CN105555710A - 用于制备气凝胶材料的方法 - Google Patents

用于制备气凝胶材料的方法 Download PDF

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Publication number
CN105555710A
CN105555710A CN201480050734.9A CN201480050734A CN105555710A CN 105555710 A CN105555710 A CN 105555710A CN 201480050734 A CN201480050734 A CN 201480050734A CN 105555710 A CN105555710 A CN 105555710A
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China
Prior art keywords
gel
suo shu
hydrophobization
sol
hydrophobizing
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CN201480050734.9A
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English (en)
Chinese (zh)
Inventor
M.凯贝尔
赵善宇
S.布伦纳
C.西门
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Eidgenoessische Materialpruefungs und Forschungsanstalt
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Eidgenoessische Materialpruefungs und Forschungsanstalt
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Priority to CN202111139256.7A priority Critical patent/CN114408931A/zh
Publication of CN105555710A publication Critical patent/CN105555710A/zh
Pending legal-status Critical Current

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    • EFIXED CONSTRUCTIONS
    • E04BUILDING
    • E04BGENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
    • E04B1/00Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
    • E04B1/62Insulation or other protection; Elements or use of specified material therefor
    • E04B1/74Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
    • E04B1/76Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls specifically with respect to heat only
    • E04B1/78Heat insulating elements
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/145Preparation of hydroorganosols, organosols or dispersions in an organic medium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/155Preparation of hydroorganogels or organogels
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/157After-treatment of gels
    • C01B33/158Purification; Drying; Dehydrating
    • C01B33/1585Dehydration into aerogels

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Architecture (AREA)
  • Acoustics & Sound (AREA)
  • Electromagnetism (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Silicon Compounds (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Thermal Insulation (AREA)
CN201480050734.9A 2013-08-02 2014-07-28 用于制备气凝胶材料的方法 Pending CN105555710A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111139256.7A CN114408931A (zh) 2013-08-02 2014-07-28 用于制备气凝胶材料的方法

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP13179185.7A EP2832690A1 (de) 2013-08-02 2013-08-02 Verfahren zur Herstellung eines Aerogelmaterials
EP13179185.7 2013-08-02
PCT/EP2014/066213 WO2015014813A1 (de) 2013-08-02 2014-07-28 Verfahren zur herstellung eines aerogelmaterials

Related Child Applications (1)

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CN202111139256.7A Division CN114408931A (zh) 2013-08-02 2014-07-28 用于制备气凝胶材料的方法

Publications (1)

Publication Number Publication Date
CN105555710A true CN105555710A (zh) 2016-05-04

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CN201480050734.9A Pending CN105555710A (zh) 2013-08-02 2014-07-28 用于制备气凝胶材料的方法
CN202111139256.7A Pending CN114408931A (zh) 2013-08-02 2014-07-28 用于制备气凝胶材料的方法

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Country Status (8)

Country Link
US (1) US20160258153A1 (https=)
EP (2) EP2832690A1 (https=)
JP (1) JP6449279B2 (https=)
KR (1) KR101813898B1 (https=)
CN (2) CN105555710A (https=)
AU (1) AU2014298538B2 (https=)
BR (1) BR112016002360A2 (https=)
WO (1) WO2015014813A1 (https=)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106955650A (zh) * 2017-04-01 2017-07-18 东华大学 一种三维多孔框架增强纤维气凝胶材料及其制备方法
CN109475833A (zh) * 2016-05-20 2019-03-15 罗克伍尔国际公司 用于制备气凝胶复合材料的设备和方法以及气凝胶复合材料
CN111818994A (zh) * 2018-03-05 2020-10-23 赢创运营有限公司 生产气凝胶材料的方法
CN115485239A (zh) * 2020-04-30 2022-12-16 赢创运营有限公司 具有增大的碱性稳定性的二氧化硅气凝胶

Families Citing this family (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SG10201907591UA (en) * 2014-02-26 2019-10-30 Hitachi Chemical Co Ltd Aerogel
CH710694B1 (de) * 2015-02-04 2019-05-15 Rockwool Int Verfahren zur Herstellung eines Aerogels resp. eines Aerogel-Verbundwerkstoffs, sowie Aerogel resp. Aerogel-Verbundwerkstoff erhältlich nach dem Verfahren.
KR101789371B1 (ko) 2015-02-13 2017-10-23 주식회사 엘지화학 실리카 에어로겔 함유 블랑켓의 제조방법 및 이에 따라 제조된 실리카 에어로겔 함유 블랑켓
GB201502613D0 (en) * 2015-02-17 2015-04-01 Univ Newcastle Aerogels
DE102015211812A1 (de) * 2015-06-25 2016-12-29 Wacker Chemie Ag Wirtschaftliches Verfahren zur Herstellung von organisch modifizierten Lyo- oder Aerogelen
EP3124443A1 (de) * 2015-07-28 2017-02-01 D. Swarovski KG Kontinuierliches sol-gel verfahren zur herstellung von quarzglas
KR101931569B1 (ko) 2015-11-03 2018-12-21 주식회사 엘지화학 소수성의 산화금속-실리카 복합 에어로겔의 제조방법 및 이로부터 제조된 소수성의 산화금속-실리카 복합 에어로겔
KR101953371B1 (ko) 2016-01-19 2019-02-28 주식회사 엘지화학 에어로겔 시트의 제조방법 및 장치
KR101774140B1 (ko) * 2016-01-19 2017-09-01 주식회사 엘지화학 에어로겔 시트의 제조방법 및 장치
KR101962207B1 (ko) 2016-02-17 2019-03-27 주식회사 엘지화학 에어로겔 시트를 포함하는 복합시트 제조방법 및 제조장치
KR101968648B1 (ko) * 2016-02-19 2019-04-12 주식회사 엘지화학 에어로겔 시트의 제조방법 및 장치
KR101962206B1 (ko) * 2016-02-19 2019-03-27 주식회사 엘지화학 에어로겔 시트를 포함하는 복합시트 제조방법 및 제조장치
KR20170110993A (ko) 2016-03-24 2017-10-12 주식회사 엘지화학 실리카 에어로겔 제조시스템
FR3050013B1 (fr) * 2016-04-11 2019-08-02 Saint-Gobain Isover Fours et produits d'isolation pour fours
FR3053263B1 (fr) * 2016-07-04 2018-08-31 Keey Aerogrl Procede continu de fabrication d'un aerogel
WO2018019599A1 (de) 2016-07-29 2018-02-01 Evonik Degussa Gmbh Verfahren zur herstellung eines hydrophoben, wärmedämmenden materiales
EP3281920A1 (de) * 2016-08-12 2018-02-14 D. Swarovski KG Kontinuierliches sol-gel-verfahren zur herstellung von silicathaltigen gläsern oder glaskeramiken
CN108602681B (zh) 2016-09-12 2021-12-17 株式会社Lg化学 二氧化硅气凝胶的制备方法以及由其制备的二氧化硅气凝胶
KR101942474B1 (ko) * 2016-11-18 2019-01-25 주식회사 엘지화학 전가수분해된 알킬 폴리실리케이트의 합성방법
RU2759942C2 (ru) 2017-01-18 2021-11-18 Эвоник Оперейшенс ГмбХ Гранулированный теплоизоляционный материал и способ его получения
DE102017209782A1 (de) 2017-06-09 2018-12-13 Evonik Degussa Gmbh Verfahren zur Wärmedämmung eines evakuierbaren Behälters
EP3498671A1 (en) * 2017-12-15 2019-06-19 EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt Superinsulating silica aerogel with high stiffness and density
CA3105678C (en) 2018-07-17 2022-10-18 Evonik Operations Gmbh Thermal insulating composition based on silica granulates
EP3597615A1 (en) 2018-07-17 2020-01-22 Evonik Operations GmbH Granular mixed oxide material and thermal insulating composition on its basis
JP7086266B2 (ja) 2018-07-18 2022-06-17 エボニック オペレーションズ ゲーエムベーハー シリカをベースとする成形断熱体を周囲圧力で疎水化する方法
CN111039583B (zh) * 2018-10-11 2022-10-11 卢孟磊 一种低成本快速制备微纳结构气凝胶膨胀珍珠岩的方法
DE102018128410A1 (de) * 2018-11-13 2020-05-14 Fraunhofer Gesellschaft zur Förderung der angewandten Forschung e.V. Verfahren zur Herstellung von Aerogelen und mit diesem erhältliche Aerogele
WO2020125956A1 (de) 2018-12-18 2020-06-25 Wacker Chemie Ag Verfahren zur herstellung abgerundeter gelpartikel
FR3094975B1 (fr) * 2019-04-10 2022-11-18 Keey Aerogel Procédé de synthèse d’un aérogel de silice hydrophobique de type « one pot » à partir d’un précurseur de silice
AU2021208280A1 (en) 2020-01-14 2022-09-08 Evonik Operations Gmbh Silica-based hydrophobic granular material with an increased polarity
EP3896035A1 (en) * 2020-04-15 2021-10-20 EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt Silica aerogels and silica aerogel blankets
WO2021204815A1 (en) * 2020-04-06 2021-10-14 Empa Eidgenössische Materialprüfungs- Und Forschungsanstalt Silica aerogels
CN113563012B (zh) * 2020-04-29 2022-11-04 台湾气凝胶科技材料开发股份有限公司 御寒、隔热的疏水性气凝胶复合胶状物的制备方法及其相关产物
CH717558A1 (de) 2020-06-22 2021-12-30 Rockwool Int Aerogel-Verbundwerkstoffen, sowie Wärmedämmelement.
EP4177231A1 (de) 2021-11-03 2023-05-10 Evonik Operations GmbH Wärmedämmsysteme mit verbesserter kosteneffizienz
CN117510181B (zh) * 2023-11-07 2024-04-16 武汉中科先进材料科技有限公司 一种超疏水、增强型二氧化硅气凝胶毡及其制备方法
CN117658589A (zh) * 2023-12-07 2024-03-08 翌江新材(江苏)有限公司 一种制备气凝胶材料的新型方法
CN118561286A (zh) * 2024-04-15 2024-08-30 湖南尚成新材料科技有限责任公司 采用醇混合溶液的亚临界态流体制备疏水气凝胶的方法

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101014535A (zh) * 2004-01-06 2007-08-08 白杨气凝胶股份有限公司 含有键合硅的聚甲基丙烯酸酯的有机改性的二氧化硅气凝胶
CN101372337A (zh) * 2008-09-28 2009-02-25 厦门大学 共前驱体法常压干燥制备透明二氧化硅气凝胶的方法
CN101646622A (zh) * 2007-03-27 2010-02-10 Neb株式会社 制备疏水气凝胶的方法以及由其制备的疏水气凝胶
CN101691227A (zh) * 2009-10-13 2010-04-07 厦门大学 二氧化硅气凝胶材料的制备方法
CN102951650A (zh) * 2012-08-31 2013-03-06 卢斌 一种快速制备SiO2气凝胶的常压干燥方法
WO2013053951A1 (en) * 2011-10-14 2013-04-18 Enersens Process for manufacturing xerogels

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2659155B2 (ja) * 1992-02-03 1997-09-30 松下電工株式会社 疎水性エアロゲルの製造方法
EP0585456B1 (en) * 1992-02-18 1997-05-07 Matsushita Electric Works Ltd Process for producing hydrophobic aerogel
US5565142A (en) 1992-04-01 1996-10-15 Deshpande; Ravindra Preparation of high porosity xerogels by chemical surface modification.
DK0716641T3 (da) 1993-08-31 1998-02-09 Basf Ag Hydrofobe kiselsyreaerogeler
DE19631267C1 (de) 1996-08-02 1998-04-30 Hoechst Ag Verfahren zur Herstellung von organisch modifizierten Aerogelen
DE19648798C2 (de) * 1996-11-26 1998-11-19 Hoechst Ag Verfahren zur Herstellung von organisch modifizierten Aerogelen durch Oberflächenmodifikation des wäßrigen Gels (ohne vorherigen Lösungsmitteltausch) und anschließender Trocknung
JP3954842B2 (ja) * 2001-08-02 2007-08-08 株式会社アルバック 疎水性多孔質材料の製造方法
FR2849444B1 (fr) * 2002-12-30 2006-07-28 Rhodia Chimie Sa Procede de preparation d'un suspension de silice dans une matiere silicone eventuellement reticulable
FR2873677B1 (fr) * 2004-07-29 2007-08-17 Armines Ass Pour La Rech Et Le Procede d'elaboration de serogels de silice hydrophobes
JP2007134420A (ja) * 2005-11-09 2007-05-31 Ulvac Japan Ltd 疎水性多孔質シリカ材料による構造物内部の埋め込み方法
JP5376124B2 (ja) * 2007-02-02 2013-12-25 日産化学工業株式会社 反応性モノマー分散シリカゾル、その製造方法、硬化用組成物及びその硬化体
KR100924781B1 (ko) * 2007-09-19 2009-11-03 주식회사 넵 영구적인 소수성을 갖는 고투광성 입상형 에어로겔제조방법 및 이로부터 제조된 입상형 에어로겔
KR101187568B1 (ko) 2010-09-29 2012-10-04 한국에너지기술연구원 실리카 에어로겔 과립의 제조방법
JP5669617B2 (ja) * 2011-02-21 2015-02-12 株式会社トクヤマ エアロゲル及び該エアロゲルを用いた断熱材
KR102172825B1 (ko) * 2013-06-10 2020-11-02 닛산 가가쿠 가부시키가이샤 실리카 함유 수지 조성물 및 그 제조 방법 그리고 실리카 함유 수지 조성물의 성형품

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101014535A (zh) * 2004-01-06 2007-08-08 白杨气凝胶股份有限公司 含有键合硅的聚甲基丙烯酸酯的有机改性的二氧化硅气凝胶
CN101646622A (zh) * 2007-03-27 2010-02-10 Neb株式会社 制备疏水气凝胶的方法以及由其制备的疏水气凝胶
CN101372337A (zh) * 2008-09-28 2009-02-25 厦门大学 共前驱体法常压干燥制备透明二氧化硅气凝胶的方法
CN101691227A (zh) * 2009-10-13 2010-04-07 厦门大学 二氧化硅气凝胶材料的制备方法
WO2013053951A1 (en) * 2011-10-14 2013-04-18 Enersens Process for manufacturing xerogels
CN102951650A (zh) * 2012-08-31 2013-03-06 卢斌 一种快速制备SiO2气凝胶的常压干燥方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
MICHEL A. AEGERTER ET AL.: "《Aerogels Handbook》", 31 December 2011, SPRINGER *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109475833A (zh) * 2016-05-20 2019-03-15 罗克伍尔国际公司 用于制备气凝胶复合材料的设备和方法以及气凝胶复合材料
CN106955650A (zh) * 2017-04-01 2017-07-18 东华大学 一种三维多孔框架增强纤维气凝胶材料及其制备方法
CN111818994A (zh) * 2018-03-05 2020-10-23 赢创运营有限公司 生产气凝胶材料的方法
CN115485239A (zh) * 2020-04-30 2022-12-16 赢创运营有限公司 具有增大的碱性稳定性的二氧化硅气凝胶

Also Published As

Publication number Publication date
US20160258153A1 (en) 2016-09-08
AU2014298538A1 (en) 2016-02-25
CN114408931A (zh) 2022-04-29
JP2016530199A (ja) 2016-09-29
EP3027558A1 (de) 2016-06-08
BR112016002360A2 (pt) 2017-08-01
EP2832690A1 (de) 2015-02-04
JP6449279B2 (ja) 2019-01-09
KR101813898B1 (ko) 2018-01-02
AU2014298538B2 (en) 2018-02-22
KR20160054462A (ko) 2016-05-16
WO2015014813A1 (de) 2015-02-05

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