CN105596261B - A kind of Yak-skin Gelatin original product and preparation method with beautifying face and moistering lotion - Google Patents
A kind of Yak-skin Gelatin original product and preparation method with beautifying face and moistering lotion Download PDFInfo
- Publication number
- CN105596261B CN105596261B CN201610063666.0A CN201610063666A CN105596261B CN 105596261 B CN105596261 B CN 105596261B CN 201610063666 A CN201610063666 A CN 201610063666A CN 105596261 B CN105596261 B CN 105596261B
- Authority
- CN
- China
- Prior art keywords
- yak
- skin
- extracting solution
- root
- refers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 108010010803 Gelatin Proteins 0.000 title claims abstract description 34
- 229920000159 gelatin Polymers 0.000 title claims abstract description 34
- 239000008273 gelatin Substances 0.000 title claims abstract description 34
- 235000019322 gelatine Nutrition 0.000 title claims abstract description 34
- 235000011852 gelatine desserts Nutrition 0.000 title claims abstract description 34
- 239000006210 lotion Substances 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 title description 2
- 235000001287 Guettarda speciosa Nutrition 0.000 claims abstract description 53
- 239000012141 concentrate Substances 0.000 claims abstract description 49
- 239000000047 product Substances 0.000 claims abstract description 35
- 241000628997 Flos Species 0.000 claims abstract description 34
- 239000000341 volatile oil Substances 0.000 claims abstract description 26
- 239000002994 raw material Substances 0.000 claims abstract description 14
- 241000125175 Angelica Species 0.000 claims description 52
- 238000000605 extraction Methods 0.000 claims description 52
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 33
- 239000012467 final product Substances 0.000 claims description 26
- 238000001914 filtration Methods 0.000 claims description 23
- 238000004140 cleaning Methods 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 11
- 239000012528 membrane Substances 0.000 claims description 10
- 238000005374 membrane filtration Methods 0.000 claims description 4
- 238000007796 conventional method Methods 0.000 claims description 3
- 102000008186 Collagen Human genes 0.000 abstract description 11
- 108010035532 Collagen Proteins 0.000 abstract description 11
- 229920001436 collagen Polymers 0.000 abstract description 11
- 241000213006 Angelica dahurica Species 0.000 abstract description 2
- 244000241838 Lycium barbarum Species 0.000 abstract description 2
- 235000015459 Lycium barbarum Nutrition 0.000 abstract description 2
- 239000002537 cosmetic Substances 0.000 abstract description 2
- 239000000835 fiber Substances 0.000 abstract description 2
- 239000013589 supplement Substances 0.000 abstract description 2
- 230000037303 wrinkles Effects 0.000 abstract description 2
- 230000000694 effects Effects 0.000 abstract 3
- 244000061520 Angelica archangelica Species 0.000 abstract 1
- 239000011149 active material Substances 0.000 abstract 1
- 230000004060 metabolic process Effects 0.000 abstract 1
- 230000003020 moisturizing effect Effects 0.000 abstract 1
- 210000003491 skin Anatomy 0.000 description 55
- 238000000194 supercritical-fluid extraction Methods 0.000 description 18
- 239000003921 oil Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 3
- 230000032683 aging Effects 0.000 description 2
- 230000003796 beauty Effects 0.000 description 2
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 description 1
- SQDAZGGFXASXDW-UHFFFAOYSA-N 5-bromo-2-(trifluoromethoxy)pyridine Chemical compound FC(F)(F)OC1=CC=C(Br)C=N1 SQDAZGGFXASXDW-UHFFFAOYSA-N 0.000 description 1
- 229920001287 Chondroitin sulfate Polymers 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 108010037362 Extracellular Matrix Proteins Proteins 0.000 description 1
- 102000010834 Extracellular Matrix Proteins Human genes 0.000 description 1
- 102000008946 Fibrinogen Human genes 0.000 description 1
- 108010049003 Fibrinogen Proteins 0.000 description 1
- 102000003886 Glycoproteins Human genes 0.000 description 1
- 108090000288 Glycoproteins Proteins 0.000 description 1
- 229920002683 Glycosaminoglycan Polymers 0.000 description 1
- 241000699666 Mus <mouse, genus> Species 0.000 description 1
- 241000699670 Mus sp. Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000010171 animal model Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 229940059329 chondroitin sulfate Drugs 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 210000002744 extracellular matrix Anatomy 0.000 description 1
- 229940012952 fibrinogen Drugs 0.000 description 1
- 230000003328 fibroblastic effect Effects 0.000 description 1
- 238000003304 gavage Methods 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 229920002674 hyaluronan Polymers 0.000 description 1
- 229960003160 hyaluronic acid Drugs 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 206010033675 panniculitis Diseases 0.000 description 1
- 210000003859 smegma Anatomy 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 210000004304 subcutaneous tissue Anatomy 0.000 description 1
- 210000000106 sweat gland Anatomy 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/92—Oral administration
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical & Material Sciences (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to a kind of Yak-skin Gelatin original product with beautifying face and moistering lotion, which is made from the following raw materials in parts by weight：200 ~ 400 parts of yak skin lamina reticularis extracting solution, 10 ~ 30 parts of Flos Lycii concentrate, 5 ~ 20 parts of root of Dahurain angelica concentrate, 0.5 ~ 3.5 part of Essential Oil of Radix Angelicae Dahuricae.The invention also discloses the preparation methods of the Yak-skin Gelatin original product.The present invention supplements collagen by raw material of the lamina reticularis collagen in yak in Qinghai-tibet skin, it is aided with the western fresh matrimony vine flower extract of Qinghai Province and Angelica Dahurica extract, using the snap action of Essential Oil of Radix Angelicae Dahuricae by active material in cosmetics, it is diffused into the deep layer of skin, enhance the collagen activity in skin, the integrality for keeping cuticula moisture and fibre structure, promotes the metabolism of skin histology, to achieve the purpose that generate good moist moisturizing, effect wrinkles eliminating vanishing effect to skin.
Description
Technical field
The present invention relates to cosmetic composition and its preparing technical field more particularly to a kind of yak skins with beautifying face and moistering lotion
Collagen and preparation method.
Background technology
Collagen is the main component of extracellular matrix, contains hyaluronic acid, chondroitin sulfate etc..Collagen and people
The structure of body skin collagen is similar, contains glycoprotein for non-soluble fiber shape, has surface-active and good compatibility, point
Contain a large amount of hydroxyl in son, there is moisture-keeping function, skin is made to keep elasticity.
Skin is made of epidermis, corium and subcutaneous tissue.Corium divides papillaris pars and lamina reticularis, collagenous fibres to be the master of corium
Ingredient is wanted, accounts for about 95%.With advancing age, fibroblastic synthesis capability declines, and lacks collagen, glue in skin
Connection solidification will occur for fibrinogen, and iuntercellular mucopolysaccharide is made to reduce, and skin will lose soft, elasticity and gloss, and aging occurs,
The fibrous fracture, lipoatrophia of corium, sweat gland and smegma are reduced simultaneously, so that skin color spot, wrinkle etc. is occurred a series of
Aging phenomenon.
Invention content
Technical problem to be solved by the invention is to provide a kind of effective Yak-skin Gelatin with beautifying face and moistering lotion is former
Product.
Another technical problem to be solved by this invention is to provide the preparation method of the Yak-skin Gelatin original product.
To solve the above problems, a kind of Yak-skin Gelatin original product with beautifying face and moistering lotion of the present invention, feature exist
In：The Yak-skin Gelatin original product is made from the following raw materials in parts by weight：200 ~ 400 parts of yak skin lamina reticularis extracting solution, Flos Lycii
10 ~ 30 parts of concentrate, 5 ~ 20 parts of root of Dahurain angelica concentrate, 0.5 ~ 3.5 part of Essential Oil of Radix Angelicae Dahuricae.
The yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakThe cleaning of yak skin it is dry
Only, yak hair is then rejected, long 5cm, width 5cm fritters is cut into, and remove papillaris pars above section and hypodermis layer, obtains yak
Ox-hide lamina reticularis；The yak skin lamina reticularis clean up after carry out water carry, obtain extracting solution, the extracting solution after membrane filtration,
Obtain subnatant；The subnatant is concentrated into 1：1.15 ~ 1.35 to obtain the final product.
The condition that the water carries refers to that solid-liquid ratio is 1：5 ~ 10, temperature is 60 ~ 100 DEG C, extraction time 2 ~ 3 times, every time 4 ~
24 hours.
The condition of the membrane filtration refers to that miillpore filter membrane aperture is 0.2 μm ~ 5.0 μm.
The condition of the concentration is that finger pressure is 0.09MPa, and vacuum degree is 00 ~ 620mmHg.
The Flos Lycii concentrate refers to being added to be equivalent to 5 ~ 10 times of amount water of its weight grams after cleaning fresh Flos Lycii,
It is extracted at a temperature of 60 ~ 100 DEG C, extraction time 2 ~ 3 times, 1 ~ 6 hour each extraction time, merging obtains extracting solution A, the extraction
Liquid A is through filtering, being concentrated into 1：1.20 ~ 1.35 to obtain the final product.
The root of Dahurain angelica concentrate refers to that the root of Dahurain angelica is obtained the dregs of a decoction using after supercritical extract；Its quality 5 is added in the dregs of a decoction
~ 10 times of amount water, extract, extraction time 2 ~ 3 times, 2 ~ 6 hours each extraction times at a temperature of 60 ~ 100 DEG C, merge extracting solution B,
Extracting solution B is concentrated into 1 through filtering under conditions of pressure is 0.09MPa, vacuum degree is 500 ~ 620mmHg：1.20~1.35
To obtain the final product.
The Essential Oil of Radix Angelicae Dahuricae refers to that the root of Dahurain angelica concentrate refers to extracting the root of Dahurain angelica using supercritical extraction, i.e.,
Obtain Essential Oil of Radix Angelicae Dahuricae.
The condition of the supercritical extraction refers to that extracting pressure is 15 ~ 25MPa, and temperature is 25 ~ 45 DEG C, and the time is 1 ~ 3
Hour, parsing pressure is 4 ~ 8 MPa, and resolution temperature is 25 ~ 55 DEG C.
A kind of preparation method of the Yak-skin Gelatin original product with beautifying face and moistering lotion as described above, it is characterised in that：First
It weighs, Flos Lycii concentrate, root of Dahurain angelica concentrate is added in yak skin lamina reticularis extracting solution according to the ratio then, be uniformly mixed,
Essential Oil of Radix Angelicae Dahuricae is added after spray-dried, pelletized, packed according to a conventional method.
Compared with the prior art, the present invention has the following advantages：
1, the present invention supplements collagen by raw material of the lamina reticularis collagen in yak in Qinghai-tibet skin, is aided with Qinghai Province west
Fresh matrimony vine flower extract and Angelica Dahurica extract.
2, the raw materials used in the present invention concentrated reflection be lamina reticularis collagen, solvent for use is pure water, avoid alkaline process,
The organic solvents such as enzyme process, acid system, gained molecular weight are concentrated, and are the quality products of beauty.
3, products obtained therefrom of the present invention has the function of beautifying face and moistering lotion after tested（Referring to table 1）.
With healthy Kunming small white mouse（Half male and half female, 4 week old, weight are tested at 18 ~ 22 grams by Gansu Chinese of Traditional Chinese Medicine SPF grades
Animal center provides【Quality certification number is SCXK (sweet)】）For experimental animal, by prepared Yak-skin Gelatin original product, with 3g/kg/
Experimental mice continuous gavage is administered 20 days in d, and sets blank control group.Detect blood and skin weight.
Influence of the 1 Yak-skin Gelatin original product of table to beauty
4, the present invention is not only simple for process, it is easy to accomplish, and without any additive, can use safely.
Specific implementation mode
A kind of Yak-skin Gelatin original product with beautifying face and moistering lotion of embodiment 1, the Yak-skin Gelatin original product is by following parts by weight
（g）Raw material be made：200 parts of yak skin lamina reticularis extracting solution, 10 parts of Flos Lycii concentrate, 5 parts of root of Dahurain angelica concentrate, root of Dahurain angelica volatilization
0.5 part of oil.
Preparation method refers to：It weighs according to the ratio first, Flos Lycii concentrate, root of Dahurain angelica concentrate is then added to yak
It in skin lamina reticularis extracting solution, is uniformly mixed, Essential Oil of Radix Angelicae Dahuricae is added after spray-dried, pelletized, packed according to a conventional method
.
Wherein：
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis；Yak skin lamina reticularis clean up after in solid-liquid ratio（g/g）It is 1：5, temperature be 60 DEG C, extraction time 2 times, every time 4
Water is carried out under conditions of hour to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 0.2 μm through film mistake
After filter, subnatant is obtained；Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 500mmHg：1.15 i.e.
.
Flos Lycii concentrate refers to being added to be equivalent to 5 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 60 DEG C
At a temperature of extract, extraction time 2 times, 1 hour each extraction time, merging obtain extracting solution A, extracting solution A exists after filtering
Pressure is 0.09MPa, vacuum degree is concentrated into 1 under conditions of being 500mmHg：1.20 to obtain the final product.
Root of Dahurain angelica concentrate refers to that the root of Dahurain angelica is obtained the dregs of a decoction using after supercritical extract；6 times of amount water of its quality are added in the dregs of a decoction,
It is extracted at a temperature of 60 DEG C, extraction time 2 times, 2 hours each extraction times, merges extracting solution B, extracting solution B is after filtering
It is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 500mmHg：1.20 to obtain the final product.
Essential Oil of Radix Angelicae Dahuricae refers to extracting the root of Dahurain angelica to get Essential Oil of Radix Angelicae Dahuricae using supercritical extraction.
The condition of above-mentioned supercritical extraction refers to that extracting pressure is 15MPa, and temperature is 25 DEG C, and the time is 1 hour, parsing
Pressure is 4 MPa, and resolution temperature is 25 DEG C.
A kind of Yak-skin Gelatin original product with beautifying face and moistering lotion of embodiment 2, the Yak-skin Gelatin original product is by following parts by weight
（g）Raw material be made：400 parts of yak skin lamina reticularis extracting solution, 30 parts of Flos Lycii concentrate, 20 parts of root of Dahurain angelica concentrate, the root of Dahurain angelica are waved
3.5 parts of hair oil.
Preparation method is the same as embodiment 1.
Wherein：
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis；Yak skin lamina reticularis clean up after in solid-liquid ratio（g/g）It is 1：10, temperature be 100 DEG C, extraction time 3 times, every time
Water is carried out under conditions of 24 hours to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 5.0 μm through film
After filtering, subnatant is obtained；Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 620mmHg：1.35
To obtain the final product.
Flos Lycii concentrate refers to being added to be equivalent to 10 times of amount water of its weight grams after cleaning fresh Flos Lycii, 100
It is extracted at a temperature of DEG C, extraction time 3 times, 6 hours each extraction times, merging obtains extracting solution A, and extracting solution A is after filtering
It is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 620mmHg：1.35 to obtain the final product.
Root of Dahurain angelica concentrate refers to that the root of Dahurain angelica is obtained the dregs of a decoction using after supercritical extract；10 times of amount water of its quality are added in the dregs of a decoction,
It is extracted at a temperature of 100 DEG C, extraction time 2 times, 6 hours each extraction times, merges extracting solution B, extracting solution B is after filtering
It is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 620mmHg：1.35 to obtain the final product.
Essential Oil of Radix Angelicae Dahuricae refers to extracting the root of Dahurain angelica to get Essential Oil of Radix Angelicae Dahuricae using supercritical extraction.
The condition of above-mentioned supercritical extraction refers to that extracting pressure is 25MPa, and temperature is 45 DEG C, and the time is 3 hours, parsing
Pressure is 8 MPa, and resolution temperature is 55 DEG C.
A kind of Yak-skin Gelatin original product with beautifying face and moistering lotion of embodiment 3, the Yak-skin Gelatin original product is by following parts by weight
（g）Raw material be made：200 parts of yak skin lamina reticularis extracting solution, 30 parts of Flos Lycii concentrate, 20 parts of root of Dahurain angelica concentrate, the root of Dahurain angelica are waved
0.8 part of hair oil.
Preparation method is the same as embodiment 1.
Wherein：
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis；Yak skin lamina reticularis clean up after in solid-liquid ratio（g/g）It is 1：5, temperature be 100 DEG C, extraction time 3 times, every time
Water is carried out under conditions of 24 hours to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 0.8 μm through film
After filtering, subnatant is obtained；Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 550mmHg：1.25
To obtain the final product.
Flos Lycii concentrate refers to being added to be equivalent to 5 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 100 DEG C
At a temperature of extract, extraction time 3 times, 6 hours each extraction times, merging obtain extracting solution A, extracting solution A exists after filtering
Pressure is 0.09MPa, vacuum degree is concentrated into 1 under conditions of being 550mmHg：1.25 to obtain the final product.
Root of Dahurain angelica concentrate refers to that the root of Dahurain angelica is obtained the dregs of a decoction using after supercritical extract；10 times of amount water of its quality are added in the dregs of a decoction,
It is extracted at a temperature of 70 DEG C, extraction time 2 times, 6 hours each extraction times, merges extracting solution B, extracting solution B is after filtering
It is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 550mmHg：1.25 to obtain the final product.
Essential Oil of Radix Angelicae Dahuricae refers to extracting the root of Dahurain angelica to get Essential Oil of Radix Angelicae Dahuricae using supercritical extraction.
The condition of above-mentioned supercritical extraction refers to that extracting pressure is 15MPa, and temperature is 45 DEG C, and the time is 1 hour, parsing
Pressure is 8 MPa, and resolution temperature is 25 DEG C.
A kind of Yak-skin Gelatin original product with beautifying face and moistering lotion of embodiment 4, the Yak-skin Gelatin original product is by following parts by weight
（g）Raw material be made：400 parts of yak skin lamina reticularis extracting solution, 10 parts of Flos Lycii concentrate, 5 parts of root of Dahurain angelica concentrate, root of Dahurain angelica volatilization
1.5 parts of oil.
Preparation method is the same as embodiment 1.
Wherein：
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis；Yak skin lamina reticularis clean up after in solid-liquid ratio（g/g）It is 1：10, temperature be 80 DEG C, extraction time 2 times, every time
Water is carried out under conditions of 14 hours to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 3.0 μm through film
After filtering, subnatant is obtained；Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 580mmHg：1.28
To obtain the final product.
Flos Lycii concentrate refers to being added to be equivalent to 10 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 60 DEG C
At a temperature of extract, extraction time 2 times, 1 hour each extraction time, merging obtain extracting solution A, extracting solution A exists after filtering
Pressure is 0.09MPa, vacuum degree is concentrated into 1 under conditions of being 580mmHg：1.28 to obtain the final product.
Root of Dahurain angelica concentrate refers to that the root of Dahurain angelica is obtained the dregs of a decoction using after supercritical extract；10 times of amount water of its quality are added in the dregs of a decoction,
It is extracted at a temperature of 60 ~ 100 DEG C, extraction time 2 times, 6 hours each extraction times, merges extracting solution B, extracting solution B passes through
After filter 1 is concentrated under conditions of pressure is 0.09MPa, vacuum degree is 580mmHg：1.30 to obtain the final product.
Essential Oil of Radix Angelicae Dahuricae refers to extracting the root of Dahurain angelica to get Essential Oil of Radix Angelicae Dahuricae using supercritical extraction.
The condition of above-mentioned supercritical extraction refers to that extracting pressure is 25MPa, and temperature is 25 DEG C, and the time is 1 hour, parsing
Pressure is 8 MPa, and resolution temperature is 25 DEG C.
A kind of Yak-skin Gelatin original product with beautifying face and moistering lotion of embodiment 5, the Yak-skin Gelatin original product is by following parts by weight
（g）Raw material be made：300 parts of yak skin lamina reticularis extracting solution, 20 parts of Flos Lycii concentrate, 10 parts of root of Dahurain angelica concentrate, the root of Dahurain angelica are waved
2.5 parts of hair oil.
Preparation method is the same as embodiment 1.
Wherein：
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis；Yak skin lamina reticularis clean up after in solid-liquid ratio（g/g）It is 1：8, temperature be 75 DEG C, extraction time 3 times, every time 18
Water is carried out under conditions of hour to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 4.0 μm through film mistake
After filter, subnatant is obtained；Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 590mmHg：1.30 i.e.
.
Flos Lycii concentrate refers to being added to be equivalent to 8 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 90 DEG C
At a temperature of extract, extraction time 2 times, 3 hours each extraction times, merging obtain extracting solution A, extracting solution A exists after filtering
Pressure is 0.09MPa, vacuum degree is concentrated into 1 under conditions of being 590mmHg：1.32 to obtain the final product.
Root of Dahurain angelica concentrate refers to that the root of Dahurain angelica is obtained the dregs of a decoction using after supercritical extract；8 times of amount water of its quality are added in the dregs of a decoction,
It is extracted at a temperature of 95 DEG C, extraction time 2 times, 4 hours each extraction times, merges extracting solution B, extracting solution B is after filtering
It is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 600mmHg：1.28 to obtain the final product.
Essential Oil of Radix Angelicae Dahuricae refers to extracting the root of Dahurain angelica to get Essential Oil of Radix Angelicae Dahuricae using supercritical extraction.
The condition of above-mentioned supercritical extraction refers to that extracting pressure is 20MPa, and temperature is 30 DEG C, and the time is 2 hours, parsing
Pressure is 6 MPa, and resolution temperature is 35 DEG C.
A kind of Yak-skin Gelatin original product with beautifying face and moistering lotion of embodiment 6, the Yak-skin Gelatin original product is by following parts by weight
（g）Raw material be made：250 parts of yak skin lamina reticularis extracting solution, 15 parts of Flos Lycii concentrate, 10 parts of root of Dahurain angelica concentrate, the root of Dahurain angelica are waved
1.0 parts of hair oil.
Preparation method is the same as embodiment 1.
Wherein：
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis；Yak skin lamina reticularis clean up after in solid-liquid ratio（g/g）It is 1：6, temperature be 85 DEG C, extraction time 2 times, every time 8
Water is carried out under conditions of hour to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 4.5 μm through film mistake
After filter, subnatant is obtained；Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 530mmHg：1.30 i.e.
.
Flos Lycii concentrate refers to being added to be equivalent to 6 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 80 DEG C
At a temperature of extract, extraction time 3 times, 2 hours each extraction times, merging obtain extracting solution A, extracting solution A exists after filtering
Pressure is 0.09MPa, vacuum degree is concentrated into 1 under conditions of being 530mmHg：1.30 to obtain the final product.
Root of Dahurain angelica concentrate refers to that the root of Dahurain angelica is obtained the dregs of a decoction using after supercritical extract；7 times of amount water of its quality are added in the dregs of a decoction,
It is extracted at a temperature of 75 DEG C, extraction time 2 times, 3 hours each extraction times, merges extracting solution B, extracting solution B is after filtering
It is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 590mmHg：1.32 to obtain the final product.
Essential Oil of Radix Angelicae Dahuricae refers to extracting the root of Dahurain angelica to get Essential Oil of Radix Angelicae Dahuricae using supercritical extraction.
The condition of above-mentioned supercritical extraction refers to that extracting pressure is 25MPa, and temperature is 30 DEG C, and the time is 2 hours, parsing
Pressure is 7 MPa, and resolution temperature is 40 DEG C.
A kind of Yak-skin Gelatin original product with beautifying face and moistering lotion of embodiment 7, the Yak-skin Gelatin original product is by following parts by weight
（g）Raw material be made：400 parts of yak skin lamina reticularis extracting solution, 30 parts of Flos Lycii concentrate, 12 parts of root of Dahurain angelica concentrate, the root of Dahurain angelica are waved
0.7 part of hair oil.
Preparation method is the same as embodiment 1.
Wherein：
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis；Yak skin lamina reticularis clean up after in solid-liquid ratio（g/g）It is 1：9, temperature be 65 DEG C, extraction time 3 times, every time 20
Water is carried out under conditions of hour to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 1.5 μm through film mistake
After filter, subnatant is obtained；Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 560mmHg：1.20 i.e.
.
Flos Lycii concentrate refers to being added to be equivalent to 8 times of amount water of its weight grams after cleaning fresh Flos Lycii, at 70 DEG C
At a temperature of extract, extraction time 3 times, 2 hours each extraction times, merging obtain extracting solution A, extracting solution A exists after filtering
Pressure is 0.09MPa, vacuum degree is concentrated into 1 under conditions of being 560mmHg：1.28 to obtain the final product.
Root of Dahurain angelica concentrate refers to that the root of Dahurain angelica is obtained the dregs of a decoction using after supercritical extract；10 times of amount water of its quality are added in the dregs of a decoction,
It is extracted at a temperature of 80 DEG C, extraction time 2 times, 3 hours each extraction times, merges extracting solution B, extracting solution B is after filtering
It is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 530mmHg：1.25 to obtain the final product.
Essential Oil of Radix Angelicae Dahuricae refers to extracting the root of Dahurain angelica to get Essential Oil of Radix Angelicae Dahuricae using supercritical extraction.
The condition of above-mentioned supercritical extraction refers to that extracting pressure is 22MPa, and temperature is 30 DEG C, and the time is 1.5 hours, solution
Analysis pressure is 6 MPa, and resolution temperature is 45 DEG C.
A kind of Yak-skin Gelatin original product with beautifying face and moistering lotion of embodiment 8, the Yak-skin Gelatin original product is by following parts by weight
（g）Raw material be made：380 parts of yak skin lamina reticularis extracting solution, 27 parts of Flos Lycii concentrate, 13 parts of root of Dahurain angelica concentrate, the root of Dahurain angelica are waved
3.0 parts of hair oil.
Preparation method is the same as embodiment 1.
Wherein：
Yak skin lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, so
After reject yak hair, be cut into long 5cm, width 5cm fritters, and remove papillaris pars above section and hypodermis layer, obtain yak skin
Lamina reticularis；Yak skin lamina reticularis clean up after in solid-liquid ratio（g/g）It is 1：5.5, temperature be 95 DEG C, extraction time 3 times, every time
Water is carried out under conditions of 24 hours to carry, and obtains extracting solution, the extracting solution is under conditions of miillpore filter membrane aperture is 2.5 μm through film
After filtering, subnatant is obtained；Subnatant is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 610mmHg：1.35
To obtain the final product.
Flos Lycii concentrate refers to being added to be equivalent to 10 times of amount water of its weight grams after cleaning fresh Flos Lycii, 100
It is extracted at a temperature of DEG C, extraction time 3 times, 6 hours each extraction times, merging obtains extracting solution A, and extracting solution A is after filtering
It is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 610mmHg：1.35 to obtain the final product.
Root of Dahurain angelica concentrate refers to that the root of Dahurain angelica is obtained the dregs of a decoction using after supercritical extract；7 times of amount water of its quality are added in the dregs of a decoction,
It is extracted at a temperature of 90 DEG C, extraction time 2 times, 3 hours each extraction times, merges extracting solution B, extracting solution B is after filtering
It is concentrated into 1 under conditions of pressure is 0.09MPa, vacuum degree is 600mmHg：1.22 to obtain the final product.
Essential Oil of Radix Angelicae Dahuricae refers to extracting the root of Dahurain angelica to get Essential Oil of Radix Angelicae Dahuricae using supercritical extraction.
The condition of above-mentioned supercritical extraction refers to that extracting pressure is 15MPa, and temperature is 45 DEG C, and the time is 2 hours, parsing
Pressure is 5 MPa, and resolution temperature is 35 DEG C.
Claims (6)
1. a kind of Yak-skin Gelatin original product with beautifying face and moistering lotion, it is characterised in that：The Yak-skin Gelatin original product is by following weight
The raw material of part is made：200 ~ 400 parts of yak skin lamina reticularis extracting solution, 10 ~ 30 parts of Flos Lycii concentrate, root of Dahurain angelica concentrate 5 ~ 20
Part, 0.5 ~ 3.5 part of Essential Oil of Radix Angelicae Dahuricae；The Flos Lycii concentrate refers to being added to be equivalent to its weight after cleaning fresh Flos Lycii
5 ~ 10 times of amount water of grams, are extracted, extraction time 2 ~ 3 times, merges 1 ~ 6 hour each extraction time at a temperature of 60 ~ 100 DEG C
To extracting solution A, extracting solution A is through filtering, being concentrated into 1：1.20 ~ 1.35 to obtain the final product；The root of Dahurain angelica concentrate refers to using the root of Dahurain angelica
After supercritical extract, the dregs of a decoction are obtained；5 ~ 10 times of amount water of its quality are added in the dregs of a decoction, extract, extract at a temperature of 60 ~ 100 DEG C
Number 2 ~ 3 times, merges extracting solution B at 2 ~ 6 hours each extraction times, and extracting solution B is 0.09MPa, very in pressure through filtering
Reciprocal of duty cycle is concentrated into 1 under conditions of being 500 ~ 620mmHg：1.20 ~ 1.35 to obtain the final product；The Essential Oil of Radix Angelicae Dahuricae refers to by the root of Dahurain angelica using super
Gained after critical extraction；
Preparation method：It weighs according to the ratio first, Flos Lycii concentrate, root of Dahurain angelica concentrate is then added to yak skin lamina reticularis
It in extracting solution, is uniformly mixed, Essential Oil of Radix Angelicae Dahuricae is added after spray-dried, pelletized, packed according to a conventional method.
2. a kind of Yak-skin Gelatin original product with beautifying face and moistering lotion as described in claim 1, it is characterised in that：The yak skin
Lamina reticularis extracting solution refers to by fresh yak in Qinghai-tibetWild YakYak skin clean up, then reject yak hair,
It is cut into long 5cm, width 5cm fritters, and removes papillaris pars above section and hypodermis layer, obtains yak skin lamina reticularis；The yak
Ox-hide lamina reticularis carries out water after cleaning up and carries, and obtains extracting solution, which obtains subnatant after membrane filtration；It will be described
Subnatant is concentrated into 1：1.15 ~ 1.35 to obtain the final product.
3. a kind of Yak-skin Gelatin original product with beautifying face and moistering lotion as claimed in claim 2, it is characterised in that：What the water carried
Condition refers to that solid-liquid ratio is 1：5 ~ 10, temperature is 60 ~ 100 DEG C, extraction time 2 ~ 3 times, 4 ~ 24 hours every time.
4. a kind of Yak-skin Gelatin original product with beautifying face and moistering lotion as claimed in claim 2, it is characterised in that：The membrane filtration
Condition refer to miillpore filter membrane aperture be 0.2 μm ~ 5.0 μm.
5. a kind of Yak-skin Gelatin original product with beautifying face and moistering lotion as claimed in claim 2, it is characterised in that：The concentration
Condition is that finger pressure is 0.09MPa, and vacuum degree is 500 ~ 620mmHg.
6. a kind of Yak-skin Gelatin original product with beautifying face and moistering lotion as described in claim 1, it is characterised in that：It is described overcritical
The condition of extraction refers to that extracting pressure is 15 ~ 25MPa, and temperature is 25 ~ 45 DEG C, and the time is 1 ~ 3 hour, and parsing pressure is 4 ~ 8
MPa, resolution temperature are 25 ~ 55 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610063666.0A CN105596261B (en) | 2016-01-29 | 2016-01-29 | A kind of Yak-skin Gelatin original product and preparation method with beautifying face and moistering lotion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610063666.0A CN105596261B (en) | 2016-01-29 | 2016-01-29 | A kind of Yak-skin Gelatin original product and preparation method with beautifying face and moistering lotion |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105596261A CN105596261A (en) | 2016-05-25 |
| CN105596261B true CN105596261B (en) | 2018-10-09 |
Family
ID=55976999
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610063666.0A Expired - Fee Related CN105596261B (en) | 2016-01-29 | 2016-01-29 | A kind of Yak-skin Gelatin original product and preparation method with beautifying face and moistering lotion |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105596261B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107353322A (en) * | 2017-03-17 | 2017-11-17 | 中国科学院西北高原生物研究所 | A kind of yak skin polypeptide products with anti-oxidation efficacy, preparation method and application |
| CN107362356A (en) * | 2017-03-17 | 2017-11-21 | 中国科学院西北高原生物研究所 | A kind of Yak-skin Gelatin original protein product with hemostasia effect and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102614499B (en) * | 2012-03-15 | 2013-09-11 | 中国科学院西北高原生物研究所 | Yak skin collagen compound traditional Tibetan medicine with anti-fatigue effect and preparation process thereof |
| CN103820517B (en) * | 2014-03-06 | 2016-03-30 | 中国科学院西北高原生物研究所 | The preparation method of the yak skin micromolecular collagen of regulation and control human body energy metabolism |
| CN105147727A (en) * | 2015-09-21 | 2015-12-16 | 西南科技大学 | Preparation method of Qinghai-Tibet plateau yak skin colla corii asini |
-
2016
- 2016-01-29 CN CN201610063666.0A patent/CN105596261B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN105596261A (en) | 2016-05-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110731924B (en) | Enhanced anti-aging cosmetic compositions | |
| CN104042559B (en) | There is natural composition and the natural cosmetics of Whitening, spot effect | |
| US9226886B2 (en) | Method for manufacturing a cosmetic bio-cellulose mask pack sheet and use thereof | |
| RU2492850C2 (en) | Fibroblast growth agent | |
| KR20120012904A (en) | Cosmetic compositions for improving breast augmentation or skin elasticity | |
| CN102113987A (en) | Cosmetic containing natural plant extractives and preparation method thereof | |
| CN105434209A (en) | Composition for beautifying, removing wrinkles, tightening and shaping and preparation method thereof | |
| CN104055714A (en) | Moisturizing cosmetic composition and preparation method thereof | |
| KR20170012810A (en) | Hydrogel pack comprising natural petals | |
| CN115006308B (en) | Reverse age fine anti-aging essence | |
| CN105596261B (en) | A kind of Yak-skin Gelatin original product and preparation method with beautifying face and moistering lotion | |
| CN106309260B (en) | A kind of Radix Notoginseng is preserved youthful looks facial mask | |
| CN109157449B (en) | Anti-aging moisturizing essence and preparation process thereof | |
| CN106074190B (en) | A kind of anti-aging visage block cream and preparation method thereof | |
| CN103705431B (en) | A kind of fish source collagen antioxidant peptide beauty mask and preparation method thereof | |
| KR102168532B1 (en) | Cosmetic composition for enhancing skin elasticity or improving skin wrinkle containing herb extracts | |
| CN105662998B (en) | A kind of Yak-skin Gelatin original facial mask and preparation method with protectiving ultraviolet | |
| CN103550129A (en) | Plant composite polysaccharide and preparation method and application thereof | |
| CN102764226A (en) | Eyebrow nourishing liquid, and preparation method and application thereof | |
| JP2006241130A (en) | Function of ameliorating collagen fiber formation and wrinkle and flabbiness of human body skin to enhance lifting effect through using polymer component of water-soluble polysaccharide in bracket fungus of the genus fomes | |
| KR102178888B1 (en) | Cosmetic composition for enhancing skin elasticity or improving skin wrinkle containing herb extracts | |
| KR102157210B1 (en) | The functional cosmetic composition comprising extract of natural micro organism-fermented black ginseng | |
| CN106038375A (en) | Quantum cell proliferation medical skin shining facial mask and preparation method | |
| CN106214581A (en) | A kind of cosmetic composition containing black Fructus Lycii extract and disposable sleep mask | |
| CN112870098B (en) | Composition containing acetylated sodium hyaluronate and having wrinkle removing effect and preparation method and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20181009 |