CN105902461A - Essence containing snail mucus extracts and preparation method thereof - Google Patents
Essence containing snail mucus extracts and preparation method thereof Download PDFInfo
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- CN105902461A CN105902461A CN201610311786.8A CN201610311786A CN105902461A CN 105902461 A CN105902461 A CN 105902461A CN 201610311786 A CN201610311786 A CN 201610311786A CN 105902461 A CN105902461 A CN 105902461A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/618—Molluscs, e.g. fresh-water molluscs, oysters, clams, squids, octopus, cuttlefish, snails or slugs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
Abstract
The invention relates to essence containing snail mucus extracts. A recipe of the essence comprises the following raw material ingredients in percentage by weight: 1 percent to 4.0 percent of snail slime extracts, 1 percent to 4.0 percent of centella extracts, 2.5 percent to 7 percent of humectants, 1.1 percent to 2.2 percent of thickening agents, 0.01 percent to 0.15 percent of neutralizing agents and the balance de-ionized water. The essence has the advantages that the efficient scar restoration capability can be shown under the condition of low concentration of skin restoration active ingredients in the essence; the wound heeling is accelerated; the skin elasticity improving function and the skin energy improving function are added; the essence can be widely used for the restoration of easy-allergy skin, beatified skin, skin with pimples or injured skin caused by other reasons.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of essence containing Limax pituitary extract and preparation side thereof
Method.
Background technology
Along with the continuous deterioration of air quality, during in air, the ozone of excess reduces skin, vitamin C and vitamin E contains
Amount so that lipid peroxidation increases;Vehicle exhaust and polycyclic aromatic hydrocarbon, increase oxidative stress and cell injury;In air floating
Pollutant, it is easy to enter pore, heavy damage cuticular update cycle and speed;Consumer use in poor quality cosmetic or
After cosmetic surgery, there are a series of skin problems such as skin damage, sensitivity, wound infection, skin follow the string in skin.These
The performance of skin problem is as follows:
1, after cosmetic surgery, there are the skin problems such as cicatrix, pigmentation, wound infection in skin.
2, cutaneous sensibility increases, and is very easy to occur anaphylaxis, erythema occurs, play red point, the allergic symptom such as itch.
3, skin is lackluster, flexibility decrease, senilism, corse sweat pore, long coarse wool etc..
4, melanin is abnormal calm, and the colour of skin is obscure, and spot colors is deepened, and microgroove increases.
In this case, develop a have reparation cicatrix, accelerate wound healing, increase skin elasticity and improve flesh
The product of the height gentleness of skin vigor just becomes the most urgent.
Summary of the invention
In order to solve the above-mentioned problems in the prior art, the invention provides a kind of essence containing Limax pituitary extract
China's liquid, its formula is contained repairs the active component of skin at very low concentrations, just shows efficient cicatrix reparation, accelerates wound
Mouth healing, increase skin elasticity and the function of raising skin vigor, can be widely used for the skin after easy allergy skin, beauty treatment and repair
Again, the impaired skin that the skin of long pox or other reason cause.
As follows in order to realize the technical scheme that above-mentioned technical purpose used:
A kind of essence containing Limax pituitary extract, the formula of described essence includes following in percentage by weight
Material component: Limax pituitary extract 1%~4.0%;Herba Centellae extract 1%~4.0%;Wetting agent 2.5~7%;Thickening
Agent 1.1%~2.2%;Nertralizer 0.01%~0.15%;Deionized water surplus.
Further, the formula of described essence the most also includes following material component to the present invention: anti-
Quick dose 1.0~2.5%.
Further, the formula of described essence the most also includes following material component to the present invention:
Preservative 0.3%~1.0%.
Preferably, described wetting agent is selected from HANSHENGJIAO, glycerol, pantothenylol and the one or two in base hexyl glycerol
Plant above material.
Specifically, described wetting agent is selected from HANSHENGJIAO, glycerol, pantothenylol and base hexyl glycerol, and the most each component is in elite
Content in formula of liquid is in percentage by weight: HANSHENGJIAO 0.01%~0.2%;Glycerol 2.0%~6.0%;Pantothenylol
0.1%~0.8%;Base hexyl glycerol 0.05%~0.1%.
Preferred as one, described thickening agent is selected from carbomer and/or butanediol.
Specifically, described thickening agent is carbomer and butanediol, and in essence formula, its content is according to percentage by weight
Meter is respectively as follows: carbomer 0.01%~0.15%, butanediol 1.0%~2.0%.
Preferably, described anti-sensitizer is trehalose;Described preservative is caprylyl glycol;Described nertralizer is amino-propanediol.
Another technical purpose of the present invention is to provide the preparation method of the above-mentioned essence containing Limax pituitary extract, including
Following steps:
1), each component materials is weighed by formula;
2), by HANSHENGJIAO, carbomer glycerol moistening, it is subsequently adding in aqueous phase pot, opens stirring, be subsequently adding fourth two
Alcohol, is warming up to 80 DEG C~90 DEG C, is incubated 10~15 minutes, until being completely dissolved;Its vacuum is sucked in emulsifying pot and stirs
Mixing, mixing speed is maintained at 300~350 revs/min, then low speed homogenizing 5~10 minutes;
3), amino-propanediol is added step 2) described in emulsifying pot in, stir evenly, and be cooled to 45~50 DEG C;
4), Limax pituitary extract, Herba Centellae extract are sequentially added into step 3) in gained emulsifying pot, stir evenly;Stirring
When being cooled to less than 40 DEG C, adding base hexyl glycerol, caprylyl glycol, homogenizing also stirs evenly;It is down to discharging when 30~35 DEG C.
Beneficial effects of the present invention:
Compared with prior art, the essence containing Limax pituitary extract of the present invention has the advantages that
1, inventive formulation with the addition of natural origin, uses that smudge cells technology separates, rich in asiatic acid and hydroxyl
Base asiatic acid, asiaticoside and the Herba Centellae extract of asiaticoside isoreactivity composition, can participate in normal wound
In repair process, mainly protect the healing into wound by increase I-type collagen, the inflammation produced by inflammatory mediator can be suppressed
The factor.Herba Centellae extract has outstanding healing of wound and cicatrix repair, and its reason is that asiaticoside has promotion body
Interior collage synthesis and new vascular generation, stimulate the important function such as granulation growth, so beneficially wound healing.As at skin wound
The upper continuous administration preparation containing asiaticoside, can prevent wound infection from suppurating, and shortens wound healing time, it is possible to decrease skin hardness
With improve skin-nourishing, the effect of enhancing metabolism.
2, in product Limax pituitary extract contain collagen protein, elastin, chondroitin sulfate, allantoin, glycolic,
Natural antibacterial peptide, vitamin, calcium, ferrum, copper, phosphorus, etc. the nutrient substance wanted of multiple needed by human body.Use cryogenic high pressure difference Multistage Membranes
Isolation technics, have Glycerin, repair skin injury, promote wound healing, stimulate cell regeneration, horny layer softening albumin layer,
Help the skin efficacy effect to aspects such as free radical resistings, may be used for prevention and improve cicatrix.
3, the present invention uses two kinds of active component with obvious skin repair effect, and Herba Centellae extract is plant origin
, another kind is animal origin, and the different types of active skull cap components of both is organically combined, and can produce between them
Raw synergistic function.Asiaticoside in described Herba Centellae extract can effectively facilitate skin in Limax pituitary extract
The absorption of collagen component, thus be greatly improved collagen protein effect to skin repair.
4, the essence containing Limax pituitary extract of the present invention can keep skin young, fine and smooth, makes skin tight and rich
Flexible.
5, the essence containing Limax pituitary extract of the present invention can micro-stripping skin, enhance metabolism, prevent skin
The appearance of problem;Glycolic, also known as hydroxyacetic acid, glycolic acid, is simplest 'alpha '-hydroxy acids.It can be easy to penetrate into skin
Inside skin, solve the problems such as skin aging, wrinkle, black speck, skin sore at short notice.
6, the product of the present invention does not contains emulsifying agent and surfactant, is the suspension thick stabilization system of a kind of uniqueness, it
Without dioxane, without mineral origin composition, without pigment, without essence, the safety of formula system is high, can be generally applicable
In all kinds of skin quality and various people.
Detailed description of the invention
In order to make the object, technical solutions and advantages of the present invention definitely, below the preferred embodiments of the present invention are entered
The description that row is detailed.The content of each component in following embodiment calculates with percentage by weight, and unit of weight can be thousand
Gram or kilogram." the Limax pituitary extract L " that the Limax pituitary extract of the present invention produces purchased from Guangzhou network victory.The present invention's is long-pending
Snow grass extract is purchased from BIOSPECTRUM company of Korea S, its trade name HerbEx Centella ExtractTM。
One, the formula of the essence containing Limax pituitary extract
Table 1 embodiment 1~5 essence and the formula of reference examples 1
Two, the preparation method of the essence containing Limax pituitary extract
The essence preparation method containing Limax pituitary extract of the present invention, its step is as follows:
1). each component raw material of formula is weighed according to table 1.
2). by the HANSHENGJIAO in component A, carbomer glycerol moistening, it is subsequently adding in aqueous phase pot, opens stirring, successively
Add other remaining component A, be warming up to 80 DEG C, be incubated 10 minutes, until being completely dissolved.The mixing speed of emulsifying pot is maintained at
300 revs/min, component A is sucked by vacuum, low speed (speed is) homogenizing 5 minutes.
3). the raw material of B component is added in emulsifying pot, open stirring, mix and be cooled to 45 DEG C.
4). component C is sequentially added in emulsifying pot, stirs evenly;Stirring cooling 35~40 DEG C, adds D component, and homogenizing also stirs
Even;Being down to discharging when 35 DEG C, it is qualified to check, discharging fill.
Comparative example 1 uses the identical preparation method of embodiment 1~5.
Three, measure of merit
1. cicatrix repairs efficacy assessments
Cicatrix reparation evaluation methodology:
1) study subject: embodiment 1~5.
2) negative control: commercially available famous brand name scar rehabilitating solution.
3) experimenter: 240 cicatrixes repair patient, age 18~40 years old, these cicatrixes reparation patient patient are divided at random
Becoming two groups, four groups of experimenter's qualifications and record of service are basically identical, without significant difference, have a comparability:
A, treatment group 40 example, wherein male 22 example, women 18 example, mild scar 15 example, moderate 12 example, severe 13 example, scar
Average 6.5 years of age;
B, treatment group 40 example, wherein male 21 example, women 19 example, mild scar 14 example, moderate 13 example, severe 13 example, scar
Average 6.3 years of age;
C, treatment group 40 example, wherein male 20 example, women 20 example, mild scar 16 example, moderate 11 example, severe 13 example, scar
Average 6.7 years of age;
D, treatment group 40 example, wherein male 22 example, women 18 example, mild scar 15 example, moderate 11 example, severe 14 example, scar
Average 6.7 years of age;
E, treatment group 40 example, wherein male 19 example, women 21 example, mild scar 16 example, moderate 11 example, severe 13 example, scar
Average 6.6 years of age;
F, matched group 40 example, wherein male 23 example, women 17 example, mild scar 16 example, moderate 12 example, severe 12 example, scar
Average 6.6 years of age;
4) product is used
A, treatment group patient use the essence (embodiment 1~5) of the present invention, at clear water cleaning cicatrix, dry, incite somebody to action this
Invention essence uniform application is in affected part, and with referring to that abdomen is massaged into essence gently and fully absorbs, every day uses once, uses continuously
Three months.
B, matched group patient use commercially available famous brand name scar rehabilitating solution, at clear water cleaning cicatrix, dry, by this
Bright essence uniform application is in affected part, with referring to that abdomen is massaged into ointment gently and fully absorbs medication every day once, and medication three months.
5) efficacy determination:
Effective: after medication one month, cicatrix is the most thin out, medication three months, cicatrix is repaired completely;
Effective: after medication one month, cicatrix is the most thin out, is continuing with, and cicatrix take a favorable turn and is not but wholly absent;
Invalid: after medication one month, cicatrix is without significant change.
6), experimental result is as shown in table 2:
Table 2 cicatrix repairing effect test result
Conclusion: clinical treatment outcome shows, the therapeutic effect of embodiment 3~5, total effective rate will apparently higher than reference examples 1,
Also apparently higher than the embodiment 1~2 of use single component (containing only Limax pituitary extract L or only containing Herba Centellae extract),
It can be seen that the effect repairing cicatrix of the essence of the art of this patent is far superior to commercially available famous brand name cicatrix reparation
Liquid.
2, Product Safety assessment
Product safety evaluation methodology:
1), study subject: embodiment 1~5
2), negative control: reference examples 1
3), experimenter: totally 30 people, age 18~40 years old, sensitivity skin crowd.
4), speckle method for testing: select qualified speckle examination device, with closed patch test method, by tested material about 0.02ml~
0.025ml is applied in speckle examination device, and external special adhesive tape is pasted on experimenter's forearm song side, removes tested material, in going after 24 hours
Except 30min after tested material speckle examination device, after impression disappears, observe dermoreaction, by " cosmetics health specification " (version in 2007)
Dermoreaction grade scale records its result.
5), evaluation of result:
Table 3 skin adverse reaction grade scale
6), result of the test:
Table 4 cosmetics human skin patch result
Human skin patch result shows:
1), in embodiment 3~5,30 subjects skin's the most negative (grading system: 0 grade).According to " changing
Cosmetic hygienic practice " (version in 2007) human body skin class patch test criterion, sample to human body without skin adverse reaction.
A, embodiment 3~5 are compared with embodiment 1~2, reference examples 1, and embodiment 3~5 shows higher safety, i.e.
Make using the crowd at sensitive skin, any abnormal response does not the most occur;
B and individually contain sample i.e. embodiment 1 or the embodiment 2 of Herba Centellae extract or Limax pituitary extract, all
Occur in that the untoward reaction of a few example;
C, embodiment 1 are compared with reference examples 1, and embodiment 1 shows higher safety and mildness.
Obviously, the above embodiment of the present invention is only for clearly demonstrating example of the present invention, and is not right
The restriction of embodiments of the present invention.For those of ordinary skill in the field, the most also may be used
To make other changes in different forms.Here cannot all of embodiment be given exhaustive.Every belong to this
What bright technical scheme was extended out obviously changes or changes the row still in protection scope of the present invention.
Claims (9)
1. the essence containing Limax pituitary extract, it is characterised in that the formula of described essence is according to percentage by weight
Count and include following material component: Limax pituitary extract 1%~4.0%;Herba Centellae extract 1%~4.0%;Wetting agent 2.5
~7%;Thickening agent 1.1%~2.2%;Nertralizer 0.01%~0.15%;Deionized water surplus.
Essence the most according to claim 1, it is characterised in that the formula of described essence the most also wraps
Include following material component: anti-sensitizer 1.0~2.5%.
Essence the most according to claim 1, it is characterised in that the formula of described essence the most also wraps
Include following material component: preservative 0.3%~1.0%.
4. according to essence described in any one in claims 1 to 3, it is characterised in that described wetting agent is selected from HANSHENGJIAO, sweet
Oil, pantothenylol and one or more the material in base hexyl glycerol.
Essence the most according to claim 4, it is characterised in that described wetting agent is selected from HANSHENGJIAO, glycerol, pantothenylol and base
Hexyl glycerol, the most each component content in essence formula is in percentage by weight: HANSHENGJIAO 0.01%~
0.2%;Glycerol 2.0%~6.0%;Pantothenylol 0.1%~0.8%;Base hexyl glycerol 0.05%~0.1%.
6. according to essence described in any one in claim 5, it is characterised in that described thickening agent selected from carbomer and/or
Butanediol.
7. according to essence described in any one in claim 6, it is characterised in that described thickening agent is carbomer and fourth two
Alcohol, in essence formula, its content is respectively as follows: carbomer 0.01%~0.15%, butanediol in percentage by weight
1.0%~2.0%.
8. according to essence described in any one in claim 7, it is characterised in that described anti-sensitizer is trehalose;Described anti-
Rotten agent is caprylyl glycol;Described nertralizer is amino-propanediol.
9. the preparation method preparing the essence containing Limax pituitary extract as claimed in claim 8, it is characterised in that
Comprise the following steps:
1), each component materials is weighed by formula;
2), by HANSHENGJIAO, carbomer glycerol moistening, it is subsequently adding in aqueous phase pot, opens stirring, be subsequently adding butanediol, rise
Temperature, to 80 DEG C~90 DEG C, is incubated 10~15 minutes, until being completely dissolved;Its vacuum sucked in emulsifying pot and is stirred, stirring
Mix speed and be maintained at 300~350 revs/min, then low speed homogenizing 5~10 minutes;
3), amino-propanediol is added step 2) described in emulsifying pot in, stir evenly, and be cooled to 45~50 DEG C;
4), Limax pituitary extract, Herba Centellae extract are sequentially added into step 3) in gained emulsifying pot, stir evenly;Stirring cooling
During to less than 40 DEG C, adding base hexyl glycerol, caprylyl glycol, homogenizing also stirs evenly;It is down to discharging when 30~35 DEG C.
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CN106333917A (en) * | 2016-10-09 | 2017-01-18 | 上海兰葹生物科技有限公司 | Dendrobium nobile skin regeneration promotion combination essence |
CN106389293A (en) * | 2016-11-26 | 2017-02-15 | 上海兰葹生物科技有限公司 | Dendrobium huoshanense-containing combined essence capable of promoting skin regeneration |
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