CN104828869A - 一种钠锰氧化物微粉及其制备方法 - Google Patents
一种钠锰氧化物微粉及其制备方法 Download PDFInfo
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- CN104828869A CN104828869A CN201510232678.7A CN201510232678A CN104828869A CN 104828869 A CN104828869 A CN 104828869A CN 201510232678 A CN201510232678 A CN 201510232678A CN 104828869 A CN104828869 A CN 104828869A
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- Prior art keywords
- manganese oxide
- sodium
- oxide micro
- preparation
- micro mist
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- IKULXUCKGDPJMZ-UHFFFAOYSA-N sodium manganese(2+) oxygen(2-) Chemical compound [O-2].[Mn+2].[Na+] IKULXUCKGDPJMZ-UHFFFAOYSA-N 0.000 title claims abstract description 58
- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 239000000843 powder Substances 0.000 title abstract description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 57
- 238000000034 method Methods 0.000 claims abstract description 25
- 239000011734 sodium Substances 0.000 claims abstract description 25
- 238000006243 chemical reaction Methods 0.000 claims abstract description 22
- 239000000463 material Substances 0.000 claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000004519 manufacturing process Methods 0.000 claims abstract description 16
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 15
- 239000011572 manganese Substances 0.000 claims abstract description 13
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 12
- 238000001035 drying Methods 0.000 claims abstract description 7
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000005406 washing Methods 0.000 claims abstract description 5
- 229910052748 manganese Inorganic materials 0.000 claims abstract description 4
- 239000003595 mist Substances 0.000 claims description 41
- 239000000243 solution Substances 0.000 claims description 31
- 238000007664 blowing Methods 0.000 claims description 6
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 claims description 6
- 238000007254 oxidation reaction Methods 0.000 claims description 5
- 239000012266 salt solution Substances 0.000 claims description 4
- 238000007599 discharging Methods 0.000 claims description 3
- 229910002651 NO3 Inorganic materials 0.000 claims description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 2
- 238000013019 agitation Methods 0.000 claims description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims description 2
- 239000010931 gold Substances 0.000 claims description 2
- 229910052737 gold Inorganic materials 0.000 claims description 2
- 229940071125 manganese acetate Drugs 0.000 claims description 2
- UOGMEBQRZBEZQT-UHFFFAOYSA-L manganese(2+);diacetate Chemical compound [Mn+2].CC([O-])=O.CC([O-])=O UOGMEBQRZBEZQT-UHFFFAOYSA-L 0.000 claims description 2
- CNFDGXZLMLFIJV-UHFFFAOYSA-L manganese(II) chloride tetrahydrate Chemical compound O.O.O.O.[Cl-].[Cl-].[Mn+2] CNFDGXZLMLFIJV-UHFFFAOYSA-L 0.000 claims description 2
- 238000007747 plating Methods 0.000 claims description 2
- 238000004886 process control Methods 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 abstract description 7
- 238000003786 synthesis reaction Methods 0.000 abstract description 5
- 239000002002 slurry Substances 0.000 abstract description 4
- 230000035484 reaction time Effects 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 description 7
- 239000013078 crystal Substances 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000012065 filter cake Substances 0.000 description 4
- 150000002500 ions Chemical class 0.000 description 4
- 229940099596 manganese sulfate Drugs 0.000 description 4
- 239000011702 manganese sulphate Substances 0.000 description 4
- 235000007079 manganese sulphate Nutrition 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 230000001105 regulatory effect Effects 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000007791 liquid phase Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000005245 sintering Methods 0.000 description 3
- 239000002689 soil Substances 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 241000208340 Araliaceae Species 0.000 description 2
- 229910021380 Manganese Chloride Inorganic materials 0.000 description 2
- GLFNIEUTAYBVOC-UHFFFAOYSA-L Manganese chloride Chemical compound Cl[Mn]Cl GLFNIEUTAYBVOC-UHFFFAOYSA-L 0.000 description 2
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 2
- 235000003140 Panax quinquefolius Nutrition 0.000 description 2
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 description 2
- 238000002441 X-ray diffraction Methods 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- -1 formaldehyde, phenols Chemical class 0.000 description 2
- 235000008434 ginseng Nutrition 0.000 description 2
- 238000001027 hydrothermal synthesis Methods 0.000 description 2
- 238000005342 ion exchange Methods 0.000 description 2
- 239000011565 manganese chloride Substances 0.000 description 2
- 235000002867 manganese chloride Nutrition 0.000 description 2
- 229940099607 manganese chloride Drugs 0.000 description 2
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 2
- 229910001415 sodium ion Inorganic materials 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000007711 solidification Methods 0.000 description 2
- 238000000967 suction filtration Methods 0.000 description 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical group [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000009830 intercalation Methods 0.000 description 1
- 230000002687 intercalation Effects 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 229910001416 lithium ion Inorganic materials 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 150000002696 manganese Chemical class 0.000 description 1
- IPJKJLXEVHOKSE-UHFFFAOYSA-L manganese dihydroxide Chemical compound [OH-].[OH-].[Mn+2] IPJKJLXEVHOKSE-UHFFFAOYSA-L 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000002957 persistent organic pollutant Substances 0.000 description 1
- 239000004587 polysulfide sealant Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000012716 precipitator Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 150000003388 sodium compounds Chemical class 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 238000003746 solid phase reaction Methods 0.000 description 1
- 238000010532 solid phase synthesis reaction Methods 0.000 description 1
- 238000003836 solid-state method Methods 0.000 description 1
- 238000010671 solid-state reaction Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000002594 sorbent Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
Description
Claims (8)
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CN201510232678.7A CN104828869B (zh) | 2015-05-08 | 2015-05-08 | 一种钠锰氧化物微粉及其制备方法 |
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CN104828869A true CN104828869A (zh) | 2015-08-12 |
CN104828869B CN104828869B (zh) | 2016-10-05 |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105514375A (zh) * | 2015-12-11 | 2016-04-20 | 武汉理工大学 | 一种碳包覆Na0.55Mn2O4·1.5H2O纳米复合材料及其制备方法 |
CN106298249A (zh) * | 2016-09-18 | 2017-01-04 | 中南大学 | 一种K1.33Mn8O16的制备方法及应用 |
CN107601569A (zh) * | 2017-09-27 | 2018-01-19 | 江苏科技大学 | 一种带状钠锰氧化物及其制备方法与应用 |
CN107706382A (zh) * | 2017-09-27 | 2018-02-16 | 江苏科技大学 | 一种片状钠锰氧化物及其制备方法与应用 |
CN108493501A (zh) * | 2018-03-30 | 2018-09-04 | 华南师范大学 | 氟化钠双离子电池的制备方法及其在电化学除氟中的应用 |
WO2020227927A1 (zh) * | 2019-05-14 | 2020-11-19 | 浙江裕源储能科技有限公司 | 水系电池正极活性材料及其制备方法以及水溶液锌离子电池 |
CN112661191A (zh) * | 2021-01-22 | 2021-04-16 | 广西下田锰矿有限责任公司 | 电解二氧化锰用硫酸锰溶液深度除钼的方法 |
CN113387392A (zh) * | 2021-06-09 | 2021-09-14 | 南昌大学 | 一种钠锰氧化物制备方法及在超级电容中的应用 |
Citations (5)
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---|---|---|---|---|
US5939043A (en) * | 1998-06-26 | 1999-08-17 | Ga-Tek Inc. | Process for preparing Lix Mn2 O4 intercalation compounds |
CN101209414A (zh) * | 2006-12-31 | 2008-07-02 | 中国科学院理化技术研究所 | 层状介孔水钠锰矿型MnO2蜂窝状纳米球的用途 |
CN102120619A (zh) * | 2011-01-11 | 2011-07-13 | 河北师范大学 | 一种脑珊瑚状水钠锰矿型二氧化锰的制备方法 |
CN102491422A (zh) * | 2011-12-26 | 2012-06-13 | 湖南汇通科技有限责任公司 | 一种球形四氧化三锰及其制备方法 |
CN103896339A (zh) * | 2012-12-27 | 2014-07-02 | 北京汉能创昱科技有限公司 | 一种钠锰氧化物的制备方法 |
-
2015
- 2015-05-08 CN CN201510232678.7A patent/CN104828869B/zh active Active
Patent Citations (5)
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US5939043A (en) * | 1998-06-26 | 1999-08-17 | Ga-Tek Inc. | Process for preparing Lix Mn2 O4 intercalation compounds |
CN101209414A (zh) * | 2006-12-31 | 2008-07-02 | 中国科学院理化技术研究所 | 层状介孔水钠锰矿型MnO2蜂窝状纳米球的用途 |
CN102120619A (zh) * | 2011-01-11 | 2011-07-13 | 河北师范大学 | 一种脑珊瑚状水钠锰矿型二氧化锰的制备方法 |
CN102491422A (zh) * | 2011-12-26 | 2012-06-13 | 湖南汇通科技有限责任公司 | 一种球形四氧化三锰及其制备方法 |
CN103896339A (zh) * | 2012-12-27 | 2014-07-02 | 北京汉能创昱科技有限公司 | 一种钠锰氧化物的制备方法 |
Non-Patent Citations (1)
Title |
---|
冯雄汉等: ""碱性介质中合成水钠锰矿的几个影响因素"", 《地球化学》, vol. 31, no. 5, 30 September 2002 (2002-09-30) * |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105514375A (zh) * | 2015-12-11 | 2016-04-20 | 武汉理工大学 | 一种碳包覆Na0.55Mn2O4·1.5H2O纳米复合材料及其制备方法 |
CN106298249A (zh) * | 2016-09-18 | 2017-01-04 | 中南大学 | 一种K1.33Mn8O16的制备方法及应用 |
CN107601569A (zh) * | 2017-09-27 | 2018-01-19 | 江苏科技大学 | 一种带状钠锰氧化物及其制备方法与应用 |
CN107706382A (zh) * | 2017-09-27 | 2018-02-16 | 江苏科技大学 | 一种片状钠锰氧化物及其制备方法与应用 |
CN107706382B (zh) * | 2017-09-27 | 2019-12-10 | 江苏科技大学 | 一种片状钠锰氧化物及其制备方法与应用 |
CN108493501A (zh) * | 2018-03-30 | 2018-09-04 | 华南师范大学 | 氟化钠双离子电池的制备方法及其在电化学除氟中的应用 |
WO2020227927A1 (zh) * | 2019-05-14 | 2020-11-19 | 浙江裕源储能科技有限公司 | 水系电池正极活性材料及其制备方法以及水溶液锌离子电池 |
CN112661191A (zh) * | 2021-01-22 | 2021-04-16 | 广西下田锰矿有限责任公司 | 电解二氧化锰用硫酸锰溶液深度除钼的方法 |
CN113387392A (zh) * | 2021-06-09 | 2021-09-14 | 南昌大学 | 一种钠锰氧化物制备方法及在超级电容中的应用 |
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