CN104523547A - Preparation process research of andrias davidianus blanchard facial mask and application method of andrias davidianus blanchard facial mask - Google Patents
Preparation process research of andrias davidianus blanchard facial mask and application method of andrias davidianus blanchard facial mask Download PDFInfo
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- CN104523547A CN104523547A CN201410826784.3A CN201410826784A CN104523547A CN 104523547 A CN104523547 A CN 104523547A CN 201410826784 A CN201410826784 A CN 201410826784A CN 104523547 A CN104523547 A CN 104523547A
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- andrias davidianus
- davidianus blanchard
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- facial film
- facial mask
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Abstract
The invention relates to the field of application of nutritional components of andrias davidianus blanchard skins, and in particular provides a development technology research content of a facial mask which efficiently uses the nutritional components of the andrias davidianus blanchard skins. A preparation method of the facial mask comprises the following steps: separating the skins and flesh of andrias davidianus blanchard, cleaning the andrias davidianus blanchard skins, performing freeze drying on the andrias davidianus blanchard skins under the conditions that the vacuum degree is 0.06Mpa and the temperature is -56 DEG C, freeze-drying for 24 hours, grinding into powder, screening by using a 40-mesh sieve, putting the andrias davidianus blanchard skin powder, water and hydrochloric acid into a hydrolysis cylinder according to a proportion that the ratio of the andrias davidianus blanchard skin powder to water to hydrochloric acid is 1:1.3:2, soaking to the greatest extent, uniformly stirring, heating until a mixture is boiled, performing refluxing, hydrolyzing for 20 hours at 112-114 DEG C, stopping flow addition, catching acid for 4 hours, stopping heating, cooling to 60 DEG C, performing pressure reduction and filtration, and adding a 0.01-0.2M disodium hydrogen phosphate-citrate acid buffer solution of which the volume is 1-3 times that of a filtrate and the pH value is 6-8 and 1wt% of a complex enzyme into the filtrate, wherein the complex enzyme consists of 0.05-0.2% pepsin, 0.2-0.5% serine protease and 0.05-0.2% lysozyme in a ratio of 1:1:1; performing enzymolysis for 24-48 hours; and centrifuging to obtain supernatant liquid, performing separation by using an ultra-filtration membrane separator, collecting liquid with a molecular weight of less than 4000 Daltons, treating the collected liquid by using macroporous adsorption resin and activated carbon, and then freeze-drying to obtain basic substances of the facial mask.
Description
Technical field
A kind of preparation technology of Andrias davidianus Blanchard facial film is provided.
Background technology
Andrias davidianus Blanchard (Andrias davidianus Blanchard) popular name " frog WAYU ", belongs to Amphibia, Caudata, Cryptobranchidae, is national second class protection animal.Along with the increase of artificial cultivation quantity, the secondary fish of parton allows to develop.Andrias davidianus Blanchard skin and mucus are rich in several amino acids and a large amount of collagen protein, also containing multiple hormone and Magainin, have stronger antibacterial action, can alleviate the harm of external environment to skin.And energy activating cell, improve skin problem.Product of the present invention has nutritional labeling efficient absorption, protects skin, improves skin microcirculation, nurses one's health the effect of repairing skin, can maintain the health of skin.
Facial film is a kind of carrier of face beautifying health keeping product, applies ointment or plaster at 15 ~ 30 minutes on the face.After the nutrient of skin care products is slowly absorbed by the skin, the film namely unloaded down, it integrates clean, nursing, nutrition skin of face three kinds of functions, be the conventional cosmetics of a class.Along with the raising of living standards of the people, increasing women pays close attention to facial appearance, with advancing age, skin, by the effect of the pollutant in ultraviolet and air, easily lacks nutrition, destroys the keratin of skin, cause pachylosis, corse sweat pore, the colour of skin is obscure.How in daily life by the mode of facial film, nourishing can be reached, repair damaged skin, to become problem in the urgent need to address.
For solving the problems of the technologies described above, the invention provides one and skin can be allowed fully to absorb nutrition, deeply nourish and repair facial film and the using method thereof of damaged skin.
Summary of the invention
The Study on Preparation of Andrias davidianus Blanchard facial film, it is characterized in that, be separated Andrias davidianus Blanchard skin and flesh, cleaning Andrias davidianus Blanchard skin, Andrias davidianus Blanchard skin is carried out lyophilization, vacuum 0.06Mpa, temperature-56 DEG C, lyophilizing 24h, beat powder, cross 40 mesh sieves, get Andrias davidianus Blanchard corium farinosum end, water, hydrochloric acid is put in hydrolysis cylinder, by Andrias davidianus Blanchard corium farinosum end: water: hydrochloric acid (1:1.3:2) proportioning, immersion stirs evenly as far as possible, be heated to boil, backflow, 112 ~ 114 DEG C of hydrolysis 20h, stop adding stream, catch up with sour 4h, stop heating, be cooled to 60 DEG C, filtration under diminished pressure, 0.01 ~ 0.2M sodium hydrogen phosphate-citrate buffer solution and 1% compound enzyme of 1 ~ 3 times of volume pH7 ~ 8 is added to filtrate, described compound enzyme is 0.05 ~ 0.2% pepsin, 0.2 ~ 0.5% serine protease, 0.05 ~ 0.2% lysozyme, ratio is 1:1:1, enzymolysis 24 ~ 48 hours.Centrifuging and taking supernatant, adopts Ultra filtration membrane device to be separated, gets the liquid that molecular weight is below 4000 dalton, by collected liquid by macroporous adsorbent resin and active carbon postlyophilization, and obtained facial film basic substance.
Andrias davidianus Blanchard facial film Study on Preparation of the present invention, it is characterized in that, described facial film comprises as follows: Andrias davidianus Blanchard skin extract: 10 ~ 20 parts.
Andrias davidianus Blanchard facial film Study on Preparation of the present invention, it is characterized in that, described repairing paste also comprises as follows: water: 30 ~ 50, glycerol: 10-20 part, butanediol: 10 ~ 20 parts, hyaluronic acid: 10 ~ 15 parts, vitamin B3:5-10 part, Moisture factor: 5-10 part, allantoin: 8 ~ 15 parts.
The using method of facial film of the present invention, is characterized in that, the method comprises the steps:
(1) clean face and cervical region skin;
(2) take out facial film to launch to spread on full face, available finger is gently pressed and is made it completely docile, and unnecessary essence is applied in cervical region;
(3) keep taking off for 30 minutes;
(4) massage face and cervical region gently, remaining essence is absorbed completely by face.
Claims (4)
1. the Study on Preparation of Andrias davidianus Blanchard facial film, it is characterized in that, be separated Andrias davidianus Blanchard skin and flesh, cleaning Andrias davidianus Blanchard skin, Andrias davidianus Blanchard skin is carried out lyophilization, vacuum 0.06Mpa, temperature-56 DEG C, lyophilizing 24h, beat powder, cross 40 mesh sieves, get Andrias davidianus Blanchard corium farinosum end, water, hydrochloric acid is put in hydrolysis cylinder, by Andrias davidianus Blanchard corium farinosum end: water: hydrochloric acid (1:1.3:2) proportioning, immersion stirs evenly as far as possible, be heated to boil, backflow, 112 ~ 114 DEG C of hydrolysis 20h, stop adding stream, catch up with sour 4h, stop heating, be cooled to 60 DEG C, filtration under diminished pressure, 0.01 ~ 0.2M sodium hydrogen phosphate-citrate buffer solution and 1% compound enzyme of 1 ~ 3 times of volume pH7 ~ 8 is added to filtrate, described compound enzyme is 0.05 ~ 0.2% pepsin, 0.2 ~ 0.5% serine protease, 0.05 ~ 0.2% lysozyme, ratio is 1:1:1, enzymolysis 24 ~ 48 hours, centrifuging and taking supernatant, adopts Ultra filtration membrane device to be separated, gets the liquid that molecular weight is below 4000 dalton, by collected liquid by macroporous adsorbent resin and active carbon postlyophilization, and obtained Andrias davidianus Blanchard skin extraction material.
2. Andrias davidianus Blanchard facial film as claimed in claim 1, it is characterized in that, described facial film comprises Andrias davidianus Blanchard skin extract: 10 ~ 20 parts.
3. Andrias davidianus Blanchard facial film as claimed in claim 1, it is characterized in that, described facial film also comprises as follows: water: 30 ~ 50, glycerol: 10-20 part, butanediol: 10 ~ 20 parts, hyaluronic acid: 10 ~ 15 parts, vitamin B3:5-10 part, Moisture factor: 5-10 part, allantoin: 8 ~ 15 parts.
4. the using method of the facial film as described in claim 1-3 any one, is characterized in that, the method comprises the steps:
(1) clean face and cervical region skin;
(2) take out facial film to launch to spread on full face, available finger is gently pressed and is made it completely docile, and unnecessary essence is applied in cervical region;
(3) keep taking off for 30 minutes;
(4) massage face and cervical region gently, remaining essence is absorbed completely by face.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410826784.3A CN104523547A (en) | 2014-12-29 | 2014-12-29 | Preparation process research of andrias davidianus blanchard facial mask and application method of andrias davidianus blanchard facial mask |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410826784.3A CN104523547A (en) | 2014-12-29 | 2014-12-29 | Preparation process research of andrias davidianus blanchard facial mask and application method of andrias davidianus blanchard facial mask |
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| CN104523547A true CN104523547A (en) | 2015-04-22 |
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| CN201410826784.3A Pending CN104523547A (en) | 2014-12-29 | 2014-12-29 | Preparation process research of andrias davidianus blanchard facial mask and application method of andrias davidianus blanchard facial mask |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105232583A (en) * | 2015-10-23 | 2016-01-13 | 陕西龙香堂生物工程股份有限公司 | Application of andrias davidianus skin powder as anti-gastric ulcer medicine |
| CN105832645A (en) * | 2016-06-15 | 2016-08-10 | 通江县光泰科技发展有限责任公司 | Giant salamander biological organic mask and preparation method thereof |
| CN106491499A (en) * | 2016-12-06 | 2017-03-15 | 钦州市高新技术产业服务中心 | A kind of biological organic facial film and preparation method thereof |
| CN108272651A (en) * | 2018-03-13 | 2018-07-13 | 汉中天成生物工程有限公司 | The application of giant salamander collagen and the facial mask of the collagen containing giant salamander and preparation method thereof |
| CN110623860A (en) * | 2019-09-24 | 2019-12-31 | 深圳润朗医药科技有限公司 | Giant salamander active peptide and hyaluronic acid composition capable of effectively promoting fibroblast proliferation |
| CN112263528A (en) * | 2020-10-26 | 2021-01-26 | 广东美集科技有限公司 | Collagen jelly mask and preparation and use methods thereof |
| CN113398004A (en) * | 2021-07-27 | 2021-09-17 | 四川原石科技有限公司 | Giant salamander peptide-hyaluronic acid mixture and preparation method and application thereof |
-
2014
- 2014-12-29 CN CN201410826784.3A patent/CN104523547A/en active Pending
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| 叶欣，等: "人工饲养大鲵皮胶原蛋白肽提取工艺研究", 《肉类工业》 * |
| 孙翰昌: "不同规格大鲵消化酶活性的比较研究", 《水产科学》 * |
| 李华: "大鲵皮中胶原蛋白的提取及性质研究", 《淡水渔业》 * |
| 顾赛麒，等: "人工养殖大鲵皮胶原蛋白的性质研究", 《食品科学》 * |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105232583A (en) * | 2015-10-23 | 2016-01-13 | 陕西龙香堂生物工程股份有限公司 | Application of andrias davidianus skin powder as anti-gastric ulcer medicine |
| CN105832645A (en) * | 2016-06-15 | 2016-08-10 | 通江县光泰科技发展有限责任公司 | Giant salamander biological organic mask and preparation method thereof |
| CN106491499A (en) * | 2016-12-06 | 2017-03-15 | 钦州市高新技术产业服务中心 | A kind of biological organic facial film and preparation method thereof |
| CN108272651A (en) * | 2018-03-13 | 2018-07-13 | 汉中天成生物工程有限公司 | The application of giant salamander collagen and the facial mask of the collagen containing giant salamander and preparation method thereof |
| CN110623860A (en) * | 2019-09-24 | 2019-12-31 | 深圳润朗医药科技有限公司 | Giant salamander active peptide and hyaluronic acid composition capable of effectively promoting fibroblast proliferation |
| CN110623860B (en) * | 2019-09-24 | 2022-05-20 | 深圳润朗医药科技有限公司 | Giant salamander active peptide and hyaluronic acid composition capable of effectively promoting fibroblast proliferation |
| CN112263528A (en) * | 2020-10-26 | 2021-01-26 | 广东美集科技有限公司 | Collagen jelly mask and preparation and use methods thereof |
| CN113398004A (en) * | 2021-07-27 | 2021-09-17 | 四川原石科技有限公司 | Giant salamander peptide-hyaluronic acid mixture and preparation method and application thereof |
| CN113398004B (en) * | 2021-07-27 | 2022-04-26 | 四川原石科技有限公司 | Giant salamander peptide-hyaluronic acid mixture and preparation method and application thereof |
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Application publication date: 20150422 |