CN105886166B - A kind of sweet wormwood wax Manual perfumed soap and preparation method thereof - Google Patents
A kind of sweet wormwood wax Manual perfumed soap and preparation method thereof Download PDFInfo
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- CN105886166B CN105886166B CN201610253521.7A CN201610253521A CN105886166B CN 105886166 B CN105886166 B CN 105886166B CN 201610253521 A CN201610253521 A CN 201610253521A CN 105886166 B CN105886166 B CN 105886166B
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- sweet wormwood
- soap
- wax
- wormwood wax
- soap base
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- 235000001405 Artemisia annua Nutrition 0.000 title claims abstract description 158
- 240000000011 Artemisia annua Species 0.000 title claims abstract description 158
- 239000000344 soap Substances 0.000 title claims abstract description 143
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 229930101531 artemisinin Natural products 0.000 claims abstract description 49
- BLUAFEHZUWYNDE-NNWCWBAJSA-N artemisinin Chemical compound C([C@](OO1)(C)O2)C[C@H]3[C@H](C)CC[C@@H]4[C@@]31[C@@H]2OC(=O)[C@@H]4C BLUAFEHZUWYNDE-NNWCWBAJSA-N 0.000 claims abstract description 48
- 239000000341 volatile oil Substances 0.000 claims abstract description 36
- 229960004191 artemisinin Drugs 0.000 claims abstract description 28
- 229930183339 qinghaosu Natural products 0.000 claims abstract description 20
- 229930002875 chlorophyll Natural products 0.000 claims abstract description 11
- 235000019804 chlorophyll Nutrition 0.000 claims abstract description 11
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 claims abstract description 11
- 239000000126 substance Substances 0.000 claims abstract description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 239000007788 liquid Substances 0.000 claims description 21
- 239000012452 mother liquor Substances 0.000 claims description 17
- 238000010438 heat treatment Methods 0.000 claims description 15
- 239000002904 solvent Substances 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 14
- 238000005406 washing Methods 0.000 claims description 11
- 239000004615 ingredient Substances 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 claims description 7
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 claims description 7
- 244000025254 Cannabis sativa Species 0.000 claims description 7
- 244000178870 Lavandula angustifolia Species 0.000 claims description 7
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims description 7
- 229940116229 borneol Drugs 0.000 claims description 7
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 claims description 7
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 claims description 7
- 239000000284 extract Substances 0.000 claims description 7
- 239000001102 lavandula vera Substances 0.000 claims description 7
- 235000018219 lavender Nutrition 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 238000002844 melting Methods 0.000 claims description 6
- 230000008018 melting Effects 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 6
- 230000008569 process Effects 0.000 claims description 6
- 241000196324 Embryophyta Species 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 240000005153 Dodonaea viscosa Species 0.000 claims description 2
- AVFIYMSJDDGDBQ-UHFFFAOYSA-N Parthenium Chemical compound C1C=C(CCC(C)=O)C(C)CC2OC(=O)C(=C)C21 AVFIYMSJDDGDBQ-UHFFFAOYSA-N 0.000 claims 2
- 241001495454 Parthenium Species 0.000 claims 2
- 230000000694 effects Effects 0.000 abstract description 23
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 9
- 230000001954 sterilising effect Effects 0.000 abstract description 8
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 8
- 230000003110 anti-inflammatory effect Effects 0.000 abstract description 4
- 230000008901 benefit Effects 0.000 abstract description 3
- 239000001993 wax Substances 0.000 description 62
- 239000002585 base Substances 0.000 description 34
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- 238000004140 cleaning Methods 0.000 description 9
- 239000012153 distilled water Substances 0.000 description 9
- 238000000605 extraction Methods 0.000 description 6
- 238000009835 boiling Methods 0.000 description 5
- 241000894006 Bacteria Species 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 238000007792 addition Methods 0.000 description 4
- 239000000155 melt Substances 0.000 description 4
- 230000001151 other effect Effects 0.000 description 4
- 238000007127 saponification reaction Methods 0.000 description 4
- 229910002027 silica gel Inorganic materials 0.000 description 4
- 239000000741 silica gel Substances 0.000 description 4
- 229960001866 silicon dioxide Drugs 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 230000003255 anti-acne Effects 0.000 description 3
- 230000001139 anti-pruritic effect Effects 0.000 description 3
- 239000003908 antipruritic agent Substances 0.000 description 3
- 238000004090 dissolution Methods 0.000 description 3
- 239000006210 lotion Substances 0.000 description 3
- 230000003020 moisturizing effect Effects 0.000 description 3
- 238000010257 thawing Methods 0.000 description 3
- 208000002874 Acne Vulgaris Diseases 0.000 description 2
- 240000001851 Artemisia dracunculus Species 0.000 description 2
- 241000233866 Fungi Species 0.000 description 2
- 206010040943 Skin Ulcer Diseases 0.000 description 2
- 206010000496 acne Diseases 0.000 description 2
- 239000011149 active material Substances 0.000 description 2
- 230000000202 analgesic effect Effects 0.000 description 2
- 230000000157 blood function Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000005202 decontamination Methods 0.000 description 2
- 230000003588 decontaminative effect Effects 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 230000002500 effect on skin Effects 0.000 description 2
- 238000010828 elution Methods 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 230000001815 facial effect Effects 0.000 description 2
- 239000003292 glue Substances 0.000 description 2
- 239000008236 heating water Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000001114 myogenic effect Effects 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- 239000003507 refrigerant Substances 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- 230000029663 wound healing Effects 0.000 description 2
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 241000282461 Canis lupus Species 0.000 description 1
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 206010015150 Erythema Diseases 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 235000019501 Lemon oil Nutrition 0.000 description 1
- 235000006679 Mentha X verticillata Nutrition 0.000 description 1
- 235000002899 Mentha suaveolens Nutrition 0.000 description 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 1
- 241000192041 Micrococcus Species 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 241000233872 Pneumocystis carinii Species 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 241000607762 Shigella flexneri Species 0.000 description 1
- 241000223996 Toxoplasma Species 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000000078 anti-malarial effect Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 239000003430 antimalarial agent Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 238000003763 carbonization Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- BLUAFEHZUWYNDE-XRNKLDBLSA-N chembl77 Chemical compound C([C@@](OO1)(C)O2)C[C@H]3[C@H](C)CC[C@@H]4C31[C@@H]2OC(=O)[C@@H]4C BLUAFEHZUWYNDE-XRNKLDBLSA-N 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 239000000469 ethanolic extract Substances 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 230000001408 fungistatic effect Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 244000000013 helminth Species 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 239000000077 insect repellent Substances 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 239000010501 lemon oil Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000001525 mentha piperita l. herb oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- 235000019477 peppermint oil Nutrition 0.000 description 1
- 230000035755 proliferation Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 231100000241 scar Toxicity 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- ZISJLHQNEVGTIU-RFEYTNPVSA-M sodium 4-oxo-4-[[(1R,4S,5R,8S,9R,10S,12R,13R)-1,5,9-trimethyl-11,14,15,16-tetraoxatetracyclo[10.3.1.04,13.08,13]hexadecan-10-yl]oxy]butanoate Chemical compound [Na+].C[C@@H]1CC[C@H]2[C@@H](C)[C@H](OC(=O)CCC([O-])=O)O[C@@H]3O[C@@]4(C)CC[C@@H]1[C@@]23OO4 ZISJLHQNEVGTIU-RFEYTNPVSA-M 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000013076 target substance Substances 0.000 description 1
- 239000012178 vegetable wax Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/12—Soft surfaces, e.g. textile
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of sweet wormwood wax Manual perfumed soap and preparation method thereof, the sweet wormwood wax Manual perfumed soap includes sweet wormwood volatile oil, sweet wormwood wax soap base, the components such as Artemisinin；Wherein sweet wormwood wax soap base is the substance for being saponified sweet wormwood wax, and the Artemisinin mainly includes qinghaosu and chlorophyll.Preparation process of the present invention is simple, efficient, takes full advantage of the various active principles in sweet wormwood, has saved a large amount of cost, has the effects that significantly sterilization, antibacterial, skin care, anti-inflammatory.
Description
Technical field
The present invention relates to perfumed soaps, the especially technical field of sweet wormwood wax Manual perfumed soap.
Background technique
Artemisinin, especially qinghaosu have significant Antimalarial, while also having antitumor, anti-erythema wolf
Sore, other helminths such as anti-schistosome, toxoplasma, Pneumocystis carinii, Paragonismus westermani, derivative sodium artesunate is to gold
Grape, shigella flexneri, Escherichia coli, micrococcus catarrhalis, A type and Bacillus paratyphosus B have certain antibacterial action, together
When qinghaosu to inhibit scar proliferation it is inhibited.
Because qinghaosu has above-mentioned effect, apply it to washing, washing can be significantly improved in skincare product, skin care is used
The sterilization of product and health-care effect, but sweet wormwood is focused primarily upon in preparing washing and skincare product containing Artemisinin at present
Element extract and purification after the method that is added, and a large amount of active materials are led to using less to the other ingredients contained in sweet wormwood
It is wasted.
Part in the prior art utilizes the extract in other sweet wormwoods in addition to qinghaosu, such as Chinese patent Shen
The application and sweet wormwood bacterium-suppressing shower lotion of a kind of Artemisinin in bath article please be disclosed in CN101461770A, wherein making
With sweet wormwood ethanol extract, decocting liquid or sweet wormwood volatile oil, but above-mentioned technical proposal is in practical applications, and sweet wormwood ethyl alcohol extracts
Object extracted amount is few, and active principle separation is difficult；And active material qinghaosu is substantially free of in sweet wormwood decocting liquid, it is difficult to reach compared with
Good antibacterial, skin effect；Likewise, or directly use sweet wormwood volatile oil, though have certain fungistatic effect, effect compared with
Qinghaosu is poor, while lacking the skin effect of qinghaosu.
Summary of the invention
A kind of efficiently using the active principle in sweet wormwood it is an object of the present invention to proposing, antibacterial, desinsection, skin care are imitated
The outstanding sweet wormwood wax Manual perfumed soap of fruit, the second object of the present invention are to propose the preparation method of the Manual perfumed soap.
Technical scheme is as follows:
A kind of sweet wormwood wax Manual perfumed soap comprising following components: sweet wormwood volatile oil, sweet wormwood wax soap base, Artemisinin；Its
Middle sweet wormwood wax soap base is the substance for being saponified sweet wormwood wax, and the Artemisinin mainly includes qinghaosu and chlorophyll.
Wherein the sweet wormwood wax soap base is the substance for being saponified sweet wormwood wax, and the sweet wormwood wax is the vegetable wax of sweet wormwood,
Sweet wormwood wax is typically as the waste in qinghaosu extraction in the prior art；The Artemisinin be mainly qinghaosu with
On the one hand chlorophyll, Determination of Chlorophyll of the present invention are used as natural coloring agent, can increase beautiful color for perfumed soap obtained, another
Aspect can also be cooperateed with qinghaosu, provided anti-inflammatory, promoted wound healing, anti-skin ulcer, promote to increase the effectiveness of blood function, can be with
Understand, the present invention actually includes directly using qinghaosu and chlorophyll replacing as the Artemisinin in the application
For the technical solution of substance, and must not necessarily be obtained and being extracted to sweet wormwood.
A kind of preferred embodiment of the sweet wormwood wax Manual perfumed soap are as follows: further include in the sweet wormwood wax Manual perfumed soap A, B,
C, one of five kinds of D, E compositions or a variety of, in which:
A: conventional soap base and/or neat soap；
B: borneol；
C: essence；
D: glycerol；
E: plants essential oil.
Wherein, the conventional soap base and/or neat soap are the general soap base and/or neat soap that can directly buy in the market, such as
Conventional Transparent soap base or white soap base can carry out unrestricted choice according to the quality of the perfumed soap intentionally got when prepared by reality.
On the one hand the effect of borneol in the technical solution is that refrigerant, faint scent effect, another party can be increased for perfumed soap
Its effect of face can mutually be cooperateed with qinghaosu, chlorophyll, can bring desinsection, myogenic, the new effects of analgesic, to enhance the function of perfumed soap
Effect, expands the application range of perfumed soap.
The plants essential oil is the aromatic substance being obtained by extraction from plant, such as Lavender, Rosa Damascana, lemon
Oil, peppermint oil etc., can in conjunction with sweet wormwood volatile oil isoreactivity substance after generate synergistic effect, expand the application of perfumed soap
The effect of range, raising perfumed soap.
Another preferred embodiment of the sweet wormwood wax Manual perfumed soap are as follows: the sweet wormwood wax Manual perfumed soap includes with the following group
Point: conventional soap base and/or neat soap 70%-88.9%, sweet wormwood volatile oil 0.5%-1%, sweet wormwood wax soap base 10%-30%, Artemisinin
0.5%-1%, essence 0.1%-0.3%.
The preferred embodiment is especially suited as underwear soap, and irritation is small, but has significant decontamination, sterilization effect
Fruit can effectively clean fungi, bacterium on underwear, and the clothing after washing has antibacterial effect.
Another preferred embodiment of the sweet wormwood wax Manual perfumed soap are as follows: the Manual perfumed soap includes soap base and/or neat soap
85%-96%, sweet wormwood volatile oil 0.5%-1%, sweet wormwood wax soap base 1%-15%, Artemisinin 0.5%-1%, glycerol 1%-5%, lavender
Essential oil 0.1%-0.5%, essence 0.1%-0.3%.
The preferred embodiment is especially suited as bath soap, can fungi, bacterium effectively on cleaning skin, and there is skin to stop
Itch, the effect of mosquito repellent.
Another preferred embodiment of the sweet wormwood wax Manual perfumed soap are as follows: the sweet wormwood wax Manual perfumed soap includes with the following group
Point: soap base and/or neat soap 90%-96%, sweet wormwood volatile oil 0.5%-1%, sweet wormwood wax soap base 1%-5%, Artemisinin 0.5%-1%,
Glycerol 1%-5%, Lavender 0.1%-0.5%, essence 0.1%-0.3%.
The preferred embodiment is especially suited as face cleaning perfumed soap, has cleaning, moisturizing, anti-acne, goes acne print and other one
The effect of a little facial skin diseases.
Present invention simultaneously discloses a kind of preparation methods of sweet wormwood wax Manual perfumed soap, comprising the following steps:
(1) Artemisinin is extracted from sweet wormwood grass using edible alcohol；
(2) sweet wormwood grass is extracted using solvent naphtha, obtained extracting solution is separated, by oil obtained in separation
Shape liquid is concentrated to arrive sweet wormwood mother liquor；
(3) sweet wormwood mother liquor is rinsed using vapor, the steam escaped in steam flush is condensed into liquid, then will
The liquid carries out water-oil separating, obtains the sweet wormwood volatile oil for being mixed with a small amount of solvent naphtha, and liquid is released after being heated to get blueness is arrived
Wormwood artemisia volatile oil；
(4) the sweet wormwood mother liquor cooling by steam washing is obtained into the sweet wormwood wax and water of solid, is arrived after separating water into
Sweet wormwood wax；
(5) obtained sweet wormwood wax is saponified to get sweet wormwood wax soap base is arrived；
(6) the sweet wormwood volatile oil, Artemisinin will be sequentially added after the soap base ingredient heating and melting in perfumed soap,
If there are also other components afterwards, other components are added, are formed after mixing to get the sweet wormwood wax Manual perfumed soap is arrived；
The soap base ingredient is sweet wormwood wax soap base, or conventional soap base and/or neat soap and sweet wormwood wax soap base.
In above-mentioned steps (2), solvent naphtha is further preferably No. 6 solvent naphthas.
It is mostly the method by the distillation of the water of high temperature or solvent extraction to the extraction of sweet wormwood volatile oil in the prior art, wherein
Solvent extraction will increase complicated solvent separating step, significantly increase product cost, while increase the quality peace of product
Full hidden danger, and be mutually mixed using water distillation Shi Shuiyu wax, it is very easy to the phenomenon that viscous pot occur, on the one hand can reduce subsequent
Separating effect, on the other hand glue pot wax will appear carbonization, cause mass loss, in addition, also be container recycling
Puzzlement is brought, cleaning cost is increased, and in the technical program, step has used steam to be rinsed in (3), and steam is not
Largely, it directly, is muchly mixed into mother liquor, the phenomenon that viscous pot occurs after leading to water, wax mixing.
In above-mentioned steps (3) when being separated solvent naphtha with sweet wormwood volatile oil, the temperature of the heating is preferably 60 ~
95 DEG C, the loss its object is to can sufficiently vapor away solvent naphtha, without causing sweet wormwood volatile oil.
Saponification described in step (5), which refers to the process of, to react after target substance and water and highly basic mixing, the technical program
Middle highly basic is more preferably sodium hydroxide, and compared with potassium hydroxide, calcium hydroxide etc., obtained perfumed soap quality is more preferable.
The technical program step is saponified further preferred embodiment described in (5) are as follows: distilled water is added by several times mixed
Have in the sweet wormwood wax of highly basic, and non-disposable all additions, distilled water 200ml is such as measured first, after sodium hydroxide dissolution is added,
Sweet wormwood wax is weighed again, and heating makes its boiling, after being saponified 2h, then 200ml distilled water is added into beaker and continues to be saponified 3h；This is preferably
The purpose of embodiment is addition water by several times, and alkali concentration is higher when can make to be saponified for the first time, is conducive to the progress of saponification, and
Thereafter the addition of water can promote the progress of reaction, and as far as possible reduce the mixture ph obtained after reaction, can save auxiliary
The dosage of material and reduce cost.
The other preferred embodiment of the preparation method are as follows: the temperature of heating described in the step (6) is 50 ~ 100 DEG C.
Conventional heating method can be used when heated, it is possible to use microwave stove heating.
Another preferred embodiment of the preparation method are as follows: the process that vapor described in the step (3) is rinsed
Are as follows: sweet wormwood mother liquor is fitted into tank, enters vapor in tank from tank bottom thereafter, is escaped from tank top, continues 1 ~ 2h.
The invention has the benefit that
(1) present invention takes full advantage of the various active principles in sweet wormwood, has significant sterilization, antibacterial, skin care, disappears
The effects of inflammation, expelling parasite；
(2) present invention passes through the addition of qinghaosu wax soap base, not only increases sterilization, antibacterial, skin care, anti-inflammatory of perfumed soap etc.
Effect, while by this meeting abandoned in qinghaosu extraction process or using the sweet wormwood wax of more complicated method separation and Extraction again
It is applied in the perfumed soap using simple method, reduces the manufacturing cost of perfumed soap, improve the utilization rate of sweet wormwood grass, simultaneously
The effect of also enhancing perfumed soap；
(3) chlorophyll in Artemisinin is utilized in the present invention simultaneously, and one side can dye for perfumed soap, on the other hand
It can also be cooperateed with qinghaosu, anti-inflammatory is provided, promotes wound healing, anti-skin ulcer, promote to increase the effectiveness of blood function；
(4) it joined borneol in the preferred embodiment of the present invention, one side is that refrigerant, faint scent can be increased for perfumed soap
Effect, on the other hand its effect can mutually be cooperateed with qinghaosu, chlorophyll, desinsection, myogenic, the new effects of analgesic can be brought,
The effect of enhancing perfumed soap expands the application range of perfumed soap；
(5) present invention simultaneously propose the sweet wormwood wax Manual perfumed soap of three kinds of different component ratios, because its component ratio not
Together, the effect of stressing is different, can be used as underwear soap, facial soap, bath soap respectively and uses；
(6) method for using steam flush to the extraction of sweet wormwood volatile oil in preparation method of the invention, steam is from blueness
Enter below wormwood artemisia mother liquor, top evolution, a large amount of, directly, muchly will not be mixed into mother liquor, causes to glue after there is water, wax mixing
The phenomenon that pot；
(7) preparation process of the present invention is simple, and preparation continuity, universality are good, significantly reduces production cost, significantly improves
Product quality.
Specific embodiment
In the following, the present invention will be further described in detail by way of specific embodiments, but this should not be interpreted as to the present invention
Range be only limitted to example below.Without departing from the idea of the above method of the present invention, according to ordinary skill
The various replacements or change that knowledge and customary means are made, should be included in the scope of the present invention.
Embodiment 1
Artemisinin, sweet wormwood wax soap base and the preparation of sweet wormwood volatile oil:
(1) sweet wormwood hay 50g is weighed in 500ml conical flask, the edible alcohol 100ml that purity is 95% is added, with 75 DEG C
Heating water bath, heat 1h after obtain extracting solution, extracting solution is concentrated to get lotion, as Artemisinin, predominantly blueness
Artemisin and chlorophyll；
(2) sweet wormwood grass is extracted using No. 6 solvent naphthas, obtained extracting solution is separated by silicagel column, it should
Process is also referred to as upper liquid, from upper liquid to elution during, oily liquids can be flowed out in silicagel column, be concentrated to get
To sweet wormwood mother liquor；
(3) sweet wormwood mother liquor is fitted into tank, enters vapor in tank from tank bottom thereafter, escaped from top, this process is
For steam washing, continue 1h, the steam that will escape out is condensed into liquid, then the liquid is carried out water-oil separating, obtains being mixed with a small amount of 6
It is heated at 100 DEG C and releases liquid after 0.5h to get to sweet wormwood volatile oil by the sweet wormwood volatile oil of number solvent naphtha；
(4) by by the sweet wormwood mother liquor natural cooling of steam washing, the sweet wormwood wax and water of solid are obtained after cooling, by moisture
From after to get arrive sweet wormwood wax；
(5) it measures distilled water 200ml and 8g sodium hydroxide to be added in 500ml beaker, after its dissolution, weighs 40g sweet wormwood
Wax is added in beaker, and heating makes its boiling, carries out saponification 2h, and 200ml distilled water is added into beaker again thereafter and continues to be saponified 3h,
Thereafter 200ml distilled water is added, and makes its boiling, 30g sodium chloride is eventually adding and obtained sweet wormwood wax soap base is washed,
The pH value of cleaning solution is detected, until to get to the sweet wormwood wax soap base that can be used directly when it is near neutral (pH=7 ~ 8).
Embodiment 2
Artemisinin, sweet wormwood wax soap base and the preparation of sweet wormwood volatile oil:
(1) sweet wormwood hay 50g is weighed in 500ml conical flask, the edible alcohol 100ml that purity is 95% is added, with 80 DEG C
Heating water bath 1h after obtain extracting solution, extracting solution is concentrated to get lotion, as Artemisinin, be mainly qinghaosu and
Chlorophyll；
(2) sweet wormwood grass is extracted using No. 6 solvent naphthas, obtained extracting solution is separated by silicagel column, from
During upper liquid to elution, oily liquids can be flowed out in silicagel column, be concentrated to get sweet wormwood mother liquor is arrived；
(3) sweet wormwood mother liquor is fitted into tank, enters vapor in tank from tank bottom thereafter, escaped from top, this process is
For steam washing, continue 1.5h, the steam that will escape out is condensed into liquid, then the liquid is carried out water-oil separating, obtains being mixed with few
The sweet wormwood volatile oil for measuring No. 6 solvent naphthas releases liquid after it to be heated to 1h at 60 DEG C to get sweet wormwood volatile oil is arrived；
(4) by by the sweet wormwood mother liquor natural cooling of steam washing, the sweet wormwood wax and water of solid are obtained after cooling, by moisture
From after to get arrive sweet wormwood wax；
(5) it measures distilled water 200ml and 8g sodium hydroxide to be added in 500ml beaker, after its dissolution, weighs 40g sweet wormwood
Wax is added in beaker, and heating makes its boiling, carries out saponification 2h, and 200ml distilled water is added into beaker again thereafter and continues to be saponified 3h,
Thereafter 200ml distilled water is added, and makes its boiling, 30g sodium chloride is eventually adding and obtained sweet wormwood wax soap base is washed,
The pH value of cleaning solution is detected, until to get to the sweet wormwood wax soap base that can be used directly when it is near neutral.
Embodiment 3:
The preparation of sweet wormwood wax Manual perfumed soap:
Transparent soap base 94g is weighed, is cut into small pieces, heating and melting in container is put into, until embodiment is added after it melts completely
Sweet wormwood wax soap base 1g made from 1 sequentially adds sweet wormwood volatile oil made from embodiment 1 to its thawing and after mixing evenly
0.5g, Artemisinin 1g and Lavender 0.3g, borneol 0.5g, glycerol 2g, lemon extract 0.2g, stir evenly, pour into
In mould of soap, it is cooled and shaped to get sweet wormwood wax Manual perfumed soap is arrived, this perfumed soap has especially suitable for taking a shower and sterilizes, is anti-
Bacterium, antipruritic and other effects.
Embodiment 4:
The preparation of sweet wormwood wax Manual perfumed soap:
Transparent soap base 87g is weighed, is cut into small pieces, heating and melting in container is put into, until embodiment is added after it melts completely
Sweet wormwood wax soap base 20g made from 1 sequentially adds sweet wormwood volatile oil made from embodiment 1 to its thawing and after mixing evenly
1g, Artemisinin 1g, flavoring rose essence 0.3g, stir evenly, pour into mould of soap, are cooled and shaped to get sweet wormwood wax hand is arrived
Work perfumed soap, this perfumed soap have very strong cleaning decontamination, sterilization, antibacterial and other effects especially suitable for underwear washing.
Embodiment 5:
The preparation of sweet wormwood wax Manual perfumed soap:
Transparent soap base 93g is weighed, is cut into small pieces, heating and melting in container is put into, until being sequentially added after it melts completely
It is sweet wormwood volatile oil 0.5g, Artemisinin 1g and Lavender 0.4g made from embodiment 2, borneol 0.5g, glycerol 4g, thin
Lotus essence 0.2g, stirs evenly, pours into mould of soap, is cooled and shaped to get sweet wormwood wax Manual perfumed soap is arrived, this perfumed soap is applicable in
In face cleaning, there is sterilization, antibacterial, antipruritic, moisturizing, anti-acne and other effects.
Embodiment 6:
The preparation of sweet wormwood wax Manual perfumed soap:
Transparent soap base 90g is weighed, is cut into small pieces, heating and melting in container is put into, until being sequentially added after it melts completely
Sweet wormwood wax soap base 4g made from embodiment 2 adds sweet wormwood volatile oil made from embodiment 2 to its thawing and after mixing evenly
0.5g, Artemisinin 1g and Lavender 0.4g, borneol 0.5g, glycerol 4g, Mint Essence 0.2g, stir evenly, pour into
In mould of soap, it is cooled and shaped to get sweet wormwood wax Manual perfumed soap is arrived, this perfumed soap has sterilization, suppression especially suitable for face cleaning
Bacterium, antipruritic, moisturizing, anti-acne, acne print and other effects, and its curative effect compared with embodiment 5 sweet wormwood wax Manual perfumed soap more preferably.
Claims (8)
1. a kind of preparation method of sweet wormwood wax Manual perfumed soap, it is characterised in that: it includes preparation step below:
(1) Artemisinin is extracted from sweet wormwood grass using edible alcohol；
(2) sweet wormwood grass is extracted using solvent naphtha, obtained extracting solution is separated, by oily liquid obtained in separation
Body is concentrated to arrive sweet wormwood mother liquor；
(3) sweet wormwood mother liquor is rinsed using vapor, the steam escaped in steam flush is condensed into liquid, then by the liquid
Body carries out water-oil separating, obtains the sweet wormwood volatile oil for being mixed with a small amount of solvent naphtha, and liquid is released after being heated and is waved to get to sweet wormwood
Hair oil；
(4) the sweet wormwood mother liquor cooling by steam washing is obtained into the sweet wormwood wax and water of solid, arrives sweet wormwood after separating water into
Wax；
(5) obtained sweet wormwood wax is saponified to get sweet wormwood wax soap base is arrived；
(6) the sweet wormwood volatile oil, Artemisinin will be sequentially added after the soap base ingredient heating and melting in perfumed soap, thereafter again
Other components are added, are formed after mixing to get the sweet wormwood wax Manual perfumed soap is arrived；
The soap base ingredient is sweet wormwood wax soap base, or conventional soap base and/or neat soap and sweet wormwood wax soap base；
And the sweet wormwood wax Manual perfumed soap consists of the following compositions: sweet wormwood volatile oil, sweet wormwood wax soap base, Artemisinin, and under
State one of five kinds of A, B, C, D, E compositions or a variety of:
A: conventional soap base and/or neat soap；
B: borneol；
C: essence；
D: glycerol；
E: plants essential oil；
Wherein the content of the sweet wormwood volatile oil is 0.5 ~ 1%, and the content of the sweet wormwood wax soap base is 1 ~ 30%, and the sweet wormwood extracts
The content of object is 0.5 ~ 1%, when in the sweet wormwood wax Manual perfumed soap containing conventional soap base and/or when neat soap, conventional soap base and/or
The content of neat soap is 70 ~ 96%, and the gross mass of the ingredient is 100%, and wherein sweet wormwood wax soap base is what sweet wormwood wax was saponified
Substance, the Artemisinin mainly include qinghaosu and chlorophyll.
2. the preparation method of sweet wormwood wax Manual perfumed soap according to claim 1, it is characterised in that: the sweet wormwood wax is fragrant by hand
Soap includes following components: conventional soap base and/or neat soap 70%-88.9%, sweet wormwood volatile oil 0.5%-1%, sweet wormwood wax soap base 10%-
30%, Artemisinin 0.5%-1%, essence 0.1%-0.3%, and the gross mass of the ingredient is 100%.
3. the preparation method of sweet wormwood wax Manual perfumed soap according to claim 1, it is characterised in that: the sweet wormwood wax is fragrant by hand
Soap includes following components: conventional soap base and/or neat soap 85%-96%, sweet wormwood volatile oil 0.5%-1%, sweet wormwood wax soap base 1%-15%, green
Total matter of parthenium extract 0.5%-1%, glycerol 1%-5%, Lavender 0.1%-0.5%, essence 0.1%-0.3%, and the ingredient
Amount is 100%.
4. the preparation method of sweet wormwood wax Manual perfumed soap according to claim 1, it is characterised in that: the sweet wormwood wax is fragrant by hand
Soap includes following components: conventional soap base and/or neat soap 90%-96%, sweet wormwood volatile oil 0.5%-1%, sweet wormwood wax soap base 1%-5%, blueness
Total matter of parthenium extract 0.5%-1%, glycerol 1%-5%, Lavender 0.1%-0.5%, essence 0.1%-0.3%, and the ingredient
Amount is 100%.
5. a kind of preparation method of sweet wormwood wax Manual perfumed soap according to claim 1, it is characterised in that: the step (2)
Described in solvent naphtha be No. 6 solvent naphthas.
6. a kind of preparation method of sweet wormwood wax Manual perfumed soap according to claim 1, it is characterised in that: the step (3)
Described in heating temperature be 60 ~ 95 DEG C.
7. a kind of preparation method of sweet wormwood wax Manual perfumed soap according to claim 1, it is characterised in that: the step (6)
Described in heating temperature be 50 ~ 100 DEG C.
8. a kind of preparation method of sweet wormwood wax Manual perfumed soap according to claim 1, it is characterised in that: the step (3)
Described in the process that is rinsed of vapor are as follows: sweet wormwood mother liquor is fitted into tank, enters vapor in tank from tank bottom thereafter, from
Tank top evolution, continues 1 ~ 2h.
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Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106726663A (en) * | 2017-03-14 | 2017-05-31 | 四川蓝伯特生物科技股份有限公司 | A kind of sweet wormwood bacteriostatic hand sanitizer |
| CN106726789A (en) * | 2017-03-14 | 2017-05-31 | 四川蓝伯特生物科技股份有限公司 | A kind of sweet wormwood bacterium-suppressing shower lotion and preparation method thereof |
| CN109337770A (en) * | 2018-11-12 | 2019-02-15 | 重庆菩璞生物科技有限公司 | A kind of sweet wormwood soap composition |
| CN109609283A (en) * | 2018-12-27 | 2019-04-12 | 广西仙草堂制药有限责任公司 | A kind of purification sweet wormwood wax and preparation method thereof |
| CN112812120A (en) * | 2019-11-15 | 2021-05-18 | 中华全国供销合作总社南京野生植物综合利用研究所 | Method for extracting chlorophyll from artemisinin leftovers |
| CN112812893A (en) * | 2019-11-15 | 2021-05-18 | 中华全国供销合作总社南京野生植物综合利用研究所 | Method for extracting plant wax from artemisinin leftovers |
| CN111088127B (en) * | 2019-12-31 | 2021-05-04 | 广西仙草堂制药有限责任公司 | Artemisia apiacea handmade soap and preparation method thereof |
| CN111616987A (en) * | 2020-05-28 | 2020-09-04 | 郑州中科新兴产业技术研究院 | Artemisia apiacea wax oil mosquito-repellent, antibacterial, disinfectant and skin-care water-free hand sanitizer and preparation method thereof |
| CN112694953A (en) * | 2020-12-28 | 2021-04-23 | 张家港威胜生物医药有限公司 | Sweet wormwood soap and preparation method thereof |
| CN113186045A (en) * | 2021-04-21 | 2021-07-30 | 禹州市天源生物科技有限公司 | Preparation method of sweet wormwood essential oil soap |
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