOYSA-N hexacosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCO IRHTZOCLLONTOC-UHFFFAOYSA-N 0.000 description 2
- 230000003834 intracellular effect Effects 0.000 description 2
- IGGUPRCHHJZPBS-UHFFFAOYSA-N nonacosane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCC IGGUPRCHHJZPBS-UHFFFAOYSA-N 0.000 description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 description 2
- 235000013824 polyphenols Nutrition 0.000 description 2
- 208000011580 syndromic disease Diseases 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- KZJWDPNRJALLNS-VPUBHVLGSA-N (-)-beta-Sitosterol Natural products O[C@@H]1CC=2[C@@](C)([C@@H]3[C@H]([C@H]4[C@@](C)([C@H]([C@H](CC[C@@H](C(C)C)CC)C)CC4)CC3)CC=2)CC1 KZJWDPNRJALLNS-VPUBHVLGSA-N 0.000 description 1
- CSVWWLUMXNHWSU-UHFFFAOYSA-N (22E)-(24xi)-24-ethyl-5alpha-cholest-22-en-3beta-ol Natural products C1CC2CC(O)CCC2(C)C2C1C1CCC(C(C)C=CC(CC)C(C)C)C1(C)CC2 CSVWWLUMXNHWSU-UHFFFAOYSA-N 0.000 description 1
- OILXMJHPFNGGTO-UHFFFAOYSA-N (22E)-(24xi)-24-methylcholesta-5,22-dien-3beta-ol Natural products C1C=C2CC(O)CCC2(C)C2C1C1CCC(C(C)C=CC(C)C(C)C)C1(C)CC2 OILXMJHPFNGGTO-UHFFFAOYSA-N 0.000 description 1
- KLEXDBGYSOIREE-UHFFFAOYSA-N 24xi-n-propylcholesterol Natural products C1C=C2CC(O)CCC2(C)C2C1C1CCC(C(C)CCC(CCC)C(C)C)C1(C)CC2 KLEXDBGYSOIREE-UHFFFAOYSA-N 0.000 description 1
- OQMZNAMGEHIHNN-UHFFFAOYSA-N 7-Dehydrostigmasterol Natural products C1C(O)CCC2(C)C(CCC3(C(C(C)C=CC(CC)C(C)C)CCC33)C)C3=CC=C21 OQMZNAMGEHIHNN-UHFFFAOYSA-N 0.000 description 1
- LPZCCMIISIBREI-MTFRKTCUSA-N Citrostadienol Natural products CC=C(CC[C@@H](C)[C@H]1CC[C@H]2C3=CC[C@H]4[C@H](C)[C@@H](O)CC[C@]4(C)[C@H]3CC[C@]12C)C(C)C LPZCCMIISIBREI-MTFRKTCUSA-N 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- ARVGMISWLZPBCH-UHFFFAOYSA-N Dehydro-beta-sitosterol Natural products C1C(O)CCC2(C)C(CCC3(C(C(C)CCC(CC)C(C)C)CCC33)C)C3=CC=C21 ARVGMISWLZPBCH-UHFFFAOYSA-N 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- 206010040943 Skin Ulcer Diseases 0.000 description 1
- HZYXFRGVBOPPNZ-UHFFFAOYSA-N UNPD88870 Natural products C1C=C2CC(O)CCC2(C)C2C1C1CCC(C(C)=CCC(CC)C(C)C)C1(C)CC2 HZYXFRGVBOPPNZ-UHFFFAOYSA-N 0.000 description 1
- 206010046792 Uterine hypotonus Diseases 0.000 description 1
- 229930003270 Vitamin B Natural products 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- MJVXAPPOFPTTCA-UHFFFAOYSA-N beta-Sistosterol Natural products CCC(CCC(C)C1CCC2C3CC=C4C(C)C(O)CCC4(C)C3CCC12C)C(C)C MJVXAPPOFPTTCA-UHFFFAOYSA-N 0.000 description 1
- NJKOMDUNNDKEAI-UHFFFAOYSA-N beta-sitosterol Natural products CCC(CCC(C)C1CCC2(C)C3CC=C4CC(O)CCC4C3CCC12C)C(C)C NJKOMDUNNDKEAI-UHFFFAOYSA-N 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 210000003850 cellular structure Anatomy 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000035619 diuresis Effects 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 229920001206 natural gum Polymers 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 235000015500 sitosterol Nutrition 0.000 description 1
- KZJWDPNRJALLNS-VJSFXXLFSA-N sitosterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CC[C@@H](CC)C(C)C)[C@@]1(C)CC2 KZJWDPNRJALLNS-VJSFXXLFSA-N 0.000 description 1
- 229950005143 sitosterol Drugs 0.000 description 1
- NLQLSVXGSXCXFE-UHFFFAOYSA-N sitosterol Natural products CC=C(/CCC(C)C1CC2C3=CCC4C(C)C(O)CCC4(C)C3CCC2(C)C1)C(C)C NLQLSVXGSXCXFE-UHFFFAOYSA-N 0.000 description 1
- 231100000019 skin ulcer Toxicity 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- HCXVJBMSMIARIN-PHZDYDNGSA-N stigmasterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)/C=C/[C@@H](CC)C(C)C)[C@@]1(C)CC2 HCXVJBMSMIARIN-PHZDYDNGSA-N 0.000 description 1
- 235000016831 stigmasterol Nutrition 0.000 description 1
- 229940032091 stigmasterol Drugs 0.000 description 1
- BFDNMXAIBMJLBB-UHFFFAOYSA-N stigmasterol Natural products CCC(C=CC(C)C1CCCC2C3CC=C4CC(O)CCC4(C)C3CCC12C)C(C)C BFDNMXAIBMJLBB-UHFFFAOYSA-N 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000019156 vitamin B Nutrition 0.000 description 1
- 239000011720 vitamin B Substances 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 230000036642 wellbeing Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a peony plant edible gum preparing method. The mechanical extraction technology and the biological enzymolysis extraction technology are utilized comprehensively, cell walls of Chinese honeylocust fruits, seeds and branches are broken firstly through superfine powder grinding, stirring and ultrasonic vibration so that beneficial substances inside cells can be released, and then beneficial substances including pectin and liquid cement in cells of Chinese honeylocust fruits, seeds and branches are extracted with the biological enzymolysis technology. Traditional substance extraction technological difficulties are overcome, active substances in Chinese honeylocust fruits, seeds and branches are preserved to the maximum degree, the functions of inducing resuscitation, eliminating phlegm, treating dermatophytosis and treating constipation are realized, and cancer resistance and AIDS immunity improvement are realized.
Description
Technical field
The present invention relates to the preparation method of a kind of plant gum, select that Paeonia suffruticosa branch, Paeonia suffruticosa bar, Paeonia suffruticosa be dry, Paeonia suffruticosa stem is main
A kind of preparation method of the Paeonia suffruticosa plant edible food glue of raw material.
Background technology
It is known that honey locust belongs to Eco-economic Type seeds, drought-enduring water saving, well developed root system, can be used as shelter-forest and water
Soil keeps.Fructus Gleditsia seed gel content is up to 30% ~ 40%, and Fructus Gleditsia seed contains abundant galactomannan gum and becomes with protein
Point, galactomannan gum is because of the rheological characteristic of its uniqueness, and at present, the utilization to Fructus Gleditsia is only limited to utilize Fructus Gleditsia seed to produce
Industrial plant glue, but the angle of honey locust fruit, seed, scolus all can be used as medicine, angle fruit be used as medicine can eliminate the phlegm, diuresis, seed is used as medicine
Tinea can be controlled and relieving constipation is secret；Spina Gleditsiae is used as medicine and can invigorate blood circulation and control skin ulcer tinea, according to data find, in Fructus Gleditsia containing saponin, tannin,
Ceryl alcohol, nonacosane, stigmasterol, sitosterol etc., the function have eliminating the phlegm, having one's ideas straightened out, the most anticancer and improve the merit such as acquired immune deficiency syndrome (AIDS) immunity
Effect.But the speed of growth of honey locust is very slow, belongs to deep-rootedness seeds, needs 6～8 years nourish and grow just can yield positive results, because of
This thus constrain the processing of utilization energetically of diagonal angle fruit, seed and scolus.
In recent years, China greatly develops Paeonia suffruticosa plantation, and the year two thousand twenty is striven in Ministry of Agriculture's plan, and the plantation of Paeonia suffruticosa reaches 1,000 ten thousand
Mu, the planting site of Paeonia suffruticosa mostly is knob, but, knob is all poor area, young and middle-aged labour force's major part stream
Moving developed regions, remaining labour force mostly is more weak labour force, and the agricultural plant as planted needs substantial amounts of labor
Power, if but plantation Paeonia suffruticosa, once plant, the collection period of available 30-40, the most laborsaving, and also economic well-being of workers and staff is gathered in the crops relatively
Greatly.So, generally when planting Paeonia suffruticosa, seed of Flos Moutan can make oil, but Paeonia suffruticosa branch, bar, dry, stem cannot utilize, through inspection always
Survey Paeonia suffruticosa branch, bar, dry, stem are also enriched in colloid, and containing medical values such as flavonoid, polyphenol, vitamin C and vitamin Bs, are badly in need of
A kind of method uses the branch of this Paeonia suffruticosa, bar, dry, stem, used to make the best.
Summary of the invention
The invention aims to solve the deficiency that above-mentioned technical problem exists, it is provided that one makes Fructus Gleditsia element and Paeonia suffruticosa
Organically blending of element, changes Fructus Gleditsia element and is only used for the conventional thought of industry, and without any pollution, without any huge sum of money
Belong to the preparation method of the Paeonia suffruticosa plant edible food glue of doping.
The technical solution adopted in the present invention is, the preparation method of this Paeonia suffruticosa plant edible food glue is:
Step one, the angle of Fructus Gleditsia fruit, seed and scolus are washed, be dried in the cool, put into grinding machine for grinding 1-3 little
Time, making the granularity of mixture of angle fruit, seed and the scolus of Fructus Gleditsia in 1 μm ~ 10 μm, add water, the amount adding water is Fructus Gleditsia
Angle fruit, seed and total weight of the mixture 4-8 times of scolus, stir, carry out vibration of ultrasonic wave 20-30 minute, add soap
The pectase of the 3-15% of the total weight of the mixture of angle fruit, seed and the scolus at angle, boils 1-2h, next mixture is cooled down,
Fried juice is filtered by the nylon mesh of 50 μm, and filtrate carries out separating 2～3 times in centrifuge, and each 10 min are then
Collect supernatant liquid, being centrifuged separating until not having precipitate to separate out collecting liquid, united extraction liquid, finally obtaining
Angle fruit, seed and the thick glue of extraction of branch of Fructus Gleditsia；
Step 2, the angle fruit of the Fructus Gleditsia that step one is obtained, the extraction thick liquid Flavonoids by Macroporous Adsorption Resin of seed and branch are carried out point
From, to extract thick liquid pH and control at 7-9, loading is adsorbed with 2.5-4.5BV/h flow velocitys, and concentration of alcohol is 85%, elution flow rate
Use 2BV/h, collect angle fruit, seed and the Hydrolysis kinetics glue of branch obtaining Fructus Gleditsia；
Step 3, gather fresh Paeonia suffruticosa branch, bar, dry, stem, wash, dry, put into grinding machine for grinding 1-3 hour, make
Paeonia suffruticosa branch, bar, dry, granularity the appointing in 0 0.044 mm, 0.044mm 0.074mm, 0.074-1mm of stem mixture
One grain size intervals；Putting into high-temperature retorting reactor, after heating, in still, product enters condenser along reactor upper pipe,
Cool down, i.e. can get Paeonia suffruticosa branch, bar, dry, the extracting solution of stem；
The Paeonia suffruticosa that step 4, the angle fruit of the Fructus Gleditsia that step 2 is obtained, the Hydrolysis kinetics glue of seed and branch obtain with step 3
Branch, bar, dry, the extracting solution mixing of stem, mixed in the ratio of 2:8, be stirred, and adding fruit juice during stirring increases mouth
Taste, addition be the angle fruit of the Fructus Gleditsia that step 2 obtains, the Hydrolysis kinetics glue of seed and branch obtain with step 3 Paeonia suffruticosa branch,
Bar, the 5-10% of extracting solution gross weight of dry, stem, after stirring, vacuum packaging, i.e. obtain this Paeonia suffruticosa plant edible food glue.
Wherein the granularity of the mixture of angle fruit, seed and the scolus of the Fructus Gleditsia of step one is in 1 μm ~ 10 μm, is because Fructus Gleditsia
Angle fruit, seed and scolus quality hard, cell wall is thicker, general broken angle fruit, seed and the branch that cannot break Fructus Gleditsia
The cell wall of thorn, in cell, the dissolution of effective medicinal component needs guiding through several even dozens of cell wall, and quite a few
Cell Component can not pass cell wall, and this part can only waste, and intracellular effective ingredient therefore cannot be made complete
Portion fully discharges, and the present invention reaches superfine powder by the way of grinding, makes intracellular effective ingredient the most abundant
Discharge, improve dissolution rate and the dissolution rate of effective ingredient in angle fruit, seed and the scolus of Fructus Gleditsia, our experiments show that, molten
Go out rate and can reach 90-98%.
Wherein the stirring of step one, carries out vibration of ultrasonic wave 20-30 minute, is in order at the angle of Fructus Gleditsia fruit, seed
On the basis of the mixture superfine powder cell wall breaking of scolus, utilize vibration of ultrasonic wave to make continuation to cell wall breaking, improve Fructus Gleditsia
Angle fruit, seed and the bioavailability of scolus, beneficially human body be to the absorption of benefit materials and utilization.
The wherein pectase of the 3-15% of the total weight of the mixture of the angle fruit, seed and the scolus that add Fructus Gleditsia of step one, be
For the pectin in angle fruit, seed and the scolus of Fructus Gleditsia, glue, natural gum, mucilagenous precipitation.
The wherein thick liquid of extraction of the angle of Fructus Gleditsia fruit, seed and branch being purified with Flavonoids by Macroporous Adsorption Resin of step 2,
Eliminate the harmful substance such as impurity, heavy metal.
Wherein step 3 make Paeonia suffruticosa branch, bar, dry, stem mixture granularity at 0 0.044 mm, 0.044mm
Arbitrary grain size intervals in 0.074mm, 0.074-1mm, is to preferably extract Paeonia suffruticosa branch, bar, dry, the essence of stem.
Wherein angle fruit, seed and the Hydrolysis kinetics glue of branch and the step 3 of the Fructus Gleditsia that step 2 is obtained in step 4
The Paeonia suffruticosa branch that obtains, bar, dry, the extracting solution of stem, mixed in the ratio of 2:8, and the speed of growth being because honey locust is very slow, cost
Higher, and the branch of Paeonia suffruticosa, bar, dry, stem is with low cost, such that it is able to reduce the totle drilling cost of final products, can make the present invention's
Health product enter into huge numbers of families.
The wherein addition fruit juice in step 4, for one or more the combination such as Fructus Mali pumilae, pears, Fructus Mangifera Indicae, Fructus Ananadis comosi, Fructus Persicae.
The invention comprehensively utilizes mechanical means extraction process and biological enzymolysis technology extraction process, first with grinding to form
The cell wall of the angle of Fructus Gleditsia fruit, seed and branch is broken by the methods such as superfine powder, stirring, vibration of ultrasonic wave, allows in its release cells
The benefit materials in portion, then utilizes biological enzymolysis technology to carry out extracting the pectin in angle fruit, seed and the branch cell of Fructus Gleditsia, glue
Deng benefit materials.The present invention breaks through conventional matter extractive technique bottleneck in production technology, farthest remains Fructus Gleditsia
Active substance in angle fruit, seed and branch, not only has and has one's ideas straightened out, eliminates the phlegm, controls tinea and the secret function of relieving constipation, and the most anticancer and
Improve the effects such as acquired immune deficiency syndrome (AIDS) immunity；Flavonoid during the present invention also retains Paeonia suffruticosa branch, bar, dry, stem simultaneously, polyphenol, dimension are raw
The element medicinal ingredient such as C and vitamin B, has good health-care effect to human body.The present invention innovatively makes Fructus Gleditsia element and Paeonia suffruticosa
Organically blending of element, changes Fructus Gleditsia element and is only used for the conventional thought of industry, be also fully utilized by China and greatly develop
The opportunity of Paeonia suffruticosa, turns waste into wealth Paeonia suffruticosa Paeonia suffruticosa branch, bar, dry, stem, makes the production chain of Paeonia suffruticosa deep processing be extended and perfect,
Paeonia suffruticosa industry is made to have accomplished that thing is worth to the greatest extent from plantation to deep processing cyclic production chain.
Detailed description of the invention
Following example are described in detail the present invention.
Embodiment 1
Step one, the angle of Fructus Gleditsia fruit, seed and scolus are washed, be dried in the cool, put into grinding machine for grinding 1 little
Time, making the granularity of mixture of angle fruit, seed and the scolus of Fructus Gleditsia in 1 μm ~ 10 μm, add water, the amount adding water is Fructus Gleditsia
Angle fruit, seed and total weight of the mixture 4-8 times of scolus, stir, carry out vibration of ultrasonic wave 20 minutes, add Fructus Gleditsia
The pectase of the 3% of the total weight of the mixture of angle fruit, seed and scolus, boils 1h, next mixture is cooled down, fried juice
Being filtered by the nylon mesh of 50 μm, filtrate carries out separating 2 times in centrifuge, and then each 10 min collect upper liquid
Body, is centrifuged separating until not having precipitate to separate out collecting liquid, united extraction liquid, the angle of the Fructus Gleditsia finally obtained
Really, the thick glue of the extraction of seed and branch；
Step 2, the angle fruit of the Fructus Gleditsia that step one is obtained, the extraction thick liquid Flavonoids by Macroporous Adsorption Resin of seed and branch are carried out point
From, to extract thick liquid pH and control 7, loading is adsorbed with 2.5 BV/h flow velocitys, concentration of alcohol is 85%, and elution flow rate uses
2BV/h, collects angle fruit, seed and the Hydrolysis kinetics glue of branch obtaining Fructus Gleditsia；
Step 3, gather fresh Paeonia suffruticosa branch, bar, dry, stem, wash, dry, put into grinding machine for grinding 1-3 hour, make
Paeonia suffruticosa branch, bar, dry, granularity the appointing in 0 0.044 mm, 0.044mm 0.074mm, 0.074-1mm of stem mixture
One grain size intervals；Putting into high-temperature retorting reactor, after heating, in still, product enters condenser along reactor upper pipe,
Cool down, i.e. can get Paeonia suffruticosa branch, bar, dry, the extracting solution of stem；
The Paeonia suffruticosa that step 4, the angle fruit of the Fructus Gleditsia that step 2 is obtained, the Hydrolysis kinetics glue of seed and branch obtain with step 3
Branch, bar, dry, the extracting solution of stem, mixed in the ratio of 2:8, be stirred, and can add apple fumet to increase taste during stirring,
Addition be the angle fruit of the Fructus Gleditsia that step 2 obtains, the Hydrolysis kinetics glue of seed and branch obtain with step 3 Paeonia suffruticosa branch, bar,
The 5% of the extracting solution gross weight of dry, stem, after stirring, vacuum packaging, i.e. obtain this Paeonia suffruticosa plant edible food glue.
Embodiment 2
Step one, the angle of Fructus Gleditsia fruit, seed and scolus are washed, be dried in the cool, put into grinding machine for grinding 3 little
Time, making the granularity of mixture of angle fruit, seed and the scolus of Fructus Gleditsia in 1 μm ~ 10 μm, add water, the amount adding water is Fructus Gleditsia
Angle fruit, seed and total weight of the mixture 4-8 times of scolus, stir, carry out vibration of ultrasonic wave 30 minutes, add Fructus Gleditsia
The pectase of the 15% of the total weight of the mixture of angle fruit, seed and scolus, boils 2h, next mixture is cooled down, fried juice
Being filtered by the nylon mesh of 50 μm, filtrate carries out separating 3 times in centrifuge, and then each 10 min collect upper liquid
Body, is centrifuged separating until not having precipitate to separate out collecting liquid, united extraction liquid, the angle of the Fructus Gleditsia finally obtained
Really, the thick glue of the extraction of seed and branch；
Step 2, the angle fruit of the Fructus Gleditsia that step one is obtained, the extraction thick liquid Flavonoids by Macroporous Adsorption Resin of seed and branch are carried out point
From, to extract thick liquid pH and control 9, loading is adsorbed with 4.5BV/h flow velocity, and concentration of alcohol is 85%, and elution flow rate uses
2BV/h, collects angle fruit, seed and the Hydrolysis kinetics glue of branch obtaining Fructus Gleditsia；
Step 3, gather fresh Paeonia suffruticosa branch, bar, dry, stem, wash, dry, put into grinding machine for grinding 3 hours, make male
Red branch, bar, arbitrary in 0 0.044 mm, 0.044mm 0.074mm, 0.074-1mm of granularity of dry, stem mixture
Grain size intervals；Putting into high-temperature retorting reactor, after heating, in still, product enters condenser along reactor upper pipe, enters
Row cooling, i.e. can get Paeonia suffruticosa branch, bar, dry, the extracting solution of stem；
The Paeonia suffruticosa that step 4, the angle fruit of the Fructus Gleditsia that step 2 is obtained, the Hydrolysis kinetics glue of seed and branch obtain with step 3
Branch, bar, dry, the extracting solution of stem, mixed in the ratio of 2:8, be stirred, and can add Fructus Mangifera Indicae natural juice to increase taste during stirring,
Addition be the angle fruit of the Fructus Gleditsia that step 2 obtains, the Hydrolysis kinetics glue of seed and branch obtain with step 3 Paeonia suffruticosa branch, bar,
The 10% of the extracting solution gross weight of dry, stem, after stirring, vacuum packaging, i.e. obtain this Paeonia suffruticosa plant edible food glue.
Claims (5)
1. the preparation method of a Paeonia suffruticosa plant edible food glue, it is characterised in that: step one, the angle of Fructus Gleditsia fruit, seed and scolus
Wash, be dried in the cool, put into grinding machine for grinding 1-3 hour, add water, the amount adding water be the angle fruit of Fructus Gleditsia,
Seed and total weight of the mixture 4-8 times of scolus, stir, and carries out vibration of ultrasonic wave 20-30 minute, adds the angle of Fructus Gleditsia
Really, the pectase of the 3-15% of the total weight of the mixture of seed and scolus, boil 1-2h, next mixture cooled down, fried
Juice is filtered by the nylon mesh of 50 μm, and filtrate carries out separating 2～3 times in centrifuge, and then each 10 min collect
Layer liquid, is centrifuged separating until not having precipitate to separate out collecting liquid, united extraction liquid, the Fructus Gleditsia finally obtained
Angle fruit, seed and the thick glue of extraction of branch；Step 2, angle fruit, seed and the thick liquid of extraction of branch of the Fructus Gleditsia that step one is obtained
Separating with Flavonoids by Macroporous Adsorption Resin, extract thick liquid pH and control at 7-9, loading is adsorbed with 2.5-4.5BV/h flow velocitys,
Concentration of alcohol is 85%, and elution flow rate uses 2BV/h, collects angle fruit, seed and the Hydrolysis kinetics glue of branch obtaining Fructus Gleditsia；Step
Rapid three, gather fresh Paeonia suffruticosa branch, bar, dry, stem, wash, dry, put into grinding machine for grinding 1-3 hour, put into high temperature
In dry distillation reactor still, after heating, in still, product enters condenser along reactor upper pipe, cools down, i.e. can get male
Red branch, bar, dry, the extracting solution of stem；Step 4, angle fruit, seed and the Hydrolysis kinetics glue of branch of the Fructus Gleditsia that step 2 is obtained
The Paeonia suffruticosa branch that obtains with step 3, bar, dry, the extracting solution of stem mixs, are stirred, and during stirring, addition fruit juice increases mouth
Taste, addition be the angle fruit of the Fructus Gleditsia that step 2 obtains, the Hydrolysis kinetics glue of seed and branch obtain with step 3 Paeonia suffruticosa branch,
Bar, the 5-10% of extracting solution gross weight of dry, stem, after stirring, vacuum packaging, i.e. obtain this Paeonia suffruticosa plant edible food glue.
The preparation method of a kind of Paeonia suffruticosa plant edible food glue the most according to claim 1, it is characterised in that: step one is ground
The granularity of the mixture of angle fruit, seed and the scolus of rear Fructus Gleditsia is in 1 μm ~ 10 μm.
The preparation method of a kind of Paeonia suffruticosa plant edible food glue the most according to claim 1, it is characterised in that: step 3 is ground
After make Paeonia suffruticosa branch, bar, dry, stem mixture granularity in 0 0.044 mm, 0.044mm 0.074mm, 0.074-1mm
Arbitrary grain size intervals.
The preparation method of a kind of Paeonia suffruticosa plant edible food glue the most according to claim 1, it is characterised in that: step in step 4
Paeonia suffruticosa branch that the angle fruit of rapid two Fructus Gleditsia obtained, the Hydrolysis kinetics glue of seed and branch obtain with step 3, bar, do, the carrying of stem
Take liquid, mix in the ratio of 2:8.
The preparation method of a kind of Paeonia suffruticosa plant edible food glue the most according to claim 1, it is characterised in that: adding in step 4
Enter fruit juice, for one or more the combination such as Fructus Mali pumilae, pears, Fructus Mangifera Indicae, Fructus Ananadis comosi, Fructus Persicae.
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