CN101190277B - Method for preparing stemmacantha uniflora blood circulation-activating, stasis-removing and wind-damp-expelling wine - Google Patents
Method for preparing stemmacantha uniflora blood circulation-activating, stasis-removing and wind-damp-expelling wine Download PDFInfo
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Abstract
The invention provides a preparation method ground beetle activating blood circulation to dissipate blood stasis and eliminating rheumatism wine. The invention consists of the following weight units of raw materials and steps: a. 3-40 parts of ground beetle, 5-20 radix achyranthis bidentatae, 3-16 parts of ledebourellae, 3-16 parts of licorice root, 3-16 parts of ramulus cinnamomi, 5-20 parts of paeoniae alba, 5-20 parts of papaya, 5-20 parts of cibot rhizome, 5-20 parts of eucommia are pulverized into crude powder; b. gelatin is added with 0-0.5% of weight of the crude powder, then 5-75% concentration of wine equivalent to 20-30 times medical substances is added, diffusion is carried out under normal temperature and pressure for 1-4 times, with 1-7 days every time, and then the medicine stands for 0.5-2 days to remove precipitation; c. the wine is added with precipitant after being seasoned and removing precipitation, then stired and filtered carefully, finally the product is obtained after filling and sterilization. The product is transparent and no precipitation formed after long-term standing; the invention has good effect in eliminating rheumatism.
Description
Technical field:
The present invention relates to field of food, relate to a kind of preparation method of turtle blood-activating blood stasis dispelling wind-damp dispelling wine more specifically.
Technical background:
Di Bie is salty-cold, go into the heart, liver, spleen channel.Its function cures mainly and is removing blood stasis, removing mass, and collateral dredging, reason is hindered.Control enclosed mass, lump and tumor and gather, amenorrhea due to stagnation of blood, postnatal blood stasis stomachache, traumatic injury.All on the books at " herbal classic ", " property of medicine opinion ", " detailed outline ", amplification on Canon of Materia Medica, " the logical cloud of book on Chinese herbal medicine " etc.
People Dui Di Bie worm oils and fats, aminoacid, protein, vitamin in recent years, the kind and the content of inorganic salt etc. are studied.Di Bie worm is nontoxic substantially, edible, is a kind of nutritious insect food.Studies show that further ， Di Bie worm contains the present octacosanol that the resisting fatigue effect is best of thinking in the world.Have the Se, the cupreol that benefit cardiovascular system, unsaturated fatty acid (as oleic acid, linoleic acid, Palmic acid, wherein oleic acid content accounts for 75-86% in the oils and fats) etc.Have blood pressure regulation, enhance metabolism, delay atherosclerotic formation, blood coagulation resisting function is arranged, experiment shows also have good thrombolytic effect.Antioxidant effect is arranged, and experiment shows that Di Bie worm can improve cardiac muscle and brain to the tolerance of ischemia.Anti-radical action is arranged: 60 routine coronary heart disease Blood stasis patients take that lipid peroxide obviously descends in Di Bie powder 4 all blood, and reduced glutathion obviously rises.， Di Bie worm also has antimutagenic effect in addition, for antitumor action provides experimental data.
Development along with medical and health care system, the raising Di Bie worm of living standards of the people is because of demand is more and more big both at home and abroad, after artificial breeding's technical barrier was broken through, it was that a cost is low that artificial greenhouse cellar formula is raised Di Bie worm, and it is fast to produce effects, feed resource is wide, consume and lack, the household sideline production that method for breeding is easy, a subsidiary labour power annual income does not wait for ten thousand yuan at 0.5-3.Form the pattern that company adds peasant household in many places of China, wide farmers has been cultured and the batch production utilization combines, begun to move towards the road of raising production, applied research, processing, sale.
Er Di Bie worm is more and more wider in the application of aspects such as medicine, food, health product.Zai Di Bie raiser, Di Bie culture zone, the people of some edible Di Bie feels that gradually Di Bie is invigorating blood circulation, the effect of aspects such as synthetism, strong body, Qi Di Bie of You is in the effect of promoting blood circulation by removing wind aspect wet, and is more unique.In China, be that the health promoting wine of the treatment rheumatism made of base stock is of a great variety with Chinese medicine.But Jian Di Bie is not the health preparation of the wind-damp dispelling of main material production as yet.This Products Development not only benefits the rheumatism patient, also helps the comprehensive utilization of ground Bie, promotes the economic development of ground Bie raiser and associated companies.
Summary of the invention:
The purpose of this invention is to provide according to the medical value of Di Bie worm with the needs and the deficiencies in the prior art of the development and use of Di Bie worm, Yi Di Bie worm of the present invention is the preparation method that development of raw materials is produced the health promoting wine turtle blood-activating blood stasis dispelling wind-damp dispelling wine of blood circulation promoting and blood stasis dispelling dispelling the wind and dampness pathogens.
Purpose of the present invention can realize by following technical measures:
This method comprises following raw materials in weight portion and step:
A. the Radix Achyranthis Bidentatae of 3-40 De Di Bie, 5-20, the Radix Saposhnikoviae of 3-16, the Radix Glycyrrhizae of 3-16, the Ramulus Cinnamomi of 3-16, the Radix Paeoniae Alba of 5-20, the Fructus Chaenomelis of 5-20, the Rhizoma Cibotii of 5-20, the Cortex Eucommiae powder of 5-20 are broken into coarser powder;
B. elder generation adds the gelatin of the 0-0.5% of medical material coarser powder amount, adds the edible wine of 20-30 times of medical material coarser powder amount wine volumetric concentration 5-75% again, and lixiviate is 1-4 time under the normal temperature and pressure, each 1-7 days, leaves standstill then and removes precipitation in 0.5-2 days;
C. the wine liquid of removing post precipitation adds precipitant after seasoning, again through stir, fine straining, last fill, sterilize product.
Purpose of the present invention also can realize by following technical measures:
When the wine volumetric concentration in the above-mentioned b operation was 5-45%, the addition of gelatin was selected from 0.1-0.5%; Described precipitant is selected from lixiviate with the tricalcium phosphate of the 0.3-0.8% of capacity for liquor and the active hargil of 0.3-0.8%; When described precipitant is 5-45% in the wine volumetric concentration, also comprise active carbon and the 0.1-0.4% kieselguhr of 0.3-0.8%; Described speed of agitator is 80-250r/min, and mixing time is 0.5-2 hour; Described fine straining selects for use the flame filter press under the 0.1-0.3MPa to filter; When wine volumetric concentration＜20%, select the gamma-radiation radiation sterilization for use.
1, the wine liquid concentration of immersion medical material can be any concentration, and generally controlling the wine volumetric concentration is 5-75%, the soak active constituent content height of high wine, and tannin is few; The active ingredient of low concentration wine soak is few, and impurity such as tannin are many, and the wine liquid concentration of bubble medical material needn't add the heavy tannin of gelatin between 45-75 the time.
2, as made wine concentration below 20%, need carry out sterilization treatment behind the filling bottle.
3, medicine soaks with high wine, and bubble liquid is through sedimentation and filtration, and it is clear and bright that the product wine liquid keeps.If but convert into the wine soak of low concentration with the high wine soak, and need in active hargil and calcium phosphate precipitation agent, add Powdered Activated Carbon and kieselguhr again, agitation and filtration can get clear and bright liquid then.Perhaps the high wine of sedimentation and filtration is converted into low concentration wine, and it is muddy that wine liquid becomes.Need to add in the muddy wine liquid of blending Powdered Activated Carbon and kieselguhr, agitation and filtration can get clear and bright wine liquid then again.
Ramulus Cinnamomi: be the twig of Lauraceae aiphyllium Cortex Cinnamomi Cinna momu cassia Presl.
Radix Saposhnikoviae: be the Umbelliferae root of herbaceous plant Radix Saposhnikoviae Saposhnikovia divaricata (Turez.) Schischk. for many years.
Fructus Chaenomelis: be Rosaceae machaka chaenomeles lagenaria Chaenomeles
Speciosa (Sweet) Nakai and Fructus Chaenomelis C.The mature fruit of sinensis (Thouin) Koehne.
Rhizoma Cibotii: be the root stock of concha Anodonta seu Cristaria fern herbaceos perennial Rhizoma Cibotii Cibotium barometz (L.) J.Sm..
Di Bie worm: Wei Bie Lian insecticide Di Bie Eupolyphaga sinensis Walker of section or the female worm of Ji Di Bie Steleophaga plancyi (Boleny) all.
Radix Achyranthis Bidentatae: be Radix Achyranthis Bidentatae (Radix Achyranthis Bidentatae) the Achyranthes bidentata BL. of Amaranthaceae perennial grass wood plant and the root of Radix Cyathulae Cyathula officinalis Kuan.
Radix Glycyrrhizae: be the pulse family root and rhizome of draft liquorice root Glycyrrhiza uralensis Fisch or Glycyrrhiza inflata Bat. Glycyrrhiza inflata Bat. or Glycyrrhiza glabra L. Glycyrrhiza glabra L for many years.
The Radix Paeoniae Alba: be the Ranunculaceae root of draft plant peony Paeonia lactiflora Pall for many years.
The Cortex Eucommiae: be the bark of Eucommiaceae deciduous tree plant Cortex Eucommiae Eucommia ulmoides 0liv.
Function cures mainly:
Blood circulation promoting and blood stasis dispelling, eliminating evil collateral dredging, relieving spasm to stop pain is used for the resistance of all meridians numbness, the pain that muscle, muscles and bones, the joint due to QI-blood circulation is smooth takes place, thinly jerk, numb, joint stuffiness.
Bie worm salty in the mouth, property is hot cold, is good at blood circulation promoting and blood stasis dispelling, collateral dredging, analgesia, what all QI and blood cohesion parts all can be opened it, intrinsic " it is long-pending to dehematize, search pick extremely solid " says.Through sick institute.Monarch drug for we.The Fructus Chaenomelis sour in the mouth, acid can be gone into liver, so beneficial muscle and blood, sick waist kidney foot knee joint is unable, all also indispensable; Radix Achyranthis Bidentatae is the foot the moon of fainting, the medicine of few the moon, and kind invigorating the liver and kidney, bone and muscle strengthening, sharp joint, on the whole the main disease of institute gets wine then can invigorating the liver and kidney, has again and merit that can benefit; Cortex Eucommiae Liver Channel edema caused by disorder of QI medicine can make the muscles and bones phase, and the effect of analgesia is arranged again, and this medicine is we's ministerial drug altogether with Fructus Chaenomelis, Radix Achyranthis Bidentatae.Ramulus Cinnamomi and battalion, activate yang the cold relieving pain relieving; Radix Paeoniae Alba picric acid nourishes blood and holds back sun, easing the affected liver to relieve pain; The Radix Saposhnikoviae acrid in the mouth, expelling pathogenic wind from the body surface, winning wet spasmolytic and Ramulus Cinnamomi, the Radix Paeoniae Alba is adjuvant drug altogether.Radix Glycyrrhizae is the meridian dredging first, sharp joint, and second coordinating the actions of various ingredients in a prescription is a messenger drug.Take a broad view of full side's blood circulation promoting and blood stasis dispelling, eliminating evil collateral dredging, relieving spasm to stop pain, amount to blood and and the battalion defend unobstructed, the effect that passages through which vital energy circulates is mixed well.
2, the wine made of method of the present invention is to the analgesic activity of mice.
Get the female kunming mouse of 18-22g, each 1, be placed on 55 ± 0.5 ℃ the hot plate of water-bath, the pain threshold of sufficient required time (second) as this Mus appears adding to mice.This value was less than 5 seconds or give it up greater than 30 seconds persons or leaper, divided 2 groups at random with the qualified mice that this method is chosen.Repeat to survey its normal pain threshold, get two subnormal threshold of pain meansigma methodss, as pain threshold before this Mus administration.2 treated animals are respectively the normal saline group, wind-damp dispelling wine group, and all per os gives, and administration begins to survey the mice pain threshold after 15 minutes, still do not react in 60 seconds as mice, takes off mice in order to avoid scald, and calculated by 60 seconds its threshold of pain, the results are shown in following table:
Di Bie wind-damp dispelling wine is to mice analgesic activity (X ± SD)
Experimental result shows that normal saline group and ground Bie wind-damp dispelling wine group compare respectively with before the administration, normal saline group no significant difference, and ground Bie wind-damp dispelling wine group obvious difference shows that this wine has significant analgesia role.
2, the influence of increasing of the mouse skin capillary permeability due to the wine xylol made of method of the present invention.Adopt kunming mouse (body weight 18-22g) male and female half and half, be divided into two groups at random, normal saline group and wind-damp dispelling wine group, all per os gives.
After the administration 15 minutes, inject 0.5% azovan blue normal saline solution 0.1ml/10g body weight in the tail vein.Immediately on the skin of unhairing of position, mouse web portion center melted paraxylene 0.03ml/ only, mice takes off cervical vertebra and causes death after 20 minutes.Peel skin of abdomen and according to each blue speckle color and luster depth it is divided into 7-10 rank, 1 rank is remembered 1 fen.Every skin locus coeruleus is shredded in the input plug teat glass with operating scissors, pour acetone-sodium sulfate extracting solution 10ml into, putting the dark place places, shake this test tube gently 2-3 every day, 2000rpm is centrifugal 10 minutes after 3 days, get supernatant in 590nm place colorimetric determination optical density, with the acetone-sodium sulfate liquid school zero of not steeping skin.Its experiment the results are shown in following table.
The influence that this wine xylol induced mice capillary of skin permeability increases
| Medicine | Dosage (ml/kg) | Mus number (only) | The locus coeruleus color and luster depth (level) | Blue speckle amount of dye ug |
| Normal saline | 2 | 15 | 5.9±1.4 | 2.0±0.3 |
| Said preparation | 2 | 15 | 3.0±0.8** | 1.3±0.4** |
Dimethylbenzene is dripped in the mouse web portion skin of unhairing, because of its local irritant effect causes capillary permeability hyperfunction.After injecting the ivens orchid in intravenous, the ivens orchid promptly will go out with the vascular exosmosis in hyperfunction blood capillary, form blue mottle piece in the position of melted paraxylene, how much can be used as of dyestuff seepage discharge judges whether medicine can the hyperfunction index of the early stage capillary permeability of inflammation-inhibiting.
The explanation of this experimental result, no matter be that the scoring of the blue speckle color and luster of the skin depth is compared, or compare to extract dyestuff spectrophotometric result, the empirical value of this wine is starkly lower than the normal saline matched group, and it is hyperfunction to show that this wine can obviously suppress dimethylbenzene induced mice skin of abdomen capillary permeability.
The effect of the wine that method of the present invention is made:
The patient who chooses pain such as lumbago, skelalgia knee joint is totally 28 people, drinks 30% wind-damp dispelling wine.Wherein, 40-49 year patient 3 people are the women entirely, and knee-joint pain and skelalgia can be drunk a small amount of wine.Drink 100ml every day, divide secondary or once drink, drink afterwards pain symptom obviously alleviates, and after especially drinking evening, rest effect immediately is best.
50-59 year women 8 people, wherein lumbago 3 people drink this wine of 100ml for each person every day; Knee joint and skelalgia 4 people can drink this wine of 200ml for each person every day.Omarthralgia 1 people (woman) drinks 100ml every day; Feel immediately after the drink that the state of an illness alleviates, wherein some pain still after each 1 people of lumbago and omarthralgia patient drink.
60-69 year patient 13 people, lumbago patient 7 people all are the male, and knee joint, elbow joint, shoulder joint and ankle joint and foot pain patient 6 people drink 100 or 200ml every day, and wherein a lumbago utmost point very alleviates after patient's drink not obviously, and other drink back pain are rapidly and obviously.
70-79 year patient 4 people are the male, and extremity pain, fiber crops, joint stuffiness are drunk 200ml every day, and the extremity pain obviously alleviates, and can stretch in the wrong.
Preliminary on probation through to this wine, generally the amount of drinking with every day 100-200ml be advisable, can 1 time or repeatedly drink is down.This wine has obviously to alleviate after drinking to patient's pain symptom.
The specific embodiment:
Embodiment 1:
The Radix Glycyrrhizae of 40g De Di Bie, 5g Radix Achyranthis Bidentatae, 16g Radix Saposhnikoviae, 3g, the Ramulus Cinnamomi of 16g, the Radix Paeoniae Alba of 5g, the Fructus Chaenomelis of 20g, the Rhizoma Cibotii of 5g, the Cortex Eucommiae powder of 20g are broken into coarser powder, 0.5% the gelatin that adds medical material coarser powder weight, add 30 times of medical material coarser powder amount wine volumetric concentrations again and be 5% edible wine, lixiviate is 1 time under the normal temperature and pressure, time is 7 days, mix every day and turn over 2 times, left standstill then 2 days, remove bottom precipitation; Adding tap water in the medicinal residues after lixiviate soaked 0.5 hour, waste, liquid filtering, replace the blending liquid of water as next new drug soaking wine, the sucrose that in wine liquid, adds wine liquid volume 2% again through removing post precipitation, 3% Mel, the capable seasoning that progresses greatly of 1% aroma, and then the tricalcium phosphate of 0.3% (W/V) of adding wine liquid volume and 0.8% active hargil, 0.3% active carbon, 0.4% kieselguhr, with the rotating speed is that 80r/min stirred 2 hours, filter with the flame filter press under the 0.1MPa, canned, getting the wine volumetric concentration with the gamma-radiation radiation sterilization is 5% clear and bright wine liquid.
Embodiment 2:
The Radix Glycyrrhizae of 3g De Di Bie, 20g Radix Achyranthis Bidentatae, 3g Radix Saposhnikoviae, 16g, the Ramulus Cinnamomi of 3g, the Radix Paeoniae Alba of 20g, the Fructus Chaenomelis of 5g, the Rhizoma Cibotii of 20g, the Cortex Eucommiae powder of 5g are broken into coarser powder, 0.5% the gelatin that adds medical material coarser powder weight, add 20 times of medical material coarser powder amount wine volumetric concentrations again and be 45% edible wine, lixiviate is 4 times under the normal temperature and pressure, time is 1 day, mix every day and turn over 4 times, left standstill then 0.5 day, remove bottom precipitation; Adding tap water in the medicinal residues after lixiviate soaked 3 hours, waste, liquid filtering, replace the blending liquid of water as next new drug soaking wine, sucrose, 1% Mel, 1.5% the aroma that in wine liquid, the adds wine liquid volume 3% more capable seasoning that progresses greatly through removing post precipitation, and then the tricalcium phosphate of 0.8% (W/V) of adding wine liquid volume and 0.3% active hargil, 0.8% active carbon, 0.1% kieselguhr, with the rotating speed is that 250r/min stirred 0.5 hour, filter with the flame filter press under the 0.3MPa, canned wine volumetric concentration is 45% clear and bright wine liquid.
Embodiment 3:
The Radix Glycyrrhizae of 20g De Di Bie, 10g Radix Achyranthis Bidentatae, 10g Radix Saposhnikoviae, 10g, the Ramulus Cinnamomi of 10g, the Radix Paeoniae Alba of 10g, the Fructus Chaenomelis of 10g, the Rhizoma Cibotii of 10g, the Cortex Eucommiae powder of 10g are broken into coarser powder, 0.3% the gelatin that adds medical material coarser powder weight, add 25 times of medical material coarser powder amount wine volumetric concentrations again and be 25% edible wine, lixiviate is 3 times under the normal temperature and pressure, time is 4 days, mix every day and turn over 3 times, left standstill then 1.5 days, remove bottom precipitation; Adding tap water in the medicinal residues after lixiviate soaked 1.5 hours, waste, liquid filtering, replace the blending liquid of water as next new drug soaking wine, the sucrose that in wine liquid, adds wine liquid volume 2.5% again through removing post precipitation, 2% Mel, the capable seasoning that progresses greatly of 1.2% aroma, and then the tricalcium phosphate of 0.6% (W/V) of adding wine liquid volume and 0.6% active hargil, 0.5% active carbon, 0.3% kieselguhr, with the rotating speed is that 150r/min stirred 1 hour, filter with the flame filter press under the 0.2MPa, canned wine volumetric concentration is 25% clear and bright wine liquid.
Embodiment 4:
Different is that lixiviate is 50% with the wine volumetric concentration that eats wine, does not add gelatin in the leaching process, and other are respectively with embodiment 1,2,3.
Embodiment 5:
Lixiviate that different is is 50% with the wine volumetric concentration of edible wine, adds the capable seasoning that progresses greatly of the sucrose of wine liquid volume 3.5% and aroma again in the wine liquid through removing post precipitation, only adds tricalcium phosphate and active hargil then, canned do not need to sterilize product.Other are respectively with embodiment 1,2,3.
Embodiment 6:
Different is that lixiviate is 75% with the wine volumetric concentration that eats wine, and other are with embodiment 5.
Claims (6)
1. the preparation method of turtle blood-activating blood stasis dispelling wind-damp dispelling wine is characterized in that may further comprise the steps:
A. the Radix Achyranthis Bidentatae of 3-40 weight portion De Di Bie, 5-20 weight portion, the Radix Saposhnikoviae of 3-16 weight portion, the Radix Glycyrrhizae of 3-16 weight portion, the Ramulus Cinnamomi of 3-16 weight portion, the Radix Paeoniae Alba of 5-20 weight portion, the Fructus Chaenomelis of 5-20 weight portion, the Rhizoma Cibotii of 5-20 weight portion, the Cortex Eucommiae powder of 5-20 weight portion are broken into coarser powder;
B. elder generation adds the gelatin of the 0.1-0.5% of medical material coarser powder amount, adds the edible wine of 20-30 times of medical material coarser powder amount wine volumetric concentration 5-45% again, and lixiviate is 1-4 time under the normal temperature and pressure, each 1-7 days, leaves standstill then and removes precipitation in 0.5-2 days; Perhaps add the edible wine of 20-30 times of medical material coarser powder amount wine volumetric concentration 50-75% in the medical material coarser powder, lixiviate is 1-4 time under the normal temperature and pressure, each 1-7 days, leaves standstill then and removes precipitation in 0.5-2 days;
C. the wine liquid of removing post precipitation adds precipitant after seasoning, again through stir, fine straining, last fill, sterilize product.
2. according to the preparation method of claims 1 described turtle blood-activating blood stasis dispelling wind-damp dispelling wine, it is characterized in that described precipitant is 50-75% and when not adding gelatin in the wine volumetric concentration, precipitant is selected from lixiviate with the tricalcium phosphate of the 0.3-0.8% of capacity for liquor and the active hargil of 0.3-0.8%.
3. according to the preparation method of claims 1 described turtle blood-activating blood stasis dispelling wind-damp dispelling wine, it is characterized in that described precipitant is that 5-45% and gelatin addition are when being the 0.1-0.5% of medical material coarser powder amount in the wine volumetric concentration, precipitant is selected from lixiviate with the tricalcium phosphate of the 0.3-0.8% of capacity for liquor and the active hargil of 0.3-0.8%, also comprises active carbon and the 0.1-0.4% kieselguhr of 0.3-0.8%.
4. according to the preparation method of claims 1 described turtle blood-activating blood stasis dispelling wind-damp dispelling wine, it is characterized in that described speed of agitator is 80-250r/min, mixing time is 0.5-2 hour.
5. according to the preparation method of claims 1 described turtle blood-activating blood stasis dispelling wind-damp dispelling wine, it is characterized in that described fine straining selects for use the flame filter press under the 0.1-0.3MPa to filter.
6. according to the preparation method of claims 1 described turtle blood-activating blood stasis dispelling wind-damp dispelling wine, it is characterized in that when wine volumetric concentration＜20%, selecting the gamma-radiation radiation sterilization for use.
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| CN2006100703712A CN101190277B (en) | 2006-11-29 | 2006-11-29 | Method for preparing stemmacantha uniflora blood circulation-activating, stasis-removing and wind-damp-expelling wine |
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| CN103223062A (en) * | 2013-04-25 | 2013-07-31 | 苏州谷力生物科技有限公司 | Rheumatism dispelling wine and preparation method thereof |
| CN103937648B (en) * | 2014-03-24 | 2015-08-19 | 烟台新时代健康产业有限公司 | A kind of dispel rheumatism health promoting wine promoting blood circulation and removing blood stasis and preparation thereof |
| CN104857402A (en) * | 2015-05-30 | 2015-08-26 | 孟钧 | Traditional Chinese medicine composition for treating ankylosing spondylitis |
| CN114224828B (en) * | 2022-01-17 | 2023-09-26 | 郝翠娟 | External ointment for treating bone pain and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1257715A (en) * | 1998-12-21 | 2000-06-28 | 任岩东 | Tincture for treating rheumatoid arthritis and its preparing process |
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| CN1257715A (en) * | 1998-12-21 | 2000-06-28 | 任岩东 | Tincture for treating rheumatoid arthritis and its preparing process |
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