CN104513737A - Transparent water lily flower handmade soap and method for manufacturing same - Google Patents

Abstract

The invention relates to a piece of transparent water lily flower handmade soap and a method for manufacturing the same. The handmade soap comprises effective components of natural vegetable oil such as water lily flower oil, tea tree oil, olive oil, coconut oil and palm oil, and is refined through a series of processes under the function of ethanol. According to the invention, the handmade soap contains a low content of an alkaline component, can be used for a long term with no dry skin and skin peeling and with no damage to weak-acid environment of the skin. The handmade soap contains pigment and spice, which are natural components of plants themselves, have a mild smell, can nourish skin, can protect skin in normal physiological environment, and are safe and stable. The handmade soap is transparent and unique, and can be manufactured according to people's favor and image, so that the soap is converted from a soap having a single washing function into an artistic work for appreciation, and the compound multi-functional water lily flower art handmade soap can be used for washing hands and resisting bacteria. The handmade soap is particularly suitable for women and people who have skin allergy, has good quality, provides fine, dense and stable foam, and makes the body smooth after people use the handmade soap.

Description

Transparent oral shui solution handmade soap and making thereof

technical fieldthe present invention relates to a kind of transparent oral shui solution handmade soap and making thereof, its effective constituent adopts water lily caul-fat, tea tree oil, sweet oil, Oleum Cocois, palm wet goods crude vegetal, under the effect of ethanol, refines form through series of process.In the market as handmade soap related products, tinkling of jadesly to meet the eye on every side, kind is general many, the impact of performance but differs, and effective constituent mostly is chemical high grease and high bases etc., and its efficiency is low, poor stability, toxic, corrodibility and irritating smell, there is certain damage to skin, add the peculiar smell of chemosynthesis essence, cannot select to make perfumed soap according to the skin properties of oneself.The present invention due to alkaline components low, life-time service, can not make xerosis cutis peeling to skin, and meanwhile, the slightly acidic environment in skin also can not be destroyed; Contained pigment and spices are the natural component of plant itself, taste is light, nourishes rough skin, keep skin normal physiological context, safety and stability, owing to being transparent individual character handmade soap, allow people according to oneself imagination and make the handmade soap oneself liked, wash one's hands single, be transformed into and view and admire and artistic work, and the composite multifunction oral shui solution of sterilization again while washing one's hands art handmade soap.Be particularly suitable for women and allergic crowd use, because quality is good, fine and smooth, tight and stable foam during use, can be produced, very salubrious with rear somatosensory.

background technologythe Shennong Bencaojing of Han dynasty is listed in Chinese honey locust, this very general plant of umbellate pore furgus medicinal already.Containing saponin in Chinese honey locust, its aqueous solution energy foam generated, has detergency ability.Afterwards, people further mashed the Chinese honey locust eliminating seed, did glomeration, size as orange, for washing one's face, ablution, were commonly called as " soap group ".Its making method is also described: " October adopts pod, boils and mashes, and ball made by fine flour and all perfume (or spice), bath body face de-sludging and greasy profit is better than Chinese honey locust also in the Compendium of Materia Medica of Ming Dynasty's LI Shi-Zhen." compare with present perfumed soap, also quite similar in shape system.The Qianjin Yao Fang of the Tang Dynasty SUN Si miao and Qianjin Yi Fang were once recorded multiple " bath beans " for " face of washing one's hands " and were manufactured formula, mostly will use the various bean flour such as " white peas or beans face ", " finishing bean flour ", " soybean end ".As can be seen from these formulas, the smalls that bath beans are ground into using bean or pea is exactly as major ingredient, and the making of " bath beans " is very exquisite, and except beans end, also will use pig pancreas, Chinese honey locust etc., to strengthen the effect of scale removal of deoiling, in addition, precious spices is essential especially.After this all Raw material processing process, dry, be pounded loose end, be finely incorporated into together, must finished product.Umbellate pore furgus is the more rich talent's, has added a little spices in umbellate pore furgus, has stronger fragrance after using.On the Process ba-sis making bath beans, in pig pancreas process of lapping, add noisy sugar, and replace bean powder with soda ash, then add the lard after melting and spices etc., evenly, compacting balling-up or bulk.The perfumed soap of its chemical constitution and today is similar to.Along with the rise of modern industry, severe environmental pollution, particularly chemical article bring catastrophic pollution to the earth, and people are difficult to cleaning ambient and the health of oneself more.Handmade soap is natural, has a lot of advantages, and shortcoming is exactly softer, and facilitation is adjusted, and can not use for a long time.This is because the shortcoming of handmade soap that natural fats and oils is made.Generally speaking, in most cases, a lot of producer selects some ways like this: the ratio improving hard oil: as: improve Oleum Cocois, palmitic content, the shortcoming of this way is exactly: hard oil may make the soap of working it out more irritant at high proportion, responsive people may experience, so a lot of formula all considers the ratio limiting hard oil.Irritant too after Oleum Cocois, plam oil, theobroma oil equivalent height, responsive people also may experience, so, generally limit.Handmade soap is also called " art designing's soap " or " processing soap ", and the soap that soap base does belongs to the hot method for making of what.Its benefit is that the soapmaking time is short, namely does and namely uses.Shortcoming is destroyed under continuous high temperature in a lot of nutrition of what.They cause with industrial " soap base " or " neat soap " processing, soap base is ready-made large soap blank, as long as it is chopped up post-heating thawing, reverse mould, cools just shaping at once can using, unacceptable words energy repetitiousness heating and melting, because be very easy to make, become children art designing's thing. certainly also add other additives, in order to make soap transparent when producing soap base, just add alcohol, but alcohol can make the skin universe dry.As everyone knows, real handmade soap is not because naturally add sanitas, and the shelf time is shorter, preservation condition is comparatively harsh, and not resembling commercially available chemical industry chemistry perfumed soap can preservation year in year out.Many natural components and the moisturizing grease having neither part nor lot in saponification, therefore, perfumed soap will be left in shady and cool dry place at ordinary times, the moist composition in soap soap just can be fresh-keeping.Object of the present invention overcomes deficiency as above, handmade soap is designed to industrial art individual character transparent soap, can according to individual creation make mould, tile oral shui solution soap handmade soap in the heart, by the product of washing one's hands, be transformed into do it yourself make, happy play in arts and crafts entertaining handmade soap works.For gift, makeup, children special-purpose product and allergic crowd use, select materials 80% be natural, matter is measured, the green product belonging to nontoxic, non-stimulated, corrosion-free, have no side effect without irritated, colorless and odorless, there is disinfecting skin-care, taste dispelled in good stability, sterilization, carry with, convenient and practical, fine and smooth, tight and stable foam can be produced, with the product of the features such as rear somatosensory is very salubrious during use.

summary of the inventionmain points of the present invention are to select suitable component, and carry out rational mixture, through refining, saponification, saltout, wash, arrange and continue to process the handmade soap into different process art form again.

The formula that the present invention selects following (component and weight percent % thereof): water lily caul-fat 20-30; Tea tree oil 10-15; Sweet oil 10-15; Oleum Cocois 10-15; Plam oil 40-50; Triple pressed stearic acid 3-4; The cured 3-4 of honey; Laurylamide diethanolamine 1.0-2.0; Sodium hydroxide 5.0-10.0; Sodium-chlor 5.0-10.0; Ethanol 3-4; Water 10.0-15.0.

The DNA purity of water lily caul-fat water lily procyanidins is 98%, and the oligomer of water lily pycnogenols is the highest, and water lily pycnogenols is the most easily absorbed, and activity is also larger.Pycnogenols (OPC) is a kind of new and effective antioxidant, is very strong free-radical scavengers, has very strong activity in vivo.Experiment proves, the Green Tea Extract oxidation capacity of OPC is 50 times of vitamin-E, ascorbic 20 times.The foeign elements such as the makeup of dirty air, the injury of UV sunlight have activated free radical, allow skin suffer the attack of more polyradical at nominal conditions.Free radical is attacked and is destroyed in cell processes, cause cell mortality and metabolism disorder, in cell, impurity metabolism cannot go out body rubber, cause pigment deposition, and dead aged cells has increased the weight of the color of skin, make gloomy skin matt, and dead cell makes cell tissue division growth speed slow down, a large amount of economization of neonatal cell quantity (neonatal cell be skin U.S. important factor).

Tea tree oil tea tree Tea tree decontamination effect improving is excellent, improves the suppuration phenomenon of wound infection, and furuncle and carbuncle.Remove varicella and the little small pox caused by zoster and unclean part, scalp overdrying and dandruff can be treated.

Sweet oil sweet oil is rich in the squalene splendid with skin avidity and essential fatty acid, absorbs rapidly, effectively keeps skin elasticity with moist; Monounsaturated fatty acids contained abundant in sweet oil and vitamin-E, K, A, D etc. and phenols antioxidant, facial wrinkles can be eliminated, prevent skin aging, there is the effect such as skin or hair care and control hand and foot from chapping, be the cosmetics and skincare product that can " eat ", smear skin with sweet oil in addition and can resist ultraviolet and prevent skin carcinoma.Because sweet oil contains polyphenol and lipopolysaccharide components, so sweet oil also has radiation-resistant function, therefore sweet oil is often used to the food making cosmonaut.Computer user is often made more to regard it as the good merchantable brand of health-care and skin-care.Before long-time use computer, with sweet oil massage face and canthus, also can reach identical effect by using the Articles for shower being rich in sweet oil.

The principal constituent of Oleum Cocois Oleum Cocois is that other greases are compared and had very large specificity, Oleum Cocois saponification value is very high, and refractive index is very low, can differentiate whether Oleum Cocois is mixed with other greases by this method, even can be quantitative, this change is mainly made up of the lipid acid of Oleum Cocois and causes.In the lipid acid composition of Oleum Cocois, saturated content reaches more than 90%, but fusing point only has 24-27 degree, and this is due to the high reason of carbonic acid content.This is also the reason that Polenske value and Reichert-Meissl value are high.The reason that complete hydrogenation is very little on the fusing point impact of Oleum Cocois can also be explained from the lipid acid composition of Oleum Cocois.

The refined palm oil of plam oil industrial application, requires that fusing point is not less than 44 DEG C.In developed country, a large amount of plam oil is applied to industrial circle.In China, industrial plam oil has the title of " industrial monosodium glutamate ", can see that its application is extensively completely.In addition, along with rising steadily of crude oil price in recent years, bio-fuel-oil receives publicity day by day, and plam oil also can produce biofuel, and this may become the new growing point of its Future Consumption.Palmitic industrial use mainly divides two classes: a class can directly obtain from plam oil, as soap class, epoxy palm oil and polyvalent alcohol thereof, urethane and polyacrylic ester series products; An other class is oil and fat chemical series products, as lipid acid, ester, fatty alcohol, nitrogenous compound and glycerine, on the basis of this several prods, can also be produced various derived product by different chemical modes.The main raw material of oil and fat chemical is rich in the grease of length in C12-C14 and C16-C18 carbochain, and wherein palm-kernel oil, palm stearin, palmitinic acid are all main raw materials.

In the little Individual existence what nature of stearic acid (Stearic Acid), not synthetics, often exist with the form of glyceryl ester, exist in the most of vegeto-animal grease of what, particularly in butter, storage is the abundantest.Theobroma oil and missible oil wood fruit fat all containing have an appointment about 40% stearic acid.Add the stearic acid of 3%, about wait what to add theobroma oil or the stearic acid amount of missible oil wood fruit contained by fat of 7.5%.Pure stearic acid melting point 69.4 DEG C, stearic acid is organic acid, therefore can work with bases, generates sodium stearate, just becomes a kind of soap.Stearic acid saponification value 0.1412, INS197.Also can buy in present chemical industry shop from plant, the vegetalitas stearic acid such as extract.When stearic acid one is to manufacture, the number of times of final stage squeezing represents, as single pressure, two pressures, three pressures, three pressures less containing oleic acid, so the qualities of three pressures are best, the quality of single pressure is the poorest, the purity about 99% of three pressures, melting point 55.2 DEG C.Stearic acid is not easily melted into water and is not suitable for being added in liquid soap.

The present invention has following soapmaking base technique: the basic chemical reaction of soap preparing process is that grease and alkali interaction generate soap and glycerine, and the soap of reaction gained, after saltouing, wash, arranging, is called soap base, then continues to process the soap into different commercial form.1) refining: except the impurity in degrease.Refining process comprises de-clear and bright, alkali refining (depickling) decolouring.Come unstuck is except colloids such as the phosphatide in degrease.The Main Function of alkali refining is to remove the free fatty acids in grease, but owing to generating cotton-shaped soap, absorption and the pigment that eliminates in grease and impurity;

2) saponification: carry out saponification reaction with alkali after oil and fat refining.Boiling process is main method for saponification, and soap pot is cylindrical.Except being furnished with the transport pipe of grease, alkali lye, water, salt solution etc., open steam or steam coils are also housed, to pass into steam and to stir evenly soap stock.The bottom of a pan is tapered, under have vomit pipe to release to shake the head pipe discharge after remaining raffinate.Grease and caustic soda boil and reach about 95% to saponification degree in soap pot, stop saponification operation when soap stock is uniform closure state.　　

3) saltout: in closed soap stock, with salt, soap is separated with rare glycerol liquor.Closed soap glue is after saltouing, and the soap on upper strata is called neat soap; The glycerol liquor of underlying band salt is discharged from soap pot bottom, to reclaim glycerine.　　

4) washing: after separating waste liquid, adds water and steam boils neat soap, and making it becomes even soap glue by analysing open state, washes out residual glycerine, pigment and impurity.　

5) alkali is analysed: for making grease residual in neat soap fully saponified, analyse the glycerine washed out further in neat soap, salt, pigment and impurity through alkali.The minimum paper mill wastewater that half spent lye is separated out completely is called half spent lye threshold concentration.　　

6) arrange: adjustment alkali analyses rear neat soap Inner electrolysis matter and fatty acid content, reduces impurity, improves color and luster, obtain and maximum go out soap rate and up-to-standard soap base.

7) shaping: soap base is condensed into large cake soap plate, then cuts into soap base.

One-tenth soap step of the present invention:

1) the molding bone external fixation system of alternative gypsum, fully biodegradable, namely plasticity-is had in 55 ~ 70 DEG C of warm water, safety, convenient, clean, no side effects, can the external immobilization material of reusable new medical, make difform mould according to individual character, interior deposited heat resistant plastice film;

2) first soap base is cut into small pieces, puts into thermally resistant container;

3). put on the heating such as microwave oven apparatus and heat about 60 seconds, allow soap base melt completely, in addition water lily anthocyanidin in the soap base liquid of fusing, ethanol by soap base liquid agitation, until melt completely, to transparence;

4). soap base liquid to be poured in the individual character mould made at this by reverse mould, and cooling in about 20 to 30 minutes is formed;

5) demoulding transparent soap demoulding, the mould of the external immobilization material of new medical can be reused.

Feature of the present invention has following precaution:

1) seeing whether soap face has small bubbles because soap base, when melting mould, is easy to bubbling, so cooling rear surface just has short grained bubble, after entering mould, spraying alcohol make lather collapse.

2). soap base is exactly watery after melting, and can not experience the thick thick stage, so can precipitate.Except certain special rendering effect.

3). cut soap soap and see jelly effect.If layering soap, the soap soap two pieces of so soap base processing is easy to come off separately, and one day after lancing, these depths clearly level will be desalinated gradually and disappear.And the soap color that soap base is made is uniform.

4). after oil mixes with alkali lye, first with hand operated mixing, oil and alkali lye are stirred a little, then bring into use electric mixer.

5). with the electric mixer of speed governing, a stirring at a slow speed can be selected just passable.

6) because the speed of saponification in the end can be more and more faster, water lily essential oil can accelerate saponification, so suggestion will add water lily essential oil when soap lye becomes.

7). other additives can add together, just have time enough to be stirred to evenly.

8). use electric mixer easily to produce bubble, place after stirring, allow bubble emit up, stir gently occasionally and help bubble to emerge, wait bubble next to nothing to emerge and reenter mould

9) mould can be struck gently after entering mould, allow dense thick soap lye fill up space, allow remaining bubble emersion, also can allow the surfacing of soap.

embodimentbelow in conjunction with embodiment, the present invention is described in further detail:

Be configured according to data listed in Table (weight percent %) and affiliated step thereof:

1. the formula following (component and weight percent % thereof) of the present invention's selection: water lily caul-fat 20-30; Tea tree oil 10-15; Sweet oil 10-15; Oleum Cocois 10-15; Plam oil 40-50; Triple pressed stearic acid 3-4; The cured 3-4 of honey; Laurylamide diethanolamine 1.0-2.0; Sodium hydroxide 5.0-10.0; Sodium-chlor 5.0-10.0; Ethanol 3-4; Water 10.0-15.0.

2. one-tenth soap step of the present invention:

1). the molding bone external fixation system of alternative gypsum, fully biodegradable, namely plasticity-is had in 55 ~ 70 DEG C of warm water, safety, convenient, clean, no side effects, can the external immobilization material of reusable new medical, make difform mould according to individual character, interior deposited heat resistant plastice film;

2) first soap base is cut into small pieces, puts into thermally resistant container;

3). put on the heating such as microwave oven apparatus and heat about 60 seconds, allow soap base melt completely, in addition water lily anthocyanidin in the soap base liquid of fusing, ethanol by soap base liquid agitation, until melt completely, to transparence;

4). soap base liquid to be poured in the individual character mould made at this by reverse mould, and cooling in about 20 to 30 minutes is formed;

5) demoulding transparent soap demoulding, the mould of the external immobilization material of new medical can be reused.

3. feature of the present invention has following precaution:

1). seeing whether soap face has small bubbles because soap base, when melting mould, is easy to bubbling, so cooling rear surface just has short grained bubble, after entering mould, spraying alcohol make lather collapse;

2). soap base is exactly watery after melting, and can not experience the thick thick stage, so can precipitate, except special rendering effect;

3). cut soap soap and see jelly effect if layering soap, the soap soap two pieces of so soap base processing is easy to come off separately, and one day after lancing, these depths clearly level will be desalinated gradually and disappear, and the soap color that soap base is made is uniform;

4). after oil mixes with alkali lye, first with hand operated mixing, oil and alkali lye are stirred a little, then bring into use electric mixer;

5). with the electric mixer of speed governing, a stirring at a slow speed can be selected just passable;

6) because the speed of saponification in the end can be more and more faster, water lily essential oil can accelerate saponification, so suggestion will add water lily essential oil when soap lye becomes;

7). other additives can add together, just have time enough to be stirred to evenly;

8). use electric mixer easily to produce bubble, place after stirring, allow bubble emit up, stir gently occasionally and help bubble to emerge, wait bubble next to nothing to emerge and reenter mould;

9), enter mould after mould can be struck gently, allow dense thick soap lye fill up space, allow remaining bubble emersion, also can allow the surfacing of soap.

Claims (3)

1. the present invention relates to a kind of transparent oral shui solution handmade soap and making thereof, it is characterized in that there is following formula (component and weight percent % thereof): water lily caul-fat 20-30; Tea tree oil 10-15; Sweet oil 10-15; Oleum Cocois 10-15; Plam oil 40-50; Triple pressed stearic acid 3-4; The cured 3-4 of honey; Laurylamide diethanolamine 1.0-2.0; Sodium hydroxide 5.0-10.0; Sodium-chlor 5.0-10.0; Ethanol 3-4; Water 10.0-15.0.

2. a kind of transparent oral shui solution handmade soap and making thereof according to claim 1, is characterized in that having following one-tenth soap technique:

1). the molding bone external fixation system of alternative gypsum, fully biodegradable, namely plasticity-is had in 55 ~ 70 DEG C of warm water, safety, convenient, clean, no side effects, can the external immobilization material of reusable new medical, difform mould is made, interior deposited heat resistant plastice film according to individual character;

2) first soap base is cut into small pieces, puts into thermally resistant container;

3). put on the heating such as microwave oven apparatus and heat about 60 seconds, allow soap base melt completely, in addition water lily anthocyanidin in the soap base liquid of fusing, ethanol by soap base liquid agitation, until melt completely, to transparence;

4). soap base liquid to be poured in the individual character mould made at this by reverse mould, and cooling in about 20 to 30 minutes is formed;

5) demoulding transparent soap demoulding, the mould of the external immobilization material of new medical can be reused.

3. a kind of transparent oral shui solution handmade soap and making thereof according to claim 1, is characterized in that having following technology precaution:

1). seeing whether soap face has small bubbles because soap base, when melting mould, is easy to bubbling, so cooling rear surface just has short grained bubble, after entering mould, spraying alcohol make lather collapse;

2). soap base is exactly watery after melting, and can not experience the thick thick stage, so can precipitate, except special rendering effect;

3). cut soap soap and see jelly effect if layering soap, the soap soap two pieces of so soap base processing is easy to come off separately, and one day after lancing, these depths clearly level will be desalinated gradually and disappear, and the soap color that soap base is made is uniform;

4). after oil mixes with alkali lye, first with hand operated mixing, oil and alkali lye are stirred a little, then bring into use electric mixer;

5). with the electric mixer of speed governing, a stirring at a slow speed can be selected just passable;

6) because the speed of saponification in the end can be more and more faster, water lily essential oil can accelerate saponification, so suggestion will add water lily essential oil, ethanol when soap lye becomes;

7). other additives can add together, just have time enough to be stirred to evenly;

8). use electric mixer easily to produce bubble, place after stirring, allow bubble emit up, stir gently occasionally and help bubble to emerge, wait bubble next to nothing to emerge and reenter mould;

9), enter mould after mould can be struck gently, allow dense thick soap lye fill up space, allow remaining bubble emersion, also can allow the surfacing of soap.