CN105906309A - 一种仿古陶瓷及其制备方法 - Google Patents

一种仿古陶瓷及其制备方法 Download PDF

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CN105906309A
CN105906309A CN201610194225.4A CN201610194225A CN105906309A CN 105906309 A CN105906309 A CN 105906309A CN 201610194225 A CN201610194225 A CN 201610194225A CN 105906309 A CN105906309 A CN 105906309A
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董翠
赵文琰
何菲
李锋
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Jingdezhen Tongmen porcelain Co.,Ltd.
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Abstract

本发明公开了一种仿古陶瓷及其制备方法,陶瓷胚体由以下重量份的原料制备而成:高岭土30‑40份、葛仙米粉5‑10份、碱土7‑15份、石英5‑7份、膨润土22‑30份、木鱼石粉1‑4份、蛇纹石粉10‑15份、叶腊石粉3‑6份、硼铝镁石粉4‑6份、AS树脂1‑3份、竹纤维1‑3份;所述的AS树脂的重均分子量为3‑10W,AN含量为20‑35%。本发明通过合理的胚料原料选择和配比,使得所得的陶瓷能呈现一种仿古的色彩,通过竹纤维和葛仙米发酵粉的引入,可以使得胚体表面呈现出不规则的纹路,装饰性强,同时制备工艺简单。

Description

一种仿古陶瓷及其制备方法
技术领域
本发明涉及陶瓷制备领域,具体涉及一种仿古陶瓷及其制备方法。
背景技术
仿古瓷,是中国古代瓷器中一种带有鲜明时代特色的工艺现象,主要萌芽于两宋,形成于元代,成熟于明代,繁荣于清代前期,衰落于清代后期。总之,其基本上存在于中国古代瓷器发展的后半期,并对这一时期瓷器的发展进程起到了很大的促进作用,在中国古代瓷器中占有重要地位。
现有的仿古陶瓷普遍存在制备工艺复杂,所得工艺品装饰性差、颜色仿古性差的缺陷,且大多采用颜料进行上色,上色不均匀。
发明内容
为解决上述问题,本发明提供了一种仿古陶瓷及其制备方法,通过合理的胚料原料的选择和配比,使得所得的陶瓷能呈现一种仿古的色彩,通过竹纤维和葛仙米发酵粉的引入,可以使得胚体表面呈现出不规则的纹路,装饰性强,同时制备工艺简单。
为实现上述目的,本发明采取的技术方案为:
一种仿古陶瓷,陶瓷胚体由以下重量份的原料制备而成:
高岭土30-40份、葛仙米粉5-10份、碱土7-15份、石英5-7份、膨润土22-30份、木鱼石粉1-4份、蛇纹石粉10-15份、叶腊石粉3-6份、硼铝镁石粉4-6份、AS树脂1-3份、竹纤维1-3份;
所述的AS树脂的重均分子量为3-10W,AN含量为20-35%。
其中,所述葛仙米粉通过以下步骤制备所得:称取葛仙米20-30份置于汽爆罐内,先通入氮气至汽爆罐内压力为0.7-1.6MPa,爆破处理15-29min;然后迅速通入蒸汽至汽爆罐内压力为1.6-1.9MPa,蒸汽爆破处理1.1-3.3min,降温至室温后,低温烘干,得葛仙米粉。
上述一种仿古陶瓷的制备方法,包括如下步骤:
S1、按权利要求1所述的配方称取高岭土、葛仙米粉、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉、AS树脂、竹纤维,并将所称取的高岭土、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉混合后,以混合料∶球∶水重量比为1∶1.6∶0.7-0.9装入球磨设备,球磨1-2小时,将料浆陈腐24-36小时后过100-200目筛,得泥浆;
S2、将所得的泥浆与步骤S1称取的葛仙米粉、AS树脂、竹纤维置于高速搅拌机中搅拌5-30min后出料得到混浆料;
S3、将步骤S2所得的混合浆料注入模具,20-30min后脱模,取出坯体,烘干、修坯上水,得陶瓷泥坯体;
S4、将所得的陶瓷泥坯体浸入透明釉浆中6-15秒,使陶瓷泥坯体表面釉层的厚度达到3-10mm后,取出,干燥;
S5、将步骤S4所得的坯体装窑,氧化气氛下在200-800℃时每小时升温180-200℃,800-1100℃时每小时升温90-100℃,到达1000-1180℃时烧制1-2小时,转还原气氛,升温至1180-1230℃烧制0.5-1小时,停火降温,自然冷却,得到仿古陶瓷。
本发明具有以下有益效果:
通过合理的胚料原料的选择和配比,使得所得的陶瓷能呈现一种仿古的色彩;通过竹纤维和葛仙米发酵粉的引入,可以使得胚体表面呈现出不规则的纹路,装饰性强;通过低分子AS树脂的引入,增加了胚体材料的流动性,从而使得原料分散更加彻底和均匀;同时制备工艺简单。
具体实施方式
为了使本发明的目的及优点更加清楚明白,以下结合实施例对本发明进行进一步详细说明。应当理解,此处所描述的具体实施例仅仅用以解释本发明,并不用于限定本发明。
以下实施例中,所使用的AS树脂的重均分子量为3-10W,AN含量为20-35%,所使用的葛仙米粉通过以下步骤制备所得:称取葛仙米20-30份置于汽爆罐内,先通入氮气至汽爆罐内压力为0.7-1.6MPa,爆破处理15-29min;然后迅速通入蒸汽至汽爆罐内压力为1.6-1.9MPa,蒸汽爆破处理1.1-3.3min,降温至室温后,低温烘干,得葛仙米粉。
实施例1
S1、称取高岭土30份、葛仙米粉5份、碱土7份、石英5份、膨润土22份、木鱼石粉1份、蛇纹石粉10份、叶腊石粉3份、硼铝镁石粉4份、AS树脂1份、竹纤维1份,并将所称取的高岭土、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉混合后,以混合料∶球∶水重量比为1∶1.6∶0.7装入球磨设备,球磨1小时,将料浆陈腐24小时后过100目筛,得泥浆;
S2、将所得的泥浆与步骤S1称取的葛仙米粉、AS树脂、竹纤维置于高速搅拌机中搅拌5min后出料得到混浆料;
S3、将步骤S2所得的混合浆料注入模具,20min后脱模,取出坯体,烘干、修坯上水,得陶瓷泥坯体;
S4、将所得的陶瓷泥坯体浸入透明釉浆中6-15秒,使陶瓷泥坯体表面釉层的厚度达到3mm后,取出,干燥;
S5、将步骤S4所得的坯体装窑,氧化气氛下在200-800℃时每小时升温180-200℃,800-1100℃时每小时升温90-100℃,到达1000-1180℃时烧制1-2小时,转还原气氛,升温至1180-1230℃烧制0.5-1小时,停火降温,自然冷却,得到仿古陶瓷。
实施例2
S1、称取高岭土40份、葛仙米粉10份、碱土15份、石英7份、膨润土30份、木鱼石粉4份、蛇纹石粉15份、叶腊石粉6份、硼铝镁石粉6份、AS树脂3份、竹纤维3份,并将所称取的高岭土、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉混合后,以混合料∶球∶水重量比为1∶1.6∶0.9装入球磨设备,球磨2小时,将料浆陈腐36小时后过200目筛,得泥浆;
S2、将所得的泥浆与步骤S1称取的葛仙米粉、AS树脂、竹纤维置于高速搅拌机中搅拌30min后出料得到混浆料;
S3、将步骤S2所得的混合浆料注入模具,30min后脱模,取出坯体,烘干、俢坯上水,得陶瓷泥坯体;
S4、将所得的陶瓷泥坯体浸入透明釉浆中15秒,使陶瓷泥坯体表面釉层的厚度达到10mm后,取出,干燥;
S5、将步骤S4所得的坯体装窑,氧化气氛下在200-800℃时每小时升温180-200℃,800-1100℃时每小时升温90-100℃,到达1000-1180℃时烧制1-2小时,转还原气氛,升温至1180-1230℃烧制0.5-1小时,停火降温,自然冷却,得到仿古陶瓷。
实施例3
S1、称取高岭土35份、葛仙米粉7.5份、碱土11份、石英6份、膨润土26份、木鱼石粉2.5份、蛇纹石粉12.5份、叶腊石粉4.5份、硼铝镁石粉5份、AS树脂2份、竹纤维2份,并将所称取的高岭土、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉混合后,以混合料∶球∶水重量比为1∶1.6∶0.8装入球磨设备,球磨1.5小时,将料浆陈腐24-36小时后过150目筛,得泥浆;
S2、将所得的泥浆与步骤S1称取的葛仙米粉、AS树脂、竹纤维置于高速搅拌机中搅拌17.5min后出料得到混浆料;
S3、将步骤S2所得的混合浆料注入模具,25min后脱模,取出坯体,烘干、俢坯上水,得陶瓷泥坯体;
S4、将所得的陶瓷泥坯体浸入透明釉浆中6-15秒,使陶瓷泥坯体表面釉层的厚度达到6.5mm后,取出,干燥;
S5、将步骤S4所得的坯体装窑,氧化气氛下在200-800℃时每小时升温180-200℃,800-1100℃时每小时升温90-100℃,到达1000-1180℃时烧制1-2小时,转还原气氛,升温至1180-1230℃烧制0.5-1小时,停火降温,自然冷却,得到仿古陶瓷。
以上所述仅是本发明的优选实施方式,应当指出,对于本技术领域的普通技术人员来说,在不脱离本发明原理的前提下,还可以作出若干改进和润饰,这些改进和润饰也应视为本发明的保护范围。

Claims (3)

1.一种仿古陶瓷,其特征在于,陶瓷胚体由以下重量份的原料制备而成:
高岭土30-40份、葛仙米粉5-10份、碱土7-15份、石英5-7份、膨润土22-30份、木鱼石粉1-4份、蛇纹石粉10-15份、叶腊石粉3-6份、硼铝镁石粉4-6份、AS树脂1-3份、竹纤维1-3份;
所述的AS树脂的重均分子量为3-10W,AN含量为20-35%。
2.如权利要求1所述的一种仿古陶瓷,其特征在于,所述葛仙米粉通过以下步骤制备所得:称取葛仙米20-30份置于汽爆罐内,先通入氮气至汽爆罐内压力为0.7-1.6MPa,爆破处理15-29min;然后迅速通入蒸汽至汽爆罐内压力为1.6-1.9MPa,蒸汽爆破处理1.1-3.3min,降温至室温后,低温烘干,得葛仙米粉。
3.如权利要求1所述的一种仿古陶瓷的制备方法,其特征在于,包括如下步骤:
S1、按权利要求1所述的配方称取高岭土、葛仙米粉、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉、AS树脂、竹纤维,并将所称取的高岭土、碱土、石英、膨润土、木鱼石粉、蛇纹石粉、叶腊石粉、硼铝镁石粉混合后,以混合料∶球∶水重量比为1∶1.6∶0.7-0.9装入球磨设备,球磨1-2小时,将料浆陈腐24-36小时后过100-200目筛,得泥浆;
S2、将所得的泥浆与步骤S1称取的葛仙米粉、AS树脂、竹纤维置于高速搅拌机中搅拌5-30min后出料得到混浆料;
S3、将步骤S2所得的混合浆料注入模具,20-30min后脱模,取出坯体,烘干、修坯上水,得陶瓷泥坯体;
S4、将所得的陶瓷泥坯体浸入透明釉浆中6-15秒,使陶瓷泥坯体表面釉层的厚度达到3-10mm后,取出,干燥;
S5、将步骤S4所得的坯体装窑,氧化气氛下在200-800℃时每小时升温180-200℃,800-1100℃时每小时升温90-100℃,到达1000-1180℃时烧制1-2小时,转还原气氛,升温至1180-1230℃烧制0.5-1小时,停火降温,自然冷却,得到仿古陶瓷。
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