CN105330542A - 草酸二甲酯的生产方法 - Google Patents

草酸二甲酯的生产方法 Download PDF

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Publication number
CN105330542A
CN105330542A CN201410314462.0A CN201410314462A CN105330542A CN 105330542 A CN105330542 A CN 105330542A CN 201410314462 A CN201410314462 A CN 201410314462A CN 105330542 A CN105330542 A CN 105330542A
Authority
CN
China
Prior art keywords
dimethyl oxalate
tower
production method
recovery tower
reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410314462.0A
Other languages
English (en)
Chinese (zh)
Inventor
杨卫胜
贺来宾
施德
胡松
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Petroleum and Chemical Corp
Sinopec Shanghai Research Institute of Petrochemical Technology
Original Assignee
China Petroleum and Chemical Corp
Sinopec Shanghai Research Institute of Petrochemical Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Petroleum and Chemical Corp, Sinopec Shanghai Research Institute of Petrochemical Technology filed Critical China Petroleum and Chemical Corp
Priority to CN201410314462.0A priority Critical patent/CN105330542A/zh
Priority to RU2015126664A priority patent/RU2692099C2/ru
Priority to AU2015203732A priority patent/AU2015203732B2/en
Priority to BR102015016125A priority patent/BR102015016125B8/pt
Priority to CA2896290A priority patent/CA2896290C/en
Publication of CN105330542A publication Critical patent/CN105330542A/zh
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/36—Preparation of carboxylic acid esters by reaction with carbon monoxide or formates
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201410314462.0A 2014-07-03 2014-07-03 草酸二甲酯的生产方法 Pending CN105330542A (zh)

Priority Applications (5)

Application Number Priority Date Filing Date Title
CN201410314462.0A CN105330542A (zh) 2014-07-03 2014-07-03 草酸二甲酯的生产方法
RU2015126664A RU2692099C2 (ru) 2014-07-03 2015-07-03 Способ получения диметилоксалата
AU2015203732A AU2015203732B2 (en) 2014-07-03 2015-07-03 Method for producing dimethyl oxalate
BR102015016125A BR102015016125B8 (pt) 2014-07-03 2015-07-03 método para produzir oxalato de dimetila e método para produzir oxalato de dimetila e carbonato de dimetila como um subproduto
CA2896290A CA2896290C (en) 2014-07-03 2015-07-03 Method for producing dimethyl oxalate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410314462.0A CN105330542A (zh) 2014-07-03 2014-07-03 草酸二甲酯的生产方法

Publications (1)

Publication Number Publication Date
CN105330542A true CN105330542A (zh) 2016-02-17

Family

ID=55027883

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410314462.0A Pending CN105330542A (zh) 2014-07-03 2014-07-03 草酸二甲酯的生产方法

Country Status (5)

Country Link
CN (1) CN105330542A (ru)
AU (1) AU2015203732B2 (ru)
BR (1) BR102015016125B8 (ru)
CA (1) CA2896290C (ru)
RU (1) RU2692099C2 (ru)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106693431A (zh) * 2017-03-17 2017-05-24 河南中托力合化学有限公司 新型庚烷精密分馏装置
CN109096049A (zh) * 2018-07-03 2018-12-28 沈阳化工大学 一种酯化反应消除二甲酯中草酸并得到聚酯级乙二醇的方法
CN112174821A (zh) * 2020-09-04 2021-01-05 中盐安徽红四方股份有限公司 草酸二甲酯的精馏方法

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107954830A (zh) * 2016-10-17 2018-04-24 上海浦景化工技术股份有限公司 一种降低草酸二甲酯加氢制乙二醇中产物分离能耗的方法
CN107362563A (zh) * 2017-08-22 2017-11-21 南通泰利达化工有限公司 一种硝化棉的乙醇蒸馏工艺及装置
CN111454151B (zh) * 2020-04-26 2023-04-14 宁波中科远东催化工程技术有限公司 一种草酸二甲酯汽化的方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102911046A (zh) * 2011-08-02 2013-02-06 中国石油化工股份有限公司 Co偶联合成草酸二甲酯的过程中草酸二甲酯的提纯方法
CN202968431U (zh) * 2012-11-01 2013-06-05 安徽淮化股份有限公司 一种乙二醇工业生产分离中间产物草酸二甲酯和甲醇的复合塔器
CN103483150A (zh) * 2013-08-31 2014-01-01 安徽淮化股份有限公司 一种以煤为原料生产合成乙二醇的方法和装置

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1078033B (it) * 1977-04-07 1985-05-08 Snam Progetti Processo per la preparazione di esteri dell'acido ossalico
US5534648A (en) * 1993-11-30 1996-07-09 Ube Industries, Ltd. Process for continuously producing dimethyl carbonate

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102911046A (zh) * 2011-08-02 2013-02-06 中国石油化工股份有限公司 Co偶联合成草酸二甲酯的过程中草酸二甲酯的提纯方法
CN202968431U (zh) * 2012-11-01 2013-06-05 安徽淮化股份有限公司 一种乙二醇工业生产分离中间产物草酸二甲酯和甲醇的复合塔器
CN103483150A (zh) * 2013-08-31 2014-01-01 安徽淮化股份有限公司 一种以煤为原料生产合成乙二醇的方法和装置

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106693431A (zh) * 2017-03-17 2017-05-24 河南中托力合化学有限公司 新型庚烷精密分馏装置
CN109096049A (zh) * 2018-07-03 2018-12-28 沈阳化工大学 一种酯化反应消除二甲酯中草酸并得到聚酯级乙二醇的方法
CN112174821A (zh) * 2020-09-04 2021-01-05 中盐安徽红四方股份有限公司 草酸二甲酯的精馏方法
CN112174821B (zh) * 2020-09-04 2023-08-18 中盐安徽红四方股份有限公司 草酸二甲酯的精馏方法

Also Published As

Publication number Publication date
RU2015126664A3 (ru) 2019-01-31
AU2015203732B2 (en) 2019-04-04
BR102015016125B8 (pt) 2021-05-18
CA2896290C (en) 2022-08-16
AU2015203732A1 (en) 2016-01-21
RU2692099C2 (ru) 2019-06-21
BR102015016125B1 (pt) 2020-12-08
CA2896290A1 (en) 2016-01-03
RU2015126664A (ru) 2017-01-12
BR102015016125A2 (pt) 2018-06-12

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Application publication date: 20160217

RJ01 Rejection of invention patent application after publication