CN105662998B - A kind of Yak-skin Gelatin original facial mask and preparation method with protectiving ultraviolet - Google Patents
A kind of Yak-skin Gelatin original facial mask and preparation method with protectiving ultraviolet Download PDFInfo
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- CN105662998B CN105662998B CN201610063680.0A CN201610063680A CN105662998B CN 105662998 B CN105662998 B CN 105662998B CN 201610063680 A CN201610063680 A CN 201610063680A CN 105662998 B CN105662998 B CN 105662998B
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- yak
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- extracting solution
- facial mask
- lamina reticularis
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- 230000001815 facial effect Effects 0.000 title claims abstract description 32
- 108010010803 Gelatin Proteins 0.000 title claims abstract description 21
- 229920000159 gelatin Polymers 0.000 title claims abstract description 21
- 235000019322 gelatine Nutrition 0.000 title claims abstract description 21
- 235000011852 gelatine desserts Nutrition 0.000 title claims abstract description 21
- 239000008273 gelatin Substances 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 241000628997 Flos Species 0.000 claims abstract description 40
- 239000012141 concentrate Substances 0.000 claims abstract description 31
- 239000002994 raw material Substances 0.000 claims abstract description 4
- 235000015459 Lycium barbarum Nutrition 0.000 claims abstract description 3
- 244000241838 Lycium barbarum Species 0.000 claims abstract description 3
- 238000000605 extraction Methods 0.000 claims description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
- 239000007788 liquid Substances 0.000 claims description 20
- 239000012467 final product Substances 0.000 claims description 14
- 238000004140 cleaning Methods 0.000 claims description 11
- 238000001914 filtration Methods 0.000 claims description 11
- 238000007796 conventional method Methods 0.000 claims description 10
- 239000012528 membrane Substances 0.000 claims description 10
- 238000000465 moulding Methods 0.000 claims description 10
- 238000004806 packaging method and process Methods 0.000 claims description 10
- 238000003825 pressing Methods 0.000 claims description 8
- 238000005374 membrane filtration Methods 0.000 claims description 4
- 230000006837 decompression Effects 0.000 claims 1
- 102000008186 Collagen Human genes 0.000 abstract description 10
- 108010035532 Collagen Proteins 0.000 abstract description 10
- 229920001436 collagen Polymers 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 4
- 230000037303 wrinkles Effects 0.000 abstract description 3
- 230000003020 moisturizing effect Effects 0.000 abstract description 2
- 210000003491 skin Anatomy 0.000 description 72
- 239000000463 material Substances 0.000 description 9
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- 201000009030 Carcinoma Diseases 0.000 description 2
- 206010015150 Erythema Diseases 0.000 description 2
- 206010061218 Inflammation Diseases 0.000 description 2
- 241000699666 Mus <mouse, genus> Species 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 230000003796 beauty Effects 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 230000004054 inflammatory process Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000009759 skin aging Effects 0.000 description 2
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 description 1
- SQDAZGGFXASXDW-UHFFFAOYSA-N 5-bromo-2-(trifluoromethoxy)pyridine Chemical compound FC(F)(F)OC1=CC=C(Br)C=N1 SQDAZGGFXASXDW-UHFFFAOYSA-N 0.000 description 1
- 229920001287 Chondroitin sulfate Polymers 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000010834 Extracellular Matrix Proteins Human genes 0.000 description 1
- 108010037362 Extracellular Matrix Proteins Proteins 0.000 description 1
- 102000008946 Fibrinogen Human genes 0.000 description 1
- 108010049003 Fibrinogen Proteins 0.000 description 1
- 102000003886 Glycoproteins Human genes 0.000 description 1
- 108090000288 Glycoproteins Proteins 0.000 description 1
- 229920002683 Glycosaminoglycan Polymers 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241000699670 Mus sp. Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000010171 animal model Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229940059329 chondroitin sulfate Drugs 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007123 defense Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 231100000321 erythema Toxicity 0.000 description 1
- 210000002744 extracellular matrix Anatomy 0.000 description 1
- 229940012952 fibrinogen Drugs 0.000 description 1
- 230000003328 fibroblastic effect Effects 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 229920002674 hyaluronan Polymers 0.000 description 1
- 229960003160 hyaluronic acid Drugs 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 206010033675 panniculitis Diseases 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 210000003859 smegma Anatomy 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 210000004304 subcutaneous tissue Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 210000000106 sweat gland Anatomy 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
- A61K8/985—Skin or skin outgrowth, e.g. hair, nails
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Dermatology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Zoology (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to a kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet, the facial mask are made from the following raw materials in parts by weight:20 ~ 40 parts of yak skin lamina reticularis extracting solution, 5 ~ 10 parts of Flos Lycii concentrate.The invention also discloses the preparation methods of the Yak-skin Gelatin original facial mask.The fresh matrimony vine flower extract of lamina reticularis collagen and plateau in yak in Qinghai-tibet skin is carried out reasonable compatibility by the present invention, good moist moisturizing, effect wrinkles eliminating vanishing effect is generated to skin, to achieve the purpose that protectiving ultraviolet.
Description
Technical field
The present invention relates to beauty mask and its preparing technical field more particularly to a kind of yak skins with protectiving ultraviolet
Collagen mask and preparation method.
Background technology
Although with disinfection, promotion skeleton development etc. when acting on skin, actinic skin can occur for ultraviolet light
Inflammation, makes skin that irreversible damage, illuminated position dermal vascular expansion occur, and skin may occur in which the symptoms such as redness, bubble.
The reason of permanent irradiation skin will appear erythema, inflammation, makes skin aging and becomes coarse, skin aging 85% is from ultraviolet
Line, the irradiation of long-time ultraviolet light not only will appear various color spots, also the collagen in skin can be made rapidly losing, serious to go back
It can cause cutaneum carcinoma.
Ultraviolet light all exists throughout the year, although winter solar light comparison is mild, ultraviolet light only than summer it is weaker about
20%, still can the positions such as human skin be caused with very big harm, so the four seasons still need to that ultraviolet light is avoided to irradiate.
The main ultraviolet linear light source of nature is the sun, and ultraviolet light is the ozone in atmosphere when sunlight penetrates atmosphere
It absorbs.Due to industrializing development of advancing by leaps and bounds, a large amount of chemical substances destroy the ozone layer in atmosphere, this pipe protection mankind are strong
The natural cover for defense of health ozone layer between 20 years reduces 14%, and ozone layer often successively decreases 1%, and the incidence of cutaneum carcinoma will rise
3%。
Collagen is the main component of extracellular matrix, containing hyaluronic acid, chondroitin sulfate etc., contains a large amount of polarity
Group, collagen is similar to the structure of human skin collagen, contains glycoprotein for non-soluble fiber shape, has surface-active
With good compatibility, a large amount of hydroxyl is contained in molecule, there is moisture-keeping function, skin is made to keep elasticity.
Skin is made of epidermis, corium and subcutaneous tissue.Corium divides papillaris pars and lamina reticularis, collagenous fibres to be the master of corium
Ingredient is wanted, accounts for about 95%.With advancing age, fibroblastic synthesis capability declines, and lacks collagen, glue in skin
Connection solidification will occur for fibrinogen, and iuntercellular mucopolysaccharide is made to reduce, and skin will lose soft, elasticity and gloss, and aging occurs,
The fibrous fracture, lipoatrophia of corium, sweat gland and smegma are reduced simultaneously, so that skin color spot, wrinkle etc. is occurred a series of
Aging phenomenon.
Invention content
Technical problem to be solved by the invention is to provide a kind of effective Yak-skin Gelatins with protectiving ultraviolet
Former facial mask and preparation method.
Another technical problem to be solved by this invention is to provide the preparation method of the Yak-skin Gelatin original facial mask.
To solve the above problems, a kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet of the present invention, feature
It is:The facial mask is made from the following raw materials in parts by weight:20 ~ 40 parts of yak skin lamina reticularis extracting solution, Flos Lycii concentrate 5 ~ 10
Part.
The yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakThe cleaning of yak skin it is dry
Only, yak hair is then rejected, long 5cm, width 5cm fritters is cut into, and remove papillaris pars above section and hypodermis layer, obtains yak
Ox-hide lamina reticularis;The yak skin lamina reticularis clean up after carry out water carry, obtain extracting solution, the extracting solution after membrane filtration,
Obtain subnatant;The subnatant is concentrated into 1:1.05 ~ 1.32 to obtain the final product.
The condition that the water carries refers to that solid-liquid ratio is 1:5 ~ 10, temperature is 60 ~ 100 DEG C, extraction time 2 ~ 3 times, every time 2 ~
24 hours.
The condition of the membrane filtration refers to that miillpore filter membrane aperture is 0.2 μm ~ 5.0 μm.
The condition of the concentration is that finger pressure is 0.09MPa, and vacuum degree is 500 ~ 620mmHg.
The Flos Lycii concentrate refers to being added to be equivalent to 5 ~ 10 times of amount water of its weight grams after cleaning fresh Flos Lycii,
It is extracted at a temperature of 60 ~ 100 DEG C, extraction time 2 ~ 3 times, 1 ~ 6 hour each extraction time, merging obtains extracting solution, the extraction
Liquid is through filtering, being concentrated under reduced pressure into 1:1.10 ~ 1.35 to obtain the final product.
The condition of the reduced pressure is that finger pressure is 0.5MPa, and vacuum degree is 500~600mmHg.
A kind of preparation method of the Yak-skin Gelatin original facial mask with protectiving ultraviolet as described above, it is characterised in that:It is first
It first weighs, Flos Lycii concentrate is added in yak skin lamina reticularis extracting solution according to the ratio then, be uniformly mixed, be in pressure
Under conditions of 500 ~ 800MPa, temperature are 10 ~ 30 DEG C, holding 10 ~ carry out molding, packaging according to a conventional method after forty minutes.
Compared with the prior art, the present invention has the following advantages:
1, the present invention is original with the fresh matrimony vine flower extract of lamina reticularis collagen and plateau in yak in Qinghai-tibet skin
Material, and reasonable compatibility is carried out, when by active material in cosmetics, it is diffused into the deep layer of skin, enhances the collagen in skin
Protein active keeps the integrality of cuticula moisture and fibre structure, promotes the metabolism of skin histology, is generated to skin
Good moist moisturizing, effect wrinkles eliminating vanishing effect, to achieve the purpose that carry out effective protection to the skin irradiated by ultraviolet light.
2, the raw materials used in the present invention concentrated reflection be lamina reticularis collagen, solvent for use is pure water, avoid alkaline process,
The organic solvents such as enzyme process, acid system, gained molecular weight are concentrated, and are the quality products of beauty.
3, products obtained therefrom of the present invention has the function of protectiving ultraviolet after tested(Referring to table 1).
With healthy Kunming small white mouse(Half male and half female, 4 week old, weight are tested at 18 ~ 22 grams by Gansu Chinese of Traditional Chinese Medicine SPF grades
Animal center provides【Quality certification number is SCXK (sweet)】)For experimental animal, every group of animal rejects left and right dorsal body setae, by Yak-skin Gelatin
Former facial mask liquid is applied to the left back of the body, and the right back of the body compares, and to each experimental mice successive administration 10 days, and sets blank, model control group.
1 mouse ultraviolet irradiation of table and recovery situation
4, the present invention is not only simple for process, it is easy to accomplish, and without any additive, can use safely.
Specific implementation mode
A kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet of embodiment 1, the facial mask is by following parts by weight(g)Original
Material is made:20 parts of yak skin lamina reticularis extracting solution, 5 parts of Flos Lycii concentrate.
Preparation method refers to:It weighs according to the ratio first, Flos Lycii concentrate, which is then added to yak skin lamina reticularis, carries
It takes in liquid, is uniformly mixed, under conditions of pressure is 500MPa, temperature is 10 DEG C, holding carries out according to a conventional method after ten minutes
Molding, packaging.
Wherein:
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis;Yak skin lamina reticularis clean up after in solid-liquid ratio(g/g)It is 1:5, temperature be 60 DEG C, extraction time 2 times, every time 2
Water is carried out under conditions of hour to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 0.2 μm through film mistake
After filter, subnatant is obtained;Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 500mmHg:1.05 i.e.
.
Flos Lycii concentrate refers to being added to be equivalent to 5 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 60 DEG C
At a temperature of extract, extraction time 2 times, 1 hour each extraction time, merging obtain extracting solution, which is pressing after filtering
Power is 0.5MPa, vacuum degree is concentrated under reduced pressure into 1 under conditions of being 500mmHg:1.10 to obtain the final product.
A kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet of embodiment 2, the facial mask is by following parts by weight(g)Original
Material is made:40 parts of yak skin lamina reticularis extracting solution, 10 parts of Flos Lycii concentrate.
Preparation method refers to:It weighs according to the ratio first, Flos Lycii concentrate, which is then added to yak skin lamina reticularis, carries
It takes in liquid, is uniformly mixed, under conditions of pressure is 800MPa, temperature is 30 DEG C, holding carries out according to a conventional method after forty minutes
Molding, packaging.
Wherein:
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis;Yak skin lamina reticularis clean up after in solid-liquid ratio(g/g)It is 1:10, temperature be 100 DEG C, extraction time 3 times, every time
Water is carried out under conditions of 24 hours to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 5.0 μm through film
After filtering, subnatant is obtained;Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 620mmHg:1.32
To obtain the final product.
Flos Lycii concentrate refers to being added to be equivalent to 10 times of amount water of its weight grams after cleaning fresh Flos Lycii, 100
It is extracted at a temperature of DEG C, extraction time 3 times, 6 hours each extraction times, merging obtains extracting solution, which exists after filtering
Pressure is 0.5MPa, vacuum degree is concentrated under reduced pressure into 1 under conditions of being 600mmHg:1.35 to obtain the final product.
A kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet of embodiment 3, the facial mask is by following parts by weight(g)Original
Material is made:20 parts of yak skin lamina reticularis extracting solution, 10 parts of Flos Lycii concentrate.
Preparation method refers to:It weighs according to the ratio first, Flos Lycii concentrate, which is then added to yak skin lamina reticularis, carries
It takes in liquid, is uniformly mixed, under conditions of pressure is 500MPa, temperature is 30 DEG C, holding carries out according to a conventional method after ten minutes
Molding, packaging.
Wherein:
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis;Yak skin lamina reticularis clean up after in solid-liquid ratio(g/g)It is 1:8, temperature be 90 DEG C, extraction time 3 times, every time 8
Water is carried out under conditions of hour to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 2.0 μm through film mistake
After filter, subnatant is obtained;Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 600mmHg:1.22 i.e.
.
Flos Lycii concentrate refers to being added to be equivalent to 5 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 100 DEG C
At a temperature of extract, extraction time 2 times, 6 hours each extraction times, merging obtain extracting solution, which is pressing after filtering
Power be 0.5MPa, vacuum degree 550mmHg under conditions of be concentrated under reduced pressure into 1:1.15 to obtain the final product.
A kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet of embodiment 4, the facial mask is by following parts by weight(g)Original
Material is made:40 parts of yak skin lamina reticularis extracting solution, 5 parts of Flos Lycii concentrate.
Preparation method refers to:It weighs according to the ratio first, Flos Lycii concentrate, which is then added to yak skin lamina reticularis, carries
It takes in liquid, is uniformly mixed, under conditions of pressure is 800MPa, temperature is 10 DEG C, holding carries out according to a conventional method after forty minutes
Molding, packaging.
Wherein:
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis;Yak skin lamina reticularis clean up after in solid-liquid ratio(g/g)It is 1:8, temperature be 80 DEG C, extraction time 2 times, every time 18
Water is carried out under conditions of hour to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 0.8 μm through film mistake
After filter, subnatant is obtained;Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 550mmHg:1.10 i.e.
.
Flos Lycii concentrate refers to being added to be equivalent to 10 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 60 DEG C
At a temperature of extract, extraction time 3 times, 1 hour each extraction time, merging obtain extracting solution, which is pressing after filtering
Power is 0.5MPa, vacuum degree is concentrated under reduced pressure into 1 under conditions of being 580mmHg:1.20 to obtain the final product.
A kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet of embodiment 5, the facial mask is by following parts by weight(g)Original
Material is made:30 parts of yak skin lamina reticularis extracting solution, 7 parts of Flos Lycii concentrate.
Preparation method refers to:It weighs according to the ratio first, Flos Lycii concentrate, which is then added to yak skin lamina reticularis, carries
It takes in liquid, is uniformly mixed, under conditions of pressure is 600MPa, temperature is 20 DEG C, carried out according to a conventional method after being kept for 30 minutes
Molding, packaging.
Wherein:
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis;Yak skin lamina reticularis clean up after in solid-liquid ratio(g/g)It is 1:6, temperature be 65 DEG C, extraction time 2 times, every time 12
Water is carried out under conditions of hour to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 3.0 μm through film mistake
After filter, subnatant is obtained;Subnatant is concentrated into 1 under the conditions of pressure is 0.09MPa, vacuum degree is 590mmHg:1.15 i.e.
.
Flos Lycii concentrate refers to being added to be equivalent to 8 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 80 DEG C
At a temperature of extract, extraction time 3 times, 4 hours each extraction times, merging obtain extracting solution, which is pressing after filtering
Power is 0.5MPa, vacuum degree is concentrated under reduced pressure into 1 under conditions of being 570mmHg:1.25 to obtain the final product.
A kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet of embodiment 6, the facial mask is by following parts by weight(g)Original
Material is made:15 parts of yak skin lamina reticularis extracting solution, 9 parts of Flos Lycii concentrate.
Preparation method refers to:It weighs according to the ratio first, Flos Lycii concentrate, which is then added to yak skin lamina reticularis, carries
It takes in liquid, is uniformly mixed, under conditions of pressure is 700MPa, temperature is 15 DEG C, carried out according to a conventional method after being kept for 25 minutes
Molding, packaging.
Wherein:
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis;Yak skin lamina reticularis clean up after in solid-liquid ratio(g/g)It is 1:8, temperature be 95 DEG C, extraction time 3 times, every time 10
Water is carried out under conditions of hour to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 4.0 μm through film mistake
After filter, subnatant is obtained;Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 5700mmHg:1.25
To obtain the final product.
Flos Lycii concentrate refers to being added to be equivalent to 6 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 90 DEG C
At a temperature of extract, extraction time 2 times, 3 hours each extraction times, merging obtain extracting solution, which is pressing after filtering
Power is 0.5MPa, vacuum degree is concentrated under reduced pressure into 1 under conditions of being 585mmHg:1.33 to obtain the final product.
A kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet of embodiment 7, the facial mask is by following parts by weight(g)Original
Material is made:20 parts of yak skin lamina reticularis extracting solution, 8 parts of Flos Lycii concentrate.
Preparation method refers to:It weighs according to the ratio first, Flos Lycii concentrate, which is then added to yak skin lamina reticularis, carries
It takes in liquid, is uniformly mixed, under conditions of pressure is 550MPa, temperature is 25 DEG C, carried out according to a conventional method after being kept for 30 minutes
Molding, packaging.
Wherein:
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis;Yak skin lamina reticularis clean up after in solid-liquid ratio(g/g)It is 1:7, temperature be 70 DEG C, extraction time 3 times, every time 24
Water is carried out under conditions of hour to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 4.5 μm through film mistake
After filter, subnatant is obtained;Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 590mmHg:1.30 i.e.
.
Flos Lycii concentrate refers to being added to be equivalent to 8 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 100 DEG C
At a temperature of extract, extraction time 2 times, 6 hours each extraction times, merging obtain extracting solution, which is pressing after filtering
Power is 0.5MPa, vacuum degree is concentrated under reduced pressure into 1 under conditions of being 550mmHg:1.18 to obtain the final product.
A kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet of embodiment 8, the facial mask is by following parts by weight(g)Original
Material is made:25 parts of yak skin lamina reticularis extracting solution, 6 parts of Flos Lycii concentrate.
Preparation method refers to:It weighs according to the ratio first, Flos Lycii concentrate, which is then added to yak skin lamina reticularis, carries
It takes in liquid, is uniformly mixed, under conditions of pressure is 650MPa, temperature is 20 DEG C, carried out according to a conventional method after being kept for 15 minutes
Molding, packaging.
Wherein:
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis;Yak skin lamina reticularis clean up after in solid-liquid ratio(g/g)It is 1:7, temperature be 85 DEG C, extraction time 3 times, every time 20
Water is carried out under conditions of hour to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 4.3 μm through film mistake
After filter, subnatant is obtained;Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 610mmHg:1.27 i.e.
.
Flos Lycii concentrate refers to being added to be equivalent to 10 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 60 DEG C
At a temperature of extract, extraction time 2 times, 6 hours each extraction times, merging obtain extracting solution, which is pressing after filtering
Power is 0.5MPa, vacuum degree is concentrated under reduced pressure into 1 under conditions of being 5750mmHg:1.28 to obtain the final product.
Claims (4)
1. a kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet, it is characterised in that:The facial mask by following parts by weight raw material
It is made:20 ~ 40 parts of yak skin lamina reticularis extracting solution, 5 ~ 10 parts of Flos Lycii concentrate;The yak skin lamina reticularis extracting solution refers to
By fresh yak in Qinghai-tibetWild YakYak skin clean up, then reject yak hair, it is small to be cut into long 5cm, width 5cm
Block, and papillaris pars above section and hypodermis layer are removed, obtain yak skin lamina reticularis;The yak skin lamina reticularis cleans up
Water is carried out afterwards to carry, and obtains extracting solution, which obtains subnatant after membrane filtration;The subnatant is concentrated into 1:1.05~
1.32 to obtain the final product;The condition that the water carries refers to that solid-liquid ratio is 1:5 ~ 10, temperature is 60 ~ 100 DEG C, extraction time 2 ~ 3 times, every time 2 ~
24 hours;The condition of the membrane filtration refers to that miillpore filter membrane aperture is 0.2 μm ~ 5.0 μm;The condition of the concentration is finger pressure
For 0.09MPa, vacuum degree is 500 ~ 620mmHg.
2. a kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet as described in claim 1, it is characterised in that:The matrimony vine
Flower concentrate refers to being added to be equivalent to 5 ~ 10 times of amount water of its weight grams after cleaning fresh Flos Lycii, at a temperature of 60 ~ 100 DEG C
Extraction, extraction time 2 ~ 3 times, 1 ~ 6 hour each extraction time, merging obtain extracting solution, and the extracting solution is through filtering, being concentrated under reduced pressure
To 1:1.10 ~ 1.35 to obtain the final product.
3. a kind of Yak-skin Gelatin original facial mask with protectiving ultraviolet as claimed in claim 2, it is characterised in that:The decompression
The condition of concentration is that finger pressure is 0.5MPa, and vacuum degree is 500~600mmHg.
4. a kind of preparation method of the Yak-skin Gelatin original facial mask with protectiving ultraviolet as described in claim 1, feature exist
In:It weighs, then Flos Lycii concentrate is added in yak skin lamina reticularis extracting solution according to the ratio first, be uniformly mixed, pressing
Under conditions of power is 500 ~ 800MPa, temperature is 10 ~ 30 DEG C, holding 10 ~ carry out molding according to a conventional method after forty minutes, packaging is
It can.
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CN110742824B (en) * | 2019-10-29 | 2022-12-27 | 南宁学院 | Preparation and application of cow hide composite extract |
Citations (4)
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CN103820517A (en) * | 2014-03-06 | 2014-05-28 | 中国科学院西北高原生物研究所 | Preparation method for yak skin micromolecular collagen capable of regulating human body energy metabolism |
CN104434741A (en) * | 2014-12-23 | 2015-03-25 | 吴辰 | Black wolfberry facial mask |
CN104940038A (en) * | 2015-05-28 | 2015-09-30 | 秦春哲 | Application of lycium ruthenicum anthocyanin in preparation of cosmetic and cosmetic containing lycium ruthenicum anthocyanin |
CN105273436A (en) * | 2014-07-18 | 2016-01-27 | 周子童 | Medlar flower pigment extraction technology |
-
2016
- 2016-01-29 CN CN201610063680.0A patent/CN105662998B/en not_active Expired - Fee Related
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103820517A (en) * | 2014-03-06 | 2014-05-28 | 中国科学院西北高原生物研究所 | Preparation method for yak skin micromolecular collagen capable of regulating human body energy metabolism |
CN105273436A (en) * | 2014-07-18 | 2016-01-27 | 周子童 | Medlar flower pigment extraction technology |
CN104434741A (en) * | 2014-12-23 | 2015-03-25 | 吴辰 | Black wolfberry facial mask |
CN104940038A (en) * | 2015-05-28 | 2015-09-30 | 秦春哲 | Application of lycium ruthenicum anthocyanin in preparation of cosmetic and cosmetic containing lycium ruthenicum anthocyanin |
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