CN105130191A - Low-temperature transmutation indigo copper glaze formula for light ceramic, preparation method and using method - Google Patents
Low-temperature transmutation indigo copper glaze formula for light ceramic, preparation method and using method Download PDFInfo
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- CN105130191A CN105130191A CN201510534458.XA CN201510534458A CN105130191A CN 105130191 A CN105130191 A CN 105130191A CN 201510534458 A CN201510534458 A CN 201510534458A CN 105130191 A CN105130191 A CN 105130191A
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Abstract
The invention belongs to the field of ceramic manufacturing, and particularly relates to a low-temperature transmutation indigo copper glaze formula for a light ceramic, a preparation method and a using method. The low-temperature transmutation indigo copper glaze formula for the light ceramic comprises glass powder, boric acid, kaolin, sodium carbonate, basic cupric carbonate, fluorite, cryolite and bentonite. The low-temperature transmutation indigo copper glaze formula for the light ceramic is low in cost of glaze, convenient to use and low in sintering temperature, and has a unique artistic sense. The glaze effect fired by the transmutation indigo copper glaze formula has a indigo copper bottom color, irregular black spots are uniformly distributed on the bottom color, and the sizes and distribution densities of the black spots change according to the type of ceramic ware and the glazing thickness, so that the formula has a unique artistic effect. The ceramic ware manufactured by using the glaze improves the product grade and the marketing price and has relatively high economical value; in addition, the glaze can be industrially produced in batches, can be quickly popularized, is simple to use, and has relatively strong competitiveness in the market.
Description
Technical field
The invention belongs to ceramic manufacture field, be specifically related to a kind of furnace transmutation glaze formula, preparation method and the using method fired for light china.
Background technology
When furnace transmutation glaze and implements burn till in kiln, owing to containing multiple pigmentation element in kiln, through oxidation or reductive action, after kiln discharge, present beyond thought glaze chromatic effect.Traditional furnace transmutation glaze is that middle high temperature burns till, and firing temperature is more than 1200 DEG C, and firing time is mostly more than 12 hours, and its firing temperature is high, the time is long, and energy loss is large, causes cost high and not environmentally; And the glazing effect of existing lightweight white clouds pottery furnace transmutation glaze is single, kind is dull, cannot cater to the consumer demand of different individual character.
For solving the problem, the patent No. be 201110133469.9 patent of invention disclose a kind of Transmutation glaze white cloud ceramics and manufacture craft thereof, this kind of Transmutation glaze white cloud ceramics, comprise white clouds greenwave body and impose on the glaze layer on white clouds greenwave surface, this glaze layer comprises the ground-coat enamel directly executed in white clouds greenwave surface and the cover-coat enamel imposed on ground-coat enamel face; Each component of ground-coat enamel comprises low-temperature lead-free frit, coloring oxide, calcium carbonate, alkaline earth metal compound, part kaolin; Each component of described cover-coat enamel is low-temperature lead-free frit, part zinc oxide, part titanium oxide, coloring oxide, part kaolin by weight ratio.The firing temperature of this kind of furnace transmutation glaze is appointed need between 1080-1100 DEG C, and the glazed surface burnt out forms natural crystallization flower.Along with improving constantly of people's living standard, aesthetic diversified demand is also constantly changed, if it is low to develop a kind of firing temperature, there is the glaze being different from traditional transmutation effect, aesthetic diversified demand can be met there is again positive meaning.
Summary of the invention
In order to solve deficiency of the prior art, the invention provides a kind of light china low temperature transmutation covellite colour glaze formula, method of preparation and use.
Light china low temperature transmutation covellite colour glaze is filled a prescription, and it is characterized in that,
Described glaze formula is as follows according to parts by weight: glass powder 30-40 part, boric acid 20-30 part, kaolin 10-15 part, sodium carbonate 10-15 part, ventilation breather 5-10 part, fluorite 3-8 part, sodium aluminum fluoride 3-8 part, wilkinite 0-5.
Optimize, glaze formula is as follows according to parts by weight: 35 parts, glass powder, boric acid 28 parts, kaolin 12 parts, 12 parts, sodium carbonate, ventilation breather 5 parts, fluorite 5 parts, sodium aluminum fluoride 3 parts.
Optimize, glaze formula is as follows according to parts by weight: 38 parts, glass powder, boric acid 21 parts, kaolin 13 parts, 14 parts, sodium carbonate, ventilation breather 7 parts, fluorite 3 parts, sodium aluminum fluoride 4 parts.
Optimize, glaze formula is as follows according to parts by weight: 32 parts, glass powder, boric acid 25 parts, kaolin 11 parts, 15 parts, sodium carbonate, ventilation breather 6 parts, fluorite 6 parts, sodium aluminum fluoride 5 parts.
Optimize, glaze formula is as follows according to parts by weight: 40 parts, glass powder, boric acid 20 parts, kaolin 14 parts, 13 parts, sodium carbonate, ventilation breather 4 parts, fluorite 8 parts, sodium aluminum fluoride 3 parts.
The preparation method of light china low temperature transmutation covellite colour glaze, is characterized in that, comprise the following steps:
Step one, according to glaze formula weighing and proportioning, puts into ball grinder by glass powder, boric acid, kaolin, sodium carbonate, ventilation breather, fluorite, sodium aluminum fluoride, and adds the water of 40-50%;
Step 2, after ball milling 12-18 hour, if having glaze slip to precipitate add wilkinite;
Step 3, sieves stand-by by the glaze that step 2 obtains, obtained transmutation covellite colour glaze.
Further, 200 mesh sieves crossed by the glaze in step 3.
The using method of light china low temperature transmutation covellite colour glaze, is characterized in that, comprise the following steps:
Step 1, prepares light ceramics base substrate;
Step 2, imposes on light ceramics base substrate by transmutation covellite colour glaze, places 5-10 hour;
Step 3, by have the ceramic body of transmutation covellite colour glaze to put into kiln oxydizing flame to fire, firing temperature is between 980 DEG C-1060 DEG C.
Further, the enameling method in step 2 is leaching glaze or glaze spraying.
Further, in step 3, after ceramic body enters kiln, kiln rapid temperature increases, to firing temperature, burns till rear naturally cooling.
Seen from the above description, light china low temperature transmutation covellite colour glaze formula provided by the invention, method of preparation and use, have following beneficial effect: one is glaze cost raw material that is low, that use is all easily obtain, and manufacture craft is simple; Two is easy to use, uses this kind of low temperature transmutation covellite colour glaze only need at billet surface last layer glaze without the need to ground-coat enamel; Three is that firing temperature is low, and the firing temperature of this kind of transmutation covellite colour glaze only needs can realize transmutation effect, save energy between 980 DEG C-1060 DEG C; Four is have unique artistic feeling, the glazing effect that this kind of transmutation covellite colour glaze burns out has the background color of covellite look, background color distributed irregular black splotch uniformly, the size of black splotch and respectively density change according to ceramic ware type and glazing thickness, have unique artistic effect; The porcelain using this kind of glaze to make improves product specification and selling price, has higher economic worth; In addition this kind of glaze can bulk industrial produce, can Rapid Popularization, use simple, commercially there is stronger competitive power.
Embodiment
Technical scheme for a better understanding of the present invention, is described below in detail embodiment provided by the invention.
Light china low temperature transmutation covellite colour glaze is filled a prescription, as follows according to parts by weight: glaze formula is as follows according to parts by weight: glass powder 30-40 part, boric acid 20-30 part, kaolin 10-15 part, sodium carbonate 10-15 part, ventilation breather 5-10 part, fluorite 3-8 part, sodium aluminum fluoride 3-8 part, wilkinite 0-5.
Specific embodiment one:
Glaze formula is as follows according to parts by weight: 35 parts, glass powder, boric acid 28 parts, kaolin 12 parts, 12 parts, sodium carbonate, ventilation breather 5 parts, fluorite 5 parts, sodium aluminum fluoride 3 parts.
The preparation method of above-mentioned light china low temperature transmutation covellite colour glaze, comprises the following steps:
Step one, according to glaze formula weighing and proportioning, puts into ball grinder by glass powder, boric acid, kaolin, sodium carbonate, ventilation breather, fluorite, sodium aluminum fluoride, and adds the water of 50%;
Step 2, ball milling is after 16 hours, if having glaze slip to precipitate add wilkinite;
Step 3, crosses 200 mesh sieves by the glaze that step 2 obtains stand-by, obtained transmutation covellite colour glaze.
The using method of light china low temperature transmutation covellite colour glaze, is characterized in that, comprise the following steps:
Step 1, prepares light ceramics base substrate;
Step 2, imposes on light ceramics base substrate by transmutation covellite colour glaze, places 8 hours, and enameling method is leaching glaze or glaze spraying;
Step 3, by have the ceramic body of transmutation covellite colour glaze to put into kiln oxydizing flame to fire, firing temperature is between 980 DEG C-1060 DEG C, and after ceramic body enters kiln, kiln rapid temperature increases, to firing temperature, burns till rear naturally cooling.
Specific embodiment two:
Glaze formula is as follows according to parts by weight: 38 parts, glass powder, boric acid 21 parts, kaolin 13 parts, 14 parts, sodium carbonate, ventilation breather 7 parts, fluorite 3 parts, sodium aluminum fluoride 4 parts.
Specific embodiment three:
Glaze formula is as follows according to parts by weight: 32 parts, glass powder, boric acid 25 parts, kaolin 11 parts, 15 parts, sodium carbonate, ventilation breather 6 parts, fluorite 6 parts, sodium aluminum fluoride 5 parts.
Specific embodiment four:
Glaze formula is as follows according to parts by weight: 40 parts, glass powder, boric acid 20 parts, kaolin 14 parts, 13 parts, sodium carbonate, ventilation breather 4 parts, fluorite 8 parts, sodium aluminum fluoride 3 parts.
The preparation method of the light china low temperature transmutation covellite colour glaze described in specific embodiment two to four, comprises the following steps:
Step one, according to glaze formula weighing and proportioning, puts into ball grinder by glass powder, boric acid, kaolin, sodium carbonate, ventilation breather, fluorite, sodium aluminum fluoride, and adds the water of 40-50%;
Step 2, after ball milling 12-18 hour, if having glaze slip to precipitate add wilkinite;
Step 3, crosses 200 mesh sieves by the glaze that step 2 obtains stand-by, obtained transmutation covellite colour glaze.
The using method of the light china low temperature transmutation covellite colour glaze described in specific embodiment two to four, comprises the following steps:
Step 1, prepares light ceramics base substrate;
Step 2, imposes on light ceramics base substrate by transmutation covellite colour glaze, places 5-10 hour, and enameling method is leaching glaze or glaze spraying;
Step 3, by have the ceramic body of transmutation covellite colour glaze to put into kiln oxydizing flame to fire, firing temperature is between 980 DEG C-1060 DEG C, and after ceramic body enters kiln, kiln rapid temperature increases, to firing temperature, burns till rear naturally cooling.
Above-mentioned light china low temperature transmutation covellite colour glaze formula, method of preparation and use, glaze cost raw material that is low, that use is all easily obtain, and manufacture craft is simple; Easy to use, use this kind of low temperature transmutation covellite color glaze only need at billet surface last layer glaze without the need to ground-coat enamel; Firing temperature is low, and the firing temperature of this kind of transmutation covellite colour glaze only needs can realize transmutation effect, save energy between 980 DEG C-1060 DEG C; There is unique artistic feeling, the glazing effect that this kind of transmutation covellite colour glaze burns out has the background color of covellite look, background color distributed irregular black splotch uniformly, the size of black splotch and respectively density change according to ceramic ware type and glazing thickness, have unique artistic effect;
The porcelain using this kind of glaze to make improves product specification and selling price, has higher economic worth; In addition this kind of glaze can bulk industrial produce, can Rapid Popularization, use simple, commercially there is stronger competitive power.
The above, be only present pre-ferred embodiments, therefore can not limit scope of the invention process with this, and the equivalence namely done according to the present patent application the scope of the claims and description changes and modifies, and all should still remain within the scope of the patent.
Claims (10)
1. light china low temperature transmutation covellite colour glaze formula, is characterized in that,
Described glaze formula is as follows according to parts by weight: glass powder 30-40 part, boric acid 20-30 part, kaolin 10-15 part, sodium carbonate 10-15 part, ventilation breather 5-10 part, fluorite 3-8 part, sodium aluminum fluoride 3-8 part, wilkinite 0-5.
2. light china low temperature transmutation covellite colour glaze formula according to claim 1, it is characterized in that, described glaze formula is as follows according to parts by weight: 35 parts, glass powder, boric acid 28 parts, kaolin 12 parts, 12 parts, sodium carbonate, ventilation breather 5 parts, fluorite 5 parts, sodium aluminum fluoride 3 parts.
3. light china low temperature transmutation covellite colour glaze formula according to claim 1, it is characterized in that, described glaze formula is as follows according to parts by weight: 38 parts, glass powder, boric acid 21 parts, kaolin 13 parts, 14 parts, sodium carbonate, ventilation breather 7 parts, fluorite 3 parts, sodium aluminum fluoride 4 parts.
4. light china low temperature transmutation covellite colour glaze formula according to claim 1, it is characterized in that, described glaze formula is as follows according to parts by weight: 32 parts, glass powder, boric acid 25 parts, kaolin 11 parts, 15 parts, sodium carbonate, ventilation breather 6 parts, fluorite 6 parts, sodium aluminum fluoride 5 parts.
5. light china low temperature transmutation covellite colour glaze formula according to claim 1, it is characterized in that, described glaze formula is as follows according to parts by weight: 40 parts, glass powder, boric acid 20 parts, kaolin 14 parts, 13 parts, sodium carbonate, ventilation breather 4 parts, fluorite 8 parts, sodium aluminum fluoride 3 parts.
6. the preparation method of light china low temperature transmutation covellite colour glaze, is characterized in that, comprise the following steps:
Step one, according to glaze formula weighing and proportioning, puts into ball grinder by glass powder, boric acid, kaolin, sodium carbonate, ventilation breather, fluorite, sodium aluminum fluoride, and adds the water of 40-50%;
Step 2, after ball milling 12-18 hour, if having glaze slip to precipitate add wilkinite;
Step 3, sieves stand-by by the glaze that step 2 obtains, obtained transmutation covellite colour glaze.
7. the preparation method of light china low temperature transmutation covellite colour glaze according to claim 6, is characterized in that: 200 mesh sieves crossed by the glaze in step 3.
8. the using method of the light china low temperature transmutation covellite colour glaze according to claim 1 to 5 any one, is characterized in that, comprise the following steps:
Step 1, prepares light ceramics base substrate;
Step 2, imposes on light ceramics base substrate by transmutation covellite colour glaze, places 5-10 hour;
Step 3, by have the ceramic body of transmutation covellite colour glaze to put into kiln oxydizing flame to fire, firing temperature is between 980 DEG C-1060 DEG C.
9. the using method of institute's light china low temperature transmutation covellite colour glaze according to Claim 8, is characterized in that: the enameling method in described step 2 is leaching glaze or glaze spraying.
10. the using method of light china low temperature transmutation covellite colour glaze according to claim 8, it is characterized in that: in described step 3, after ceramic body enters kiln, kiln rapid temperature increases, to firing temperature, burns till rear naturally cooling.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106565092A (en) * | 2016-08-31 | 2017-04-19 | 福建省德化县臻晖陶瓷有限公司 | Lightweight low-temperature fancy golden silk white glazed porcelain and manufacturing process |
| CN112479591A (en) * | 2020-12-24 | 2021-03-12 | 湖州海程塑业有限公司 | Sacrificial red glaze and preparation method thereof |
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| CN1440944A (en) * | 2003-04-04 | 2003-09-10 | 张连峰 | Prepn of bake-free glaze |
| CN103601534A (en) * | 2013-10-11 | 2014-02-26 | 福建省泉州龙鹏集团有限公司 | High-whiteness under-glaze colorful low-temperature ceramic and preparation method thereof |
| CN103964900A (en) * | 2014-05-12 | 2014-08-06 | 成都朋和科技有限公司 | formula and preparation method of Sky blue transmutation glaze |
| CN104261884A (en) * | 2014-09-22 | 2015-01-07 | 广西北流仲礼瓷业有限公司 | Ceramic glaze fired at ultralow temperature and preparation method of ceramic glaze |
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2015
- 2015-08-27 CN CN201510534458.XA patent/CN105130191B/en active Active
Patent Citations (4)
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| CN1440944A (en) * | 2003-04-04 | 2003-09-10 | 张连峰 | Prepn of bake-free glaze |
| CN103601534A (en) * | 2013-10-11 | 2014-02-26 | 福建省泉州龙鹏集团有限公司 | High-whiteness under-glaze colorful low-temperature ceramic and preparation method thereof |
| CN103964900A (en) * | 2014-05-12 | 2014-08-06 | 成都朋和科技有限公司 | formula and preparation method of Sky blue transmutation glaze |
| CN104261884A (en) * | 2014-09-22 | 2015-01-07 | 广西北流仲礼瓷业有限公司 | Ceramic glaze fired at ultralow temperature and preparation method of ceramic glaze |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106565092A (en) * | 2016-08-31 | 2017-04-19 | 福建省德化县臻晖陶瓷有限公司 | Lightweight low-temperature fancy golden silk white glazed porcelain and manufacturing process |
| CN112479591A (en) * | 2020-12-24 | 2021-03-12 | 湖州海程塑业有限公司 | Sacrificial red glaze and preparation method thereof |
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