CN104083299A - Preparation method and product of deep sea fish skin collagen polypeptide peeling mask - Google Patents
Preparation method and product of deep sea fish skin collagen polypeptide peeling mask Download PDFInfo
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- CN104083299A CN104083299A CN201410305857.4A CN201410305857A CN104083299A CN 104083299 A CN104083299 A CN 104083299A CN 201410305857 A CN201410305857 A CN 201410305857A CN 104083299 A CN104083299 A CN 104083299A
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Abstract
The invention discloses a collagen polypeptide peeling mask which is mainly prepared from the following raw materials in parts by weight: 2-5 parts of hydroxyethyl cellulose, 3-7 parts of arbutin, 1-1.5 parts of sodium alga acid, 4-5 parts of polyethylene glycol, 3.5-4.0 parts of fish skin collagen polypeptide, 6.3-7.0 parts of trehalose, 0.15-0.3 part of grape seed extract, 2-4 parts of licorice root extract, 0.1-0.2 part of phycocyanin, 0.05-0.15 part of antioxidant, 0.5-1.5 parts of preservative, 0.3-0.6 part of compound antibacterial agent, 3-7 parts of glycerinum, 1-3 parts of water-soluble azone and 100-120 parts of natural hydrosol or flower water. The preparation method comprises the following steps: obtaining an intermediate product solution A; obtaining an intermediate product solution B on the basis of the intermediate product solution A; obtaining an intermediate product solution C on the basis of the intermediate product solution B; and finally, adding the residual raw materials into the intermediate product solution C, pouring the obtained materials into a mold for molding, drying at the temperature of 50 DEG C, thereby obtaining the collagen polypeptide peeling mask. The invention also discloses a preparation method of the collagen polypeptide peeling mask.
Description
Technical field
The present invention relates to a kind of daily chemical product, be specifically related to a kind of preparation method and collagen polypeptide washing facial film thereof of deep-sea fish skin collagen polypeptide washing facial film.
Background technology
Collagen exists in a large number in animal connective tissue, accounts for 30 of total protein concentration, is distributed in the tissue such as skin, skeleton, tendon, flesh sheath, ligament, sarolemma, blood vessel, cornea of animal.Its peculiar property is to form high-intensity insoluble fibre, not only in ripe tissue, plays structure function, and developmental tissue is had to orientation.
Collagen protein is a kind of white, transparent, branchiess fibril, and molecular weight is 300,000 dalton, is the right-handed helix structure being wound by the α chain of three left hand helixs.The filamentary structure of collagen protein uniqueness and good biocompatibility thereof and low antigenicity become the popular research topic of the cosmetics of super quality, functional health product and biomedical material.Collagen protein is the main protein composition of skin peptide tissue, and its chemical composition, structure are given the basis of its beauty treatment, and it has the beauty treatment effects such as whitening, moisturizing, wrinkle resistant, reparation, nutrition, fat-reducing.
With advancing age, fibroblastic synthesis capability in skin declines, collagen fiber have occurred crosslinked, iuntercellular mucopolysaccharide is reduced, skin just can follow the string and gloss, simultaneously, due to factors such as fibrous fracture, lipoatrophy, sweat gland and the smegma minimizings of skin corium, skin is prone to a series of catabiosis such as mottle, wrinkle.Supplementing enough collagen protein can stimulate the secretion from differentiation row collagen protein of fibroblast in skin corium, and generting machanism and metabolic function recover normal, and then effective delaying skin lax and aging voluntarily to make collagen protein.Zoopery shows, uses after the mastic coating skin that contains collagen protein, and epiderm skin and dermis can be improved effectively, and has promoted the synthetic of the interior collagen of skin.
At present, the source of collagen protein is mainly confined to Lu Sheng mammal.But in recent years, due to taking place frequently and religious reasons of bovine spongiform encephalopathy, foot and mouth disease, aquatic collagen protein receives people's concern gradually.China is a processing of aquatic products big country.
In aquatic products processing enterprise production process, can produce a large amount of fish skin, fishbone, fish head, internal organs, shell the like waste, these garbages are used to produce feedstuff except fraction, and major part is dropped, and has caused the waste of environmental pollution and resource.Wherein fish skin is main garbage, in its dry, more than 70 be collagen protein, the market demand of collagen protein is very large, and international market price does not coexist 300～2000 yuan of per kilograms not etc. according to quality, if this resource obtains effective exploitation, will produce the added value of several hundred million units.In addition, collagen protein of fish skin rich content, is easy to extract function admirable.Raw material used in the present invention is got so deep-sea, pure free of contamination Alaska wall pollack fish skin on daytime.Wall pollack is one of important processing of aquatic products fingerling of China, and main concentrated Shandong District can obtain the disposal from fishery product processing of a large amount of production collagen polypeptides like this.
It has been generally acknowledged that and in cosmetics, directly add macromolecular natural collagen to be difficult to be absorbed by the skin, therefore collagen egg all adopts the hydrolytic collagen of molecular weight when as skin protection raw material.Deep-sea fish skin collagen peptide used in the present invention, is that the collagen scleroprotein orientation that adopts enzyme directional enzymatic technology that human body is difficult to digest and assimilate cuts into the small active peptides that is applicable to absorption of human body, has strengthened its water solublity and permeability.In facial film, collagen polypeptide combines with MEIGUI CHUNLU, trehalose, inulin isoreactivity material, supplement skin nutrition composition, increase skin elasticity, prevention and to anti-wrinkle, slow down aging.Trehalose can be used as skin penetrant and wetting agent in addition, increases the absorption of skin to nutritional labeling.
Summary of the invention
For the deficiencies in the prior art, the invention provides a kind of preparation method and collagen polypeptide washing facial film goods thereof of the deep-sea fish skin collagen polypeptide washing facial film addressing the above problem.
The present invention for achieving the above object and adopt technical scheme be:
A preparation method for deep-sea fish skin collagen polypeptide washing facial film, it comprises the steps:
(1). the preparation of raw material
Prepare following raw material according to following parts by weight:
(2). the preparation of intermediate product A solution
Arbutin, hydroxyethyl-cellulose, sodium alginate, the Polyethylene Glycol in step (1), prepared are joined to parts by weight is: 48～52 natural plants hydrosol or Hua Shuizhong, carry out heated and stirred, and being heated to temperature is 60 DEG C～70 DEG C; Mixing speed is 100r/min～150r/min, until after Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol dissolve completely, be cooled to 20 DEG C～30 DEG C, obtains intermediate product A solution, for subsequent use;
(3). the preparation of intermediate product B solution
Fishskin collagen polypeptide, the trehalose in step (1), prepared are joined to parts by weight is: 20～30 natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 10 DEG C～20 DEG C; In temperature be again: 10 DEG C～20 DEG C, pressure is: under the vacuum condition of 1500pa～1800pa, stir, mixing speed is 130r/min～150r/min, until fishskin collagen polypeptide, trehalose dissolve completely, then heat, after being heated to temperature and being 20 DEG C～30 DEG C, step (2) is obtained to intermediate product A solution to add wherein, insulation, obtains intermediate product B solution, for subsequent use;
(4). the preparation of intermediate product C solution
Semen Vitis viniferae extract, licorice root extract, the phycocyanin in step (1), prepared are joined to remaining natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 20 DEG C～30 DEG C; In temperature be again: 20 DEG C～30 DEG C, pressure is: under the vacuum condition of 1200pa～1500pa, stir, mixing speed is 120r/min～130r/min, until Semen Vitis viniferae extract, licorice root extract, phycocyanin dissolve completely, step (3) is obtained to intermediate product B solution to add wherein, cooling, obtain intermediate product C solution, for subsequent use;
(5). the preparation of collagen polypeptide washing facial film
Antioxidant, antiseptic, Compound Resisting microbial inoculum, glycerol, the water-solubleazone in step (1), prepared are joined to step (4) to be obtained in intermediate product C solution, under the condition of 40 DEG C～50 DEG C of temperature, mixing speed is under the condition of 100r/min～120r/min, after stirring 2～2.5h, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Described step (2), it also comprises the steps:
(21) extraction of Arbutin
Leaf of pear tree being dried, pulverizing, being sieved, use alcoholic solution dipping, is, under the temperature conditions of 45 DEG C～55 DEG C, after dipping 6.5～7.5h, to use ultrafiltration membrance filter in temperature, collects filter liquor; Use macroporous resin, filter liquor is carried out to Adsorption and desorption attached, collect stripping liquid, be rotated evaporation, concentrate, vacuum freeze-drying, obtain Arbutin.
Natural plants hydrosol in described step (1) or flower water, it is a kind of and combination in rose wate, lavender flower water, Flos Osmanthi Fragrantis water, Magnolia denudata Desr. flower water, Flos Lilii viriduli water and Cananga odorata hydrosol, Lignum Santali Albi hydrosol, Camellia sinensis hydrosol; Fishskin collagen polypeptide in described step (1), its raw material is taken from natural pure free of contamination deep-sea wall pollack fish skin.
Described natural plants hydrosol or flower water, it be by the natural plants hydrosol of normal concentration or flower water, the 100 saturated hydrosols that are condensed into by the way of distillation or colored water.
Antiseptic in described step (1), it is methyl hydroxybenzoate and propylparaben, described methyl hydroxybenzoate and the weight ratio of propylparaben are: 2.5～3:1.2～1.5.
Antioxidant in described step (1), it is tertiary butyl-4-hydroxy methoxybenzene.
The collagen polypeptide washing facial film that adopts the preparation method of above-mentioned deep-sea fish skin collagen polypeptide washing facial film to prepare, it is mainly prepared from by the raw material of following parts by weight:
First, Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol being dissolved in to parts by weight is: 48～52 natural plants hydrosol or flower water, obtain intermediate product A solution;
Secondly, fishskin collagen polypeptide, trehalose are dissolved in to parts by weight are: 20～30 natural plants hydrosol or Hua Shuizhong, then intermediate product A solution is added wherein, obtain intermediate product B solution;
Again, Semen Vitis viniferae extract, licorice root extract, phycocyanin are dissolved in to remaining natural plants hydrosol or Hua Shuizhong, then intermediate product B solution is added wherein, obtain intermediate product C solution;
Finally, remaining raw material is joined in intermediate product C solution, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Described natural plants hydrosol or flower water, it is a kind of and combination in rose wate, lavender flower water, Flos Osmanthi Fragrantis water, Magnolia denudata Desr. flower water, Flos Lilii viriduli water and Cananga odorata hydrosol, Lignum Santali Albi hydrosol, Camellia sinensis hydrosol; Described natural plants hydrosol or flower water, it be by the natural plants hydrosol of normal concentration or flower water, the 100 saturated hydrosols that are condensed into by the way of distillation or colored water; Described fishskin collagen polypeptide, its raw material is taken from natural pure free of contamination deep-sea wall pollack fish skin.
Described antiseptic, it is methyl hydroxybenzoate and propylparaben, described methyl hydroxybenzoate and the weight ratio of propylparaben are: 2.5～3:1.2～1.5.
Described antioxidant, it is tertiary butyl-4-hydroxy methoxybenzene.
Beneficial effect of the present invention:
1. collagen polypeptide used in the present invention, raw material, from processing of aquatic products garbage, makes full use of processing of aquatic products garbage, not only can reduce the waste of environmental pollution and resource, and can increase the added value of processing of aquatic products, increases economic efficiency.
2. in collagen protein of fish skin, aminoacid composition approaches with the aminoacid composition of human body skin collagen protein, and with respect to the collagen polypeptide that is organized as raw material production with terrestrial animal or fresh water animals have pollution-free, without advantages such as source of disease (as bovine spongiform encephalopathy, foot and mouth disease, bird flu etc.) hidden danger.
3. the present invention has adopted Arbutin, Arbutin has the effect that makes skin bright, can infiltrate skin rapidly and does not affect skin cell, activity that can restraint of tyrosinase (tyrosinase), and then hinder melanic formation, meanwhile, the generation of Mai Laning (melanin) be can effectively block, decomposition and the eliminating of Mai Laning accelerated, thereby, the source producing from speckle, stops the generation of speckle, the problem of profound solution speckle.
4. the Arbutin that the present invention adopts, can also protect skin to exempt from the infringement of what free radical, and hydrophilic is good, therefore often adds in the commercially available whitening product of what.
5. deep-sea fish skin collagen polypeptide washing facial film of the present invention, the component proportioning of each component, scientific and reasonable, the deep-sea fish skin collagen polypeptide washing facial film that preparation generates, no side effects, preparation technology simplifies, and facilitates producer's large-scale production.
6. the present invention adopts natural plants hydrosol or flower water, replaces existing deionized water, makes the essence preparing, there is the natural fragrance of a flower or plant breath, meanwhile, the present invention adopt through the concentrated natural plants hydrosol of the way of distillation or flower water, effect better obviously.
7. in component of the present invention, add efficient penetrating agent water-solubleazone, with trehalose collaborative work, help nutrition better to infiltrate skin, better bring into play effect.
8. it is scientific and reasonable that the present invention adopts the proportioning of antioxidant, antiseptic, Compound Resisting microbial inoculum, makes facial film have better treatment effect, better stability, better storage life.
9. processing technology of the present invention is simplified, first, by Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol is dissolved in natural plants hydrosol or Hua Shuizhong completely, secondly, in vacuum, 10 DEG C～20 DEG C of low temperature, under the condition of high pressure 1500pa～1800pa, make fishskin collagen polypeptide, trehalose is dissolved in natural plants hydrosol or Hua Shuizhong completely, by the mode of this kind of vacuum and low temperature high pressure, avoid fishskin collagen polypeptide, under the rejoice of high temperature, there is degeneration in trehalose, again, in vacuum, 20 DEG C～30 DEG C of low temperature, under the condition of high pressure: 1200pa～1500pa, by Semen Vitis viniferae extract, licorice root extract, phycocyanin is dissolved in natural plants hydrosol or Hua Shuizhong completely, avoid the degeneration of polymer substance, finally, remaining raw material is joined in intermediate product C solution, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, obtain the preparation technology of collagen polypeptide washing facial film, suitable popularization.
Detailed description of the invention
Embodiment 1:
The preparation method of deep-sea fish skin collagen polypeptide washing facial film provided by the invention, it comprises the steps:
(1). the preparation of raw material
Prepare following raw material according to following parts by weight:
(2). the preparation of intermediate product A solution
Arbutin, hydroxyethyl-cellulose, sodium alginate, the Polyethylene Glycol in step (1), prepared are joined to parts by weight is: 48～52 natural plants hydrosol or Hua Shuizhong, carry out heated and stirred, and being heated to temperature is 60 DEG C～70 DEG C; Mixing speed is 100r/min～150r/min, until after Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol dissolve completely, be cooled to 20 DEG C～30 DEG C, obtains intermediate product A solution, for subsequent use;
(3). the preparation of intermediate product B solution
Fishskin collagen polypeptide, the trehalose in step (1), prepared are joined to parts by weight is: 20～30 natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 10 DEG C～20 DEG C; In temperature be again: 10 DEG C～20 DEG C, pressure is: under the vacuum condition of 1500pa～1800pa, stir, mixing speed is 130r/min～150r/min, until fishskin collagen polypeptide, trehalose dissolve completely, then heat, after being heated to temperature and being 20 DEG C～30 DEG C, step (2) is obtained to intermediate product A solution to add wherein, insulation, obtains intermediate product B solution, for subsequent use;
(4). the preparation of intermediate product C solution
Semen Vitis viniferae extract, licorice root extract, the phycocyanin in step (1), prepared are joined to remaining natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 20 DEG C～30 DEG C; In temperature be again: 20 DEG C～30 DEG C, pressure is: under the vacuum condition of 1200pa～1500pa, stir, mixing speed is 120r/min～130r/min, until Semen Vitis viniferae extract, licorice root extract, phycocyanin dissolve completely, step (3) is obtained to intermediate product B solution to add wherein, cooling, obtain intermediate product C solution, for subsequent use;
(5). the preparation of collagen polypeptide washing facial film
Antioxidant, antiseptic, Compound Resisting microbial inoculum, glycerol, the water-solubleazone in step (1), prepared are joined to step (4) to be obtained in intermediate product C solution, under the condition of 40 DEG C～50 DEG C of temperature, mixing speed is under the condition of 100r/min～120r/min, after stirring 2～2.5h, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Described step (2), it also comprises the steps:
(21) extraction of Arbutin
Leaf of pear tree being dried, pulverizing, being sieved, use alcoholic solution dipping, is, under the temperature conditions of 45 DEG C～55 DEG C, after dipping 6.5～7.5h, to use ultrafiltration membrance filter in temperature, collects filter liquor; Use macroporous resin, filter liquor is carried out to Adsorption and desorption attached, collect stripping liquid, be rotated evaporation, concentrate, vacuum freeze-drying, obtain Arbutin.
Natural plants hydrosol in described step (1) or flower water, it is a kind of and combination in rose wate, lavender flower water, Flos Osmanthi Fragrantis water, Magnolia denudata Desr. flower water, Flos Lilii viriduli water and Cananga odorata hydrosol, Lignum Santali Albi hydrosol, Camellia sinensis hydrosol; Fishskin collagen polypeptide in described step (1), its raw material is taken from natural pure free of contamination deep-sea wall pollack fish skin.
Described natural plants hydrosol or flower water, it be by the natural plants hydrosol of normal concentration or flower water, the 100 saturated hydrosols that are condensed into by the way of distillation or colored water.
Antiseptic in described step (1), it is methyl hydroxybenzoate and propylparaben, described methyl hydroxybenzoate and the weight ratio of propylparaben are: 2.5～3:1.2～1.5.
Antioxidant in described step (1), it is tertiary butyl-4-hydroxy methoxybenzene.
The collagen polypeptide washing facial film that adopts the preparation method of above-mentioned deep-sea fish skin collagen polypeptide washing facial film to prepare, its raw material by following parts by weight is prepared from:
First, Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol being dissolved in to parts by weight is: 48～52 natural plants hydrosol or flower water, obtain intermediate product A solution;
Secondly, fishskin collagen polypeptide, trehalose are dissolved in to parts by weight are: 20～30 natural plants hydrosol or Hua Shuizhong, then intermediate product A solution is added wherein, obtain intermediate product B solution;
Again, Semen Vitis viniferae extract, licorice root extract, phycocyanin are dissolved in to remaining natural plants hydrosol or Hua Shuizhong, then intermediate product B solution is added wherein, obtain intermediate product C solution;
Finally, remaining raw material is joined in intermediate product C solution, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Described natural plants hydrosol or flower water, it is a kind of and combination in rose wate, lavender flower water, Flos Osmanthi Fragrantis water, Magnolia denudata Desr. flower water, Flos Lilii viriduli water and Cananga odorata hydrosol, Lignum Santali Albi hydrosol, Camellia sinensis hydrosol; Described natural plants hydrosol or flower water, it be by the natural plants hydrosol of normal concentration or flower water, the 100 saturated hydrosols that are condensed into by the way of distillation or colored water; Described fishskin collagen polypeptide, its raw material is taken from natural pure free of contamination deep-sea wall pollack fish skin.
Described antiseptic, it is methyl hydroxybenzoate and propylparaben, described methyl hydroxybenzoate and the weight ratio of propylparaben are: 2.5～3:1.2～1.5.
Described antioxidant, it is tertiary butyl-4-hydroxy methoxybenzene.
Embodiment 2:
The preparation method of the deep-sea fish skin collagen polypeptide washing facial film that the present embodiment provides and deep-sea fish skin collagen polypeptide washing facial film goods thereof, it is substantially the same manner as Example 1, and its difference is:
The preparation method of deep-sea fish skin collagen polypeptide washing facial film, it comprises the steps:
(1). the preparation of raw material
Prepare following raw material according to following parts by weight:
(2). the preparation of intermediate product A solution
Arbutin, hydroxyethyl-cellulose, sodium alginate, the Polyethylene Glycol in step (1), prepared are joined to parts by weight is: 48 natural plants hydrosol or Hua Shuizhong, carry out heated and stirred, and being heated to temperature is 60 DEG C; Mixing speed is 120r/min, until after Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol dissolve completely, be cooled to 20 DEG C, obtains intermediate product A solution, for subsequent use;
(3). the preparation of intermediate product B solution
Fishskin collagen polypeptide, the trehalose in step (1), prepared are joined to parts by weight is: 25 natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 15 DEG C; In temperature be again: 15 DEG C, pressure is: under the vacuum condition of 1650pa, stir, mixing speed is 140r/min, until fishskin collagen polypeptide, trehalose dissolve completely, then heat, after being heated to temperature and being 20 DEG C, step (2) is obtained to intermediate product A solution to add wherein, insulation, obtains intermediate product B solution, for subsequent use;
(4). the preparation of intermediate product C solution
Semen Vitis viniferae extract, licorice root extract, the phycocyanin in step (1), prepared are joined to remaining natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 25 DEG C; In temperature be again: 25 DEG C, pressure is: under the vacuum condition of 1200pa, stir, mixing speed is 125r/min, until Semen Vitis viniferae extract, licorice root extract, phycocyanin dissolve completely, step (3) is obtained to intermediate product B solution to add wherein, cooling, obtain intermediate product C solution, for subsequent use;
(5). the preparation of collagen polypeptide washing facial film
Antioxidant, antiseptic, Compound Resisting microbial inoculum, glycerol, the water-solubleazone in step (1), prepared are joined to step (4) to be obtained in intermediate product C solution, under the condition of temperature 45 C, mixing speed is under the condition of 115r/min, after stirring 2h, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Described step (2), it also comprises the steps:
(21) extraction of Arbutin
Leaf of pear tree being dried, pulverizing, being sieved, use alcoholic solution dipping, is, under the temperature conditions of 50 DEG C, after dipping 6.5h, to use ultrafiltration membrance filter in temperature, collects filter liquor; Use macroporous resin, filter liquor is carried out to Adsorption and desorption attached, collect stripping liquid, be rotated evaporation, concentrate, vacuum freeze-drying, obtain Arbutin.
Natural plants hydrosol in described step (1) or flower water, it is the combination of rose wate, lavender flower water, Flos Osmanthi Fragrantis water, Magnolia denudata Desr. flower water, Flos Lilii viriduli water.
Antiseptic in described step (1), it is methyl hydroxybenzoate and propylparaben, described methyl hydroxybenzoate and the weight ratio of propylparaben are: 2.7:1.4.
The collagen polypeptide washing facial film that adopts the preparation method of above-mentioned deep-sea fish skin collagen polypeptide washing facial film to prepare, its raw material by following parts by weight is prepared from:
First, Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol being dissolved in to parts by weight is: 48 natural plants hydrosol or flower water, obtain intermediate product A solution;
Secondly, fishskin collagen polypeptide, trehalose are dissolved in to parts by weight are: 25 natural plants hydrosol or Hua Shuizhong, then intermediate product A solution is added wherein, obtain intermediate product B solution;
Again, Semen Vitis viniferae extract, licorice root extract, phycocyanin are dissolved in to remaining natural plants hydrosol or Hua Shuizhong, then intermediate product B solution is added wherein, obtain intermediate product C solution;
Finally, remaining raw material is joined in intermediate product C solution, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Embodiment 3:
The preparation method of deep-sea fish skin collagen polypeptide that the present embodiment provides washing facial film and deep-sea fish skin collagen polypeptide washing facial film thereof, itself and embodiment 1,2 are basic identical, and its difference is:
The preparation method of deep-sea fish skin collagen polypeptide washing facial film, it comprises the steps:
(1). the preparation of raw material
Prepare following raw material according to following parts by weight:
(2). the preparation of intermediate product A solution
Arbutin, hydroxyethyl-cellulose, sodium alginate, the Polyethylene Glycol in step (1), prepared are joined to parts by weight is: 50 natural plants hydrosol or Hua Shuizhong, carry out heated and stirred, and being heated to temperature is 65 DEG C; Mixing speed is 120r/min, until after Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol dissolve completely, be cooled to 20 DEG C, obtains intermediate product A solution, for subsequent use;
(3). the preparation of intermediate product B solution
It is 30 natural plants hydrosol or Hua Shuizhong that fishskin collagen polypeptide, the trehalose prepared in step (1) are joined to parts by weight, and being first heated to temperature is 10 DEG C; In temperature be again: 10 DEG C, pressure is: under the vacuum condition of 1500pa, stir, mixing speed is 150r/min, until fishskin collagen polypeptide, trehalose dissolve completely, then heat, after being heated to temperature and being 20 DEG C, step (2) is obtained to intermediate product A solution to add wherein, insulation, obtains intermediate product B solution, for subsequent use;
(4). the preparation of intermediate product C solution
Semen Vitis viniferae extract, licorice root extract, the phycocyanin in step (1), prepared are joined to remaining natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 20 DEG C; In temperature be again: 20 DEG C, pressure is: under the vacuum condition of 1200pa, stir, mixing speed is 120r/min, until Semen Vitis viniferae extract, licorice root extract, phycocyanin dissolve completely, step (3) is obtained to intermediate product B solution to add wherein, cooling, obtain intermediate product C solution, for subsequent use;
(5). the preparation of collagen polypeptide washing facial film
Antioxidant, antiseptic, Compound Resisting microbial inoculum, glycerol, the water-solubleazone in step (1), prepared are joined to step (4) to be obtained in intermediate product C solution, under the condition of 40 DEG C of temperature, mixing speed is under the condition of 100r/min, after stirring 2.5h, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Described step (2), it also comprises the steps:
(21) extraction of Arbutin
Leaf of pear tree being dried, pulverizing, being sieved, use alcoholic solution dipping, is, under the temperature conditions of 45 DEG C, after dipping 7h, to use ultrafiltration membrance filter in temperature, collects filter liquor; Use macroporous resin, filter liquor is carried out to Adsorption and desorption attached, collect stripping liquid, be rotated evaporation, concentrate, vacuum freeze-drying, obtain Arbutin.
Natural plants hydrosol in described step (1) or flower water, it is the combination of Magnolia denudata Desr. flower water, Flos Lilii viriduli water and Cananga odorata hydrosol, Lignum Santali Albi hydrosol.
Antiseptic in described step (1), it is methyl hydroxybenzoate and propylparaben, described methyl hydroxybenzoate and the weight ratio of propylparaben are: 2.5:1.2.
The collagen polypeptide washing facial film that adopts the preparation method of above-mentioned deep-sea fish skin collagen polypeptide washing facial film to prepare, it is mainly prepared from by the raw material of following parts by weight:
First, Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol being dissolved in to parts by weight is: 50 natural plants hydrosol or flower water, obtain intermediate product A solution;
Secondly, fishskin collagen polypeptide, trehalose are dissolved in to parts by weight are: 30 natural plants hydrosol or Hua Shuizhong, then intermediate product A solution is added wherein, obtain intermediate product B solution;
Again, Semen Vitis viniferae extract, licorice root extract, phycocyanin are dissolved in to remaining natural plants hydrosol or Hua Shuizhong, then intermediate product B solution is added wherein, obtain intermediate product C solution;
Finally, remaining raw material is joined in intermediate product C solution, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Embodiment 4:
The preparation method of deep-sea fish skin collagen polypeptide that the present embodiment provides washing facial film and deep-sea fish skin collagen polypeptide washing facial film thereof, itself and embodiment 1,2,3 are basic identical, and its difference is:
The preparation method of deep-sea fish skin collagen polypeptide washing facial film, it comprises the steps:
(1). the preparation of raw material
Prepare following raw material according to following parts by weight:
(2). the preparation of intermediate product A solution
Arbutin, hydroxyethyl-cellulose, sodium alginate, the Polyethylene Glycol in step (1), prepared are joined to parts by weight is: 52 natural plants hydrosol or Hua Shuizhong, carry out heated and stirred, and being heated to temperature is 70 DEG C; Mixing speed is 100r/min, until after Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol dissolve completely, be cooled to 30 DEG C, obtains intermediate product A solution, for subsequent use;
(3). the preparation of intermediate product B solution
Fishskin collagen polypeptide, the trehalose in step (1), prepared are joined to parts by weight is: 20 natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 20 DEG C; In temperature be again: 20 DEG C, pressure is: under the vacuum condition of 1800pa, stir, mixing speed is 130r/min, until fishskin collagen polypeptide, trehalose dissolve completely, then heat, after being heated to temperature and being 30 DEG C, step (2) is obtained to intermediate product A solution to add wherein, insulation, obtains intermediate product B solution, for subsequent use;
(4). the preparation of intermediate product C solution
Semen Vitis viniferae extract, licorice root extract, the phycocyanin in step (1), prepared are joined to remaining natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 30 DEG C; In temperature be again: 30 DEG C, pressure is: under the vacuum condition of 1500pa, stir, mixing speed is 130r/min, until Semen Vitis viniferae extract, licorice root extract, phycocyanin dissolve completely, step (3) is obtained to intermediate product B solution to add wherein, cooling, obtain intermediate product C solution, for subsequent use;
(5). the preparation of collagen polypeptide washing facial film
Antioxidant, antiseptic, Compound Resisting microbial inoculum, glycerol, the water-solubleazone in step (1), prepared are joined to step (4) to be obtained in intermediate product C solution, under the condition of temperature 50 C, mixing speed is under the condition of 120r/min, after stirring 2.3h, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Described step (2), it also comprises the steps:
(21) extraction of Arbutin
Leaf of pear tree being dried, pulverizing, being sieved, use alcoholic solution dipping, is, under the temperature conditions of 55 DEG C, after dipping 7.5h, to use ultrafiltration membrance filter in temperature, collects filter liquor; Use macroporous resin, filter liquor is carried out to Adsorption and desorption attached, collect stripping liquid, be rotated evaporation, concentrate, vacuum freeze-drying, obtain Arbutin.
Natural plants hydrosol in described step (1) or flower water, it is the combination of rose wate, lavender flower water, Flos Osmanthi Fragrantis water, Magnolia denudata Desr. flower water, Flos Lilii viriduli water and Cananga odorata hydrosol, Lignum Santali Albi hydrosol, Camellia sinensis hydrosol.
Antiseptic in described step (1), it is methyl hydroxybenzoate and propylparaben, described methyl hydroxybenzoate and the weight ratio of propylparaben are: 3:1.5.
The collagen polypeptide washing facial film that adopts the preparation method of above-mentioned deep-sea fish skin collagen polypeptide washing facial film to prepare, it is mainly prepared from by the raw material of following parts by weight:
First, Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol being dissolved in to parts by weight is: 52 natural plants hydrosol or flower water, obtain intermediate product A solution;
Secondly, fishskin collagen polypeptide, trehalose are dissolved in to parts by weight are: 20 natural plants hydrosol or Hua Shuizhong, then intermediate product A solution is added wherein, obtain intermediate product B solution;
Again, Semen Vitis viniferae extract, licorice root extract, phycocyanin are dissolved in to remaining natural plants hydrosol or Hua Shuizhong, then intermediate product B solution is added wherein, obtain intermediate product C solution;
Finally, remaining raw material is joined in intermediate product C solution, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Embodiment 5:
The preparation method of deep-sea fish skin collagen polypeptide that the present embodiment provides washing facial film and deep-sea fish skin collagen polypeptide washing facial film thereof, itself and embodiment 1,2,3,4 are basic identical, and its difference is:
The preparation method of deep-sea fish skin collagen polypeptide washing facial film, it comprises the steps:
(1). the preparation of raw material
Prepare following raw material according to following parts by weight:
(2). the preparation of intermediate product A solution
Arbutin, hydroxyethyl-cellulose, sodium alginate, the Polyethylene Glycol in step (1), prepared are joined to parts by weight is: 51 natural plants hydrosol or Hua Shuizhong, carry out heated and stirred, and being heated to temperature is 63 DEG C; Mixing speed is 125r/min, until after Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol dissolve completely, be cooled to 23 DEG C, obtains intermediate product A solution, for subsequent use;
(3). the preparation of intermediate product B solution
Fishskin collagen polypeptide, the trehalose in step (1), prepared are joined to parts by weight is: 25 natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 15 DEG C; In temperature be again: 15 DEG C, pressure is: under the vacuum condition of 1700pa, stir, mixing speed is 140r/min, until fishskin collagen polypeptide, trehalose dissolve completely, then heat, after being heated to temperature and being 25 DEG C, step (2) is obtained to intermediate product A solution to add wherein, insulation, obtains intermediate product B solution, for subsequent use;
(4). the preparation of intermediate product C solution
Semen Vitis viniferae extract, licorice root extract, the phycocyanin in step (1), prepared are joined to remaining natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 25 DEG C; In temperature be again: 25, pressure is: under the vacuum condition of 1300pa, stir, mixing speed is 125r/min, until Semen Vitis viniferae extract, licorice root extract, phycocyanin dissolve completely, step (3) is obtained to intermediate product B solution to add wherein, cooling, obtain intermediate product C solution, for subsequent use;
(5). the preparation of collagen polypeptide washing facial film
Antioxidant, antiseptic, Compound Resisting microbial inoculum, glycerol, the water-solubleazone in step (1), prepared are joined to step (4) to be obtained in intermediate product C solution, under the condition of 47 DEG C of temperature, mixing speed is under the condition of 110r/min, after stirring 2.3h, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Described step (2), it also comprises the steps:
(21) extraction of Arbutin
Leaf of pear tree being dried, pulverizing, being sieved, use alcoholic solution dipping, is, under the temperature conditions of 50 DEG C, after dipping 6.9h, to use ultrafiltration membrance filter in temperature, collects filter liquor; Use macroporous resin, filter liquor is carried out to Adsorption and desorption attached, collect stripping liquid, be rotated evaporation, concentrate, vacuum freeze-drying, obtain Arbutin.
Natural plants hydrosol in described step (1) or flower water, it is the combination of Cananga odorata hydrosol, Lignum Santali Albi hydrosol, Camellia sinensis hydrosol.
Antiseptic in described step (1), it is methyl hydroxybenzoate and propylparaben, described methyl hydroxybenzoate and the weight ratio of propylparaben are: 2.5:1.2.
The collagen polypeptide washing facial film that adopts the preparation method of above-mentioned deep-sea fish skin collagen polypeptide washing facial film to prepare, it is mainly prepared from by the raw material of following parts by weight:
First, Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol being dissolved in to parts by weight is: 51 natural plants hydrosol or flower water, obtain intermediate product A solution;
Secondly, fishskin collagen polypeptide, trehalose are dissolved in to parts by weight are: 25 natural plants hydrosol or Hua Shuizhong, then intermediate product A solution is added wherein, obtain intermediate product B solution;
Again, Semen Vitis viniferae extract, licorice root extract, phycocyanin are dissolved in to remaining natural plants hydrosol or Hua Shuizhong, then intermediate product B solution is added wherein, obtain intermediate product C solution;
Finally, remaining raw material is joined in intermediate product C solution, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
Beneficial effect of the present invention:
1. collagen polypeptide used in the present invention, raw material, from processing of aquatic products garbage, makes full use of processing of aquatic products garbage, not only can reduce the waste of environmental pollution and resource, and can increase the added value of processing of aquatic products, increases economic efficiency.
2. in collagen protein of fish skin, aminoacid composition approaches with the aminoacid composition of human body skin collagen protein, and with respect to the collagen polypeptide that is organized as raw material production with terrestrial animal or fresh water animals have pollution-free, without advantages such as source of disease (as bovine spongiform encephalopathy, foot and mouth disease, bird flu etc.) hidden danger.
3. the present invention has adopted Arbutin, Arbutin has the effect that makes skin bright, can infiltrate skin rapidly and does not affect skin cell, activity that can restraint of tyrosinase (tyrosinase), and then hinder melanic formation, meanwhile, the generation of Mai Laning (melanin) be can effectively block, decomposition and the eliminating of Mai Laning accelerated, thereby, the source producing from speckle, stops the generation of speckle, the problem of profound solution speckle.
4. the Arbutin that the present invention adopts, can also protect skin to exempt from the infringement of what free radical, and hydrophilic is good, therefore often adds in the commercially available whitening product of what.
5. deep-sea fish skin collagen polypeptide washing facial film of the present invention, the component proportioning of each component, scientific and reasonable, the deep-sea fish skin collagen polypeptide washing facial film that preparation generates, no side effects, preparation technology simplifies, and facilitates producer's large-scale production.
6. the present invention adopts natural plants hydrosol or flower water, replaces existing deionized water, makes the essence preparing, there is the natural fragrance of a flower or plant breath, meanwhile, the present invention adopt through the concentrated natural plants hydrosol of the way of distillation or flower water, effect better obviously.
7. in component of the present invention, add efficient penetrating agent water-solubleazone, with trehalose collaborative work, help nutrition better to infiltrate skin, better bring into play effect.
8. it is scientific and reasonable that the present invention adopts the proportioning of antioxidant, antiseptic, Compound Resisting microbial inoculum, makes facial film have better treatment effect, better stability, better storage life.
9. processing technology of the present invention is simplified, first, by Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol is dissolved in natural plants hydrosol or Hua Shuizhong completely, secondly, in vacuum, 10 DEG C～20 DEG C of low temperature, under the condition of high pressure 1500pa～1800pa, make fishskin collagen polypeptide, trehalose is dissolved in natural plants hydrosol or Hua Shuizhong completely, by the mode of this kind of vacuum and low temperature high pressure, avoid fishskin collagen polypeptide, under the rejoice of high temperature, there is degeneration in trehalose, again, in vacuum, 20 DEG C～30 DEG C of low temperature, under the condition of high pressure: 1200pa～1500pa, by Semen Vitis viniferae extract, licorice root extract, phycocyanin is dissolved in natural plants hydrosol or Hua Shuizhong completely, avoid the degeneration of polymer substance, finally, remaining raw material is joined in intermediate product C solution, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, obtain the preparation technology of collagen polypeptide washing facial film, suitable popularization.
The above embodiments are not all embodiment of the present invention, and the composition range that description is recorded, all can realize the present invention.
As described in the present embodiment of the invention; adopt and the same or analogous step of the present invention and component; and in the scope of listing, the preparation method of the deep-sea fish skin collagen polypeptide washing facial film obtaining and deep-sea fish skin collagen polypeptide washing facial film thereof, all within protection scope of the present invention.
Claims (10)
1. a preparation method for deep-sea fish skin collagen polypeptide washing facial film, is characterized in that, it comprises the steps:
(1). the preparation of raw material
Prepare following raw material according to following parts by weight:
(2). the preparation of intermediate product A solution
Arbutin, hydroxyethyl-cellulose, sodium alginate, the Polyethylene Glycol in step (1), prepared are joined to parts by weight is: 48～52 natural plants hydrosol or Hua Shuizhong, carry out heated and stirred, and being heated to temperature is 60 DEG C～70 DEG C; Mixing speed is 100r/min～150r/min, until after Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol dissolve completely, be cooled to 20 DEG C～30 DEG C, obtains intermediate product A solution, for subsequent use;
(3). the preparation of intermediate product B solution
Fishskin collagen polypeptide, the trehalose in step (1), prepared are joined to parts by weight is: 20～30 natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 10 DEG C～20 DEG C; In temperature be again: 10 DEG C～20 DEG C, pressure is: under the vacuum condition of 1500pa～1800pa, stir, mixing speed is 130r/min～150r/min, until fishskin collagen polypeptide, trehalose dissolve completely, then heat, after being heated to temperature and being 20 DEG C～30 DEG C, step (2) is obtained to intermediate product A solution to add wherein, insulation, obtains intermediate product B solution, for subsequent use;
(4). the preparation of intermediate product C solution
Semen Vitis viniferae extract, licorice root extract, the phycocyanin in step (1), prepared are joined to remaining natural plants hydrosol or Hua Shuizhong, and being first heated to temperature is 20 DEG C～30 DEG C; In temperature be again: 20 DEG C～30 DEG C, pressure is: under the vacuum condition of 1200pa～1500pa, stir, mixing speed is 120r/min～130r/min, until Semen Vitis viniferae extract, licorice root extract, phycocyanin dissolve completely, step (3) is obtained to intermediate product B solution to add wherein, cooling, obtain intermediate product C solution, for subsequent use;
(5). the preparation of collagen polypeptide washing facial film
Antioxidant, antiseptic, Compound Resisting microbial inoculum, glycerol, the water-solubleazone in step (1), prepared are joined to step (4) to be obtained in intermediate product C solution, under the condition of 40 DEG C～50 DEG C of temperature, mixing speed is under the condition of 100r/min～120r/min, after stirring 2～2.5h, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
2. the preparation method of deep-sea fish skin collagen polypeptide washing facial film according to claim 1, is characterized in that: described step (2), it also comprises the steps:
(21) extraction of Arbutin
Leaf of pear tree being dried, pulverizing, being sieved, use alcoholic solution dipping, is, under the temperature conditions of 45 DEG C～55 DEG C, after dipping 6.5～7.5h, to use ultrafiltration membrance filter in temperature, collects filter liquor; Use macroporous resin, filter liquor is carried out to Adsorption and desorption attached, collect stripping liquid, be rotated evaporation, concentrate, vacuum freeze-drying, obtain Arbutin.
3. the preparation method of deep-sea fish skin collagen polypeptide washing facial film according to claim 1, it is characterized in that: the natural plants hydrosol in described step (1) or flower water, it is a kind of and combination in rose wate, lavender flower water, Flos Osmanthi Fragrantis water, Magnolia denudata Desr. flower water, Flos Lilii viriduli water and Cananga odorata hydrosol, Lignum Santali Albi hydrosol, Camellia sinensis hydrosol; Fishskin collagen polypeptide in described step (1), its raw material is taken from natural pure free of contamination deep-sea wall pollack fish skin.
4. the preparation method of deep-sea fish skin collagen polypeptide washing facial film according to claim 2, it is characterized in that: described natural plants hydrosol or flower water, it is by the natural plants hydrosol of normal concentration or flower water, the 100 saturated hydrosols that are condensed into by the way of distillation or flower water.
5. the preparation method of deep-sea fish skin collagen polypeptide washing facial film according to claim 1, it is characterized in that: the antiseptic in described step (1), it is methyl hydroxybenzoate and propylparaben, and described methyl hydroxybenzoate and the weight ratio of propylparaben are: 2.5～3:1.2～1.5.
6. the preparation method of deep-sea fish skin collagen polypeptide washing facial film according to claim 1, is characterized in that: the antioxidant in described step (1), it is tertiary butyl-4-hydroxy methoxybenzene.
7. the collagen polypeptide washing facial film of preparing according to the preparation method of the deep-sea fish skin collagen polypeptide washing facial film one of claim 1～6 Suo Shu, is characterized in that, its raw material by following parts by weight is prepared from:
First, Arbutin, hydroxyethyl-cellulose, sodium alginate, Polyethylene Glycol being dissolved in to parts by weight is: 48～52 natural plants hydrosol or flower water, obtain intermediate product A solution;
Secondly, fishskin collagen polypeptide, trehalose are dissolved in to parts by weight are: 20～30 natural plants hydrosol or Hua Shuizhong, then intermediate product A solution is added wherein, obtain intermediate product B solution;
Again, Semen Vitis viniferae extract, licorice root extract, phycocyanin are dissolved in to remaining natural plants hydrosol or Hua Shuizhong, then intermediate product B solution is added wherein, obtain intermediate product C solution;
Finally, remaining raw material is joined in intermediate product C solution, gains are poured in mould and are shaped, dry at 50 DEG C of temperature, can obtain collagen polypeptide washing facial film.
8. collagen polypeptide washing facial film according to claim 7, it is characterized in that: described natural plants hydrosol or flower water, it is a kind of and combination in rose wate, lavender flower water, Flos Osmanthi Fragrantis water, Magnolia denudata Desr. flower water, Flos Lilii viriduli water and Cananga odorata hydrosol, Lignum Santali Albi hydrosol, Camellia sinensis hydrosol; Described natural plants hydrosol or flower water, it be by the natural plants hydrosol of normal concentration or flower water, the 100 saturated hydrosols that are condensed into by the way of distillation or colored water; Described fishskin collagen polypeptide, its raw material is taken from natural pure free of contamination deep-sea wall pollack fish skin.
9. collagen polypeptide washing facial film according to claim 6, is characterized in that: described antiseptic, and it is methyl hydroxybenzoate and propylparaben, described methyl hydroxybenzoate and the weight ratio of propylparaben are: 2.5～3:1.2～1.5.
10. collagen polypeptide washing facial film according to claim 6, is characterized in that: described antioxidant, it is tertiary butyl-4-hydroxy methoxybenzene.
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