CN105767397A - Spleen-invigorating and stomach-harmonizing gingko tea - Google Patents
Spleen-invigorating and stomach-harmonizing gingko tea Download PDFInfo
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Abstract
The invention discloses spleen-invigorating and stomach-harmonizing gingko tea, which is prepared from the following raw materials: poria, a lily, radix glycyrrhizae preparata, tangerine peel, rhizoma atractylodis macrocephalae, a mulberry, radix puerariae, maltodextrin, ginkgetin, tea polyphenol, stevioside, a vitamin, a thickening agent, a latent solvent, a dispersing agent, an antioxidant, a flavor enhancer and a flavoring agent. The spleen-invigorating and stomach-harmonizing gingko tea is prepared through the steps of liquid medicine extraction, clear paste preparation, pelletizing, sterilization and the like. The gingko tea provided by the invention has the effects of spleen invigoration, stomach harmonization and the like, and is good in taste and fragrant and mellow in flavor when being made into a beverage; any preservative and pigment are not added in the spleen-invigorating and stomach-harmonizing gingko tea provided by the invention, essence is refined from pure natural plants; the technique of making tea by cold water is broken through; by utilizing a low-temperature extraction technique, active ingredients in the plants are guaranteed not to be destroyed; the spleen-invigorating and stomach-harmonizing gingko tea is easily absorbed by a body after being drunk; the disadvantages of a conventional product are solved as the spleen-invigorating and stomach-harmonizing gingko tea is easily dissolved and easily absorbed.
Description
[technical field]
The invention belongs to tea processing technique field, be specifically related to a kind of invigorating the spleen and regulating the stomach Folium Ginkgo tea and preparation method thereof.
[background technology]
Ginkgoaceae plant Ginkgo biloba is the endemic tree of China, has another name called maidenhair tree, and the age of tree, up to more than thousand, is the Permian Period in ancient times Relict Plant, has the title of " living fossil " in plant kingdom, is Relict Plant the most ancient in existing seed plant.Modern science shows, the chemical composition of Folium Ginkgo is sufficiently complex, wherein containing effective ingredient such as flavonoid, terpenoid, phenols, healthy trace elements with household and several amino acids in Folium Ginkgo.Folium Ginkgo extract contains substantial amounts of ginkgetin; ginkgetin is highly resistant to and prevents the infringement that human body is caused by the electromagnetic radiation such as computer, mobile phone; particularly that the protective effect of brain cell is obvious, also there is vessel softening, remove rubbish in blood, drop the effects such as three fat, scavenging free radicals.In active substance, the content of flavone decides the medical value of Folium Ginkgo, it is desirable to obtain more flavone, it is critical only that the extracting method of Folium Ginkgo；In traditional extraction process, solvent is easily accessible cell when heating, but solable matter is higher at the condition dissolubility of heat, is successively dissolved and significantly high permeability occurs, causes that extraction ratio is low, active component is low, and technique is loaded down with trivial details, and the production cycle is long.
Tea polyphenols is the general name of Polyphenols of Tea, is a kind of pure natural complex, and its content accounts for the 10%-25% (Forint phenol method) of dry matter of tea total amount.Tea polyphenols is made up of catechin (flavanol compound), anthocyan (leucoanthocyanidin and anthocyanidin), anthoxanthins (flavone and flavonols), phenolic acid and the big material of depside four, wherein catechin is mostly important, activity is the highest, accounts for the 70%-80% of tea polyphenols total amount.Tea polyphenols is a kind of high-efficient pure natural antioxidant, human free radical, enhancing human body immunity power can be removed, there is the multiple medical health care functions such as antitumor, radioprotective, antiviral, defying age, lowering blood-fat and reducing weight, also there is suppression atherosclerosis, remove halitosis, strengthen the effects such as vascular resistance ability.The oxidation resistance of tea polyphenols, than strong 3-9 times of VE, Butylated hydroxyanisole (BHA) and dibenzylatiooluene (BHT), is widely used to the every field such as the oxidation resistanct fresh-keeping of varieties of food items, medicine, health product, cosmetics and article of everyday use at present.Extraction is that tea polyphenols produces and the first step of preparation, how to improve the extraction ratio of tea polyphenols at low cost, and keeps the biological activity of tea polyphenols, is the bottleneck problem in producing.Commercial production is usually first by Folium Camelliae sinensis grinding and sieving, more under the high temperature conditions with water or high concentration ethanol aqueous solution lixiviate.Used high-temp extracting method Problems existing has: (1) energy consumption is high；(2) Product Activity low (tea polyphenols is oxidizable)；(3) extract impurity content high (high temperature easily leaches impurity)；(4) subsequent purification is often, and tea polyphenols loss amount is big；(5) easy gelatinizing during tea-leaf power high-temp extracting, not easily filters；(6) equipment requirements is high.Therefore the improvement of Methods of Extraction of Tea-polyphenols is significant with innovation.
Stevioside has excellent physiological property and stability, is widely used in the industries such as food, beverage, wine brewing, medicine, daily-use chemical industry as a kind of new food additive, and not only extraction process reaches its maturity, and extraction ratio also improves day by day.The method extracting stevioside at present from Stevia leaves mainly has organic solvent extraction and water extraction method, and wherein organic solvent extraction solvent consumption is big, cost is high, practicality is not good enough.Hot water extraction is current Application comparison extracting method widely, in industry, the general technology flow process of stevioside's water extraction is as follows: leaf of Folium Stevlae Rebaudianae → water logging (8-10h) → coarse filtration → removing impurity by means of precipitation → fine straining → purification → decolouring → desalination → concentrate drying, wherein water logging extraction and purification are the committed step of this technique, use and compare the hot water extracted many times that extracting process widely is 80 DEG C, the method of purification now more adopts resin absorption to separate, and the method for decolouring mainly has activated carbon decolorizing and resin decolorization two kinds.The shortcoming of this technique is that extraction time is long, and thermal energy consumption is high, and equipment processing safety is required height by High Temperature High Pressure, purification and in decolorization seriality poor, resin and reagent dosage are big simultaneously, and resin utilization rate is low, operates length consuming time.
Health tea, in China also known as medicated tea, mainly with Folium Camelliae sinensis such as green tea, black tea or oolong teas for raw material, it is simultaneously introduced medicable single or herbal mixture is made, the record that China cures the disease with regard to useful tea health preserving since ancient times, the healthcare knowledge to tea, the prehistoric phase can be traced back to the earliest, as far back as the Watermelon seedlings of B.C. 200 years, using Folium Camelliae sinensis as medicinal.After the Tang Dynasty, developing to some extent with tea compatibility Chinese medicine, there is medicated tea monograph the Song dynasty, and modern age, health tea was more general.Research and application to medicated tea, there is long history in China.
Now, along with economic fast development, people's dinner party increases, and for the frequent heavy drinking that works, the daily schedule is irregular, and diet is abnormal, not only results in uncomfortable, is also easy to cause disease of stomach, reduces body immunity, makes people's mood irritated, hypomnesis.
At present, market also has a lot of invigorating the spleen and regulating the stomach tea product, but does not reach desirable effect.
[summary of the invention]
The technical problem to be solved in the present invention is to provide a kind of invigorating the spleen and regulating the stomach Folium Ginkgo tea, and to solve to prepare ginkgetin extraction ratio in prior art and active component is low, technique is loaded down with trivial details, and the production cycle is long；The tea polyphenols activity low (tea polyphenols is oxidizable) of preparation and extract impurity content high (high temperature easily leaches impurity)；In stevioside's purification and decolorization, seriality is poor, and resin and reagent dosage are big, and resin utilization rate is low, operates length consuming time；The problems such as tea product invigorating the spleen and regulating the stomach effect is undesirable.The Folium Ginkgo tea of the present invention have the effects such as invigorating the spleen and regulating the stomach, make that beverage mouthfeel is good, taste is aromatic；The invigorating the spleen and regulating the stomach Folium Ginkgo tea of the present invention are without any preservative and pigment, pure natural plant refines elite, breach cold water to make tea technology, utilize low-temperature extraction technology, ensure that the active component in plant is not subjected to destroy, easily being absorbed by the body after drinking, it is readily soluble and is easily absorbed the short slab solving traditional product；The invigorating the spleen and regulating the stomach Folium Ginkgo tea frozen water of the present invention, cold water, brewed in hot water even can, unique flavor, facilitate all ages drunk by people.
In order to solve above technical problem, the present invention by the following technical solutions:
A kind of invigorating the spleen and regulating the stomach Folium Ginkgo tea, in units of weight portion, including following raw material: Poria 100-600 part, Bulbus Lilii 100-600 part, Radix Glycyrrhizae Preparata 100-600 part, Pericarpium Citri Reticulatae 60-240 part, Rhizoma Atractylodis Macrocephalae 60-240 part, Fructus Mori 40-120 part, Radix Puerariae 40-120 part, malt extract stick with paste 30-60 part, ginkgetin 1-3 part, tea polyphenols 1-3 part, stevioside's 1-3 part, vitamin 1-3 part, thickening agent 0.8-2 part, cosolvent 0.8-2 part, dispersant 0.8-2 part, antioxidant 0.8-2 part, tasty agents 0.5-1.5 part, flavouring agent 0.5-1.5 part；
The preparation method of described invigorating the spleen and regulating the stomach Folium Ginkgo tea, comprises the following steps:
S1: pulverize after Poria, Bulbus Lilii, Radix Glycyrrhizae Preparata, Pericarpium Citri Reticulatae, the Rhizoma Atractylodis Macrocephalae, Fructus Mori, Radix Puerariae are respectively dried, cross 40-60 mesh sieve, put in ultrasonic extraction equipment, extract after adding the 1500-9000 abundant moistening of part water, the condition extracted is: ultrasonic power is 120-180W, Extracting temperature is 40-70 DEG C, and extraction time is 30-60min；
S2: step S1 is extracted medical filtration, is sequentially added into ginkgetin, tea polyphenols, stevioside, vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent after puckery, it is stirring 1-3min under 200-500r/min at rotating speed, be uniformly mixed liquid, and concentrating the filtrate to relative density when temperature is 64-66 DEG C is the clear paste of 1.32-1.38；
S3: the clear paste of step S2 spray drying at temperature 200-220 DEG C, to water content≤6%, is crossed the sieve of 200-400 order after pulverizing, prepares powder；
S4: the powder of step S3 and malt extract are stuck with paste, 50-100 part water adopts comminutor to make granule after being sufficiently mixed; finally prepared described granule is 134-136 DEG C in temperature; pressure is 210-230KPa, and the time is sterilizing under 20-40s, obtains invigorating the spleen and regulating the stomach Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) undertaken pulverizing and cross 40-80 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) adopting the water of 38-62 DEG C to carry out lixiviate the Ginkgo Leaf that step 1 prepares, in lixiviate, solid-to-liquid ratio is 1:12-14 (W/V), and extraction time is 2.5-3.5h, extracts 2-3 time, filtration, merging filtrate after extraction, prepares mixing lixiviating solution；
(3) the mixing lixiviating solution concentrate drying that step 2 is prepared, prepare lixiviate cream, the water of be used in lixiviate 5.5-6 times of volume of cream 45-55 DEG C dissolves, anhydrous ethyl acetate solvent is adopted to carry out extracting 2-3 time, continuation anhydrous ethyl acetate carries out repeatedly crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.2-5.4 (W/V), prepares crystal crude product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extracting, the condition of extraction: extraction kettle pressure is 12-18MPa, and extraction temperature is 42-45 DEG C, extraction time is 32-40min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 40-80 mesh sieve after group's sieve tea pulverizing, mix for 1:16-20 in mass ratio with the ethanol water that mass fraction is 40%-60%, extract 2-3 time at temperature is 36-40 DEG C, each 20-30min, filters, merging filtrate, concentration, prepares tea polyphenols crude extract；
B the tea polyphenols crude extract that step a prepares is joined in KCl solution by (), pH regulator is to 6.8-7.2, it is removing impurity under 4000-4500r/min at centrifugal rotational speed, adopts 0.45 μm of filter membrane at temperature is 34-36 DEG C, the solution after being centrifuged to be filtered, prepare filtrate；
(c) by step b prepare filtrate ether extraction, freezing, after drying prepare tea polyphenols；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) crossing 40-80 mesh sieve after being pulverized by Stevia leaves, be dipped in water and soak 1-1.2.h, solid-to-liquid ratio is 1:20-25 (W/V), it is 100-120W at ultrasonic power, Extracting temperature is 40-60 DEG C, and extraction time is extract under 20-30min, prepares Folium Stevlae Rebaudianae medicinal liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 120-180 order, prepares Folium Stevlae Rebaudianae filtrate；
(C) NaAl (SO of filtrate percentage by weight 0.8%-1% is added to the step B Folium Stevlae Rebaudianae filtrate prepared4)2Ca (OH) with filtrate percentage by weight 1%-1.4%2, tune pH value is 6.8-7.2, at temperature 44-48 DEG C, stands 3.2-3.5h, prepares the solution after the removal of impurity；
(D) by the solution frit after the step C removal of impurity prepared and in being concentrated into every milliliter containing stevioside 10%-25%, macroporous adsorbent resin ADS-8 separating-purifying is adopted to prepare the liquid of stevioside, condition is: resolving agent is the alcoholic solution of 55%-65%, its consumption is 1-3 times of macroporous adsorbent resin volume, water wash zone is deionized water, absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 2%-4%, adsorption zone flow velocity 6-10BV/h, desorption zone flow velocity 15-20BV/h, water wash zone flow velocity 20-25BV/h, renewing zone flow velocity 6-8BV/h, switching time is 700-750s, temperature is 40-50 DEG C, pressure is 0.4-0.9MPa；
(E) stevioside's liquid that step D prepares is concentrated, at temperature is 200-220 DEG C, carries out spray drying, prepare stevioside.
Further, described vitamin includes one or more in vitamin A, vitamin C, vitamin D and vitamin E.
Further, described thickening agent includes one or more in xanthan gum, guar gum, locust bean gum and locust bean gum.
Further, described cosolvent is polyvinylpyrrolidone.
Further, described dispersant includes following component: one or more in potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium and potassium alginate.
Further, described antioxidant includes one or more in food grade antioxidant 9701, food grade antioxidant BHT, the different VC potassium of food grade antioxidant, food grade antioxidant BHA and food grade antioxidant MSK-NE150.
Further, described tasty agents includes one or more in inosinic acid potassium and guanyl potassium.
Further, described flavouring agent is methyl cyclopentenyl ketone.
Pharmacological action of the present invention is as follows:
Poria has the effects such as eliminating dampness and diuresis, invigorating the spleen and regulating the stomach, mind tranquilizing and the heart calming, dysuria, edema distension, heating, phlegm retention cough with dyspnea, vomiting, malignant histocytosis can be controlled, have loose bowels, pass out semen, stranguria with turbid discharge, palpitation with fear, the symptom such as forgetful.
Bulbus Lilii has the effect such as removing toxic substances, reason spleen stomach invigorating, dampness removing removing food stagnancy, mind tranquilizing and the heart calming, blood circulation promoting, cures mainly the symptoms such as chronic cough, hemoptysis, fidgets due to deficiency palpitation with fear.
Radix Glycyrrhizae Preparata contains the multiple chemical compositions such as glycyrrhizin, enoxolone, Angelica Polysaccharide, there is antiinflammatory and anti-allergy action, scalable body's immunity, antitumor and analgesic effect, therefore, the primary efficacy of Radix Glycyrrhizae Preparata is and middle emergency, lung moistening, removing toxic substances, coordinating the actions of various ingredients in a prescription.It is usually used in weakness of the spleen and stomach, fatigue and weakness, severe palpitation, irregularly intermittent and regularly intermittent pulse, Radix Aconiti Lateralis Preparata poison can be solved.
Pericarpium Citri Reticulatae has the effects such as the spleen invigorating of ventilation, drying dampness to eliminate phlegm, the greasy lasting of solution, stopping nausea and vomiting by lowering the adverse flow of QI, can control the symptoms such as cough heating, distension and fullness of the chest and abdomen, anorexia, vomiting hiccup, cough with copious phlegm.
The effect of the Rhizoma Atractylodis Macrocephalae mainly have invigorating the spleen and regulating the stomach, calmness, vasodilation, anticoagulant, anti-gastric-ulcer, hepatic cholagogic, diuresis, strong, improve immunity, antioxidation, antibacterial etc..
The effects such as containing the nutrient substance such as tannic acid, fatty acid, malic acid in Fructus Mori, Fructus Mori sweet in the mouth, cold in nature, tool promoting the production of body fluid to quench thirst, the liver and the kidney tonifying, nourishing YIN and supplementing blood, improving eyesight are calmed the nerves, hair color, profit joint, relieving alcoholic intoxication, invigorating the spleen and regulating the stomach.The digestion of fat, protein and starch can be promoted, therefore have strengthening the spleen and stomach, aid digestion effect, can be used for the diarrhoea that treatment causes because of dyspepsia.
Radix Puerariae has the effects such as heat clearing away, decomposing alcohol, invigorating the spleen and regulating the stomach, relieving alcoholism and protecting the liver, and to reducing blood fat, blood pressure, blood glucose, auxiliary treatment coronary heart diseases and angina pectoris, nervous headache etc. have positive effect.
Ginkgetin is to extract from the leaf of " living fossil " ginkgo; it is highly resistant to and prevents the infringement that human body is caused by the electromagnetic radiation such as computer, mobile phone; particularly that the protective effect of brain cell is obvious, also there is vessel softening, remove rubbish in blood, drop the effects such as three fat, scavenging free radicals.
Tea polyphenols is extracting directly from a tender leaf of sieve tea and spring bud, has very strong Scavenger of ROS to act on free radical, control oxidase, elimination halitosis, protection vision etc..
Stevioside extracts from natural Stevia leaves, is a kind of have high sugariness, natural sweetener low in calories.Long-term eating will not make people get fat, and have certain adjustment blood glucose function stevioside to have no side effect, non-carcinogenesis, noresidue, safe and reliable, often edible can the disease such as prophylaxis of hypertension, heart disease, dental caries, be particularly well-suited to the health care of diabetics, phenyl ketonuria patient and obese people.Stevioside is that the current world has been found that, and through the natural low caloric value sweeting agent closest to sucrose taste of China's Ministry of Public Health, Ministry of Light Industry's approval use, it is continue to have Development volue and the healthy natural sucrose substitute praised highly outside cane suger and beet sugar, is described as " third place in the world sucrose ".
The method have the advantages that
(1) xanthan gum in the present invention, guar gum, locust bean gum, locust bean gum, it is possible to play thickening, suspension effect, improve mouthfeel, make mouthfeel smooth, improve invigorating the spleen and regulating the stomach Folium Ginkgo tea quality；
(2) present invention uses inosinic acid potassium, guanyl potassium, delicate flavour can be made to increase several times, make invigorating the spleen and regulating the stomach Folium Ginkgo tea have strong natural flavor；
(3) present invention uses cosolvent, is conducive to the dissolving of each composition, makes solution mix homogeneously；
(4) present invention uses dispersant, and system can be made uniform, and suspendability increases, and does not precipitate, makes whole system physico-chemical property the same；
(5) present invention uses antioxidant, it is to avoid the materials such as tea polyphenols lose activity in preparing invigorating the spleen and regulating the stomach Folium Ginkgo tea process；
(6) present invention uses flavouring agent to cover abnormal flavour in invigorating the spleen and regulating the stomach Folium Ginkgo tea, improves invigorating the spleen and regulating the stomach Folium Ginkgo tea palatability；
(7) present invention extracts ginkgetin rate and active component height, and technique is simple, with short production cycle；
(8) tea polyphenols activity and the extract impurity content that prepared by the present invention are high；
(9) in stevioside's purification of the present invention and decolorization, seriality is good, and resin and reagent dosage are little, and resin utilization rate is high, operates consuming time short；
(10) Folium Ginkgo tea of the present invention have the effects such as invigorating the spleen and regulating the stomach, make that beverage mouthfeel is good, taste is aromatic；
(11) compared with the Folium Ginkgo tea of traditional handicraft, fully achieve the problems such as de-bitter detoxification, safely and effectively the benefit of Semen Ginkgo is performed to ultimate attainment；
(12) the invigorating the spleen and regulating the stomach Folium Ginkgo tea of the present invention are without any preservative and pigment, pure natural plant refines elite, breach cold water to make tea technology, utilize low-temperature extraction technology, ensure that the active component in plant is not subjected to destroy, easily being absorbed by the body after drinking, it is readily soluble and is easily absorbed the short slab solving traditional product；
(13) the invigorating the spleen and regulating the stomach Folium Ginkgo tea frozen water of the present invention, cold water, brewed in hot water even can, unique flavor, facilitate drinking of each age level.
[detailed description of the invention]
For ease of being more fully understood that the present invention, being illustrated by following instance, these examples belong to protection scope of the present invention, but are not intended to protection scope of the present invention.
In an embodiment, invigorating the spleen and regulating the stomach Folium Ginkgo tea, in units of weight portion, including following raw material: Poria 100-600 part, Bulbus Lilii 100-600 part, Radix Glycyrrhizae Preparata 100-600 part, Pericarpium Citri Reticulatae 60-240 part, Rhizoma Atractylodis Macrocephalae 60-240 part, Fructus Mori 40-120 part, Radix Puerariae 40-120 part, malt extract stick with paste 30-60 part, ginkgetin 1-3 part, tea polyphenols 1-3 part, stevioside's 1-3 part, vitamin 1-3 part, thickening agent 0.8-2 part, cosolvent 0.8-2 part, dispersant 0.8-2 part, antioxidant 0.8-2 part, tasty agents 0.5-1.5 part, flavouring agent 0.5-1.5 part；
Described vitamin includes one or more in vitamin A, vitamin C, vitamin D and vitamin E；
Described thickening agent includes one or more in xanthan gum, guar gum, locust bean gum and locust bean gum；
Described cosolvent is polyvinylpyrrolidone；
Described dispersant includes following component: one or more of potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium and potassium alginate；
Described antioxidant includes one or more in food grade antioxidant 9701, food grade antioxidant BHT, the different VC potassium of food grade antioxidant, food grade antioxidant BHA and food grade antioxidant MSK-NE150；
Described tasty agents includes one or more in inosinic acid potassium and guanyl potassium；
Described flavouring agent is methyl cyclopentenyl ketone；
The preparation method of described invigorating the spleen and regulating the stomach Folium Ginkgo tea, comprises the following steps:
S1: pulverize after Poria, Bulbus Lilii, Radix Glycyrrhizae Preparata, Pericarpium Citri Reticulatae, the Rhizoma Atractylodis Macrocephalae, Fructus Mori and Radix Puerariae are respectively dried, cross 40-60 mesh sieve, put in ultrasonic extraction equipment, extract after adding 1500-9000 part abundant moistening of water water, the condition extracted is: ultrasonic power is 120-180W, Extracting temperature is 40-70 DEG C, and extraction time is 30-60min；
S2: step S1 is extracted medical filtration, is sequentially added into ginkgetin, tea polyphenols, stevioside, vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent after puckery, it is stirring 1-3min under 200-500r/min at rotating speed, be uniformly mixed liquid, and concentrating the filtrate to relative density when temperature is 64-66 DEG C is the clear paste of 1.32-1.38；
S3: the clear paste of step S2 spray drying at temperature 200-220 DEG C, to water content≤6%, is crossed the sieve of 200-400 order after pulverizing, prepares powder；
S4: the powder of step S3 and malt extract are stuck with paste, 50-100 part water adopts comminutor to make granule after being sufficiently mixed; finally prepared described granule is 134-136 DEG C in temperature; pressure is 210-230KPa, and the time is sterilizing under 20-40s, obtains invigorating the spleen and regulating the stomach Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) undertaken pulverizing and cross 40-80 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) adopting the water of 38-62 DEG C to carry out lixiviate the Ginkgo Leaf that step 1 prepares, in lixiviate, solid-to-liquid ratio is 1:12-14 (W/V), and extraction time is 2.5-3.5h, extracts 2-3 time, filtration, merging filtrate after extraction, prepares mixing lixiviating solution；
(3) the mixing lixiviating solution concentrate drying that step 2 is prepared, prepare lixiviate cream, the water of be used in lixiviate 5.5-6 times of volume of cream 45-55 DEG C dissolves, anhydrous ethyl acetate solvent is adopted to carry out extracting 2-3 time, continuation anhydrous ethyl acetate carries out repeatedly crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.2-5.4 (W/V), prepares crystal crude product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extracting, the condition of extraction: extraction kettle pressure is 12-18MPa, and extraction temperature is 42-45 DEG C, extraction time is 32-40min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 40-80 mesh sieve after group's sieve tea pulverizing, mix for 1:16-20 in mass ratio with the ethanol water that mass fraction is 40%-60%, extract 2-3 time at temperature is 36-40 DEG C, each 20-30min, filters, merging filtrate, concentration, prepares tea polyphenols crude extract；
B the tea polyphenols crude extract that step a prepares is joined in KCl solution by (), pH regulator is to 6.8-7.2, it is removing impurity under 4000-4500r/min at centrifugal rotational speed, adopts 0.45 μm of filter membrane at temperature is 34-36 DEG C, the solution after being centrifuged to be filtered, prepare filtrate；
(c) by step b prepare filtrate ether extraction, freezing, after drying prepare tea polyphenols；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) being dipped in water after being pulverized by Stevia leaves and soak 1-1.2.h, solid-to-liquid ratio is 1:20-25 (W/V), is 100-120W at ultrasonic power, and Extracting temperature is 40-60 DEG C, and extraction time is extract under 20-30min, prepares Folium Stevlae Rebaudianae medicinal liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 120-180 order, prepares Folium Stevlae Rebaudianae filtrate；
(C) NaAl (SO of filtrate percentage by weight 0.8%-1% is added to the step B Folium Stevlae Rebaudianae filtrate prepared4)2Ca (OH) with filtrate percentage by weight 1%-1.4%2, tune pH value is 6.8-7.2, at temperature 44-48 DEG C, stands 3.2-3.5h, prepares the solution after the removal of impurity；
(D) by the solution frit after the step C removal of impurity prepared and in being concentrated into every milliliter containing stevioside 10%-25%, macroporous adsorbent resin ADS-8 separating-purifying is adopted to prepare the liquid of stevioside, condition is: resolving agent is the alcoholic solution of 55%-65%, its consumption is 1-3 times of macroporous adsorbent resin volume, water wash zone is deionized water, absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 2%-4%, adsorption zone flow velocity 6-10BV/h, desorption zone flow velocity 15-20BV/h, water wash zone flow velocity 20-25BV/h, renewing zone flow velocity 6-8BV/h, switching time is 700-750s, temperature is 40-50 DEG C, pressure is 0.4-0.9MPa；
(E) stevioside's liquid that step D prepares is concentrated, at temperature is 200-220 DEG C, carries out spray drying, prepare stevioside.
Below by more specifically embodiment, the present invention will be described.
Embodiment 1
A kind of invigorating the spleen and regulating the stomach Folium Ginkgo tea, in units of weight portion, including following raw material: 350 parts of Poria, Bulbus Lilii 350 parts, Radix Glycyrrhizae Preparata 350 parts, Pericarpium Citri Reticulatae 150 parts, the Rhizoma Atractylodis Macrocephalae 150 parts, Fructus Mori 80 parts, Radix Puerariae 80 parts, malt extract paste 50 parts, ginkgetin 2 parts, tea polyphenols 2 parts, stevioside 2 parts, vitamin 2 parts, thickening agent 1.5 parts, cosolvent 1.5 parts, dispersant 1.5 parts, 1.5 parts of antioxidant, tasty agents 1 part, flavouring agent 1 part；
Described vitamin is vitamin A, vitamin C, vitamin D, vitamin E；
Described thickening agent is xanthan gum, guar gum, locust bean gum, locust bean gum；
Described cosolvent is polyvinylpyrrolidone；
Described dispersant consists of the following composition: potassium carboxymethylcellulose, agar, modified starch；
Described antioxidant is the different VC potassium of food grade antioxidant, food grade antioxidant BHA, food grade antioxidant MSK-NE150；
Described tasty agents is inosinic acid potassium, guanyl potassium；
Described flavouring agent is methyl cyclopentenyl ketone；
The preparation method of described invigorating the spleen and regulating the stomach Folium Ginkgo tea, comprises the following steps:
S1: by Poria；Bulbus Lilii, Radix Glycyrrhizae Preparata, Pericarpium Citri Reticulatae, the Rhizoma Atractylodis Macrocephalae, Fructus Mori, Radix Puerariae, be respectively dried after pulverize, cross 60 mesh sieves, put in ultrasonic extraction equipment, extract after adding 6000 parts of abundant moistenings of water, the condition extracted is: ultrasonic power is 150W, and Extracting temperature is 100 DEG C, and extraction time is 50min；
S2: step S1 is extracted medical filtration, adds ginkgetin, tea polyphenols, stevioside, vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent after puckery, it is stirring 2min under 300r/min at rotating speed, be uniformly mixed liquid, and concentrating the filtrate to relative density when temperature is 65 DEG C is the clear paste of 1.35；
S3: be 5% to water content by the clear paste of step S2 spray drying at temperature 210 DEG C, crosses the sieve of 300 orders, prepares powder after pulverizing；
S4: the powder of step S3 and malt extract stuck with paste, 80 parts of water mixs and make granule, is finally 135 DEG C prepared described granule in temperature, and pressure is 220KPa, and the time is sterilizing under 30s, prepared invigorating the spleen and regulating the stomach Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) undertaken pulverizing and cross 60 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) adopting the water of 50 DEG C to carry out lixiviate the Ginkgo Leaf that step 1 prepares, in lixiviate, solid-to-liquid ratio is 1:13 (W/V), and extraction time is 3h, extracts 2 times, filtration, merging filtrate after extraction, prepares mixing lixiviating solution；
(3) the mixing lixiviating solution concentrate drying that step 2 is prepared, prepare lixiviate cream, the water of be used in 5.8 times of volumes of lixiviate cream 50 DEG C dissolves, anhydrous ethyl acetate solvent is adopted to carry out extracting 2 times, continuation anhydrous ethyl acetate carries out repeatedly crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.3 (W/V), prepares crystal crude product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extracting, the condition of extraction: extraction kettle pressure is 15MPa, extraction temperature is 43 DEG C, and extraction time is 36min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 60 mesh sieves after group's sieve tea pulverizing, mix for 1:18 in mass ratio with the ethanol water that mass fraction is 50%, be extract 2 times at 38 DEG C in temperature, and each 25min filters, merging filtrate, concentration, prepared tea polyphenols crude extract；
B the tea polyphenols crude extract that step a prepares is joined in KCl solution by (), pH regulator, to 7, is removing impurity under 4200r/min at centrifugal rotational speed, and adopting 0.45 μm of filter membrane is at 35 DEG C, the solution after being centrifuged is filtered in temperature, prepares filtrate；
(c) by step b prepare filtrate ether extraction, freezing, after drying prepare tea polyphenols；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) being dipped in water after being pulverized by Stevia leaves and soak 1.1h, solid-to-liquid ratio is 1:22 (W/V), is 110W at ultrasonic power, and Extracting temperature is 50 DEG C, and extraction time is extract under 25min, prepares Folium Stevlae Rebaudianae medicinal liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 150 orders, prepares Folium Stevlae Rebaudianae filtrate；
(C) NaAl (SO of filtrate percentage by weight 0.9% is added to the step B Folium Stevlae Rebaudianae filtrate prepared4)2Ca (OH) with filtrate percentage by weight 1.2%2, adjusting pH value is 7, at temperature 46 DEG C, stands 3.3h, prepares the solution after the removal of impurity；
(D) by the solution frit after the step C removal of impurity prepared and in being concentrated into every milliliter containing stevioside 32%, macroporous adsorbent resin ADS-8 separating-purifying is adopted to prepare the liquid of stevioside, condition is: resolving agent is the alcoholic solution of 60%, its consumption is 2 times of macroporous adsorbent resin volume, water wash zone is deionized water, absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 3%, adsorption zone flow velocity 8BV/h, desorption zone flow velocity 18BV/h, water wash zone flow velocity 22BV/h, renewing zone flow velocity 7BV/h, switching time is 720s, temperature is 45 DEG C, pressure is 0.7MPa；
(E) stevioside's liquid that step D prepares is concentrated, be at 210 DEG C, carry out spray drying in temperature, prepare stevioside.
Embodiment 2
A kind of invigorating the spleen and regulating the stomach Folium Ginkgo tea, in units of weight portion, including following raw material: 100 parts of Poria, Bulbus Lilii 100 parts, Radix Glycyrrhizae Preparata 100 parts, Pericarpium Citri Reticulatae 60 parts, the Rhizoma Atractylodis Macrocephalae 60 parts, Fructus Mori 40 parts, Radix Puerariae 40 parts, malt extract paste 30 parts, ginkgetin 1 part, tea polyphenols 1 part, stevioside 1 part, vitamin 1 part, thickening agent 0.8 part, cosolvent 0.8 part, dispersant 0.8 part, 0.8 part of antioxidant, tasty agents 0.5 part, flavouring agent 0.5 part；
Described vitamin is vitamin；
Described thickening agent is xanthan gum；
Described cosolvent is polyvinylpyrrolidone；
Described dispersant consists of the following composition: modified starch, polyacrylic acid potassium and potassium alginate；
Described antioxidant is food grade antioxidant 9701；
Described tasty agents is inosinic acid potassium；
Described flavouring agent is methyl cyclopentenyl ketone；
The preparation method of described invigorating the spleen and regulating the stomach Folium Ginkgo tea, comprises the following steps:
S1: by Poria；Bulbus Lilii, Radix Glycyrrhizae Preparata, Pericarpium Citri Reticulatae, the Rhizoma Atractylodis Macrocephalae, Fructus Mori, Radix Puerariae, be respectively dried after pulverize, cross 40 mesh sieves, put in ultrasonic extraction equipment, extract after adding 1500 parts of abundant moistenings of water, the condition extracted is: ultrasonic power is 120W, and Extracting temperature is 40 DEG C, and extraction time is 60min；
S2: step S1 is extracted medical filtration, adds ginkgetin, tea polyphenols, stevioside, vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent after puckery, it is stirring 3min under 200r/min at rotating speed, be uniformly mixed liquid, and concentrating the filtrate to relative density when temperature is 64 DEG C is the clear paste of 1.32；
S3: be 6% to water content by the clear paste of step S2 spray drying at 200 DEG C, crosses the sieve of 200 orders, prepares powder after pulverizing；
S4: the powder of step S3 and malt extract stuck with paste, 50 parts of water mixs and make granule, is finally 134 DEG C prepared described granule in temperature, and pressure is 210KPa, and the time is sterilizing under 40s, prepared invigorating the spleen and regulating the stomach Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) undertaken pulverizing and cross 40 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) adopting the water of 38 DEG C to carry out lixiviate the Ginkgo Leaf that step 1 prepares, in lixiviate, solid-to-liquid ratio is 1:12 (W/V), and extraction time is 3.5h, extracts 2 times, filtration, merging filtrate after extraction, prepares mixing lixiviating solution；
(3) the mixing lixiviating solution concentrate drying that step 2 is prepared, prepare lixiviate cream, the water of be used in 5.5 times of volumes of lixiviate cream 45 DEG C dissolves, anhydrous ethyl acetate solvent is adopted to carry out extracting 2 times, continuation anhydrous ethyl acetate carries out repeatedly crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.2 (W/V), prepares crystal crude product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extracting, the condition of extraction: extraction kettle pressure is 12MPa, extraction temperature is 42 DEG C, and extraction time is 40min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 40 mesh sieves after group's sieve tea pulverizing, mix for 1:16 in mass ratio with the ethanol water that mass fraction is 40%, be extract 2 times at 36 DEG C in temperature, and each 30min filters, merging filtrate, concentration, prepared tea polyphenols crude extract；
B the tea polyphenols crude extract that step a prepares is joined in KCl solution by (), pH regulator, to 6.8, is removing impurity under 4000-/min at centrifugal rotational speed, and adopting 0.45 μm of filter membrane is at 34 DEG C, the solution after being centrifuged is filtered in temperature, prepares filtrate；
(c) by step b prepare filtrate ether extraction, freezing, after drying prepare tea polyphenols；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) being dipped in water after being pulverized by Stevia leaves and soak 1h, solid-to-liquid ratio is 1:20 (W/V), is 100W at ultrasonic power, and Extracting temperature is 40 DEG C, and extraction time is extract under 30min, prepares Folium Stevlae Rebaudianae medicinal liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 120 orders, prepares Folium Stevlae Rebaudianae filtrate；
(C) NaAl (SO of filtrate percentage by weight 0.8% is added to the step B Folium Stevlae Rebaudianae filtrate prepared4)2Ca (OH) with filtrate percentage by weight 1%2, adjusting pH value is 6.8, at temperature 44 DEG C, stands 3.2-3.5h, prepares the solution after the removal of impurity；
(D) by the solution frit after the step C removal of impurity prepared and in being concentrated into every milliliter containing stevioside 10%, macroporous adsorbent resin ADS-8 separating-purifying is adopted to prepare the liquid of stevioside, condition is: resolving agent is the alcoholic solution of 55%, its consumption is 1 times of macroporous adsorbent resin volume, water wash zone is deionized water, absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 2%, adsorption zone flow velocity 6BV/h, desorption zone flow velocity 15BV/h, water wash zone flow velocity 20BV/h, renewing zone flow velocity 6BV/h, switching time is 700s, temperature is 40 DEG C, pressure is 0.4MPa；
(E) stevioside's liquid that step D prepares is concentrated, be at 200 DEG C, carry out spray drying in temperature, prepare stevioside.
Embodiment 3
A kind of invigorating the spleen and regulating the stomach Folium Ginkgo tea, in units of weight portion, including following raw material: 600 parts of Poria, Bulbus Lilii 600 parts, Radix Glycyrrhizae Preparata 600 parts, Pericarpium Citri Reticulatae 240 parts, the Rhizoma Atractylodis Macrocephalae 240 parts, Fructus Mori 120 parts, Radix Puerariae 120 parts, malt extract paste 60 parts, ginkgetin 3 parts, tea polyphenols 3 parts, stevioside 3 parts, vitamin 3 parts, thickening agent 2 parts, cosolvent 2 parts, dispersant 2 parts, 2 parts of antioxidant, tasty agents 1.5 parts, fragrance 1.5 parts；
Described vitamin is vitamin C；
Described thickening agent is guar gum；
Described cosolvent is polyvinylpyrrolidone；
Described dispersant consists of the following composition: potassium carboxymethylcellulose, modified starch, potassium alginate；
Described antioxidant is food grade antioxidant BHT；
Described tasty agents is inosinic acid potassium；
Described flavouring agent is methyl cyclopentenyl ketone；
The preparation method of described invigorating the spleen and regulating the stomach Folium Ginkgo tea, comprises the following steps:
S1: by Poria；Bulbus Lilii, Radix Glycyrrhizae Preparata, Pericarpium Citri Reticulatae, the Rhizoma Atractylodis Macrocephalae, Fructus Mori, Radix Puerariae are pulverized after being respectively dried, and cross 60 mesh sieves, put in ultrasonic extraction equipment, extract after adding 9000 parts of abundant moistenings of water, the condition extracted is: ultrasonic power is 180W, and Extracting temperature is 70 DEG C, and extraction time is 30min；
S2: step S1 is extracted medical filtration, adds ginkgetin, tea polyphenols, stevioside, vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent after puckery, it is stirring 1min under 500r/min at rotating speed, be uniformly mixed liquid, and concentrating the filtrate to relative density when temperature is 66 DEG C is the clear paste of 1.38；
S3: be 4% to water content by the clear paste of step S2 spray drying at 220 DEG C, crosses the sieve of 400 orders, prepares powder after pulverizing；
S4: the powder of step S3 and malt extract stuck with paste, 100 parts of water mixs and make granule, is finally 136 DEG C prepared described granule in temperature, and pressure is 230KPa, and the time is sterilizing under 40s, prepared invigorating the spleen and regulating the stomach Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) undertaken pulverizing and cross 80 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) adopting the water of 62 DEG C to carry out lixiviate the Ginkgo Leaf that step 1 prepares, in lixiviate, solid-to-liquid ratio is 1:14 (W/V), and extraction time is 2.5h, extracts 3 times, filtration, merging filtrate after extraction, prepares mixing lixiviating solution；
(3) the mixing lixiviating solution concentrate drying that step 2 is prepared, prepare lixiviate cream, the water of be used in 6 times of volumes of lixiviate cream 55 DEG C dissolves, anhydrous ethyl acetate solvent is adopted to carry out extracting 3 times, continuation anhydrous ethyl acetate carries out repeatedly crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.4 (W/V), prepares crystal crude product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extracting, the condition of extraction: extraction kettle pressure is 18MPa, extraction temperature is 45 DEG C, and extraction time is 32min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 80 mesh sieves after group's sieve tea pulverizing, mix for 1:20 in mass ratio with the ethanol water that mass fraction is 60%, be extract 3 times at 40 DEG C in temperature, and each 20min filters, merging filtrate, concentration, prepared tea polyphenols crude extract；
B the tea polyphenols crude extract that step a prepares is joined in KCl solution by (), pH regulator, to 7.2, is removing impurity under 4500r/min at centrifugal rotational speed, and adopting 0.45 μm of filter membrane is at 36 DEG C, the solution after being centrifuged is filtered in temperature, prepares filtrate；
(c) by step b prepare filtrate ether extraction, freezing, after drying prepare tea polyphenols；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) being dipped in water after being pulverized by Stevia leaves and soak 1.2h, solid-to-liquid ratio is 1:25 (W/V), is 120W at ultrasonic power, and Extracting temperature is 60 DEG C, and extraction time is extract under 20min, prepares Folium Stevlae Rebaudianae medicinal liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 180 orders, prepares Folium Stevlae Rebaudianae filtrate；
(C) NaAl (SO of filtrate percentage by weight 1% is added to the step B Folium Stevlae Rebaudianae filtrate prepared4)2Ca (OH) with filtrate percentage by weight 1.4%2, adjusting pH value is 7.2, at temperature 48 DEG C, stands 3.2-3.5h, prepares the solution after the removal of impurity；
(D) by the solution frit after the step C removal of impurity prepared and in being concentrated into every milliliter containing stevioside 25%, macroporous adsorbent resin ADS-8 separating-purifying is adopted to prepare the liquid of stevioside, condition is: resolving agent is the alcoholic solution of 65%, its consumption is 3 times of macroporous adsorbent resin volume, water wash zone is deionized water, absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 4%, adsorption zone flow velocity 10BV/h, desorption zone flow velocity 20BV/h, water wash zone flow velocity 25BV/h, renewing zone flow velocity 8BV/h, switching time is 750s, temperature is 50 DEG C, pressure is 0.9MPa；
(E) stevioside's liquid that step D prepares is concentrated, be at 220 DEG C, carry out spray drying in temperature, prepare stevioside.
Above content is it cannot be assumed that specific embodiment of the invention is confined to these explanations; for general technical staff of the technical field of the invention; without departing from the inventive concept of the premise; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by submitted claims.
Claims (8)
1. invigorating the spleen and regulating the stomach Folium Ginkgo tea, it is characterized in that, in units of weight portion, including following raw material: Poria 100-600 part, Bulbus Lilii 100-600 part, Radix Glycyrrhizae Preparata 100-600 part, Pericarpium Citri Reticulatae 60-240 part, Rhizoma Atractylodis Macrocephalae 60-240 part, Fructus Mori 40-120 part, Radix Puerariae 40-120 part, malt extract stick with paste 30-60 part, ginkgetin 1-3 part, tea polyphenols 1-3 part, stevioside's 1-3 part, vitamin 1-3 part, thickening agent 0.8-2 part, cosolvent 0.8-2 part, dispersant 0.8-2 part, antioxidant 0.8-2 part, tasty agents 0.5-1.5 part, flavouring agent 0.5-1.5 part；
The preparation method of described invigorating the spleen and regulating the stomach Folium Ginkgo tea, comprises the following steps:
S1: pulverize after Poria, Bulbus Lilii, Radix Glycyrrhizae Preparata, Pericarpium Citri Reticulatae, the Rhizoma Atractylodis Macrocephalae, Fructus Mori, Radix Puerariae are respectively dried, cross 40-60 mesh sieve, put in ultrasonic extraction equipment, carry out after adding the 1500-9000 abundant moistening of part water extracting medicinal liquid, the condition extracted is: ultrasonic power is 120-180W, Extracting temperature is 40-70 DEG C, and extraction time is 30-60min；
S2: step S1 is extracted medical filtration, is sequentially added into ginkgetin, tea polyphenols, stevioside, vitamin, thickening agent, cosolvent, dispersant, antioxidant, tasty agents, flavouring agent after puckery, it is stirring 1-3min under 200-500r/min at rotating speed, be uniformly mixed liquid, and concentrating the filtrate to relative density when temperature is 64-66 DEG C is the clear paste of 1.32-1.38；
S3: the clear paste of step S2 spray drying at temperature 200-220 DEG C, to water content≤6%, is crossed the sieve of 200-400 order after pulverizing, prepares powder；
S4: the powder of step S3 and malt extract are stuck with paste, 50-100 part water adopts comminutor to make granule after being sufficiently mixed; finally prepared described granule is 134-136 DEG C in temperature; pressure is 210-230KPa, and the time is sterilizing under 20-40s, obtains invigorating the spleen and regulating the stomach Folium Ginkgo tea；
The preparation method of ginkgetin described in step S2 comprises the following steps:
(1) undertaken pulverizing and cross 40-80 mesh sieve by dry Folium Ginkgo, prepare Ginkgo Leaf；
(2) adopting the water of 38-62 DEG C to carry out lixiviate the Ginkgo Leaf that step 1 prepares, in lixiviate, solid-to-liquid ratio is 1:12-14 (W/V), and extraction time is 2.5-3.5h, extracts 2-3 time, filtration, merging filtrate after extraction, prepares mixing lixiviating solution；
(3) the mixing lixiviating solution concentrate drying that step 2 is prepared, prepare lixiviate cream, the water of be used in lixiviate 5.5-6 times of volume of cream 45-55 DEG C dissolves, anhydrous ethyl acetate solvent is adopted to carry out extracting 2-3 time, continuation anhydrous ethyl acetate carries out repeatedly crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.2-5.4 (W/V), prepares crystal crude product；
(4) crystal crude product step 3 prepared is through supercritical CO2Extracting, the condition of extraction: extraction kettle pressure is 12-18MPa, and extraction temperature is 42-45 DEG C, extraction time is 32-40min, prepares ginkgetin；
The preparation method of tea polyphenols described in step S2 comprises the following steps:
A () will cross 40-80 mesh sieve after group's sieve tea pulverizing, mix for 1:16-20 in mass ratio with the ethanol water that mass fraction is 40%-60%, extract 2-3 time at temperature is 36-40 DEG C, each 20-30min, filters, merging filtrate, concentration, prepares tea polyphenols crude extract；
B the tea polyphenols crude extract that step a prepares is joined in KCl solution by (), pH regulator is to 6.8-7.2, it is removing impurity under 4000-4500r/min at centrifugal rotational speed, adopts 0.45 μm of filter membrane at temperature is 34-36 DEG C, the solution after being centrifuged to be filtered, prepare filtrate；
(c) by step b prepare filtrate ether extraction, freezing, after drying prepare tea polyphenols；
The preparation method of stevioside described in step S2 comprises the following steps:
(A) being dipped in water after being pulverized by Stevia leaves and soak 1-1.2.h, solid-to-liquid ratio is 1:20-25 (W/V), is 100-120W at ultrasonic power, and Extracting temperature is 40-60 DEG C, and extraction time is extract under 20-30min, prepares Folium Stevlae Rebaudianae medicinal liquid；
(B) the Folium Stevlae Rebaudianae medicinal liquid that step A prepares is crossed the filter cloth of 120-180 order, prepares Folium Stevlae Rebaudianae filtrate；
(C) NaAl (SO of filtrate percentage by weight 0.8%-1% is added to the step B Folium Stevlae Rebaudianae filtrate prepared4)2Ca (OH) with filtrate percentage by weight 1%-1.4%2, tune pH value is 6.8-7.2, at temperature 44-48 DEG C, stands 3.2-3.5h, prepares the solution after the removal of impurity；
(D) by the solution frit after the step C removal of impurity prepared and in being concentrated into every milliliter containing stevioside 10%-25%, macroporous adsorbent resin ADS-8 separating-purifying is adopted to prepare the liquid of stevioside, condition is: resolving agent is the alcoholic solution of 55%-65%, its consumption is 1-3 times of macroporous adsorbent resin volume, water wash zone is deionized water, absorption with macroporous adsorbent resin regenerated solvent is the KOH solution of 2%-4%, adsorption zone flow velocity 6-10BV/h, desorption zone flow velocity 15-20BV/h, water wash zone flow velocity 20-25BV/h, renewing zone flow velocity 6-8BV/h, switching time is 700-750s, temperature is 40-50 DEG C, pressure is 0.4-0.9MPa；
(E) stevioside's liquid that step D prepares is concentrated, at temperature is 200-220 DEG C, carries out spray drying, prepare stevioside.
2. invigorating the spleen and regulating the stomach Folium Ginkgo tea according to claim 1, it is characterised in that described vitamin includes one or more in vitamin A, vitamin C, vitamin D and vitamin E.
3. invigorating the spleen and regulating the stomach Folium Ginkgo tea according to claim 1, it is characterised in that described thickening agent includes one or more in xanthan gum, guar gum, locust bean gum and locust bean gum.
4. invigorating the spleen and regulating the stomach Folium Ginkgo tea according to claim 1, it is characterised in that described cosolvent is polyvinylpyrrolidone.
5. invigorating the spleen and regulating the stomach Folium Ginkgo tea according to claim 1, it is characterised in that described dispersant includes following component: one or more in potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium and potassium alginate.
6. invigorating the spleen and regulating the stomach Folium Ginkgo tea according to claim 1, it is characterized in that, described antioxidant includes one or more in food grade antioxidant 9701, food grade antioxidant BHT, the different VC potassium of food grade antioxidant, food grade antioxidant BHA and food grade antioxidant MSK-NE150.
7. invigorating the spleen and regulating the stomach Folium Ginkgo tea according to claim 1, it is characterised in that described tasty agents includes one or more in inosinic acid potassium and guanyl potassium.
8. invigorating the spleen and regulating the stomach Folium Ginkgo tea according to claim 1, it is characterised in that described flavouring agent is methyl cyclopentenyl ketone.
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101717418A (en) * | 2009-12-10 | 2010-06-02 | 黑龙江省农产品加工工程技术研究中心 | Technology for separating stevioside in one step with simulated moving bed |
| CN103907723A (en) * | 2013-12-21 | 2014-07-09 | 胡安然 | Tea capable of nursing constitution of qi deficiency |
| CN104106698A (en) * | 2013-04-18 | 2014-10-22 | 李振祥 | Qi-boosting and stomach-warming tea |
| CN104387356A (en) * | 2013-11-15 | 2015-03-04 | 广西莱吉生物工程有限公司 | Method for extracting flavone from folium ginkgo |
| CN104920728A (en) * | 2015-06-26 | 2015-09-23 | 王魁兴 | Jianpi Hewei tea drink |
| CN105028804A (en) * | 2015-06-17 | 2015-11-11 | 安徽黄山云乐灵芝有限公司 | Ganoderma lucidum tea |
-
2016
- 2016-05-12 CN CN201610317131.1A patent/CN105767397A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101717418A (en) * | 2009-12-10 | 2010-06-02 | 黑龙江省农产品加工工程技术研究中心 | Technology for separating stevioside in one step with simulated moving bed |
| CN104106698A (en) * | 2013-04-18 | 2014-10-22 | 李振祥 | Qi-boosting and stomach-warming tea |
| CN104387356A (en) * | 2013-11-15 | 2015-03-04 | 广西莱吉生物工程有限公司 | Method for extracting flavone from folium ginkgo |
| CN103907723A (en) * | 2013-12-21 | 2014-07-09 | 胡安然 | Tea capable of nursing constitution of qi deficiency |
| CN105028804A (en) * | 2015-06-17 | 2015-11-11 | 安徽黄山云乐灵芝有限公司 | Ganoderma lucidum tea |
| CN104920728A (en) * | 2015-06-26 | 2015-09-23 | 王魁兴 | Jianpi Hewei tea drink |
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| US11612172B2 (en) * | 2018-10-25 | 2023-03-28 | Amorepacific Corporation | Processed products of tea with quick dispersibility in water and method for manufacturing processed products of tea |
| US11653665B2 (en) | 2019-08-21 | 2023-05-23 | Amorepacific Corporation | Processed products of tea and method for manufacturing the same |
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