CN104947499B - 硅溶胶、制备其的设备和方法和其在造纸中的应用 - Google Patents

硅溶胶、制备其的设备和方法和其在造纸中的应用 Download PDF

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Publication number
CN104947499B
CN104947499B CN201410748835.5A CN201410748835A CN104947499B CN 104947499 B CN104947499 B CN 104947499B CN 201410748835 A CN201410748835 A CN 201410748835A CN 104947499 B CN104947499 B CN 104947499B
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CN
China
Prior art keywords
colloidal silica
reaction vessel
pipeline
activator
terminator
Prior art date
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Active
Application number
CN201410748835.5A
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English (en)
Chinese (zh)
Other versions
CN104947499A (zh
Inventor
白雯
徐健
吴佳
陈跖
申建坤
R·D·小米勒
J·W·兴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ecolab USA Inc
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Ecolab USA Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to CN201711414284.9A priority Critical patent/CN108130801B/zh
Application filed by Ecolab USA Inc filed Critical Ecolab USA Inc
Priority to CN201410748835.5A priority patent/CN104947499B/zh
Priority to PCT/US2014/070927 priority patent/WO2015095377A1/en
Priority to BR112016014038-9A priority patent/BR112016014038B1/pt
Priority to US15/105,801 priority patent/US9975781B2/en
Priority to KR1020167019330A priority patent/KR102379044B1/ko
Priority to CA2934323A priority patent/CA2934323C/en
Priority to JP2016541150A priority patent/JP6595482B2/ja
Priority to EP14871356.3A priority patent/EP3083499B1/en
Publication of CN104947499A publication Critical patent/CN104947499A/zh
Application granted granted Critical
Publication of CN104947499B publication Critical patent/CN104947499B/zh
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/146—After-treatment of sols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/3045—Treatment with inorganic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/3063—Treatment with low-molecular organic compounds
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H11/00—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
    • D21H11/02—Chemical or chemomechanical or chemothermomechanical pulp
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/63—Inorganic compounds
    • D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
    • D21H17/68—Water-insoluble compounds, e.g. fillers, pigments siliceous, e.g. clays
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/06—Paper forming aids
    • D21H21/10—Retention agents or drainage improvers

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Silicon Compounds (AREA)
  • Paper (AREA)
  • Colloid Chemistry (AREA)
CN201410748835.5A 2013-12-18 2014-12-10 硅溶胶、制备其的设备和方法和其在造纸中的应用 Active CN104947499B (zh)

Priority Applications (9)

Application Number Priority Date Filing Date Title
CN201410748835.5A CN104947499B (zh) 2013-12-18 2014-12-10 硅溶胶、制备其的设备和方法和其在造纸中的应用
CN201711414284.9A CN108130801B (zh) 2013-12-18 2014-12-10 生产用于造纸的活化胶态二氧化硅的方法
BR112016014038-9A BR112016014038B1 (pt) 2013-12-18 2014-12-17 Processo para a produção de sílica coloidal ativada
US15/105,801 US9975781B2 (en) 2013-12-18 2014-12-17 Silica sols, method and apparatus for producing the same and use thereof in papermaking
PCT/US2014/070927 WO2015095377A1 (en) 2013-12-18 2014-12-17 Silica sols, method and apparatus for producing the same and use thereof in papermaking
KR1020167019330A KR102379044B1 (ko) 2013-12-18 2014-12-17 실리카 졸, 이를 제조하기 위한 방법 및 장치, 및 제지에서의 이의 용도
CA2934323A CA2934323C (en) 2013-12-18 2014-12-17 Silica sols, method and apparatus for producing the same and use thereof in papermaking
JP2016541150A JP6595482B2 (ja) 2013-12-18 2014-12-17 シリカゾル、その製造のための方法および装置ならびに製紙でのそれらの使用
EP14871356.3A EP3083499B1 (en) 2013-12-18 2014-12-17 Method for producing silica sols in papermaking

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN2013106979158 2013-12-18
CN201310697915 2013-12-18
CN201410748835.5A CN104947499B (zh) 2013-12-18 2014-12-10 硅溶胶、制备其的设备和方法和其在造纸中的应用

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN201711414284.9A Division CN108130801B (zh) 2013-12-18 2014-12-10 生产用于造纸的活化胶态二氧化硅的方法

Publications (2)

Publication Number Publication Date
CN104947499A CN104947499A (zh) 2015-09-30
CN104947499B true CN104947499B (zh) 2018-01-19

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CN201410748835.5A Active CN104947499B (zh) 2013-12-18 2014-12-10 硅溶胶、制备其的设备和方法和其在造纸中的应用
CN201711414284.9A Active CN108130801B (zh) 2013-12-18 2014-12-10 生产用于造纸的活化胶态二氧化硅的方法

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CN201711414284.9A Active CN108130801B (zh) 2013-12-18 2014-12-10 生产用于造纸的活化胶态二氧化硅的方法

Country Status (8)

Country Link
US (1) US9975781B2 (OSRAM)
EP (1) EP3083499B1 (OSRAM)
JP (1) JP6595482B2 (OSRAM)
KR (1) KR102379044B1 (OSRAM)
CN (2) CN104947499B (OSRAM)
BR (1) BR112016014038B1 (OSRAM)
CA (1) CA2934323C (OSRAM)
WO (1) WO2015095377A1 (OSRAM)

Families Citing this family (9)

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WO2017054198A1 (en) 2015-09-30 2017-04-06 Ecolab Usa Inc. Compositions and methods for treating filler in papermaking
US20210130176A1 (en) * 2017-10-11 2021-05-06 Applied Material Solutions, Inc. Multimodal Particles for Retention and Drainage for Paper-Making Machines
CN108083283B (zh) * 2017-12-07 2021-08-20 临汾博利士纳米材料有限公司 铝改性酸性硅溶胶及其制备方法
CN108277639B (zh) * 2018-02-11 2020-08-25 宜州市壮之都丝绸家纺有限公司 一种四元硅溶胶掺杂真丝丝绸的工艺
CN108277640B (zh) * 2018-02-11 2020-08-21 宜州市壮之都丝绸家纺有限公司 一种三元硅溶胶掺杂真丝丝绸的工艺
US10876258B2 (en) * 2018-11-27 2020-12-29 Solenis Technologies, L.P. Method for improving filler and fiber retention in paper making processes
EP3980500A1 (en) * 2019-06-07 2022-04-13 Ecolab Usa Inc. Hydrophilic cationic dispersion polymers for improved print quality and water fastness
CN111302347B (zh) * 2020-04-02 2020-10-16 临沂市科翰硅制品有限公司 一种高纯大粒径硅溶胶的制备方法
CN119173476A (zh) * 2022-05-13 2024-12-20 多摩化学工业株式会社 胶体二氧化硅及其制造方法

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SE500387C2 (sv) 1989-11-09 1994-06-13 Eka Nobel Ab Silikasoler, förfarande för framställning av silikasoler samt användning av solerna i pappersframställning
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AU4672293A (en) * 1992-07-10 1994-01-31 Novatech, Inc. Flavor enhancing composition containing colloidal silica and method for its preparation and use
SE501214C2 (sv) * 1992-08-31 1994-12-12 Eka Nobel Ab Silikasol samt förfarande för framställning av papper under användande av solen
FR2732368B1 (fr) 1995-03-31 1997-06-06 Roquette Freres Nouveau procede de fabrication de papier
US5573674A (en) * 1995-10-27 1996-11-12 General Chemical Corporation Activated silica sol
FR2740482B1 (fr) 1995-10-30 1997-11-21 Snf Sa Procede pour ameliorer la retention dans un procede de fabrication du papier, carton et analogue
KR100573343B1 (ko) 1997-06-13 2006-04-24 이 아이 듀폰 디 네모아 앤드 캄파니 저-농도 폴리알루미노실리케이트 마이크로겔의 개선된제조 방법
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Also Published As

Publication number Publication date
CA2934323C (en) 2020-10-06
CA2934323A1 (en) 2015-06-25
JP6595482B2 (ja) 2019-10-23
JP2017507876A (ja) 2017-03-23
KR102379044B1 (ko) 2022-03-24
CN104947499A (zh) 2015-09-30
WO2015095377A1 (en) 2015-06-25
CN108130801B (zh) 2020-11-24
EP3083499A1 (en) 2016-10-26
US9975781B2 (en) 2018-05-22
EP3083499B1 (en) 2020-01-22
KR20160098482A (ko) 2016-08-18
BR112016014038A2 (pt) 2017-08-08
CN108130801A (zh) 2018-06-08
US20160311693A1 (en) 2016-10-27
BR112016014038B1 (pt) 2021-12-07
EP3083499A4 (en) 2017-05-24

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C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
CB03 Change of inventor or designer information

Inventor after: Bai Wen

Inventor after: Xu Jian

Inventor after: Wu Jia

Inventor after: Chen Zhi

Inventor after: Shen Jiankun

Inventor after: R D little Miller

Inventor after: J, W, Xing

Inventor before: Bai Wen

Inventor before: Xu Jian

Inventor before: Wu Jia

Inventor before: Chen Zhi

COR Change of bibliographic data
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