CN106367287A - Novel beautiful millettia root health-care beverage - Google Patents
Novel beautiful millettia root health-care beverage Download PDFInfo
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- CN106367287A CN106367287A CN201610902736.7A CN201610902736A CN106367287A CN 106367287 A CN106367287 A CN 106367287A CN 201610902736 A CN201610902736 A CN 201610902736A CN 106367287 A CN106367287 A CN 106367287A
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
- C12J1/00—Vinegar; Preparation or purification thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/185—Acids; Anhydrides, halides or salts thereof, e.g. sulfur acids, imidic, hydrazonic or hydroximic acids
- A61K31/19—Carboxylic acids, e.g. valproic acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/06—Fungi, e.g. yeasts
- A61K36/07—Basidiomycota, e.g. Cryptococcus
- A61K36/076—Poria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/16—Ginkgophyta, e.g. Ginkgoaceae (Ginkgo family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/25—Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
- A61K36/258—Panax (ginseng)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/486—Millettia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/65—Paeoniaceae (Peony family), e.g. Chinese peony
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/82—Theaceae (Tea family), e.g. camellia
Abstract
The invention discloses a novel beautiful millettia root health-care beverage. The novel beautiful millettia root health-care beverage is prepared from beautiful millettia root, black tea, cortex moutan, radix notoginseng, eupatorium, cimicifugae foetidae, wolfiporia extensa, snow pear vinegar, ginkgetin, polypropylene pyrrolidone, potassium hydroxypropyl methyl cellulose, agar, DuPont EEA2112AC compatibilizer, food grade antioxidant 264, carrageenan, epoxidized soybean oil fatty acid, tartrazine, nisin, molybdenum element, manganese element, cobalt element, alanine, isoleucine, serine, tyrosine, vitamin E, vitamin B1, vitamin C, aspartame, starch sugar, dihydroisojasmone, ethyl vanillin, methyl-furfuryl fumarate, 51-disodium guanylate and potassium guanylate. The novel beautiful millettia root health-care beverage has rich nutrition, sweet and sour taste and rich tea aroma, is a novel beverage, has the effect of removing ozostomia after drinking, and has a significant role in curing or relieving ozostomia symptoms.
Description
Technical field
The invention belongs to technical field of beverage processing is and in particular to a kind of new Millettia Speciosa health functional beverage.
Background technology
Millettia Speciosa is the drying of pulse family Millettia plant beautiful millettia millettia speciosa champ.
Root, is commonly called as Tianniudali.Taste is micro- sweet, and main component contains alkaloid, coumarin and saccharide.Hainan Quan Dao is distributed.Guangxi, wide
The provinces and regions such as east, Fujian are also distributed.Initially " the SHENGCAO property of medicine standby will " be recorded: " strengthening bone and muscle, relieving heat toxin are managed internal injury, controlled traumatic injury, leaching
Wine nourishing kidney.", Guangzhou army " conventional Chinese herbal medicine handbook ": " relaxing muscles and tendons and activating QI and blood in the collateral, qi-restoratives lung moistening.Control lumbago and skelalgia, rheumatic arthralgia, Chronic Liver
Scorching, pulmonary tuberculosis.", " Guangxi book on Chinese herbal medicine a collection of selected materials ": " QI invigorating lung moistening.Control body void after being ill, cough due to deficiency of the lung, rheumatic arthralgia, lumbago and skelalgia.”、
" national Chinese herbal medicine compilation ": " control chronic bronchitiss, pass out semen, leucorrhea ", " Guangxi ethnic drug short course ": " control cough, nephritis, wind
Wet, anemia.", " Fujian medicine will ": " expelling wind and removing dampness controls pleuritis." Millettia Speciosa is used as medicine with rhizome, whole year can adopt, and clean and cut
Piece, dry or cook dry standby.Mel is perfect natural health agent and enamel, and this viewpoint is by long history institute
Confirm.Compendium of Material Medica is recorded: the work(that Mel is used as medicine has five, heat clearing away, invigorating middle warmer, removing toxic substances, profit bath, pain relieving.
Modern study shows, Millettia Speciosa root such as pterocarpan containing alkaloid: (-)-3-hydroxy-9-methoxypterocarpan (medicarpin) and saponin
Class: millettiasaponin a, b (uchiyama t, et al.heterocycles, 2003,60: 655).Root decoct or
Ethanol extraction gavages, to due to ammonia spraying draw the mice coughing have obvious antitussive action (Xu Honghua writes. Chinese herbal medicine
Coloured picture handbook (one). Guangzhou: Guangdong Science Press, 2003: 22).Millettia Speciosa polysaccharide is that Millettia Speciosa adjusts immune work(
One of main active of energy.Have dual regulation (Zheng Yuansheng, etc. Guangdong to mice t lymphopoiesis
Pharmaceutical college's journal, 2008,24: 58).The raw material that the 70's began to build kidney ball, building-up body capsule etc. as strong waist is used for middle one-tenth
The production of medicine, extensively applies in Guangdong and Guangxi Provinces area.Additionally, domestic conventional Millettia Speciosa among the people is as stewed stocks.
Functional drinkss, are the favorites of beverage market in recent years." red cattle " before more than ten years outshines others, to 2002-
" pulsation " in 2003, and beverage production enterprise afterwards is nearly all in production functional drinkss.Current commercial type
Functional beverage such as fire-toxin releasing herb tea " Wang Laoji " etc..But both at home and abroad there is not yet Millettia Speciosa health care work(about having implication effect of dispelling
The document of energy beverage aspect or patent report.
Abundant with growth in the living standard and material, people's dietetic level has very big improvement, people eat more
It is better to come, also more and more greasy, and a lot of people have different degrees of overnutrition and obesity；So not only very unsightly,
And be possible to grow a series of diseases, impact people's is healthy, thus now increasing people start except
Carry out positive sports, participate in outside exercising with oxygen, also focus on diet, take in some and can go oil removal, improve internal ring
Border, the Foods or drinkses of nutrient health, due to above reason, beverage industry development is maked rapid progress, wide in variety colorful, especially
The beverage with health care more becomes new lover, and tea vinegar drink is also just arisen at the historic moment.
Tea vinegar not only sour-sweet delicious food, tea perfume is strong, special mouthfeel, suits the taste of both old and young, and nutritious, containing multiple to people
The beneficial composition of body, such as catechin can eliminate the free radical in human body, are a kind of protective agents of natural pigment, can suppress cholesterol
Increase, vessel softening；Tea polyphenols have the effect of defying age, antioxidation, antibacterial and diseases prevention；Tea vinegar has Fructus Alpiniae Oxyphyllae of refreshing oneself, promotes the production of body fluid
Quench the thirst, diuresis removing toxic substances, the effect of allaying tiredness.
But tea vinegar drink kind is actually rare in the market, and exist production the tea vinegar drink cycle long, produce
The problems such as product storage time is short.As patent of invention " chrysanthemum tea vinegar beverage (patent No.: zl201210267461.6) " discloses one
Plant chrysanthemum tea vinegar beverage and preparation method thereof, the method needs to inoculate acetic acid bacteria fermentation 30-40 days in inoculation fermentation step, leads
Cause long the production cycle；Additionally, adopting vacuum filling, sealing in fill step, vacuum is 0.04-0.05mpa, fill temperature
Degree controls at 60-75 DEG C, and due to fill, the vacuum of sealing and temperature, low to result in product storage time short.And for example invent specially
Sharp " a kind of tea vinegar drink and preparation method thereof (patent No.: zl201210162462.4) " discloses the sugary tea juice liquid of gained
In, sealing and fermenting 22-25 days at 25-28 DEG C, then filtered, after pasteurization, obtained final product tea vinegar drink, this producer
Method there is also the problem of long the production cycle.Therefore, how to solve long the production cycle, the problems such as product storage time is short, become
The direction studied from now on.
For many years, China's tea industry is rapidly developed, but still there is Summer-autumn tea tree fresh leaf serious waste of resources etc.
Outstanding problem, in the urgent need to increasing the exploitation of tea resource, and the Development and Production of tea vinegar drink, tea resource not only can be solved
The problem wasting, and have also been enlarged the output value chain of tea resource, therefore, tea vinegar drink DEVELOPMENT PROSPECT is wide.
Content of the invention
The technical problem to be solved in the present invention is to provide a kind of new Millettia Speciosa health functional beverage, to solve prior art
Middle production Millettia Speciosa teabag drink long the production cycle, storage time is short, the problems such as mouthfeel is not good enough.The new Millettia Speciosa health care of the present invention
Drinks are nutritious, and sour-sweet tasty and refreshing, tea perfume is strong, are a kind of new Millettia Speciosa health functional beverages of new Chinese medicine；Drink
With the new Millettia Speciosa health functional beverage of the present invention, there is implication of dispelling, have notable work to treatment or mitigation implication symptom
With.
In order to solve above technical problem, the present invention employs the following technical solutions:
A kind of new Millettia Speciosa health functional beverage, in units of weight portion, including following raw material: Millettia Speciosa 153-209 part, red
Tea 72-98 part, Cortex Moutan 6-9 part, Radix Notoginseng 8-15 part, Herba Eupatorii 6-13 part, Rhizoma Cimicifugae 7-12 part, Poria 5-9 part, pear vinegar 5-9 part, silver
Flavone 2-4 part, polyvinyl pyrilodone 0.7-1.1 part, hydroxypropyl methyl cellulose potassium 0.4-0.7 part, agar 0.5-0.8
Part, Dupont eea2112ac compatilizer 0.7-1.2 part, food grade antioxidant 264 0.6-0.9 part, carrageenan 0.5-1.2
Part, epoxidized soybean oil fatty acid 0.3-0.6 part, lemon yellow pigment 0.3-0.5 part, nisin 0.5-0.8 part, molybdenum element
0.2-0.3 part, manganese element 0.2-0.3 part, cobalt element 0.1-0.2 part, alanine 0.3-0.5 part, isoleucine 0.2-0.4 part,
Serine 0.2-0.3 part, tyrosine 0.2-0.4 part, vitamin e 0.2-0.3 part, vitamin b1 0.2-0.3 part, vitamin c
0.2-0.4 part, aspartyl-phenylalanine methyl ester 0.03-0.05 part, starch sugar 1.5-2.5 part, dihydro jasmone 0.03-0.06
Part, ethyl perfume 0.02-0.04 part, vanillin 0.04-0.06 part, methyl-furfuryl fumarate 0.5-0.9 part, 51- guanosine monophosphate disodium
0.2-0.3 part, guanyl potassium 0.1-0.2 part；
The preparation method of described new Millettia Speciosa health functional beverage, comprises the following steps:
S1: the preparation of Millettia Speciosa juice, comprises the following steps；
S11: the Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 150-200 mesh sieve, prepared Millettia Speciosa minces；
S12: the Millettia Speciosa that step s11 is obtained minces and mixes loading extraction pot with the water ratio for 1:3-7 in mass ratio, in pressure
Power is under 4-6mpa, uses 4-6 layer filtered through gauze, prepared filtrate a after decocting in water 0.3-0.6h；
S13: the filtrate a rotating speed that step s12 is obtained is the centrifuge of 4000-5000r/min, in vacuum is
Sucking filtration roguing under 0.076-0.085mpa, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps:
S21: black tea is dried to water content≤8.5% pulverizing, crosses 100-140 mesh sieve, with the second for 75%-84% for the mass fraction
Alcohol-water solution mixes for 1:12-14 in mass ratio, is 150-180w in microwave power, and temperature extracts 18- at being 44-48 DEG C
30min, filters, and concentrates, prepared tea polyphenols crude extract a；
S22: by step s21 be obtained tea polyphenols crude extract a be added to concentration be 17%-19% kcl solution in, ph adjust to
5.8-6.2, removes impurity, using aperture for 0.01-0.03 μm of filter membrane in temperature under centrifugal rotational speed is for 4000-5000r/min
For filtering to the solution after centrifugation at 32-35 DEG C, prepared filtrate b；
S23: by step s22 be obtained filtrate b with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Rhizoma Cimicifugae, Poria are separately dried the co-grinding to water content≤7.6%, add water, in material
Liquor ratio is 1:14-17(w/v), microwave power is 200-240w, and Extracting temperature is 94-96 DEG C, and extraction time is 1.3-1.7h, connects
Filtering residue, prepared medicinal liquid；
S4: by medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step s1, step s2, step s3, pear vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont eea2112ac compatilizer, food stage
After antioxidant 264, carrageenan, epoxidized soybean oil fatty acid, 1300-1500 part water mix, it is 162-176w in microwave power, temperature
Spend for 64-68 DEG C, speed of agitator is to stir 0.5-0.8h under 200-400r/min, and uniform mixed liquor a is obtained；
The preparation method of described ginkgetin comprises the following steps:
S41: dry Folium Ginkgo is pulverized and is crossed 100-120 mesh sieve, prepared Ginkgo Leaf；
S42: the Ginkgo Leaf that step s41 is obtained is extracted using 45-65 DEG C of water, in extraction, microwave power is 150-
200w, solid-to-liquid ratio is 1:12-15(w/v), extraction time is 0.5-1h, extracts 2-3 time, filtration, merging filtrate after extraction, is obtained
Mixing lixiviating solution；
S43: the mixing lixiviating solution concentrate drying that step s42 is obtained, is obtained extraction cream, is used in extraction 6.5-6.8 times of body of cream
The water of long-pending 48-56 DEG C is dissolved, and carries out extraction 2-3 time using anhydrous ethyl acetate solvent, continues to use anhydrous ethyl acetate
Carry out multiple crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.5-5.8(w/v), prepared crystal crude product；
S44: by the prepared crystal crude product of step s43 through supercritical co2Extraction, the condition of extraction: extraction kettle pressure is 14-
20mpa, extraction temperature is 46-48 DEG C, and extraction time is 25-35min, prepared ginkgetin；
S5: to step s4 be obtained uniform mixed liquor a in add lemon yellow pigment, nisin, molybdenum element, manganese element,
Cobalt element, alanine, isoleucine, serine, tyrosine, vitamin e, vitamin b1, vitamin c, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, starch sugar, dihydro jasmone, ethyl perfume, vanillin, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
It is 148-153w in microwave power, temperature is 52-56 DEG C, speed of agitator is to stir 0.5-0.9h under 300-500r/min, is obtained
Uniformly mixed liquor b；
S6: the uniform mixed liquor that step s5 is obtained is 134-136 DEG C in temperature, pressure is the 2-4s that sterilizes under 210-230kpa,
Uniform mixed liquor c is obtained；
S7: the uniform mixed liquor c that step s6 is obtained is 0.089-0.093mpa in vacuum, temperature is carried out at being 88-92 DEG C
Fill, sealing, are then cooled to room temperature, and new Millettia Speciosa health functional beverage is obtained.
Preferably, microwave power described in step s3 is 240w, and Extracting temperature is 96 DEG C, and extraction time is 1.3h.
Preferably, microwave power described in step s4 is 176w, and temperature is 68 DEG C, and speed of agitator is to stir under 400r/min
0.5h.
Preferably, microwave power described in step s5 is 153w, and temperature is 56 DEG C, and speed of agitator is to stir under 500r/min
0.5h.
Preferably, temperature described in step s6 is 136 DEG C, and pressure is to sterilize 2s under 230kpa preferably, institute in step s6
State temperature and be 136 DEG C, pressure is the 2s that sterilizes under 230kpa.
Preferably, vacuum described in step s6 is 0.093mpa, and temperature carries out fill, sealing at being 92 DEG C.
The method have the advantages that
(1) the new Millettia Speciosa health functional beverage of the present invention is nutritious, and sour-sweet tasty and refreshing, tea perfume is strong, is a kind of new
Chinese medicine new Millettia Speciosa health functional beverage；
(2) the new Millettia Speciosa health functional beverage drinking the present invention has functions that implication of dispelling, to treatment or mitigation implication disease
Shape has remarkable effect；
(3) the new Millettia Speciosa health functional beverage of the present invention is with short production cycle, and shelf life of products is long；
(4) present invention is compared with prior art: fill, sealing, using higher temperature and vacuum, more can extend product storage
Time；
(5) the new Millettia Speciosa health functional beverage constitutive material source of the present invention is easy to get, preparation method uncomplicated it is easy to promote
Application.
Specific embodiment
For ease of more fully understanding the present invention, it is illustrated by following examples, these embodiments belong to the present invention's
Protection domain, but do not limit the scope of the invention.
In an embodiment, described new Millettia Speciosa health functional beverage, in units of weight portion, including following raw material: cattle
153-209 part, black tea 72-98 part, Cortex Moutan 6-9 part, Radix Notoginseng 8-15 part, Herba Eupatorii 6-13 part, Rhizoma Cimicifugae 7-12 part, Poria 5-9 energetically
Part, pear vinegar 5-9 part, ginkgetin 2-4 part, polyvinyl pyrilodone 0.7-1.1 part, hydroxypropyl methyl cellulose potassium 0.4-
0.7 part, agar 0.5-0.8 part, Dupont eea2112ac compatilizer 0.7-1.2 part, food grade antioxidant 264 0.6-0.9
Part, carrageenan 0.5-1.2 part, epoxidized soybean oil fatty acid 0.3-0.6 part, lemon yellow pigment 0.3-0.5 part, nisin
0.5-0.8 part, molybdenum element 0.2-0.3 part, manganese element 0.2-0.3 part, cobalt element 0.1-0.2 part, alanine 0.3-0.5 part, different
Leucine 0.2-0.4 part, serine 0.2-0.3 part, tyrosine 0.2-0.4 part, vitamin e 0.2-0.3 part, vitamin b1
0.2-0.3 part, vitamin c 0.2-0.4 part, aspartyl-phenylalanine methyl ester 0.03-0.05 part, starch sugar 1.5-2.5 part,
Dihydro jasmone 0.03-0.06 part, ethyl perfume 0.02-0.04 part, vanillin 0.04-0.06 part, methyl-furfuryl fumarate 0.5-
0.9 part, 51- guanosine monophosphate disodium 0.2-0.3 part, guanyl potassium 0.1-0.2 part；
The preparation method of described new Millettia Speciosa health functional beverage, comprises the following steps:
S1: the preparation of Millettia Speciosa juice, comprises the following steps；
S11: the Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 150-200 mesh sieve, prepared Millettia Speciosa minces；
S12: the Millettia Speciosa that step s11 is obtained minces and mixes loading extraction pot with the water ratio for 1:3-7 in mass ratio, in pressure
Power is under 4-6mpa, uses 4-6 layer filtered through gauze, prepared filtrate a after decocting in water 0.3-0.6h；
S13: the filtrate a rotating speed that step s12 is obtained is the centrifuge of 4000-5000r/min, in vacuum is
Sucking filtration roguing under 0.076-0.085mpa, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps:
S21: black tea is dried to water content≤8.5% pulverizing, crosses 100-140 mesh sieve, with the second for 75%-84% for the mass fraction
Alcohol-water solution mixes for 1:12-14 in mass ratio, is 150-180w in microwave power, and temperature extracts 18- at being 44-48 DEG C
30min, filters, and concentrates, prepared tea polyphenols crude extract a；
S22: by step s21 be obtained tea polyphenols crude extract a be added to concentration be 17%-19% kcl solution in, ph adjust to
5.8-6.2, removes impurity, using aperture for 0.01-0.03 μm of filter membrane in temperature under centrifugal rotational speed is for 4000-5000r/min
For filtering to the solution after centrifugation at 32-35 DEG C, prepared filtrate b；
S23: by step s22 be obtained filtrate b with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Rhizoma Cimicifugae, Poria are separately dried the co-grinding to water content≤7.6%, add water, in material
Liquor ratio is 1:14-17(w/v), microwave power is 200-240w, and Extracting temperature is 94-96 DEG C, and extraction time is 1.3-1.7h, connects
Filtering residue, prepared medicinal liquid；
S4: by medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step s1, step s2, step s3, pear vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont eea2112ac compatilizer, food stage
After antioxidant 264, carrageenan, epoxidized soybean oil fatty acid, 1300-1500 part water mix, it is 162-176w in microwave power, temperature
Spend for 64-68 DEG C, speed of agitator is to stir 0.5-0.8h under 200-400r/min, and uniform mixed liquor a is obtained；
The preparation method of described ginkgetin comprises the following steps:
S41: dry Folium Ginkgo is pulverized and is crossed 100-120 mesh sieve, prepared Ginkgo Leaf；
S42: the Ginkgo Leaf that step s41 is obtained is extracted using 45-65 DEG C of water, in extraction, microwave power is 150-
200w, solid-to-liquid ratio is 1:12-15(w/v), extraction time is 0.5-1h, extracts 2-3 time, filtration, merging filtrate after extraction, is obtained
Mixing lixiviating solution；
S43: the mixing lixiviating solution concentrate drying that step s42 is obtained, is obtained extraction cream, is used in extraction 6.5-6.8 times of body of cream
The water of long-pending 48-56 DEG C is dissolved, and carries out extraction 2-3 time using anhydrous ethyl acetate solvent, continues to use anhydrous ethyl acetate
Carry out multiple crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.5-5.8(w/v), prepared crystal crude product；
S44: by the prepared crystal crude product of step s43 through supercritical co2Extraction, the condition of extraction: extraction kettle pressure is 14-
20mpa, extraction temperature is 46-48 DEG C, and extraction time is 25-35min, prepared ginkgetin；
S5: to step s4 be obtained uniform mixed liquor a in add lemon yellow pigment, nisin, molybdenum element, manganese element,
Cobalt element, alanine, isoleucine, serine, tyrosine, vitamin e, vitamin b1, vitamin c, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, starch sugar, dihydro jasmone, ethyl perfume, vanillin, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
It is 148-153w in microwave power, temperature is 52-56 DEG C, speed of agitator is to stir 0.5-0.9h under 300-500r/min, is obtained
Uniformly mixed liquor b；
S6: the uniform mixed liquor that step s5 is obtained is 134-136 DEG C in temperature, pressure is the 2-4s that sterilizes under 210-230kpa,
Uniform mixed liquor c is obtained；
S7: the uniform mixed liquor c that step s6 is obtained is 0.089-0.093mpa in vacuum, temperature is carried out at being 88-92 DEG C
Fill, sealing, are then cooled to room temperature, and new Millettia Speciosa health functional beverage is obtained.
It is illustrated below by more specifically embodiment.
Embodiment 1
A kind of new Millettia Speciosa health functional beverage, in units of weight portion, including following raw material: 185 parts of Millettia Speciosa, black tea 90
Part, 8 parts of Cortex Moutan, 12 parts of Radix Notoginseng, 10 parts of Herba Eupatorii, 9 parts of Rhizoma Cimicifugae, 6 parts of Poria, 8 parts of pear vinegar, 3 parts of ginkgetin, polypropylene pyrroles
1 part of alkanone, 0.6 part of hydroxypropyl methyl cellulose potassium, 0.7 part of agar, 1 part of Dupont eea2112ac compatilizer, food stage resist
264 0.8 parts of oxygen agent, 0.9 part of carrageenan, 0.5 part of epoxidized soybean oil fatty acid, 0.4 part of lemon yellow pigment, nisin
0.7 part, 0.2 part of molybdenum element, 0.2 part of manganese element, 0.1 part of cobalt element, 0.4 part of alanine, 0.3 part of isoleucine, serine 0.2
Part, 0.3 part of tyrosine, 0.2 part of vitamin e, 0.2 part of vitamin b1,0.3 part of vitamin c, aspartyl-phenyl alanine first
Fragrant 0.03 part of 0.04 part of ester, 2 parts of starch sugar, 0.05 part of dihydro jasmone, ethyl, 0.05 part of vanillin, methyl-furfuryl fumarate
0.8 part, 0.2 part of 51- guanosine monophosphate disodium, 0.1 part of guanyl potassium；
The preparation method of described new Millettia Speciosa health functional beverage, comprises the following steps:
S1: the preparation of Millettia Speciosa juice, comprises the following steps；
S11: the Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 180 mesh sieve, prepared Millettia Speciosa minces；
S12: the Millettia Speciosa that step s11 is obtained minces and mixes loading extraction pot with the water ratio for 1:5 in mass ratio, in pressure
For under 5mpa, with 5 layers of filtered through gauze after decocting in water 0.5h, prepared filtrate a；
S13: the filtrate a rotating speed that step s12 is obtained is the centrifuge of 4500r/min, is 0.082mpa in vacuum
Lower sucking filtration roguing, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps:
S21: black tea is dried to water content≤8.5% pulverizing, crosses 130 mesh sieves, the ethanol water being 82% with mass fraction
Mix for 1:13 in mass ratio, be 170w in microwave power, temperature extracts 25min at being 46 DEG C, filters, and concentrates, and prepared tea is many
Phenol crude extract a；
S22: the tea polyphenols crude extract a that step s21 is obtained is added in the kcl solution that concentration is 18%, ph is adjusted to 6,
Centrifugal rotational speed is to remove impurity under 4500r/min, using aperture be 0.02 μm of filter membrane temperature be at 34 DEG C to centrifugation after molten
Liquid is filtered, prepared filtrate b；
S23: by step s22 be obtained filtrate b with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Rhizoma Cimicifugae, Poria are separately dried the co-grinding to water content≤7.5%, add water, in material
Liquor ratio is 1:15(w/v), microwave power is 200w, and Extracting temperature is 93 DEG C, and extraction time is 1.4h, then filtering residue, prepared medicine
Liquid；
S4: by medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step s1, step s2, step s3, pear vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont eea2112ac compatilizer, food stage
After antioxidant 264, carrageenan, epoxidized soybean oil fatty acid, 1200 parts of water mix, it is 165w in microwave power, temperature is 64 DEG C,
Speed of agitator is to stir 0.6h under 300r/min, and uniform mixed liquor a is obtained；
The preparation method of described ginkgetin comprises the following steps:
S41: dry Folium Ginkgo is pulverized and is crossed 100 mesh sieve, prepared Ginkgo Leaf；
S42: the Ginkgo Leaf that step s41 is obtained is extracted using 55 DEG C of water, in extraction, microwave power is 180w, Gu
Liquor ratio is 1:14(w/v), extraction time is 0.8h, extracts 2 times, filtration, merging filtrate after extraction, and mixing lixiviating solution is obtained；
S43: the mixing lixiviating solution concentrate drying that step s42 is obtained, is obtained extraction cream, is used in extraction 6.6 times of volumes of cream
52 DEG C of water is dissolved, and carries out extracting 2 times using anhydrous ethyl acetate solvent, continuation is repeatedly tied with anhydrous ethyl acetate
Brilliant process, in crystallization process, solid-to-liquid ratio is 1:5.6(w/v), prepared crystal crude product；
S44: by the prepared crystal crude product of step s43 through supercritical co2Extract, the condition of extraction: extraction kettle pressure is
18mpa, extraction temperature is 47 DEG C, and extraction time is 30min, prepared ginkgetin；
S5: to step s4 be obtained uniform mixed liquor a in add lemon yellow pigment, nisin, molybdenum element, manganese element,
Cobalt element, alanine, isoleucine, serine, tyrosine, vitamin e, vitamin b1, vitamin c, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, starch sugar, dihydro jasmone, ethyl perfume, vanillin, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
It is 145w in microwave power, temperature is 52 DEG C, speed of agitator is to stir 0.5h under 400r/min, and uniform mixed liquor b is obtained；
S6: the uniform mixed liquor that step s5 is obtained is 135 DEG C in temperature, pressure is the 3s that sterilizes under 230kpa, is obtained and uniformly mixes
Close liquid c；
S7: the uniform mixed liquor c that step s6 is obtained is 0.092mpa in vacuum, temperature carries out fill, sealing at being 90 DEG C,
It is then cooled to room temperature, new Millettia Speciosa health functional beverage is obtained.
Embodiment 2
A kind of new Millettia Speciosa health functional beverage, in units of weight portion, including following raw material: 153 parts of Millettia Speciosa, black tea 72
Part, 6 parts of Cortex Moutan, 8 parts of Radix Notoginseng, 6 parts of Herba Eupatorii, 7 parts of Rhizoma Cimicifugae, 5 parts of Poria, 5 parts of pear vinegar, 2 parts of ginkgetin, polypropylene pyrrolidine
0.7 part of ketone, 0.4 part of hydroxypropyl methyl cellulose potassium, 0.5 part of agar, 0.7 part of Dupont eea2112ac compatilizer, food stage
0.6 part of antioxidant 264,0.5 part of carrageenan, 0.3 part of epoxidized soybean oil fatty acid, 0.3 part of lemon yellow pigment, streptococcus acidi lactici
0.5 part of element, 0.2 part of molybdenum element, 0.2 part of manganese element, 0.1 part of cobalt element, 0.3 part of alanine, 0.2 part of isoleucine, serine
0.2 part, 0.2 part of tyrosine, 0.2 part of vitamin e, 0.2 part of vitamin b1,0.2 part of vitamin c, aspartyl-phenyl alanine
Fragrant 0.02 part of 0.03 part of methyl ester, 1.5 parts of starch sugar, 0.03 part of dihydro jasmone, ethyl, 0.04 part of vanillin, fumaric acid furfuryl alcohol
0.5 part of methyl ester, 0.2 part of 51- guanosine monophosphate disodium, 0.1 part of guanyl potassium；
The preparation method of described new Millettia Speciosa health functional beverage, comprises the following steps:
S1: the preparation of Millettia Speciosa juice, comprises the following steps；
S11: the Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 150 mesh sieve, prepared Millettia Speciosa minces；
S12: the Millettia Speciosa that step s11 is obtained minces and mixes loading extraction pot with the water ratio for 1:3 in mass ratio, in pressure
For under 4mpa, with 4 layers of filtered through gauze after decocting in water 0.6h, prepared filtrate a；
S13: the filtrate a rotating speed that step s12 is obtained is the centrifuge of 4000r/min, is 0.076mpa in vacuum
Lower sucking filtration roguing, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps:
S21: by black tea dry to water content be 8.2% after pulverize, cross 100 mesh sieves, the ethanol water being 75% with mass fraction
Mix for 1:12 in mass ratio, be 150w in microwave power, temperature extracts 30min at being 44 DEG C, filters, and concentrates, and prepared tea is many
Phenol crude extract a；
S22: the tea polyphenols crude extract a that step s21 is obtained is added in the kcl solution that concentration is 17%, ph is adjusted to 5.8,
Remove impurity under centrifugal rotational speed is for 4000r/min, using aperture be 0.01 μm of filter membrane temperature be at 32 DEG C to centrifugation after
Solution is filtered, prepared filtrate b；
S23: by step s22 be obtained filtrate b with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Rhizoma Cimicifugae, Poria are separately dried the co-grinding to water content≤7.6%, add water, in material
Liquor ratio is 1:14(w/v), microwave power is 200-240w, and Extracting temperature is 94 DEG C, and extraction time is 1.7h, then filtering residue, system
Obtain medicinal liquid；
S4: by medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step s1, step s2, step s3, pear vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont eea2112ac compatilizer, food stage
After antioxidant 264, carrageenan, epoxidized soybean oil fatty acid, 1300 parts of water mix, it is 162w in microwave power, temperature is 64 DEG C,
Speed of agitator is to stir 0.8h under 200r/min, and uniform mixed liquor a is obtained；
The preparation method of described ginkgetin comprises the following steps:
S41: dry Folium Ginkgo is pulverized and is crossed 100 mesh sieve, prepared Ginkgo Leaf；
S42: the Ginkgo Leaf that step s41 is obtained is extracted using 45 DEG C of water, in extraction, microwave power is 150w, Gu
Liquor ratio is 1:12(w/v), extraction time is 1h, extracts 2 times, filtration, merging filtrate after extraction, and mixing lixiviating solution is obtained；
S43: the mixing lixiviating solution concentrate drying that step s42 is obtained, is obtained extraction cream, is used in extraction 6.5 times of volumes of cream
48 DEG C of water is dissolved, and carries out extracting 2 times using anhydrous ethyl acetate solvent, continuation is repeatedly tied with anhydrous ethyl acetate
Brilliant process, in crystallization process, solid-to-liquid ratio is 1:5.5(w/v), prepared crystal crude product；
S44: by the prepared crystal crude product of step s43 through supercritical co2Extract, the condition of extraction: extraction kettle pressure is
14mpa, extraction temperature is 46 DEG C, and extraction time is 35min, prepared ginkgetin；
S5: to step s4 be obtained uniform mixed liquor a in add lemon yellow pigment, nisin, molybdenum element, manganese element,
Cobalt element, alanine, isoleucine, serine, tyrosine, vitamin e, vitamin b1, vitamin c, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, starch sugar, dihydro jasmone, ethyl perfume, vanillin, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
It is 148w in microwave power, temperature is 52 DEG C, speed of agitator is to stir 0.9h under 300r/min, and uniform mixed liquor b is obtained；
S6: the uniform mixed liquor that step s5 is obtained is 134 DEG C in temperature, pressure is the 4s that sterilizes under 210kpa, is obtained and uniformly mixes
Close liquid c；
S7: the uniform mixed liquor c that step s6 is obtained is 0.089mpa in vacuum, temperature carries out fill, sealing at being 88 DEG C,
It is then cooled to room temperature, new Millettia Speciosa health functional beverage is obtained.
Embodiment 3
A kind of new Millettia Speciosa health functional beverage, in units of weight portion, including following raw material: 209 parts of Millettia Speciosa, black tea 98
Part, 9 parts of Cortex Moutan, 15 parts of Radix Notoginseng, 13 parts of Herba Eupatorii, 12 parts of Rhizoma Cimicifugae, 9 parts of Poria, 9 parts of pear vinegar, 4 parts of ginkgetin, polypropylene pyrrole
1.1 parts of pyrrolidone, 0.7 part of hydroxypropyl methyl cellulose potassium, 0.8 part of agar, 1.2 parts of Dupont eea2112ac compatilizer, food
0.9 part of grade antioxidant 264,1.2 parts of carrageenan, 0.6 part of epoxidized soybean oil fatty acid, 0.5 part of lemon yellow pigment, lactic acid chain
0.8 part of coccus element, 0.3 part of molybdenum element, 0.3 part of manganese element, 0.2 part of cobalt element, 0.5 part of alanine, isoleucine 0.4 part, thread
0.3 part of propylhomoserin, 0.4 part of tyrosine, 0.3 part of vitamin e, 0.3 part of vitamin b1,0.4 part of vitamin c, aspartoyl phenylpropyl alcohol
Fragrant 0.04 part of 0.05 part of propylhomoserin methyl ester, 2.5 parts of starch sugar, 0.06 part of dihydro jasmone, ethyl, 0.06 part of vanillin, fumaric acid
0.9 part of furfuryl alcohol methyl ester, 0.3 part of 51- guanosine monophosphate disodium, 0.2 part of guanyl potassium；
The preparation method of described new Millettia Speciosa health functional beverage, comprises the following steps:
S1: the preparation of Millettia Speciosa juice, comprises the following steps；
S11: the Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 200 mesh sieve, prepared Millettia Speciosa minces；
S12: the Millettia Speciosa that step s11 is obtained minces and mixes loading extraction pot with the water ratio for 1:7 in mass ratio, in pressure
Power is under 6mpa, with 6 layers of filtered through gauze after decocting in water 0.3h, prepared filtrate a；
S13: the filtrate a rotating speed that step s12 is obtained is the centrifuge of 5000r/min, is 0.085mpa in vacuum
Lower sucking filtration roguing, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps:
S21: black tea is dried to water content≤8.5% pulverizing, crosses 140 mesh sieves, with the ethanol water for 75%-84% for the mass fraction
Solution mixes for 1:14 in mass ratio, is 180w in microwave power, and temperature extracts 18min at being 48 DEG C, filters, and concentrates, and is obtained
Tea polyphenols crude extract a；
S22: the tea polyphenols crude extract a that step s21 is obtained is added in the kcl solution that concentration is 19%, ph is adjusted to 6.2,
Remove impurity under centrifugal rotational speed is for 5000r/min, using aperture be 0.03 μm of filter membrane temperature be at 35 DEG C to centrifugation after
Solution is filtered, prepared filtrate b；
S23: by step s22 be obtained filtrate b with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Rhizoma Cimicifugae, Poria are separately dried the co-grinding to water content≤7.6%, add water, in material
Liquor ratio is 1:17(w/v), microwave power is 240w, and Extracting temperature is 96 DEG C, and extraction time is 1.3h, then filtering residue, prepared medicine
Liquid；
S4: by medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step s1, step s2, step s3, pear vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont eea2112ac compatilizer, food stage
After antioxidant 264, carrageenan, epoxidized soybean oil fatty acid, 1500 parts of water mix, it is 176w in microwave power, temperature is 68 DEG C,
Speed of agitator is to stir 0.5h under 400r/min, and uniform mixed liquor a is obtained；
The preparation method of described ginkgetin comprises the following steps:
S41: dry Folium Ginkgo is pulverized and is crossed 120 mesh sieve, prepared Ginkgo Leaf；
S42: the Ginkgo Leaf that step s41 is obtained is extracted using 65 DEG C of water, in extraction, microwave power is 200w, Gu
Liquor ratio is 1:15(w/v), extraction time is 0.5h, extracts 3 times, filtration, merging filtrate after extraction, and mixing lixiviating solution is obtained；
S43: the mixing lixiviating solution concentrate drying that step s42 is obtained, is obtained extraction cream, is used in extraction 6.8 times of volumes of cream
56 DEG C of water is dissolved, and carries out extracting 3 times using anhydrous ethyl acetate solvent, continuation is repeatedly tied with anhydrous ethyl acetate
Brilliant process, in crystallization process, solid-to-liquid ratio is 1:5.8(w/v), prepared crystal crude product；
S44: by the prepared crystal crude product of step s43 through supercritical co2Extract, the condition of extraction: extraction kettle pressure is
20mpa, extraction temperature is 48 DEG C, and extraction time is 25min, prepared ginkgetin；
S5: to step s4 be obtained uniform mixed liquor a in add lemon yellow pigment, nisin, molybdenum element, manganese element,
Cobalt element, alanine, isoleucine, serine, tyrosine, vitamin e, vitamin b1, vitamin c, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, starch sugar, dihydro jasmone, ethyl perfume, vanillin, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
It is 153w in microwave power, temperature is 56 DEG C, speed of agitator is to stir 0.5h under 500r/min, and uniform mixed liquor b is obtained；
S6: the uniform mixed liquor that step s5 is obtained is 136 DEG C in temperature, pressure is the 2s that sterilizes under 230kpa, is obtained and uniformly mixes
Close liquid c；
S7: the uniform mixed liquor c that step s6 is obtained is 0.093mpa in vacuum, temperature carries out fill, sealing at being 92 DEG C,
It is then cooled to room temperature, new Millettia Speciosa health functional beverage is obtained.
Organoleptic quality, physical and chemical quality, preparation are carried out to the new Millettia Speciosa health functional beverage obtained by embodiment 1-3
Timing, result is as shown in table 1,2,3.
The organoleptic quality of the new Millettia Speciosa health functional beverage of table 1
As shown in Table 1, limpid, golden yellow bright on the new Millettia Speciosa health functional beverage color and luster that the present invention is obtained；Mouthfeel tea flavour
Substantially, sour-sweet tasty and refreshing；Heavy flavour of vinegar fragrance on fragrance, has tea perfume.
The physical and chemical quality of the new Millettia Speciosa health functional beverage of table 2
As shown in Table 2, the new Millettia Speciosa health functional beverage acetic acid content that the present invention is obtained is 11.69-12.42g/l, and tea is many
Phenol content is 1.41-1.68g/l, and ph value is 6.4-6.63.
The preparation time of the new Millettia Speciosa health functional beverage of table 3
As shown in Table 3, the preparation time of the new Millettia Speciosa health functional beverage that the present invention is obtained than prior art preparation when
Between shorter, thus shortening the production cycle, reduces cost.
The new Millettia Speciosa health functional beverage of the present invention is dispelled implication effect test
Choose 98 people with implication symptom, wherein male 49 people, female 49 people.Drink the new Millettia Speciosa health care work(of the present invention daily
3 glasss of beverage of energy, every glass of 250ml, obtain result of the test after 5 days as shown in table 4.
Table 4 is dispelled implication effect test result
As shown in Table 4, the new Millettia Speciosa health functional beverage of the present invention being capable of effectively treatment or mitigation implication symptom.
Above content it cannot be assumed that the present invention be embodied as be confined to these explanations, the affiliated technology neck for the present invention
For the those of ordinary skill in domain, without departing from the inventive concept of the premise, some simple deduction or replace can also be made,
The scope of patent protection that the present invention is determined all should be considered as belonging to by the claims submitted to.
Claims (6)
1. a kind of new Millettia Speciosa health functional beverage is it is characterised in that in units of weight portion, including following raw material: Niu great
Power 153-209 part, black tea 72-98 part, Cortex Moutan 6-9 part, Radix Notoginseng 8-15 part, Herba Eupatorii 6-13 part, Rhizoma Cimicifugae 7-12 part, Poria 5-9 part,
Pear vinegar 5-9 part, ginkgetin 2-4 part, polyvinyl pyrilodone 0.7-1.1 part, hydroxypropyl methyl cellulose potassium 0.4-0.7
Part, agar 0.5-0.8 part, Dupont eea2112ac compatilizer 0.7-1.2 part, food grade antioxidant 264 0.6-0.9 part,
Carrageenan 0.5-1.2 part, epoxidized soybean oil fatty acid 0.3-0.6 part, lemon yellow pigment 0.3-0.5 part, nisin
0.5-0.8 part, molybdenum element 0.2-0.3 part, manganese element 0.2-0.3 part, cobalt element 0.1-0.2 part, alanine 0.3-0.5 part, different
Leucine 0.2-0.4 part, serine 0.2-0.3 part, tyrosine 0.2-0.4 part, vitamin e 0.2-0.3 part, vitamin b1
0.2-0.3 part, vitamin c 0.2-0.4 part, aspartyl-phenylalanine methyl ester 0.03-0.05 part, starch sugar 1.5-2.5 part,
Dihydro jasmone 0.03-0.06 part, ethyl perfume 0.02-0.04 part, vanillin 0.04-0.06 part, methyl-furfuryl fumarate 0.5-
0.9 part, 51- guanosine monophosphate disodium 0.2-0.3 part, guanyl potassium 0.1-0.2 part；
The preparation method of described new Millettia Speciosa health functional beverage, comprises the following steps:
S1: the preparation of Millettia Speciosa juice, comprises the following steps；
S11: the Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 150-200 mesh sieve, prepared Millettia Speciosa minces；
S12: the Millettia Speciosa that step s11 is obtained minces and mixes loading extraction pot with the water ratio for 1:3-7 in mass ratio, in pressure
Power is under 4-6mpa, uses 4-6 layer filtered through gauze, prepared filtrate a after decocting in water 0.3-0.6h；
S13: the filtrate a rotating speed that step s12 is obtained is the centrifuge of 4000-5000r/min, in vacuum is
Sucking filtration roguing under 0.076-0.085mpa, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps:
S21: black tea is dried to water content≤8.5% pulverizing, crosses 100-140 mesh sieve, with the second for 75%-84% for the mass fraction
Alcohol-water solution mixes for 1:12-14 in mass ratio, is 150-180w in microwave power, and temperature extracts 18- at being 44-48 DEG C
30min, filters, and concentrates, prepared tea polyphenols crude extract a；
S22: by step s21 be obtained tea polyphenols crude extract a be added to concentration be 17%-19% kcl solution in, ph adjust to
5.8-6.2, removes impurity, using aperture for 0.01-0.03 μm of filter membrane in temperature under centrifugal rotational speed is for 4000-5000r/min
For filtering to the solution after centrifugation at 32-35 DEG C, prepared filtrate b；
S23: by step s22 be obtained filtrate b with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3: Cortex Moutan, Radix Notoginseng, Herba Eupatorii, Rhizoma Cimicifugae, Poria are separately dried the co-grinding to water content≤7.6%, add water, in material
Liquor ratio is 1:14-17(w/v), microwave power is 200-240w, and Extracting temperature is 94-96 DEG C, and extraction time is 1.3-1.7h, connects
Filtering residue, prepared medicinal liquid；
S4: by medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step s1, step s2, step s3, pear vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont eea2112ac compatilizer, food stage
After antioxidant 264, carrageenan, epoxidized soybean oil fatty acid, 1300-1500 part water mix, it is 162-176w in microwave power, temperature
Spend for 64-68 DEG C, speed of agitator is to stir 0.5-0.8h under 200-400r/min, and uniform mixed liquor a is obtained；
The preparation method of described ginkgetin comprises the following steps:
S41: dry Folium Ginkgo is pulverized and is crossed 100-120 mesh sieve, prepared Ginkgo Leaf；
S42: the Ginkgo Leaf that step s41 is obtained is extracted using 45-65 DEG C of water, in extraction, microwave power is 150-
200w, solid-to-liquid ratio is 1:12-15(w/v), extraction time is 0.5-1h, extracts 2-3 time, filtration, merging filtrate after extraction, is obtained
Mixing lixiviating solution；
S43: the mixing lixiviating solution concentrate drying that step s42 is obtained, is obtained extraction cream, is used in extraction 6.5-6.8 times of body of cream
The water of long-pending 48-56 DEG C is dissolved, and carries out extraction 2-3 time using anhydrous ethyl acetate solvent, continues to use anhydrous ethyl acetate
Carry out multiple crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.5-5.8(w/v), prepared crystal crude product；
S44: by the prepared crystal crude product of step s43 through supercritical co2Extraction, the condition of extraction: extraction kettle pressure is 14-
20mpa, extraction temperature is 46-48 DEG C, and extraction time is 25-35min, prepared ginkgetin；
S5: to step s4 be obtained uniform mixed liquor a in add lemon yellow pigment, nisin, molybdenum element, manganese element,
Cobalt element, alanine, isoleucine, serine, tyrosine, vitamin e, vitamin b1, vitamin c, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, starch sugar, dihydro jasmone, ethyl perfume, vanillin, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
It is 148-153w in microwave power, temperature is 52-56 DEG C, speed of agitator is to stir 0.5-0.9h under 300-500r/min, is obtained
Uniformly mixed liquor b；
S6: the uniform mixed liquor that step s5 is obtained is 134-136 DEG C in temperature, pressure is the 2-4s that sterilizes under 210-230kpa,
Uniform mixed liquor c is obtained；
S7: the uniform mixed liquor c that step s6 is obtained is 0.089-0.093mpa in vacuum, temperature is carried out at being 88-92 DEG C
Fill, sealing, are then cooled to room temperature, and new Millettia Speciosa health functional beverage is obtained.
2. new Millettia Speciosa health functional beverage according to claim 1 is it is characterised in that microwave work(described in step s3
Rate is 240w, and Extracting temperature is 96 DEG C, and extraction time is 1.3h.
3. new Millettia Speciosa health functional beverage according to claim 2 is it is characterised in that microwave work(described in step s4
Rate is 176w, and temperature is 68 DEG C, and speed of agitator is to stir 0.5h under 400r/min.
4. new Millettia Speciosa health functional beverage according to claim 3 is it is characterised in that microwave work(described in step s5
Rate is 153w, and temperature is 56 DEG C, and speed of agitator is to stir 0.5h under 500r/min.
5. new Millettia Speciosa health functional beverage according to claim 1 is it is characterised in that temperature described in step s6 is
136 DEG C, pressure is the 2s that sterilizes under 230kpa.
6. new Millettia Speciosa health functional beverage according to claim 1 is it is characterised in that vacuum described in step s6
For 0.093mpa, temperature carries out fill, sealing at being 92 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610902736.7A CN106367287A (en) | 2016-10-17 | 2016-10-17 | Novel beautiful millettia root health-care beverage |
Applications Claiming Priority (1)
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106879998A (en) * | 2017-02-09 | 2017-06-23 | 广西南宁市韩太食品有限责任公司 | One kind dehydration sauerkraut and preparation method thereof |
| CN106942656A (en) * | 2017-02-09 | 2017-07-14 | 广西南宁市韩太食品有限责任公司 | One kind dehydration chopped spring onion and preparation method thereof |
| CN106942710A (en) * | 2017-02-09 | 2017-07-14 | 广西南宁市韩太食品有限责任公司 | One kind dehydration mushroom and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101611909A (en) * | 2009-05-05 | 2009-12-30 | 潘泰安 | Full nutrient Chinese wolfberry health-care fruit juice and production method thereof |
| CN105767396A (en) * | 2016-05-12 | 2016-07-20 | 广西科技大学鹿山学院 | Lipid-lowering ginkgo seed tea |
| CN105767397A (en) * | 2016-05-12 | 2016-07-20 | 广西科技大学鹿山学院 | Spleen-invigorating and stomach-harmonizing gingko tea |
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2016
- 2016-10-17 CN CN201610902736.7A patent/CN106367287A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101611909A (en) * | 2009-05-05 | 2009-12-30 | 潘泰安 | Full nutrient Chinese wolfberry health-care fruit juice and production method thereof |
| CN105767396A (en) * | 2016-05-12 | 2016-07-20 | 广西科技大学鹿山学院 | Lipid-lowering ginkgo seed tea |
| CN105767397A (en) * | 2016-05-12 | 2016-07-20 | 广西科技大学鹿山学院 | Spleen-invigorating and stomach-harmonizing gingko tea |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106879998A (en) * | 2017-02-09 | 2017-06-23 | 广西南宁市韩太食品有限责任公司 | One kind dehydration sauerkraut and preparation method thereof |
| CN106942656A (en) * | 2017-02-09 | 2017-07-14 | 广西南宁市韩太食品有限责任公司 | One kind dehydration chopped spring onion and preparation method thereof |
| CN106942710A (en) * | 2017-02-09 | 2017-07-14 | 广西南宁市韩太食品有限责任公司 | One kind dehydration mushroom and preparation method thereof |
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