CN105662998A - Yak hide collagen mask with ultraviolet ray resistance and preparation method - Google Patents
Yak hide collagen mask with ultraviolet ray resistance and preparation method Download PDFInfo
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- CN105662998A CN105662998A CN201610063680.0A CN201610063680A CN105662998A CN 105662998 A CN105662998 A CN 105662998A CN 201610063680 A CN201610063680 A CN 201610063680A CN 105662998 A CN105662998 A CN 105662998A
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- yak
- skin
- extracting solution
- facial film
- lamina reticularis
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- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 102000008186 Collagen Human genes 0.000 title abstract description 14
- 108010035532 Collagen Proteins 0.000 title abstract description 14
- 229920001436 collagen Polymers 0.000 title abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 239000000284 extract Substances 0.000 claims abstract description 12
- 241000628997 Flos Species 0.000 claims description 41
- 230000001815 facial effect Effects 0.000 claims description 33
- 238000000605 extraction Methods 0.000 claims description 30
- 108010010803 Gelatin Proteins 0.000 claims description 23
- 229920000159 gelatin Polymers 0.000 claims description 23
- 239000008273 gelatin Substances 0.000 claims description 23
- 235000019322 gelatine Nutrition 0.000 claims description 23
- 235000011852 gelatine desserts Nutrition 0.000 claims description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
- 239000012467 final product Substances 0.000 claims description 20
- 239000012528 membrane Substances 0.000 claims description 20
- 238000005374 membrane filtration Methods 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 11
- 241001247317 Bos mutus Species 0.000 claims description 10
- 238000007796 conventional method Methods 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- 238000000465 moulding Methods 0.000 claims description 10
- 238000004140 cleaning Methods 0.000 claims description 2
- 230000037303 wrinkles Effects 0.000 abstract description 3
- 210000003491 skin Anatomy 0.000 description 72
- 230000000694 effects Effects 0.000 description 5
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 230000005855 radiation Effects 0.000 description 4
- 241000699670 Mus sp. Species 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 206010015150 Erythema Diseases 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- 230000003796 beauty Effects 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000009759 skin aging Effects 0.000 description 2
- 201000000849 skin cancer Diseases 0.000 description 2
- 201000008261 skin carcinoma Diseases 0.000 description 2
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 description 1
- SQDAZGGFXASXDW-UHFFFAOYSA-N 5-bromo-2-(trifluoromethoxy)pyridine Chemical compound FC(F)(F)OC1=CC=C(Br)C=N1 SQDAZGGFXASXDW-UHFFFAOYSA-N 0.000 description 1
- TVEXGJYMHHTVKP-UHFFFAOYSA-N 6-oxabicyclo[3.2.1]oct-3-en-7-one Chemical compound C1C2C(=O)OC1C=CC2 TVEXGJYMHHTVKP-UHFFFAOYSA-N 0.000 description 1
- 229920001287 Chondroitin sulfate Polymers 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000010834 Extracellular Matrix Proteins Human genes 0.000 description 1
- 108010037362 Extracellular Matrix Proteins Proteins 0.000 description 1
- 102000003886 Glycoproteins Human genes 0.000 description 1
- 108090000288 Glycoproteins Proteins 0.000 description 1
- 229920002683 Glycosaminoglycan Polymers 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 206010024604 Lipoatrophy Diseases 0.000 description 1
- 206010041303 Solar dermatitis Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 238000010171 animal model Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000037396 body weight Effects 0.000 description 1
- 229940059329 chondroitin sulfate Drugs 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007123 defense Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 231100000321 erythema Toxicity 0.000 description 1
- 210000002744 extracellular matrix Anatomy 0.000 description 1
- 230000003328 fibroblastic effect Effects 0.000 description 1
- 229920002674 hyaluronan Polymers 0.000 description 1
- 229960003160 hyaluronic acid Drugs 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 206010025482 malaise Diseases 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 206010033675 panniculitis Diseases 0.000 description 1
- 230000004952 protein activity Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 210000003859 smegma Anatomy 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 210000004304 subcutaneous tissue Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 210000000106 sweat gland Anatomy 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000002792 vascular Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
- A61K8/985—Skin or skin outgrowth, e.g. hair, nails
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Dermatology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Zoology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a yak hide collagen mask with ultraviolet ray resistance and a preparation method. The mask is prepared from raw materials in parts by weight as follows: 20-40 parts of a yak hide reticular layer extracting solution and 5-10 parts of a fructus lycii flower concentrated solution. The invention further discloses a preparation method of the yak hide collagen mask. Reticular layer collagen in the Tibet plateau yak hide and plateau fresh fructus lycii flower extracts are reasonably matched, the mask has good moistening, wrinkle removal and beautifying functions on skin, and the purpose of ultraviolet ray resistance is achieved.
Description
Technical field
The present invention relates to beauty mask and preparing technical field thereof, particularly relate to a kind of former facial film of Yak-skin Gelatin with protectiving ultraviolet and preparation method.
Background technology
Although ultraviolet can disinfection, promote skeleton development etc., but when acting on skin, can there is solar dermatitis, make skin that irreversible damage to occur, illuminated position dermal vascular is expanded, and skin may occur in which the symptom such as redness, blister. The permanent skin that irradiates there will be erythema, inflammation, making skin aging become coarse, the reason of skin aging 85% originates from ultraviolet, and long-time ultraviolet radiation not only there will be various mottle, the collagen protein in skin also can be made quickly to run off, and serious also can cause skin carcinoma.
Ultraviolet all exists throughout the year, although winter solar light comparison is gentle, but ultraviolet is only than summer more weak about 20%, the positions such as human body skin still can be caused very big harm, so the four seasons still need to avoid ultraviolet radiation.
The main ultraviolet line source of nature is the sun, and when sunlight is through atmosphere, ultraviolet is the Ozone Absorption in atmosphere. Owing to industrialization is advanced by leaps and bounds development, a large amount of chemical substances destroy the ozone layer in atmosphere, and the natural cover for defense of this pipe protection human health ozone layer between 20 years decreases 14%, and ozone layer often successively decreases 1%, and the sickness rate of skin carcinoma will rise 3%.
Collagen protein is the main component of extracellular matrix, containing hyaluronic acid, chondroitin sulfate etc., containing a large amount of polar groups, collagen protein is similar to the structure of human body skin collagen, for non-soluble fiber shape containing glycoprotein, there is surface activity and the good compatibility, containing substantial amounts of hydroxyl in molecule, there is moisture-keeping function, make skin keep elasticity.
Skin is made up of epidermis, corium and subcutaneous tissue. Corium divides papillary layer and lamina reticularis, and collagen fiber are the main component of corium, account for 95%. With advancing age, fibroblastic synthesis capability declines, skin lacks collagen protein, collagen fiber will occur connection to solidify, making iuntercellular mucopolysaccharide reduce, skin will lose softness, elasticity and gloss, occurs aging, the fibrous fracture of corium, lipoatrophy, sweat gland and smegma reduce simultaneously, make skin a series of catabiosis such as mottle, wrinkle occur.
Summary of the invention
The technical problem to be solved is to provide a kind of effect and has the former facial film of Yak-skin Gelatin and the preparation method of protectiving ultraviolet significantly.
The preparation method that another technical problem to be solved by this invention is to provide the former facial film of this Yak-skin Gelatin.
For solving the problems referred to above, a kind of former facial film of Yak-skin Gelatin with protectiving ultraviolet of the present invention, it is characterised in that: this facial film is made up of the raw material of following weight portion: yak skin lamina reticularis extracting solution 20 ~ 40 parts, Flos Lycii concentrated solution 5 ~ 10 parts.
Described yak skin lamina reticularis extracting solution refers to that the yak skin by fresh yak in Qinghai-tibet WildYak cleans up, and then rejects yak hair, is cut into long 5cm, wide 5cm fritter, and removes papillary layer above section and hypodermis layer, obtains yak skin lamina reticularis; Described yak skin lamina reticularis carries out water after cleaning up and carries, and obtains extracting solution, and this extracting solution, after membrane filtration, obtains subnatant; Described subnatant is concentrated into 1:1.05 ~ 1.32 and get final product.
The condition that described water carries refers to that solid-liquid ratio is 1:5 ~ 10, and temperature is 60 ~ 100 DEG C, extraction time 2 ~ 3 times, each 2 ~ 24 hours.
The condition of described membrane filtration refers to that microporous filter membrane membrane aperture is 0.2 μm ~ 5.0 μm.
The condition of described concentration is finger pressure is 0.09MPa, and vacuum is 500 ~ 620mmHg.
Described Flos Lycii concentrated solution refers to add after being cleaned by fresh Flos Lycii and is equivalent to its weight grams 5 ~ 10 times amount water, extract at 60 ~ 100 DEG C of temperature, extraction time 2 ~ 3 times, 1 ~ 6 hour each extraction time, merging and obtain extracting solution, this extracting solution is through filtering, being evaporated to 1:1.10 ~ 1.35 and get final product.
The condition of described concentrating under reduced pressure is finger pressure is 0.5MPa, and vacuum is 500～600mmHg.
The preparation method of a kind of former facial film of Yak-skin Gelatin with protectiving ultraviolet as above, it is characterized in that: first weigh by proportioning, then Flos Lycii concentrated solution is joined in yak skin lamina reticularis extracting solution, mix homogeneously, when pressure be 500 ~ 800MPa, temperature is 10 ~ 30 DEG C, carries out molding according to a conventional method after keeping 10 ~ 40 minutes, pack.
The present invention compared with prior art has the advantage that
1, the present invention is with the fresh Flos Lycii extract of the lamina reticularis collagen protein in yak in Qinghai-tibet skin and plateau for raw material, and carry out reasonable compatibility, when active substance is used in cosmetics, it is diffused into the deep layer of skin, strengthen the collagen protein activity in skin, keep the integrity of horny layer moisture and fibre structure, promote the metabolism of skin histology, skin is produced good moist moisturizing, effect wrinkles eliminating vanishing effect, thus reaching the purpose carrying out effectively protection because of the skin of ultraviolet radiation.
2, the raw materials used concentrated reflection of the present invention is the collagen protein of lamina reticularis, solvent for use is pure water, it is to avoid the organic solvents such as alkaline process, enzyme process, acid system, and gained molecular weight is concentrated, and is the quality product of beauty treatment.
3, products obtained therefrom of the present invention has the effect (referring to table 1) of protectiving ultraviolet after tested.
With healthy Kunming white mice (male and female half and half, 4 week old, body weight is at 18 ~ 22 grams, [quality certification number is SCXK (sweet)] is provided by Gansu Chinese of Traditional Chinese Medicine SPF level Experimental Animal Center) for laboratory animal, every treated animal rejects left and right dorsal body setae, and former for Yak-skin Gelatin facial mask liquid is applied to the left back of the body, and the right back of the body compares, to each experimental mice successive administration 10 days, and set blank, model control group.
Table 1 mice ultra-vioket radiation and recovery situation
4, the present invention not only technique is simple, it is easy to accomplish, and without any additive, can use safely.
Detailed description of the invention
Embodiment 1 one kinds has the former facial film of Yak-skin Gelatin of protectiving ultraviolet, and this facial film is made up of the raw material of following weight portion (g): yak skin lamina reticularis extracting solution 20 parts, Flos Lycii concentrated solution 5 parts.
Its preparation method refers to: first weigh by proportioning, then Flos Lycii concentrated solution is joined in yak skin lamina reticularis extracting solution, mix homogeneously, when pressure be 500MPa, temperature is 10 DEG C, carries out molding according to a conventional method after keeping 10 minutes, packs.
Wherein:
Yak skin lamina reticularis extracting solution refers to that the yak skin by fresh yak in Qinghai-tibet WildYak cleans up, and then rejects yak hair, is cut into long 5cm, wide 5cm fritter, and removes papillary layer above section and hypodermis layer, obtains yak skin lamina reticularis; Yak skin lamina reticularis clean up after solid-liquid ratio (g/g) be 1:5, temperature be 60 DEG C, extraction time 2 times, each 2 hours when carry out water and carry, obtain extracting solution, this extracting solution after membrane filtration, obtains subnatant when microporous filter membrane membrane aperture is 0.2 μm; It is that 0.09MPa, vacuum are concentrated into 1:1.05 and get final product when being 500mmHg by subnatant at pressure.
Flos Lycii concentrated solution refers to add after being cleaned by fresh Flos Lycii and is equivalent to its weight grams 5 times amount water, extract at 60 DEG C of temperature, extraction time 2 times, 1 hour each extraction time, merging and obtain extracting solution, this extracting solution is that 0.5MPa, vacuum are evaporated to 1:1.10 and get final product when being 500mmHg at pressure after filtering.
Embodiment 2 one kinds has the former facial film of Yak-skin Gelatin of protectiving ultraviolet, and this facial film is made up of the raw material of following weight portion (g): yak skin lamina reticularis extracting solution 40 parts, Flos Lycii concentrated solution 10 parts.
Its preparation method refers to: first weigh by proportioning, then Flos Lycii concentrated solution is joined in yak skin lamina reticularis extracting solution, mix homogeneously, when pressure be 800MPa, temperature is 30 DEG C, carries out molding according to a conventional method after keeping 40 minutes, packs.
Wherein:
Yak skin lamina reticularis extracting solution refers to that the yak skin by fresh yak in Qinghai-tibet WildYak cleans up, and then rejects yak hair, is cut into long 5cm, wide 5cm fritter, and removes papillary layer above section and hypodermis layer, obtains yak skin lamina reticularis; Yak skin lamina reticularis clean up after solid-liquid ratio (g/g) be 1:10, temperature be 100 DEG C, extraction time 3 times, each 24 hours when carry out water and carry, obtain extracting solution, this extracting solution after membrane filtration, obtains subnatant when microporous filter membrane membrane aperture is 5.0 μm; It is that 0.09MPa, vacuum are concentrated into 1:1.32 and get final product when being 620mmHg by subnatant at pressure.
Flos Lycii concentrated solution refers to add after being cleaned by fresh Flos Lycii and is equivalent to its weight grams 10 times amount water, extract at 100 DEG C of temperature, extraction time 3 times, 6 hours each extraction times, merging and obtain extracting solution, this extracting solution is that 0.5MPa, vacuum are evaporated to 1:1.35 and get final product when being 600mmHg at pressure after filtering.
Embodiment 3 one kinds has the former facial film of Yak-skin Gelatin of protectiving ultraviolet, and this facial film is made up of the raw material of following weight portion (g): yak skin lamina reticularis extracting solution 20 parts, Flos Lycii concentrated solution 10 parts.
Its preparation method refers to: first weigh by proportioning, then Flos Lycii concentrated solution is joined in yak skin lamina reticularis extracting solution, mix homogeneously, when pressure be 500MPa, temperature is 30 DEG C, carries out molding according to a conventional method after keeping 10 minutes, packs.
Wherein:
Yak skin lamina reticularis extracting solution refers to that the yak skin by fresh yak in Qinghai-tibet WildYak cleans up, and then rejects yak hair, is cut into long 5cm, wide 5cm fritter, and removes papillary layer above section and hypodermis layer, obtains yak skin lamina reticularis;Yak skin lamina reticularis clean up after solid-liquid ratio (g/g) be 1:8, temperature be 90 DEG C, extraction time 3 times, each 8 hours when carry out water and carry, obtain extracting solution, this extracting solution after membrane filtration, obtains subnatant when microporous filter membrane membrane aperture is 2.0 μm; It is that 0.09MPa, vacuum are concentrated into 1:1.22 and get final product when being 600mmHg by subnatant at pressure.
Flos Lycii concentrated solution refers to add after being cleaned by fresh Flos Lycii and is equivalent to its weight grams 5 times amount water, extract at 100 DEG C of temperature, extraction time 2 times, 6 hours each extraction times, merging and obtain extracting solution, this extracting solution is evaporated to 1:1.15 when pressure is 0.5MPa, vacuum 550mmHg and get final product after filtering.
Embodiment 4 one kinds has the former facial film of Yak-skin Gelatin of protectiving ultraviolet, and this facial film is made up of the raw material of following weight portion (g): yak skin lamina reticularis extracting solution 40 parts, Flos Lycii concentrated solution 5 parts.
Its preparation method refers to: first weigh by proportioning, then Flos Lycii concentrated solution is joined in yak skin lamina reticularis extracting solution, mix homogeneously, when pressure be 800MPa, temperature is 10 DEG C, carries out molding according to a conventional method after keeping 40 minutes, packs.
Wherein:
Yak skin lamina reticularis extracting solution refers to that the yak skin by fresh yak in Qinghai-tibet WildYak cleans up, and then rejects yak hair, is cut into long 5cm, wide 5cm fritter, and removes papillary layer above section and hypodermis layer, obtains yak skin lamina reticularis; Yak skin lamina reticularis clean up after solid-liquid ratio (g/g) be 1:8, temperature be 80 DEG C, extraction time 2 times, each 18 hours when carry out water and carry, obtain extracting solution, this extracting solution after membrane filtration, obtains subnatant when microporous filter membrane membrane aperture is 0.8 μm; It is that 0.09MPa, vacuum are concentrated into 1:1.10 and get final product when being 550mmHg by subnatant at pressure.
Flos Lycii concentrated solution refers to add after being cleaned by fresh Flos Lycii and is equivalent to its weight grams 10 times amount water, extract at 60 DEG C of temperature, extraction time 3 times, 1 hour each extraction time, merging and obtain extracting solution, this extracting solution is that 0.5MPa, vacuum are evaporated to 1:1.20 and get final product when being 580mmHg at pressure after filtering.
Embodiment 5 one kinds has the former facial film of Yak-skin Gelatin of protectiving ultraviolet, and this facial film is made up of the raw material of following weight portion (g): yak skin lamina reticularis extracting solution 30 parts, Flos Lycii concentrated solution 7 parts.
Its preparation method refers to: first weigh by proportioning, then Flos Lycii concentrated solution is joined in yak skin lamina reticularis extracting solution, mix homogeneously, when pressure be 600MPa, temperature is 20 DEG C, carries out molding according to a conventional method after keeping 30 minutes, packs.
Wherein:
Yak skin lamina reticularis extracting solution refers to that the yak skin by fresh yak in Qinghai-tibet WildYak cleans up, and then rejects yak hair, is cut into long 5cm, wide 5cm fritter, and removes papillary layer above section and hypodermis layer, obtains yak skin lamina reticularis; Yak skin lamina reticularis clean up after solid-liquid ratio (g/g) be 1:6, temperature be 65 DEG C, extraction time 2 times, each 12 hours when carry out water and carry, obtain extracting solution, this extracting solution after membrane filtration, obtains subnatant when microporous filter membrane membrane aperture is 3.0 μm; It is that 0.09MPa, vacuum are concentrated into 1:1.15 and get final product when being 590mmHg by subnatant at pressure.
Flos Lycii concentrated solution refers to add after being cleaned by fresh Flos Lycii and is equivalent to its weight grams 8 times amount water, extract at 80 DEG C of temperature, extraction time 3 times, 4 hours each extraction times, merging and obtain extracting solution, this extracting solution is that 0.5MPa, vacuum are evaporated to 1:1.25 and get final product when being 570mmHg at pressure after filtering.
Embodiment 6 one kinds has the former facial film of Yak-skin Gelatin of protectiving ultraviolet, and this facial film is made up of the raw material of following weight portion (g): yak skin lamina reticularis extracting solution 15 parts, Flos Lycii concentrated solution 9 parts.
Its preparation method refers to: first weigh by proportioning, then Flos Lycii concentrated solution is joined in yak skin lamina reticularis extracting solution, mix homogeneously, when pressure be 700MPa, temperature is 15 DEG C, carries out molding according to a conventional method after keeping 25 minutes, packs.
Wherein:
Yak skin lamina reticularis extracting solution refers to that the yak skin by fresh yak in Qinghai-tibet WildYak cleans up, and then rejects yak hair, is cut into long 5cm, wide 5cm fritter, and removes papillary layer above section and hypodermis layer, obtains yak skin lamina reticularis; Yak skin lamina reticularis clean up after solid-liquid ratio (g/g) be 1:8, temperature be 95 DEG C, extraction time 3 times, each 10 hours when carry out water and carry, obtain extracting solution, this extracting solution after membrane filtration, obtains subnatant when microporous filter membrane membrane aperture is 4.0 μm; It is that 0.09MPa, vacuum are concentrated into 1:1.25 and get final product when being 5700mmHg by subnatant at pressure.
Flos Lycii concentrated solution refers to add after being cleaned by fresh Flos Lycii and is equivalent to its weight grams 6 times amount water, extract at 90 DEG C of temperature, extraction time 2 times, 3 hours each extraction times, merging and obtain extracting solution, this extracting solution is that 0.5MPa, vacuum are evaporated to 1:1.33 and get final product when being 585mmHg at pressure after filtering.
Embodiment 7 one kinds has the former facial film of Yak-skin Gelatin of protectiving ultraviolet, and this facial film is made up of the raw material of following weight portion (g): yak skin lamina reticularis extracting solution 20 parts, Flos Lycii concentrated solution 8 parts.
Its preparation method refers to: first weigh by proportioning, then Flos Lycii concentrated solution is joined in yak skin lamina reticularis extracting solution, mix homogeneously, when pressure be 550MPa, temperature is 25 DEG C, carries out molding according to a conventional method after keeping 30 minutes, packs.
Wherein:
Yak skin lamina reticularis extracting solution refers to that the yak skin by fresh yak in Qinghai-tibet WildYak cleans up, and then rejects yak hair, is cut into long 5cm, wide 5cm fritter, and removes papillary layer above section and hypodermis layer, obtains yak skin lamina reticularis; Yak skin lamina reticularis clean up after solid-liquid ratio (g/g) be 1:7, temperature be 70 DEG C, extraction time 3 times, each 24 hours when carry out water and carry, obtain extracting solution, this extracting solution after membrane filtration, obtains subnatant when microporous filter membrane membrane aperture is 4.5 μm; It is that 0.09MPa, vacuum are concentrated into 1:1.30 and get final product when being 590mmHg by subnatant at pressure.
Flos Lycii concentrated solution refers to add after being cleaned by fresh Flos Lycii and is equivalent to its weight grams 8 times amount water, extract at 100 DEG C of temperature, extraction time 2 times, 6 hours each extraction times, merging and obtain extracting solution, this extracting solution is that 0.5MPa, vacuum are evaporated to 1:1.18 and get final product when being 550mmHg at pressure after filtering.
Embodiment 8 one kinds has the former facial film of Yak-skin Gelatin of protectiving ultraviolet, and this facial film is made up of the raw material of following weight portion (g): yak skin lamina reticularis extracting solution 25 parts, Flos Lycii concentrated solution 6 parts.
Its preparation method refers to: first weigh by proportioning, then Flos Lycii concentrated solution is joined in yak skin lamina reticularis extracting solution, mix homogeneously, when pressure be 650MPa, temperature is 20 DEG C, carries out molding according to a conventional method after keeping 15 minutes, packs.
Wherein:
Yak skin lamina reticularis extracting solution refers to that the yak skin by fresh yak in Qinghai-tibet WildYak cleans up, and then rejects yak hair, is cut into long 5cm, wide 5cm fritter, and removes papillary layer above section and hypodermis layer, obtains yak skin lamina reticularis; Yak skin lamina reticularis clean up after solid-liquid ratio (g/g) be 1:7, temperature be 85 DEG C, extraction time 3 times, each 20 hours when carry out water and carry, obtain extracting solution, this extracting solution after membrane filtration, obtains subnatant when microporous filter membrane membrane aperture is 4.3 μm; It is that 0.09MPa, vacuum are concentrated into 1:1.27 and get final product when being 610mmHg by subnatant at pressure.
Flos Lycii concentrated solution refers to add after being cleaned by fresh Flos Lycii and is equivalent to its weight grams 10 times amount water, extract at 60 DEG C of temperature, extraction time 2 times, 6 hours each extraction times, merging and obtain extracting solution, this extracting solution is that 0.5MPa, vacuum are evaporated to 1:1.28 and get final product when being 5750mmHg at pressure after filtering.
Claims (8)
1. the former facial film of Yak-skin Gelatin with protectiving ultraviolet, it is characterised in that: this facial film is made up of the raw material of following weight portion: yak skin lamina reticularis extracting solution 20 ~ 40 parts, Flos Lycii concentrated solution 5 ~ 10 parts.
2. a kind of former facial film of Yak-skin Gelatin with protectiving ultraviolet as claimed in claim 1, it is characterized in that: described yak skin lamina reticularis extracting solution refers to that the yak skin by fresh yak in Qinghai-tibet WildYak cleans up, then yak hair is rejected, it is cut into long 5cm, wide 5cm fritter, and remove papillary layer above section and hypodermis layer, obtain yak skin lamina reticularis; Described yak skin lamina reticularis carries out water after cleaning up and carries, and obtains extracting solution, and this extracting solution, after membrane filtration, obtains subnatant; Described subnatant is concentrated into 1:1.05 ~ 1.32 and get final product.
3. a kind of former facial film of Yak-skin Gelatin with protectiving ultraviolet as claimed in claim 2, it is characterised in that: the condition that described water carries refers to that solid-liquid ratio is 1:5 ~ 10, and temperature is 60 ~ 100 DEG C, extraction time 2 ~ 3 times, each 2 ~ 24 hours.
4. a kind of former facial film of Yak-skin Gelatin with protectiving ultraviolet as claimed in claim 2, it is characterised in that: the condition of described membrane filtration refers to that microporous filter membrane membrane aperture is 0.2 μm ~ 5.0 μm.
5. a kind of former facial film of Yak-skin Gelatin with protectiving ultraviolet as claimed in claim 2, it is characterised in that: the condition of described concentration is finger pressure is 0.09MPa, and vacuum is 500 ~ 620mmHg.
6. a kind of former facial film of Yak-skin Gelatin with protectiving ultraviolet as claimed in claim 1, it is characterized in that: described Flos Lycii concentrated solution refers to add after being cleaned by fresh Flos Lycii and is equivalent to its weight grams 5 ~ 10 times amount water, extract at 60 ~ 100 DEG C of temperature, extraction time 2 ~ 3 times, 1 ~ 6 hour each extraction time, merging and obtain extracting solution, this extracting solution is through filtering, being evaporated to 1:1.10 ~ 1.35 and get final product.
7. a kind of former facial film of Yak-skin Gelatin with protectiving ultraviolet as claimed in claim 6, it is characterised in that: the condition of described concentrating under reduced pressure is finger pressure is 0.5MPa, and vacuum is 500～600mmHg.
8. the preparation method of a kind of former facial film of Yak-skin Gelatin with protectiving ultraviolet as claimed in claim 1, it is characterized in that: first weigh by proportioning, then Flos Lycii concentrated solution is joined in yak skin lamina reticularis extracting solution, mix homogeneously, when pressure be 500 ~ 800MPa, temperature is 10 ~ 30 DEG C, carries out molding according to a conventional method after keeping 10 ~ 40 minutes, pack.
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| CN110151664A (en) * | 2019-06-05 | 2019-08-23 | 中国科学院西北高原生物研究所 | A kind of Yak-skin Gelatin skin-protection product and preparation method thereof for dispelling red blood trace on face |
| CN110742824A (en) * | 2019-10-29 | 2020-02-04 | 南宁学院 | Preparation and application of cow hide composite extract |
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| CN105273436A (en) * | 2014-07-18 | 2016-01-27 | 周子童 | Medlar flower pigment extraction technology |
| CN104434741A (en) * | 2014-12-23 | 2015-03-25 | 吴辰 | Black wolfberry facial mask |
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| CN110742824B (en) * | 2019-10-29 | 2022-12-27 | 南宁学院 | Preparation and application of cow hide composite extract |
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