CN107028183A - A kind of precious preparation method of bark of eucommia - Google Patents
A kind of precious preparation method of bark of eucommia Download PDFInfo
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- CN107028183A CN107028183A CN201710167995.4A CN201710167995A CN107028183A CN 107028183 A CN107028183 A CN 107028183A CN 201710167995 A CN201710167995 A CN 201710167995A CN 107028183 A CN107028183 A CN 107028183A
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- eucommia
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- trunk
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- 241000208688 Eucommia Species 0.000 title claims abstract description 117
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 230000036541 health Effects 0.000 claims abstract description 24
- 239000003292 glue Substances 0.000 claims abstract description 21
- 239000000284 extract Substances 0.000 claims abstract description 19
- 239000000843 powder Substances 0.000 claims abstract description 16
- 238000003756 stirring Methods 0.000 claims abstract description 15
- 238000000605 extraction Methods 0.000 claims abstract description 13
- 239000000203 mixture Substances 0.000 claims description 39
- 239000007788 liquid Substances 0.000 claims description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 239000000654 additive Substances 0.000 claims description 16
- 230000000996 additive effect Effects 0.000 claims description 16
- 239000002245 particle Substances 0.000 claims description 16
- 238000001035 drying Methods 0.000 claims description 12
- 230000007062 hydrolysis Effects 0.000 claims description 11
- 238000006460 hydrolysis reaction Methods 0.000 claims description 11
- 229930003935 flavonoid Natural products 0.000 claims description 8
- 235000017173 flavonoids Nutrition 0.000 claims description 8
- 150000002215 flavonoids Chemical class 0.000 claims description 8
- 229920005989 resin Polymers 0.000 claims description 7
- 239000011347 resin Substances 0.000 claims description 7
- 238000000926 separation method Methods 0.000 claims description 7
- 238000001179 sorption measurement Methods 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000004677 Nylon Substances 0.000 claims description 6
- 239000012530 fluid Substances 0.000 claims description 6
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 6
- 235000008434 ginseng Nutrition 0.000 claims description 6
- 238000011068 loading method Methods 0.000 claims description 6
- 229920001778 nylon Polymers 0.000 claims description 6
- 239000013049 sediment Substances 0.000 claims description 6
- 239000006228 supernatant Substances 0.000 claims description 6
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 claims description 5
- 235000003140 Panax quinquefolius Nutrition 0.000 claims description 5
- 240000005001 Paeonia suffruticosa Species 0.000 claims description 4
- 235000003889 Paeonia suffruticosa Nutrition 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 241000222336 Ganoderma Species 0.000 claims description 3
- 244000269722 Thea sinensis Species 0.000 claims description 3
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 2
- 244000189548 Chrysanthemum x morifolium Species 0.000 claims description 2
- 235000013312 flour Nutrition 0.000 claims description 2
- 241000208340 Araliaceae Species 0.000 claims 2
- 238000000034 method Methods 0.000 abstract description 12
- 235000010987 pectin Nutrition 0.000 abstract description 8
- 229920001277 pectin Polymers 0.000 abstract description 8
- 239000001814 pectin Substances 0.000 abstract description 8
- 230000008901 benefit Effects 0.000 abstract description 7
- 238000005516 engineering process Methods 0.000 abstract description 7
- 210000004027 cell Anatomy 0.000 abstract description 6
- 210000000170 cell membrane Anatomy 0.000 abstract description 6
- 239000000463 material Substances 0.000 abstract description 5
- 125000003118 aryl group Chemical group 0.000 abstract description 3
- 229910001385 heavy metal Inorganic materials 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 239000011149 active material Substances 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000011812 mixed powder Substances 0.000 description 6
- 102000004190 Enzymes Human genes 0.000 description 5
- 108090000790 Enzymes Proteins 0.000 description 5
- 238000010828 elution Methods 0.000 description 5
- 240000004371 Panax ginseng Species 0.000 description 4
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 4
- 238000004090 dissolution Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 230000006870 function Effects 0.000 description 3
- 210000003205 muscle Anatomy 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000009461 vacuum packaging Methods 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- 241000208686 Eucommiaceae Species 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 210000000577 adipose tissue Anatomy 0.000 description 2
- 210000004404 adrenal cortex Anatomy 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 230000036772 blood pressure Effects 0.000 description 2
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- 235000012000 cholesterol Nutrition 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 210000000987 immune system Anatomy 0.000 description 2
- 230000003834 intracellular effect Effects 0.000 description 2
- 230000001817 pituitary effect Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000002485 urinary effect Effects 0.000 description 2
- 206010000234 Abortion spontaneous Diseases 0.000 description 1
- 229920001342 Bakelite® Polymers 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 235000002789 Panax ginseng Nutrition 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 229930003270 Vitamin B Natural products 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 208000031975 Yang Deficiency Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 239000004637 bakelite Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 230000019522 cellular metabolic process Effects 0.000 description 1
- 210000003850 cellular structure Anatomy 0.000 description 1
- 210000003169 central nervous system Anatomy 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 210000002249 digestive system Anatomy 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000035619 diuresis Effects 0.000 description 1
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- 210000003734 kidney Anatomy 0.000 description 1
- 210000000265 leukocyte Anatomy 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 210000003141 lower extremity Anatomy 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 208000015994 miscarriage Diseases 0.000 description 1
- 229920001206 natural gum Polymers 0.000 description 1
- 210000000653 nervous system Anatomy 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
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- 230000000144 pharmacologic effect Effects 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
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- 238000001556 precipitation Methods 0.000 description 1
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- 210000004706 scrotum Anatomy 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Medicines Containing Plant Substances (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a kind of precious preparation method of bark of eucommia, fully utilize mechanical means extraction process and biological enzymolysis technology extraction process, the cell membrane of the trunk, branch and leaf of the bark of eucommia is broken first with the methods such as Ultramicro-powder, stirring, vibration of ultrasonic wave are ground to form, the benefit materials for allowing it to discharge cell interior, then extract the benefit materials such as pectin, the glue in trunk, branch and the leaf cells of the bark of eucommia using biological enzymolysis technology.The present invention breaks through conventional matter extractive technique bottleneck in production technology, farthest remains the active material in the trunk, branch and leaf of the bark of eucommia, and without harmful substances such as any heavy metals.Any portion that the present invention takes full advantage of trunk, branch and leaf and the bark of eucommia has the part of medical value, the bark of eucommia is really made the best use of everything, and with technique is simple, taste is aromatic, taste is pure and fresh, fully demonstrated the health value of the bark of eucommia.
Description
Technical field
The present invention relates to a kind of precious processing method of healht-care, more particularly to a kind of Du by primary raw material of bark of eucommia powder
Zhong Zhen preparation method.
Background technology
The bark of eucommia, also known as bakelite, are Eucommiaceae plant, and the bark, branch or leaf of the bark of eucommia are fractureed, have silk thread adhesion, just
As separated but still in each other's thoughts, the silk thread of those adhesions is exactly the collodion silk of the bark of eucommia, the medicinal bark of eucommia, and as the Eucommiaceae plant bark of eucommia is dry
Dry bark, is Chinese rare tonic herb.Its is sweet, warm-natured, have tonify the liver and kidney, strengthen muscles and bones, coordinating Chong and Conception Vessels, strengthen meridian and miscarriage prevention
Effect；Pain in waist and lower extremities caused by kidney-yang deficiency can be treated or aching and limp powerless, born of the same parents' tire caused by liver- qi invasion is not solid, wet itch of scrotum waits disease, shuts out
It is secondary to there is different degrees of regulation to make to immune system, internal system, central nervous system, the circulatory system and urinary system
With, the excited Pituitary Adrenalcortical system of bark of eucommia energy strengthens adrenal cortex function,《Sheng Nong's herbal classic》In be listed in
Product.The modern study bark of eucommia, which has, removes internal rubbish, strengthens human body cell metabolism, prevents muscle skeleton aging, balances people
Body blood pressure, decomposer inner cholesterol reduces body fat, recovers blood vessel elasticity, diuresis heat-clearing, broad-spectrum antiseptic, excited maincenter god
Through improving white blood cell pharmacological action.Eucommia Tea is that the leaf of the plant bark of eucommia is raw material, is processed through traditional tea processing and the prepared slices of Chinese crude drugs
The health drink that method is made, samples slight bitter and time sweet tea is suitable for reading, often drinks good for health, health value pole of being had a drink before sleeping
Height, it is without any side effects, drink conveniently.
The method that tradition takes the bark of eucommia, the leaf of the bark of eucommia be able to can be used as medicine with brewed for drinking, the dry bark of the bark of eucommia, but Du
Zhong Zhi, bar, dry, stem can not be utilized always, and bark of eucommia branch, bar, dry, stem are also enriched in colloid after testing, and contain flavonoids, polyphenol,
The medical value such as vitamin C and vitamin B, but the method for the edible bark of eucommia of tradition can not make the bark of eucommia really be made the best use of everything；
And traditional eating method, also makes human body can not also fully absorb bark of eucommia medicinal health value.
The content of the invention
The invention aims to solve the not enough of above-mentioned technical problem presence there is provided one kind can not only fully demonstrate Du
Secondary medical value, makes the bark of eucommia really be made the best use of everything, and with technique is simple, taste is aromatic, taste is pure and fresh, abundant body
A kind of precious preparation method of bark of eucommia of eucommia health care value is showed.
The technical solution adopted in the present invention is that the precious preparation method of this bark of eucommia is：
Step 1: the trunk, branch and leaf of the bark of eucommia are eluted with water, dry in the cool, be put into crushing 3-5 in pulverizer small
When, grind 4-8 hours, make the granularity of bark of eucommia mixture at 1 μm ~ 10 μm, add water, the amount for adding water is bark of eucommia mixture total weight
4-8 times of amount, stirs, and carries out vibration of ultrasonic wave 20-30 minutes, adds the 3-15% of bark of eucommia total weight of the mixture pectin
Enzyme, boils 1-2h, next mixture is cooled down, and fried juice is filtered by 50 μm of nylon mesh, and filtered fluid is in centrifuge
In carry out separation 2~3 times, 10 min and then collect supernatant liquid every time, be centrifuged liquid is collected into until not having
Sediment is separated out, and merges extract solution, the thick glue of extraction of the bark of eucommia finally obtained；
Separated Step 2: the bark of eucommia that step one is obtained extracts thick liquid with Flavonoids by Macroporous Adsorption Resin, extract thick liquid pH controls
In 7-9, loading is adsorbed with 2.5-4.5BV/h flow velocitys, and concentration of alcohol is 85%, and elution flow rate uses 2BV/h, and collection is obtained
The Hydrolysis kinetics glue of the bark of eucommia；
Step 3: the Hydrolysis kinetics glue for the bark of eucommia that step 2 is obtained, through low temperature drying, concentration, obtains mixture of viscous form,
High temperature drying, after crushing 1-2 hours, obtains thick mixed powder, and along with the additive particles for having health value, stirring is equal
It is even, obtain bark of eucommia mixture；The bark of eucommia that the present invention is obtained after being vacuum-packed after well mixed is precious.
Trunk, branch and the leaf of the bark of eucommia are chosen wherein in step one, it is complete that this eats bark of eucommia method with traditional people
It is complete different, bark of eucommia utilization rate can be farthest improved, the bark of eucommia is really made the best use of everything.
Trunk, branch and the leaf of the bark of eucommia are chosen wherein in step one, due to the trunk of the bark of eucommia, branch and leaf cost
It is cheap, so as to reduce the totle drilling cost of final products, the health products of the present invention can be made to enter into huge numbers of families.
The wherein granularity of the bark of eucommia mixture of step one, at 1 μm ~ 10 μm, is the cell membrane because trunk, branch quality are hard
Compare thick, the general broken dissolution that can not break effective medicinal component in the cell membrane of trunk, branch and leaf, cell need to be worn
Several or even dozens of cell membrane is crossed, and quite a few Cell Component can not possibly pass through cell membrane, and this part can only be white
Slattern in vain, therefore intracellular active ingredient can not be made all fully to discharge, the present invention passes through crushing and the side ground
Formula reaches Ultramicro-powder, intracellular active ingredient is all fully discharged, and improves in trunk, branch and leaf effectively
The dissolution rate and dissolution rate of composition, our experiments show that, dissolution rate can reach 90-98%.
Wherein step one stirs, and carries out vibration of ultrasonic wave 20-30 minutes, be trunk for the bark of eucommia, branch and
On the basis of the mixture ultra micro powder cell wall breaking of leaf, make continuation to breaking-wall cell using vibration of ultrasonic wave, improve the bark of eucommia
The bioavilability of trunk, branch and leaf, is conducive to absorption and utilization of the human body to benefit materials.
The wherein 3-15% of the total weight of the mixture of the trunk of the addition bark of eucommia of step one, branch and leaf pectase, be
For the pectin in the trunk, branch and leaf of the bark of eucommia, glue, natural gum, mucilagenous precipitation.
Wherein step 2 the thick liquid of extraction of the trunk, branch and leaf of the bark of eucommia is carried out with Flavonoids by Macroporous Adsorption Resin it is pure
Change, eliminate the harmful substances such as impurity, heavy metal.
The additive particles for wherein having health value in step 3 are：Tea, glossy ganoderma powder, chrysanthemum powder, ginseng pulverate, flower of Panax ginseng
One or more of mixing in powder, tree peony coffee or yam flour etc..
Thick mixed powder and the additive particles mixed proportion for having health value are arbitrary proportion wherein in step 3.
The present invention is direct-edible, also is added in coffee, tree peony coffee, teabag drink, milk, various treasure, can improve
Mouthfeel, not only strengthens nutrition, and human body is played a role in health care.
The invention comprehensively utilizes mechanical means extraction process and biological enzymolysis technology extraction process, first with grinding to form
The methods such as Ultramicro-powder, stirring, vibration of ultrasonic wave break the cell membrane of the trunk, branch and leaf of the bark of eucommia, allow it to discharge cell
Internal benefit materials, then carried out using biological enzymolysis technology pectin in trunk, branch and the leaf cells of the extraction bark of eucommia,
The benefit materials such as glue.The present invention breaks through conventional matter extractive technique bottleneck in production technology, farthest remains Du
Active material in secondary trunk, branch and leaf, and without harmful substances such as any heavy metals.
Beneficial effects of the present invention:The present invention provides a kind of bark of eucommia precious preparation method, takes full advantage of trunk, branch
There is the part of medical value with any portion of leaf and the bark of eucommia, the bark of eucommia is really made the best use of everything, and with technique
Simply, taste is aromatic, taste is pure and fresh, fully demonstrated the health value of the bark of eucommia, can make immune system, internal system, in
Pivot nervous system, the circulatory system and urinary system have different degrees of adjustment effect, can remove internal rubbish, strengthen human body thin
Born of the same parents' metabolism, prevents muscle skeleton aging, and balanced human's blood pressure, decomposer inner cholesterol reduces body fat, recovers blood vessel
Elasticity, the bark of eucommia can excited Pituitary Adrenalcortical system, enhancing adrenal cortex function, pre- anti-cancer, improvement human brain memory power
The effects such as Deng digestive system function is improved, and it is adapted to any crowd.
Embodiment
The present invention is described in detail in following examples.
Embodiment 1
The precious preparation method of this bark of eucommia is：
Step 1: the trunk, branch and leaf of the bark of eucommia are eluted with water, dry in the cool, be put into crushing 3-5 in pulverizer small
When, grind 4-8 hours, make the granularity of bark of eucommia mixture at 1 μm ~ 10 μm, add water, the amount for adding water is bark of eucommia mixture total weight
4-8 times of amount, stirs, and carries out vibration of ultrasonic wave 20-30 minutes, adds the 3-15% of bark of eucommia total weight of the mixture pectin
Enzyme, boils 1-2h, next mixture is cooled down, and fried juice is filtered by 50 μm of nylon mesh, and filtered fluid is in centrifuge
In carry out separation 2~3 times, 10 min and then collect supernatant liquid every time, be centrifuged liquid is collected into until not having
Sediment is separated out, and merges extract solution, the thick glue of extraction of the bark of eucommia finally obtained；
Separated Step 2: the bark of eucommia that step one is obtained extracts thick liquid with Flavonoids by Macroporous Adsorption Resin, extract thick liquid pH controls
In 7-9, loading is adsorbed with 2.5-4.5BV/h flow velocitys, and concentration of alcohol is 85%, and elution flow rate uses 2BV/h, and collection is obtained
The Hydrolysis kinetics glue of the bark of eucommia；
Step 3: the Hydrolysis kinetics glue for the bark of eucommia that step 2 is obtained, through low temperature drying, concentration, obtains mixture of viscous form,
High temperature drying, after crushing 1-2 hours, obtains thick mixed powder, along with the additive particles for having health value, thick mixed
The additive particles mixed proportion closed powder and have health value is 10:0, stir, obtain bark of eucommia mixture；It is well mixed
The bark of eucommia that the present invention is obtained after being vacuum-packed afterwards is precious.
Embodiment 2
The precious preparation method of this bark of eucommia is：
Step 1: the trunk, branch and leaf of the bark of eucommia are eluted with water, dry in the cool, be put into crushing 3-5 in pulverizer small
When, grind 4-8 hours, make the granularity of bark of eucommia mixture at 1 μm ~ 10 μm, add water, the amount for adding water is bark of eucommia mixture total weight
4-8 times of amount, stirs, and carries out vibration of ultrasonic wave 20-30 minutes, adds the 3-15% of bark of eucommia total weight of the mixture pectin
Enzyme, boils 1-2h, next mixture is cooled down, and fried juice is filtered by 50 μm of nylon mesh, and filtered fluid is in centrifuge
In carry out separation 2~3 times, 10 min and then collect supernatant liquid every time, be centrifuged liquid is collected into until not having
Sediment is separated out, and merges extract solution, the thick glue of extraction of the bark of eucommia finally obtained；
Separated Step 2: the bark of eucommia that step one is obtained extracts thick liquid with Flavonoids by Macroporous Adsorption Resin, extract thick liquid pH controls
In 7-9, loading is adsorbed with 2.5-4.5BV/h flow velocitys, and concentration of alcohol is 85%, and elution flow rate uses 2BV/h, and collection is obtained
The Hydrolysis kinetics glue of the bark of eucommia；
Step 3: the Hydrolysis kinetics glue for the bark of eucommia that step 2 is obtained, through low temperature drying, concentration, obtains mixture of viscous form,
High temperature drying, after crushing 1-2 hours, obtains thick mixed powder, along with the additive particles for having health value, thick mixed
The additive particles mixed proportion closed powder and have health value is 1:1, stir, obtain bark of eucommia mixture；After well mixed
The bark of eucommia that the present invention is obtained after vacuum packaging is precious.
The additive particles for having health value are：Ginseng pulverate and ginseng pollen.
Embodiment 3
The precious preparation method of this bark of eucommia is：
Step 1: the trunk, branch and leaf of the bark of eucommia are eluted with water, dry in the cool, be put into crushing 3-5 in pulverizer small
When, grind 4-8 hours, make the granularity of bark of eucommia mixture at 1 μm ~ 10 μm, add water, the amount for adding water is bark of eucommia mixture total weight
4-8 times of amount, stirs, and carries out vibration of ultrasonic wave 20-30 minutes, adds the 3-15% of bark of eucommia total weight of the mixture pectin
Enzyme, boils 1-2h, next mixture is cooled down, and fried juice is filtered by 50 μm of nylon mesh, and filtered fluid is in centrifuge
In carry out separation 2~3 times, 10 min and then collect supernatant liquid every time, be centrifuged liquid is collected into until not having
Sediment is separated out, and merges extract solution, the thick glue of extraction of the bark of eucommia finally obtained；
Separated Step 2: the bark of eucommia that step one is obtained extracts thick liquid with Flavonoids by Macroporous Adsorption Resin, extract thick liquid pH controls
In 7-9, loading is adsorbed with 2.5-4.5BV/h flow velocitys, and concentration of alcohol is 85%, and elution flow rate uses 2BV/h, and collection is obtained
The Hydrolysis kinetics glue of the bark of eucommia；
Step 3: the Hydrolysis kinetics glue for the bark of eucommia that step 2 is obtained, through low temperature drying, concentration, obtains mixture of viscous form,
High temperature drying, after crushing 1-2 hours, obtains thick mixed powder, along with the additive particles for having health value, thick mixed
The additive particles mixed proportion closed powder and have health value is 8:2, stir, obtain bark of eucommia mixture；After well mixed
The bark of eucommia that the present invention is obtained after vacuum packaging is precious.
The additive particles for having health value are：Tree peony coffee.
Embodiment 4
The precious preparation method of this bark of eucommia is：
Step 1: the trunk, branch and leaf of the bark of eucommia are eluted with water, dry in the cool, be put into crushing 3-5 in pulverizer small
When, grind 4-8 hours, make the granularity of bark of eucommia mixture at 1 μm ~ 10 μm, add water, the amount for adding water is bark of eucommia mixture total weight
4-8 times of amount, stirs, and carries out vibration of ultrasonic wave 20-30 minutes, adds the 3-15% of bark of eucommia total weight of the mixture pectin
Enzyme, boils 1-2h, next mixture is cooled down, and fried juice is filtered by 50 μm of nylon mesh, and filtered fluid is in centrifuge
In carry out separation 2~3 times, 10 min and then collect supernatant liquid every time, be centrifuged liquid is collected into until not having
Sediment is separated out, and merges extract solution, the thick glue of extraction of the bark of eucommia finally obtained；
Separated Step 2: the bark of eucommia that step one is obtained extracts thick liquid with Flavonoids by Macroporous Adsorption Resin, extract thick liquid pH controls
In 7-9, loading is adsorbed with 2.5-4.5BV/h flow velocitys, and concentration of alcohol is 85%, and elution flow rate uses 2BV/h, and collection is obtained
The Hydrolysis kinetics glue of the bark of eucommia；
Step 3: the Hydrolysis kinetics glue for the bark of eucommia that step 2 is obtained, through low temperature drying, concentration, obtains mixture of viscous form,
High temperature drying, after crushing 1-2 hours, obtains thick mixed powder, along with the additive particles for having health value, thick mixed
The additive particles mixed proportion closed powder and have health value is 7:3, stir, obtain bark of eucommia mixture；After well mixed
The bark of eucommia that the present invention is obtained after vacuum packaging is precious.
The additive particles for having health value are：Glossy ganoderma powder.
Claims (4)
1. a kind of precious preparation method of bark of eucommia, it is characterised in that：Step 1: the trunk, branch and leaf of the bark of eucommia are eluted with water,
Dry in the cool, be put into pulverizer and crush 3-5 hours, grind 4-8 hours, add water, the amount for adding water is bark of eucommia mixing
4-8 times of thing gross weight, stirs, and carries out vibration of ultrasonic wave 20-30 minutes, adds pectase, boils 1-2h, next handle
Mixture is cooled down, and fried juice is filtered by 50 μm of nylon mesh, and filtered fluid carries out separation 2~3 times in centrifuge, every time
Then 10 min collect supernatant liquid, are centrifuged liquid is collected into until no sediment is separated out, merge extract solution,
The thick glue of extraction of the bark of eucommia finally obtained；Step 2: the bark of eucommia that step one is obtained extracts thick liquid Flavonoids by Macroporous Adsorption Resin
Separated, extract thick liquid pH controls in 7-9, loading is adsorbed with 2.5-4.5BV/h flow velocitys, and concentration of alcohol is 85%, is washed
Separation of flow speed uses 2BV/h, collects the Hydrolysis kinetics glue for obtaining the bark of eucommia；Step 3: the extraction essence for the bark of eucommia that step 2 is obtained
Glue liquid, through low temperature drying, concentration, obtains mixture of viscous form, high temperature drying after crushing 1-2 hours, obtains thick mixing
Powder, along with the additive particles for having health value, stirs, and obtains bark of eucommia mixture；After being vacuum-packed after well mixed
The bark of eucommia for obtaining the present invention is precious.
2. a kind of precious preparation method of bark of eucommia according to claim 1, it is characterised in that：Bark of eucommia mixture in step one
Granularity at 1 μm ~ 10 μm.
3. a kind of precious preparation method of bark of eucommia according to claim 1, it is characterised in that：Pectase in step one is added
Measure as the 3-15% of bark of eucommia total weight of the mixture.
4. a kind of precious preparation method of bark of eucommia according to claim 1, it is characterised in that：There is guarantor in step 3 in step 3
Being good for the additive particles being worth is：In tea, glossy ganoderma powder, chrysanthemum powder, ginseng pulverate, ginseng pollen, tree peony coffee or yam flour etc.
One or more mixing.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104403799A (en) * | 2014-11-22 | 2015-03-11 | 河南恒瑞源实业有限公司 | Comprehensive utilizing method of eucommia ulmoides |
| CN102863628B (en) * | 2012-11-05 | 2015-04-29 | 河南恒瑞源实业有限公司 | Method for preparing eucommia rubber by using eucommia seeds |
| CN105832806A (en) * | 2016-03-24 | 2016-08-10 | 浙江旭源杜仲生物科技有限公司 | Production process for eucommia ulmoides leaf extract fine powder oral health-caring tablets |
| CN105942513A (en) * | 2016-06-03 | 2016-09-21 | 河南洛阳红牡丹产业研发有限公司 | Peony plant edible gum preparing method |
| CN105996030A (en) * | 2016-05-19 | 2016-10-12 | 河南洛阳红牡丹产业研发有限公司 | Method for preparing peony powder |
-
2017
- 2017-03-21 CN CN201710167995.4A patent/CN107028183A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102863628B (en) * | 2012-11-05 | 2015-04-29 | 河南恒瑞源实业有限公司 | Method for preparing eucommia rubber by using eucommia seeds |
| CN104403799A (en) * | 2014-11-22 | 2015-03-11 | 河南恒瑞源实业有限公司 | Comprehensive utilizing method of eucommia ulmoides |
| CN105832806A (en) * | 2016-03-24 | 2016-08-10 | 浙江旭源杜仲生物科技有限公司 | Production process for eucommia ulmoides leaf extract fine powder oral health-caring tablets |
| CN105996030A (en) * | 2016-05-19 | 2016-10-12 | 河南洛阳红牡丹产业研发有限公司 | Method for preparing peony powder |
| CN105942513A (en) * | 2016-06-03 | 2016-09-21 | 河南洛阳红牡丹产业研发有限公司 | Peony plant edible gum preparing method |
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