CN104921989B - A kind of not silicate-containing oil and the shampoo and preparation method thereof with scalp care - Google Patents
A kind of not silicate-containing oil and the shampoo and preparation method thereof with scalp care Download PDFInfo
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Abstract
The present invention relates to a kind of not silicate-containing oil and has effects that the shampoo of scalp care comprising following mass percent component: mild surfactant 5~50%, scalp care agent 0.1~10%；The mixing that mild surfactant is three kinds or more in cocounut oil acyl methyl taurine sodium taurocholate, sodium methyl cocoyl taurate, sodium lauroyl sarcosine, sodium lauroyl glutamate, cocoamido sodium propionate, Cocoamidopropyl betaine, Sodium Lauroamphoacetate, Plantacare 818, Tea Saponin and soapberry fruit bark extract；Scalp care agent is mixing two or more in hydrolysed corn starch, pyrrolidone sodium carboxylate, polyglutamic acid sodium, piroctone olamine salt, ginger-root extract, False flax seed oil, Flos Eriocauli extract, raspberry juice and leaf of Mentha piperita extract.The effect of present invention is mildly non-stimulated, and scalp can be made comfortable, and hair follicle health, root of hair is firm, plays nursing scalp and reduces hair loss.
Description
Technical field
The invention belongs to daily cosmetics field, in particular to a kind of not silicate-containing oil and there is scalp care function
The shampoo of effect.
Background technique
Hair washing product is many kinds of currently on the market, but as a whole, is broadly divided into two kinds: one kind is common shampoo,
Contain silicone oil component；A kind of is not silicate-containing oil without silicone oil shampoo.
The common shampoo major advantage of siliceous oil component is submissive, easy combing using rear hair, but its there are disadvantages
It is clear that 1. silicone oil be attached on hair and scalp generate accumulation, influence hair appearance and function, even result in dandruff, head is itched
Etc. symptoms；2. dyeing and perm hair quality is not suitable for, for a long time using exacerbation hair damage；3. silicone oil is the raw material of industry, by-product can
There can be health risk；4. silicone oil is difficult to degrade, can cause environmental pollution.In view of the disadvantage mentioned above of silicate-containing oil shampoo, nothing
Silicone oil shampoo is increasingly becoming the market mainstream.
However, existing no silicone oil shampoo also mainly follows the trend of the market of no silicone oil shampoo, only simply go
Except the silicone oil in shampoo, leads to problems such as the reduction of shampoo service performance occur in this way or conditioning performance is insufficient.Just because such as
How this, rationally substitute the silicone oil in shampoo, while not reducing the service performance of shampoo, becomes no silicone oil hair washing wate research
Hot and difficult issue.
Summary of the invention
The present invention in view of the deficiencies of the prior art, provides that a kind of no silicone oil, not add coloring agent, petroleum-type surface living
Property agent, mineral oil, animal raw materials and paraben esters have effects that the shampoo of scalp care.By rationally substituting hair washing
Silicone oil component in water, while being combined using surfactant with scalp care agent, bring service performance and silicate-containing oil shampoo
It compares favourably, while having effects that scalp care.
It is a further object of the present invention to provide a kind of not silicate-containing oil and has effects that the preparation side of the shampoo of scalp care
Method.
In order to solve the above technical problems, shampoo of the invention adopts the following technical scheme that
A kind of not silicate-containing oil and have effects that the shampoo of scalp care comprising following mass percent component:
Mild surfactant 5~50%；
Scalp care agent 0.1~10%.
Preferably, the mass percent of the surfactant can be 7~30%.
Preferably, the mass percent of the scalp care agent can be 0.5~5%.
The mild surfactant is cocounut oil acyl methyl taurine sodium taurocholate, sodium methyl cocoyl taurate, the moon
Osmanthus acylsarcosine sodium, sodium lauroyl glutamate, cocoamido sodium propionate, Cocoamidopropyl betaine, lauroyl both sexes base
Three kinds or more of mixing in sodium acetate, Plantacare 818, Tea Saponin and soapberry fruit bark extract.The mild surface-active
Agent provides foam abundant and good cleaning force for the present invention, while foaming structure is good, mild non-stimulated, both solves nothing
The problem of thickening of silicone oil shampoo is difficult and hair conditioning can not get both with transparency, and greatly reduce the irritation of formula.
Preferably, the mild surfactant be sodium lauroyl sarcosine 15%, Cocoamidopropyl betaine 6%,
Plantacare 818 1%, Sodium Lauroamphoacetate 1%, sodium methyl cocoyl taurate 1% and Tea Saponin 0.3%.
Preferably, the mild surfactant is cocoamido sodium propionate 12%, Cocoamidopropyl betaine
7%, sodium methyl cocoyl taurate 2% and soapberry fruit bark extract 0.5%.
Preferably, the mild surfactant is cocounut oil acyl methyl taurine sodium taurocholate 6%, methyl cocoyl ox
Sodium sulfonate 4%, sodium lauroyl sarcosine 8%, Cocoamidopropyl betaine 4% and Plantacare 818 1%.
The scalp care agent is hydrolysed corn starch, pyrrolidone sodium carboxylate, polyglutamic acid sodium, piroctone olamine
It is two or more in salt, ginger-root extract, False flax seed oil, Flos Eriocauli extract, raspberry juice and leaf of Mentha piperita extract
Mixing.Wherein hydrolysed corn starch ingredient is maltotetraose.The scalp care agent provides nursing for scalp, makes scalp health,
Hair follicle health, root of hair is firm, reduces hair loss.
Preferably, the scalp care agent is hydrolysed corn starch 0.2%, piroctone olamine salt 0.4% and Asia
Numb shepherd's purse seed oil 0.01%.
Preferably, the scalp care agent is piroctone olamine salt 0.3%, ginger-root extract 0.1%, False flax seed
Oil 0.02% and Flos Eriocauli extract 0.2%.
Preferably, the scalp care agent is hydrolysed corn starch 0.3%, pyrrolidone sodium carboxylate 0.1%, piroctone
Ethanolamine salt 0.3%, False flax seed oil 0.01% and Flos Eriocauli extract 0.1%.
The hydrolysed corn starch can select Boai Xinkaiyuan Pharmacy stock Co., Ltd (Hayashibara
Co.Ltd. the high maltotetraose slurry (Tetrup)) produced.
The ginger-root extract can select fragrant (Shanghai) Co., Ltd. (Symrise Shanghai LTD) of moral to produce
Ginger-root extract (118998).
The False flax seed oil that the False flax seed oil can select Clariant (Clariant) (China) Co., Ltd to produce
(CAMELINA-SERUM)。
The preparation method of the Flos Eriocauli extract is that take the weight ratio of pipewort and water be 1: 20, after pipewort chopping
It is added in distilled water, is heated to 100 DEG C, the temperature is kept continuously to boil 2 hours, after filtering place to go residue, filtrate is in 60 DEG C of items
/ 10th of original water volume are concentrated under reduced pressure under part to get the Flos Eriocauli extract of active ingredient.
The raspberry juice can select fragrant (Shanghai) Co., Ltd. (Symrise Shanghai LTD) of moral to produce
Organic raspberry (Raspberry (Organic) GW).
It is organic that the leaf of Mentha piperita extract can select green science and technology Co., Ltd (GREENTECH S.A.) to produce
Mint extract (PEPPERMINT ORGANIC AQUEOUS EXTRACT (OH)).
Not silicate-containing oil of the invention and having effects that can also add its and necessary be configured in the shampoo of scalp care
Point, such as: deionized water, grease, cation opsonizing agent, chelating agent, thickener, pH adjusting agent, preservative, essence and other
Surfactant.
The not silicate-containing oil and have effects that the preparation method of scalp care shampoo comprising steps are as follows:
(1) polymeric conditioner is added to the water, 10~15min is stirred with the rate of 2500~3000 turns/min；
(2) mild surfactant and grease is added, is heated to 80~85 DEG C, scalp care agent and other additions are added
Agent, 15~20min of insulated and stirred；
(3) after being cooled to 45~50 DEG C, preservative and essence is added, obtains finished product after mixing evenly.
The polymeric conditioner can be guar hydroxypropyltrimonium chloride, Polyquaternium-10.
The additive can be EDETATE SODIUM, citric acid, sodium citrate.
The preservative can be Kathon, sodium benzoate.
Compared with prior art, the invention has the following beneficial effects: with good viscosity, while physicochemical property is steady
Fixed, foaming abundancy, conditioning effect can match in excellence or beauty the shampoo of silicate-containing oil.Its outstanding feature is protected by surfactant and scalp
The matched combined of agent is managed, collaboration reaches mild non-stimulated, protection scalp and hair follicle, nourishes the effect of scalp and hair-care, to make head
Skin, hair follicle health, root of hair is firm, and hair loss is reduced；Mild surfactant therein can reduce stimulation, and care agent can increase
Conditioning is added especially to the nursing of scalp, to be equivalent to " attenuation synergistic " effect of drug collaboration.
Detailed description of the invention
Fig. 1 is shampoo cardability test result column schematic diagram.
Specific embodiment
Below by way of specific embodiment come the present invention is further illustrated, but these embodiments simply to illustrate that,
Limitation in any form is not constituted to the present invention.
Embodiment 1
A kind of not silicate-containing oil and has effects that the shampoo of scalp care, by the mass percent component in formula as below table
It is made, wherein the mass percent of mild surfactant is 24.3%, and the mass percent of scalp care agent is 0.6%:
| Component | Mass percent % |
| Water | TO 100 |
| Sodium lauroyl sarcosine | 15.0 |
| Cocoamidopropyl betaine | 6.0 |
| Glycerol monolaurate | 2.4 |
| Sodium methyl cocoyl taurate | 1.0 |
| Sodium Lauroamphoacetate | 1.0 |
| Decyl Polyglucoside | 1.0 |
| Guar hydroxypropyltrimonium chloride | 0.6 |
| False flax seed oil | 0.001 |
| Tea Saponin | 0.3 |
| Hydrolysed corn starch | 0.4 |
| Piroctone olamine salt | 0.2 |
| EDETATE SODIUM | 0.1 |
| Citric acid | 0.5 |
| Essence | 0.4 |
| Kathon | 0.04 |
The not silicate-containing oil and have effects that the preparation method of the shampoo of scalp care the following steps are included:
(1) guar hydroxypropyltrimonium chloride is added to the water, with the rate homogenous disperse of 2500 turns/min
10min；
(2) sodium lauroyl sarcosine, Cocoamidopropyl betaine, sodium methyl cocoyl taurate, lauroyl is added
Both sexes guanidine-acetic acid sodium, Decyl Polyglucoside and Tea Saponin, stir evenly, and are heated to 80 DEG C, be added glycerol monolaurate, citric acid and
The solid materials such as EDETATE SODIUM, insulated and stirred 20min；
(3) 75 DEG C are cooled to, piroctone olamine salt is added, and stir evenly；
(4) 50 DEG C are cooled to, essence, Kathon, False flax seed oil and hydrolysed corn starch is added, stirs evenly；
(5) 40 DEG C are down to hereinafter, stopping stirring, discharging to temperature.
Embodiment 2
A kind of not silicate-containing oil and has effects that the shampoo of scalp care, by the mass percent component in formula as below table
It is made, wherein the mass percent of mild surfactant is 21%, and the mass percent of scalp care agent is 0.24%:
| Component | Mass percent % |
| Water | TO 100 |
| Cocoamido sodium propionate | 12.0 |
| Ginger-root extract | 0.04 |
| Cocoamidopropyl betaine | 7.0 |
| Coconut oleoyl amine methyl MEA | 0.4 |
| Citric acid | 0.4 |
| Sodium citrate | 0.2 |
| Plantacare 818 | 2.0 |
| Essence | 0.4 |
| Guar hydroxypropyltrimonium chloride | 0.4 |
| PPG-3 Octyl Ether | 0.2 |
| EDETATE SODIUM | 0.1 |
| Piroctone olamine salt | 0.2 |
| Dipotassium glycyrrhizinate | 0.12 |
| Sodium benzoate | 0.20 |
| Kathon | 0.05 |
| False flax seed oil | 0.001 |
| Flos Eriocauli extract | 0.003 |
The not silicate-containing oil and have effects that the preparation method of the shampoo of scalp care the following steps are included:
(1) guar hydroxypropyltrimonium chloride is added to the water, with the rate homogenous disperse of 2500 turns/min
15min；
(2) cocoamido sodium propionate, Cocoamidopropyl betaine, Plantacare 818, coconut oleoyl amine methyl MEA is added
It with PPG-3 Octyl Ether, stirs evenly, is heated to 80 DEG C, it is solid that citric acid, sodium citrate, EDETATE SODIUM and sodium benzoate etc. is added
Body raw material, insulated and stirred 15min；
(3) 75 DEG C are cooled to, piroctone olamine salt and dipotassium glycyrrhizinate is added, and stir evenly；
(4) 45 DEG C are cooled to, essence, Kathon, ginger-root extract, False flax seed oil and Flos Eriocauli extract, stirring is added
Uniformly；
(5) 40 DEG C are down to hereinafter, stopping stirring, discharging to temperature.
Embodiment 3
A kind of not silicate-containing oil and has effects that the shampoo of scalp care, by the mass percent component in formula as below table
It is made, wherein the mass percent of mild surfactant is 18.5%, and the mass percent of scalp care agent is 1.1%:
| Component | Mass percent % |
| Water | TO 100 |
| Laureth sodium sulfovinate | 4.0 |
| Soapberry fruit bark extract | 0.5 |
| Cocounut oil acyl methyl taurine sodium taurocholate | 8.0 |
| Cocaminopropionic acid sodium | 3.5 |
| Cocoamidopropyl betaine | 5.5 |
| Coconut oleoyl amine methyl MEA | 0.1 |
| Citric acid | 0.4 |
| Sodium citrate | 0.3 |
| The smooth caprylate of sorb | 0.5 |
| Sodium methyl cocoyl taurate | 1.0 |
| Essence | 0.5 |
| Guar hydroxypropyltrimonium chloride | 0.4 |
| EDETATE SODIUM | 0.1 |
| Piroctone olamine salt | 0.3 |
| Pyrrolidone sodium carboxylate | 0.5 |
| Hydrolysed corn starch | 0.3 |
| Kathon | 0.07 |
| False flax seed oil | 0.001 |
| Flos Eriocauli extract | 0.003 |
The not silicate-containing oil and have effects that the preparation method of the shampoo of scalp care the following steps are included:
(1) guar hydroxypropyltrimonium chloride is added in the smooth caprylate of sorb and is uniformly dispersed, added in water, with
The rate homogenous disperse 10min of 3000 turns/min；
(2) be added laureth sodium sulfovinate, soapberry fruit bark extract, cocounut oil acyl methyl taurine sodium taurocholate,
Cocaminopropionic acid sodium, Cocoamidopropyl betaine, sodium methyl cocoyl taurate and coconut oleoyl amine methyl MEA, are stirred
It mixes uniformly, is heated to 80 DEG C, the solid materials such as citric acid, sodium citrate and EDETATE SODIUM, insulated and stirred 20min is added；
(3) 75 DEG C are cooled to, piroctone olamine salt is added, and stir evenly；
(4) be cooled to 50 DEG C, be added essence, Kathon, pyrrolidone sodium carboxylate, hydrolysed corn starch, False flax seed oil and
Flos Eriocauli extract stirs evenly；
(5) 40 DEG C are down to hereinafter, stopping stirring, discharging to temperature.
Embodiment 4
A kind of not silicate-containing oil and has effects that the shampoo of scalp care, by the mass percent component in formula as below table
It is made, wherein the mass percent of mild surfactant is 45%, and the mass percent of scalp care agent is 2%:
| Component | Mass percent % |
| Water | TO 100 |
| Sodium lauroyl sarcosine | 16.0 |
| Cocoamidopropyl betaine | 8.0 |
| Sodium Lauroamphoacetate | 2.0 |
| Cocaminopropionic acid sodium | 8.0 |
| Tea Saponin | 5.0 |
| Sodium methyl cocoyl taurate | 3.0 |
| Decyl Polyglucoside | 3.0 |
| Guar hydroxypropyltrimonium chloride | 0.6 |
| Raspberry juice | 0.5 |
| Polyglutamic acid sodium | 0.5 |
| Piroctone olamine salt | 0.7 |
| EDETATE SODIUM | 0.1 |
| Citric acid | 0.5 |
| Essence | 0.4 |
| Kathon | 0.04 |
The not silicate-containing oil and have effects that the preparation method of the shampoo of scalp care the following steps are included:
(1) guar hydroxypropyltrimonium chloride is added to the water, with the rate homogenous disperse of 3000 turns/min
15min；
(2) sodium lauroyl sarcosine, Cocoamidopropyl betaine, Sodium Lauroamphoacetate, coconut oleoyl amine is added
Base sodium propionate, Tea Saponin, sodium methyl cocoyl taurate and Decyl Polyglucoside, stir evenly, and are heated to 85 DEG C, and citric acid is added
With the solid materials such as EDETATE SODIUM, insulated and stirred 15min；
(3) 75 DEG C are cooled to, piroctone olamine salt is added, and stir evenly；
(4) 50 DEG C are cooled to, essence, Kathon, raspberry juice and polyglutamic acid sodium is added, stirs evenly；
(5) 40 DEG C are down to hereinafter, stopping stirring, discharging to temperature.
Embodiment 5
A kind of not silicate-containing oil and has effects that the shampoo of scalp care, by the mass percent component in formula as below table
It is made, wherein the mass percent of mild surfactant is 8%, and the mass percent of scalp care agent is 6%:
| Component | Mass percent % |
| Water | TO 100 |
| Cocoamidopropyl betaine | 2.0 |
| Sodium methyl cocoyl taurate | 3.0 |
| Decyl Polyglucoside | 3.0 |
| Guar hydroxypropyltrimonium chloride | 0.6 |
| Hydrolysed corn starch | 2.0 |
| Raspberry juice | 2.0 |
| Pyrrolidone sodium carboxylate | 0.5 |
| Polyglutamic acid sodium | 0.8 |
| Piroctone olamine salt | 0.7 |
| Leaf of Mentha piperita extract | 0.001 |
| EDETATE SODIUM | 0.1 |
| Citric acid | 0.5 |
| Essence | 0.4 |
| Kathon | 0.04 |
| Flos Eriocauli extract | 0.001 |
The not silicate-containing oil and have effects that the preparation method of the shampoo of scalp care the following steps are included:
(1) guar hydroxypropyltrimonium chloride is added to the water, with the rate homogenous disperse of 2500 turns/min
10min；
(2) Cocoamidopropyl betaine, sodium methyl cocoyl taurate and Decyl Polyglucoside is added, stirs evenly, adds
The solid materials such as citric acid and EDETATE SODIUM, insulated and stirred 10min is added to 85 DEG C in heat；
(3) 75 DEG C are cooled to, piroctone olamine salt is added, and stir evenly；
(4) 50 DEG C are cooled to, essence, Kathon, hydrolysed corn starch, raspberry juice, pyrrolidone sodium carboxylate, poly- paddy is added
Propylhomoserin sodium, leaf of Mentha piperita extract and Flos Eriocauli extract, stir evenly；
(5) 40 DEG C are down to hereinafter, stopping stirring, discharging to temperature.
Comparative example
Comparative example is divided into 1 group and 2 groups without silicone oil shampoo, is made of the mass percent component in formula as below table:
Comparative example is prepared without silicone oil shampoo by following steps:
(1) laureth sodium sulfovinate is added to the water, is heated to 80 DEG C；Stirring is added to dissolving completely
Cocounut oil acyl methyl taurine sodium taurocholate, Cocoamidopropyl betaine, sodium lauroyl sarcosine, Sodium Lauroamphoacetate
And alkyl glycosides, it stirs evenly；
(3) 75 DEG C are cooled to, sodium lauroyl sarcosine, myristamide propyl pg dimonium chloride phosphate is added
And Polyquaternium-10, it stirs evenly；
(4) 60 DEG C are cooled to, glycerol is added, and stir evenly；
(5) 50 DEG C are cooled to, Hydramol PGPD esters, triethanolamine, D-pantothenyl aleohol, EUXYI K100 and essence is added,
It stirs evenly, then with lemon acid for adjusting pH value to 6.0~6.5；
(6) 40 DEG C are cooled to hereinafter, stopping stirring, discharging.
The detection of shampoo physical and chemical index
According to national standard " shampoo, hair cream " GB/T 29679-2013, to being free of for the embodiment of the present invention 1 to 3
Common shampoo without silicone oil shampoo and commercially available any silicate-containing oil prepared by silicone oil shampoo, two groups of comparative examples is steeped
Foam, cold-resistant, heat-resisting 3 physical and chemical indexes are analyzed, at the same using ultraviolet specrophotometer measurement transparence value, using viscosimeter
Measure viscosity, physico-chemical analysis the result is as follows:
The results show that the physical and chemical index of above all of sample all meets national standard " shampoo, hair cream " GB/T
29679-2013 has good stability；And in terms of foam height, the not silicate-containing oil shampoo of the embodiment of the present invention 1 to 3 and right
The shampoo for being better than existing commercially available silicate-containing oil without silicone oil shampoo of ratio；And in terms of viscosity, the embodiment of the present invention 1 to 3
Not silicate-containing oil shampoo there is suitable viscosity.The common shampoo of commercially available silicate-containing oil market stochastic buying it is a variety of do it is above-mentioned
Experiment, obtains said effect.
The test of shampoo cardability
Using the net comb instrument Combing Tester SK-3A of topknot dynamic to the not silicate-containing oil shampoo of embodiment 1 to 3,
Two groups of comparative examples carry out cardability test without silicone oil shampoo and commercially available any silicate-containing oil shampoo, are smeared, are rinsed, is wet
Comb, dry comb data.Specific test method are as follows: topknot is cleaned using cleaning agent, measures each topknot baseline after dry, will be sent out according to baseline
Beam grouping, every group of 24 beams.Every group of topknot tests a sample, and topknot is fixed, is drenched, and smears sample, and test combs after smearing
Power；It rinses, carding force is rinsed in test；After rinsing completely, squeezes and remove moisture, test wet carding force；Topknot naturally dry is tested after dry
Dry carding force；The data of collection are handled, the statistical data of each stage carding force is obtained.The results are shown in attached figure 1.
Attached drawing 1 the results show that the not silicate-containing oil shampoo of the embodiment of the present invention 1 to 3 in smearing, flushing, wet comb, dry
It is good to comb each stage combing sex expression, carding force is reduced in smearing, rinse stage and is slightly better than existing commercially available silicone oil shampoo, far
Be much better than comparative example without silicone oil shampoo；In wet comb and dry comb stage, the not silicate-containing oil hair washing of the embodiment of the present invention 1 to 3
It is aqueous can slightly poorer to existing commercially available silicate-containing oil shampoo, but be better than comparative example without silicone oil shampoo；All in all, in cardability
Can aspect, the not silicate-containing oil shampoo of the embodiment of the present invention 1 to 3 can match in excellence or beauty existing commercially available silicate-containing oil shampoo, be much better than pair
Ratio is without silicone oil shampoo.The commercially available common shampoo of silicate-containing oil does above-mentioned experiment market stochastic buying is a variety of, obtains above-mentioned
Effect.
Skin irritation test
It takes the not silicate-containing oil shampoo of the embodiment of the present invention 1 to 3, two groups of comparative examples without silicone oil shampoo, commercially available any contain
Silicone oil shampoo is diluted to 1% aqueous solution, as given the test agent.With 100 ages be 25-50 years old volunteer be test pair
As men and women is fifty-fifty, takes 0.025ml sample drop to be added on filter paper appended by spot tester with syringe, is placed in spot tester.Spot is tried
Device is affixed on subject back, while light pressing room and is uniformly distributed trier one by one to drive away air.Experiment position carries out mark
Note, to observe.It washes off once, is then checked according to the term of CTFA guide every half an hour.6 examinations have been carried out altogether
It tests, after the test the 6th day, in order to observe delayed response, has carried out additional inspection.
The standard of perfection of skin irritation test see the table below:
Skin irritation test result see the table below:
The results show that the not silicate-containing oil shampoo of the embodiment of the present invention 1 to 3 seldom stimulates, comparative example without silicon
It is suspicious reaction that oil wash shampoo, which has a small number of examples,.And comparatively, the irritation of existing commercially available silicon oil-containing shampoo is larger, even
There is weakly positive reaction.Illustrate the surfactant of not silicate-containing oil shampoo of the invention and the ingredient collocation group of scalp care agent
It closes, plays mild non-stimulated effect, be better than existing commercially available silicate-containing oil shampoo, while containing surface-active also superior to comparative example
Agent without silicone oil shampoo.Stochastic buying is a variety of on the market does above-mentioned experiment for the common shampoo of commercially available silicate-containing oil, obtains
Said effect.Therefore, not silicate-containing oil of the invention and have effects that the shampoo of scalp care has mild non-stimulated effect.
The test of scalp care efficacy assessments
It chooses 360 25-50 years old age long hair women to comb one's hair daily before test as volunteer, and records daily hair loss
Quantity, average M；Volunteer is randomly divided into 6 groups, every group of 60 people are had one's hair wash using the not silicate-containing oil of embodiment 1 to 3 respectively
Water, two groups of comparative examples without silicone oil shampoo and commercially available silicate-containing oil shampoo, hair washing is primary daily, is used continuously 10 days, record
Daily hair loss quantity and the N that averages, acquire hair loss percentage N/M；Simultaneously to using rear scalp impression to give a mark, 5 points are
Very comfortable, 1 point is very uncomfortable；Dandruff situation is recorded, 5 points are no dandruff, and 1 point more for dandruff, as a result be see the table below.
The results show that the not silicate-containing oil shampoo of the embodiment of the present invention 1 to 3 has significant effect in terms of reducing hair loss
Fruit, and the effect of not reducing hair loss without silicone oil shampoo and commercially available silicate-containing oil shampoo of comparative example.And after using
Scalp impression and dandruff situation scoring in it can be seen that the embodiment of the present invention 1 to 3 not silicate-containing oil shampoo and comparative example without
Silicone oil shampoo is compared with existing commercially available silicate-containing oil shampoo, and the scalp comfort level after use is high, and dandruff phenomenon is few.These results
Illustrate that the not silicate-containing oil shampoo of the embodiment of the present invention 1 to 3 can improve scalp environment, reduce hair loss, there is scalp shield
The effect of reason and strong root of hair.And existing commercially available silicate-containing oil shampoo and comparative example does not have corresponding scalp without silicone oil shampoo
Nursing and strong root of hair effect illustrate that surfactant and the collocation of care agent ingredient of the invention play and reduce hair loss, nursing head
Skin, strong root of hair effect.The common shampoo of commercially available silicate-containing oil does above-mentioned experiment market stochastic buying is a variety of, obtains above-mentioned
Effect.Therefore, not silicate-containing oil of the invention and have effects that scalp care shampoo have reduce hair loss, nursing scalp, by force
The effect of strong root of hair.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention,
It should be equivalent replacement mode, be included within the scope of the present invention.
Claims (4)
1. a kind of not silicate-containing oil and having effects that the shampoo of scalp care, which is characterized in that it includes following mass percent
Component:
Mild surfactant 5~50%；
Scalp care agent 0.1~10%
The mild surfactant be soapberry fruit bark extract 0.5%, cocounut oil acyl methyl taurine sodium taurocholate 8.0%,
Cocaminopropionic acid sodium 3.5%, Cocoamidopropyl betaine 5.5% and sodium methyl cocoyl taurate 1.0%；Institute
Stating scalp care agent is hydrolysed corn starch 0.3%, pyrrolidone sodium carboxylate 0.5%, piroctone olamine salt 0.3%, paddy
Smart grass extract 0.003% and False flax seed oil 0.001%.
2. a kind of not silicate-containing oil and having effects that the shampoo of scalp care, which is characterized in that it includes following mass percent
Component:
Mild surfactant 5~50%；
Scalp care agent 0.1~10%
The mild surfactant is cocoamido sodium propionate 12.0%, Cocoamidopropyl betaine 7.0% and the last of the ten Heavenly stems
Base glucoside 2.0%；The scalp care agent is ginger-root extract 0.04%, piroctone olamine salt 0.2%, False flax seed
Oil 0.001% and Flos Eriocauli extract 0.003%.
3. a kind of not silicate-containing oil and having effects that the shampoo of scalp care, which is characterized in that it includes following mass percent
Component:
Mild surfactant 5~50%；
Scalp care agent 0.1~10%
The mild surfactant is sodium lauroyl sarcosine 15.0%, Cocoamidopropyl betaine 6.0%, methyl cocoyl
Acyl taurines sodium 1.0%, Sodium Lauroamphoacetate 1.0%, Decyl Polyglucoside 1.0% and Tea Saponin 0.3%；The head
Skin care agent is hydrolysed corn starch 0.4%, piroctone olamine salt 0.2% and False flax seed oil 0.001%.
4. a kind of not silicate-containing oil according to claim 1 to 3 and having effects that the preparation side of the shampoo of scalp care
Method, it is characterised in that: the steps included are as follows for it:
(1) polymeric conditioner is added to the water, 10~15min is stirred with the rate of 2500~3000 turns/min；
(2) mild surfactant and grease is added, is heated to 80~85 DEG C, scalp care agent and other additives are added,
15~20min of insulated and stirred；
(3) after being cooled to 45~50 DEG C, preservative and essence is added, obtains finished product after mixing evenly.
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| CN201510324052.9A CN104921989B (en) | 2015-06-12 | 2015-06-12 | A kind of not silicate-containing oil and the shampoo and preparation method thereof with scalp care |
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| CN201510324052.9A CN104921989B (en) | 2015-06-12 | 2015-06-12 | A kind of not silicate-containing oil and the shampoo and preparation method thereof with scalp care |
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| CN104921989A CN104921989A (en) | 2015-09-23 |
| CN104921989B true CN104921989B (en) | 2019-05-10 |
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