CN105906309A - 一种仿古陶瓷及其制备方法 - Google Patents
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Abstract
本发明公开了一种仿古陶瓷及其制备方法，陶瓷胚体由以下重量份的原料制备而成：高岭土30‑40份、葛仙米粉5‑10份、碱土7‑15份、石英5‑7份、膨润土22‑30份、木鱼石粉1‑4份、蛇纹石粉10‑15份、叶腊石粉3‑6份、硼铝镁石粉4‑6份、AS树脂1‑3份、竹纤维1‑3份；所述的AS树脂的重均分子量为3‑10W，AN含量为20‑35％。本发明通过合理的胚料原料选择和配比，使得所得的陶瓷能呈现一种仿古的色彩，通过竹纤维和葛仙米发酵粉的引入，可以使得胚体表面呈现出不规则的纹路，装饰性强，同时制备工艺简单。
Description
技术领域
本发明涉及陶瓷制备领域，具体涉及一种仿古陶瓷及其制备方法。
背景技术
仿古瓷，是中国古代瓷器中一种带有鲜明时代特色的工艺现象，主要萌芽于两宋，形成于元代，成熟于明代，繁荣于清代前期，衰落于清代后期。总之，其基本上存在于中国古代瓷器发展的后半期，并对这一时期瓷器的发展进程起到了很大的促进作用，在中国古代瓷器中占有重要地位。
现有的仿古陶瓷普遍存在制备工艺复杂，所得工艺品装饰性差、颜色仿古性差的缺陷，且大多采用颜料进行上色，上色不均匀。
发明内容
为解决上述问题，本发明提供了一种仿古陶瓷及其制备方法，通过合理的胚料原料的选择和配比，使得所得的陶瓷能呈现一种仿古的色彩，通过竹纤维和葛仙米发酵粉的引入，可以使得胚体表面呈现出不规则的纹路，装饰性强，同时制备工艺简单。
为实现上述目的，本发明采取的技术方案为：
一种仿古陶瓷，陶瓷胚体由以下重量份的原料制备而成：
高岭土30-40份、葛仙米粉5-10份、碱土7-15份、石英5-7份、膨润土22-30份、木鱼石粉1-4份、蛇纹石粉10-15份、叶腊石粉3-6份、硼铝镁石粉4-6份、AS树脂1-3份、竹纤维1-3份；
所述的AS树脂的重均分子量为3-10W，AN含量为20-35％。
其中，所述葛仙米粉通过以下步骤制备所得：称取葛仙米20-30份置于汽爆罐内，先通入氮气至汽爆罐内压力为0.7-1.6MPa，爆破处理15-29min；然后迅速通入蒸汽至汽爆罐内压力为1.6-1.9MPa，蒸汽爆破处理1.1-3.3min，降温至室温后，低温烘干，得葛仙米粉。
上述一种仿古陶瓷的制备方法，包括如下步骤：
S1、按权利要求1所述的配方称取高岭土、葛仙米粉、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉、AS树脂、竹纤维，并将所称取的高岭土、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉混合后，以混合料∶球∶水重量比为1∶1.6∶0.7-0.9装入球磨设备，球磨1-2小时，将料浆陈腐24-36小时后过100-200目筛，得泥浆；
S2、将所得的泥浆与步骤S1称取的葛仙米粉、AS树脂、竹纤维置于高速搅拌机中搅拌5-30min后出料得到混浆料；
S3、将步骤S2所得的混合浆料注入模具，20-30min后脱模，取出坯体，烘干、修坯上水，得陶瓷泥坯体；
S4、将所得的陶瓷泥坯体浸入透明釉浆中6-15秒，使陶瓷泥坯体表面釉层的厚度达到3-10mm后，取出，干燥；
S5、将步骤S4所得的坯体装窑，氧化气氛下在200-800℃时每小时升温180-200℃，800-1100℃时每小时升温90-100℃，到达1000-1180℃时烧制1-2小时，转还原气氛，升温至1180-1230℃烧制0.5-1小时，停火降温，自然冷却，得到仿古陶瓷。
本发明具有以下有益效果：
通过合理的胚料原料的选择和配比，使得所得的陶瓷能呈现一种仿古的色彩；通过竹纤维和葛仙米发酵粉的引入，可以使得胚体表面呈现出不规则的纹路，装饰性强；通过低分子AS树脂的引入，增加了胚体材料的流动性，从而使得原料分散更加彻底和均匀；同时制备工艺简单。
具体实施方式
为了使本发明的目的及优点更加清楚明白，以下结合实施例对本发明进行进一步详细说明。应当理解，此处所描述的具体实施例仅仅用以解释本发明，并不用于限定本发明。
以下实施例中，所使用的AS树脂的重均分子量为3-10W，AN含量为20-35％，所使用的葛仙米粉通过以下步骤制备所得：称取葛仙米20-30份置于汽爆罐内，先通入氮气至汽爆罐内压力为0.7-1.6MPa，爆破处理15-29min；然后迅速通入蒸汽至汽爆罐内压力为1.6-1.9MPa，蒸汽爆破处理1.1-3.3min，降温至室温后，低温烘干，得葛仙米粉。
实施例1
S1、称取高岭土30份、葛仙米粉5份、碱土7份、石英5份、膨润土22份、木鱼石粉1份、蛇纹石粉10份、叶腊石粉3份、硼铝镁石粉4份、AS树脂1份、竹纤维1份，并将所称取的高岭土、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉混合后，以混合料∶球∶水重量比为1∶1.6∶0.7装入球磨设备，球磨1小时，将料浆陈腐24小时后过100目筛，得泥浆；
S2、将所得的泥浆与步骤S1称取的葛仙米粉、AS树脂、竹纤维置于高速搅拌机中搅拌5min后出料得到混浆料；
S3、将步骤S2所得的混合浆料注入模具，20min后脱模，取出坯体，烘干、修坯上水，得陶瓷泥坯体；
S4、将所得的陶瓷泥坯体浸入透明釉浆中6-15秒，使陶瓷泥坯体表面釉层的厚度达到3mm后，取出，干燥；
S5、将步骤S4所得的坯体装窑，氧化气氛下在200-800℃时每小时升温180-200℃，800-1100℃时每小时升温90-100℃，到达1000-1180℃时烧制1-2小时，转还原气氛，升温至1180-1230℃烧制0.5-1小时，停火降温，自然冷却，得到仿古陶瓷。
实施例2
S1、称取高岭土40份、葛仙米粉10份、碱土15份、石英7份、膨润土30份、木鱼石粉4份、蛇纹石粉15份、叶腊石粉6份、硼铝镁石粉6份、AS树脂3份、竹纤维3份，并将所称取的高岭土、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉混合后，以混合料∶球∶水重量比为1∶1.6∶0.9装入球磨设备，球磨2小时，将料浆陈腐36小时后过200目筛，得泥浆；
S2、将所得的泥浆与步骤S1称取的葛仙米粉、AS树脂、竹纤维置于高速搅拌机中搅拌30min后出料得到混浆料；
S3、将步骤S2所得的混合浆料注入模具，30min后脱模，取出坯体，烘干、俢坯上水，得陶瓷泥坯体；
S4、将所得的陶瓷泥坯体浸入透明釉浆中15秒，使陶瓷泥坯体表面釉层的厚度达到10mm后，取出，干燥；
S5、将步骤S4所得的坯体装窑，氧化气氛下在200-800℃时每小时升温180-200℃，800-1100℃时每小时升温90-100℃，到达1000-1180℃时烧制1-2小时，转还原气氛，升温至1180-1230℃烧制0.5-1小时，停火降温，自然冷却，得到仿古陶瓷。
实施例3
S1、称取高岭土35份、葛仙米粉7.5份、碱土11份、石英6份、膨润土26份、木鱼石粉2.5份、蛇纹石粉12.5份、叶腊石粉4.5份、硼铝镁石粉5份、AS树脂2份、竹纤维2份，并将所称取的高岭土、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉混合后，以混合料∶球∶水重量比为1∶1.6∶0.8装入球磨设备，球磨1.5小时，将料浆陈腐24-36小时后过150目筛，得泥浆；
S2、将所得的泥浆与步骤S1称取的葛仙米粉、AS树脂、竹纤维置于高速搅拌机中搅拌17.5min后出料得到混浆料；
S3、将步骤S2所得的混合浆料注入模具，25min后脱模，取出坯体，烘干、俢坯上水，得陶瓷泥坯体；
S4、将所得的陶瓷泥坯体浸入透明釉浆中6-15秒，使陶瓷泥坯体表面釉层的厚度达到6.5mm后，取出，干燥；
S5、将步骤S4所得的坯体装窑，氧化气氛下在200-800℃时每小时升温180-200℃，800-1100℃时每小时升温90-100℃，到达1000-1180℃时烧制1-2小时，转还原气氛，升温至1180-1230℃烧制0.5-1小时，停火降温，自然冷却，得到仿古陶瓷。
以上所述仅是本发明的优选实施方式，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明原理的前提下，还可以作出若干改进和润饰，这些改进和润饰也应视为本发明的保护范围。
Claims (3)
1.一种仿古陶瓷，其特征在于，陶瓷胚体由以下重量份的原料制备而成：
高岭土30-40份、葛仙米粉5-10份、碱土7-15份、石英5-7份、膨润土22-30份、木鱼石粉1-4份、蛇纹石粉10-15份、叶腊石粉3-6份、硼铝镁石粉4-6份、AS树脂1-3份、竹纤维1-3份；
所述的AS树脂的重均分子量为3-10W，AN含量为20-35％。
2.如权利要求1所述的一种仿古陶瓷，其特征在于，所述葛仙米粉通过以下步骤制备所得：称取葛仙米20-30份置于汽爆罐内，先通入氮气至汽爆罐内压力为0.7-1.6MPa，爆破处理15-29min；然后迅速通入蒸汽至汽爆罐内压力为1.6-1.9MPa，蒸汽爆破处理1.1-3.3min，降温至室温后，低温烘干，得葛仙米粉。
3.如权利要求1所述的一种仿古陶瓷的制备方法，其特征在于，包括如下步骤：
S1、按权利要求1所述的配方称取高岭土、葛仙米粉、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉、AS树脂、竹纤维，并将所称取的高岭土、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉混合后，以混合料∶球∶水重量比为1∶1.6∶0.7-0.9装入球磨设备，球磨1-2小时，将料浆陈腐24-36小时后过100-200目筛，得泥浆；
S2、将所得的泥浆与步骤S1称取的葛仙米粉、AS树脂、竹纤维置于高速搅拌机中搅拌5-30min后出料得到混浆料；
S3、将步骤S2所得的混合浆料注入模具，20-30min后脱模，取出坯体，烘干、修坯上水，得陶瓷泥坯体；
S4、将所得的陶瓷泥坯体浸入透明釉浆中6-15秒，使陶瓷泥坯体表面釉层的厚度达到3-10mm后，取出，干燥；
S5、将步骤S4所得的坯体装窑，氧化气氛下在200-800℃时每小时升温180-200℃，800-1100℃时每小时升温90-100℃，到达1000-1180℃时烧制1-2小时，转还原气氛，升温至1180-1230℃烧制0.5-1小时，停火降温，自然冷却，得到仿古陶瓷。
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| CN108395207A (zh) * | 2018-05-28 | 2018-08-14 | 钦州学院 | 仿古坭兴陶的制备方法 |
| CN111187056A (zh) * | 2020-01-14 | 2020-05-22 | 广西职业技术学院 | 一种仿古陶瓷工艺品的制备方法 |
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| CN107420796A (zh) * | 2017-08-08 | 2017-12-01 | 彭娟 | 一种埋地灯 |
| CN108395207A (zh) * | 2018-05-28 | 2018-08-14 | 钦州学院 | 仿古坭兴陶的制备方法 |
| CN111187056A (zh) * | 2020-01-14 | 2020-05-22 | 广西职业技术学院 | 一种仿古陶瓷工艺品的制备方法 |
| CN117819940A (zh) * | 2023-01-30 | 2024-04-05 | 山东百年技艺陶瓷艺术有限公司 | 一种含有木鱼石陶器的制备方法 |
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