CN104807913B - 一种附子复方中单酯型生物碱的含量测定方法 - Google Patents
一种附子复方中单酯型生物碱的含量测定方法 Download PDFInfo
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项目 | 过柱前面积 | 过柱后面积 | 比值 |
苯甲酰新乌头原碱 | 304247.7 | 297951.1 | 0.979 |
苯甲酰乌头原碱 | 50207.9 | 49585 | 0.988 |
苯甲酰次乌头原碱 | 61488.5 | 60221.1 | 0.979 |
苯甲酰新乌头原碱(μg/ml) | 0.9863 | 1.9726 | 5.9178 | 9.8630 | 19.7259 | 49.3148 |
峰面积 | 26743 | 53424 | 169096 | 282405 | 564705 | 1409527 |
响应因子 | 27115 | 27083 | 28574 | 28633 | 28628 | 28582 |
苯甲酰乌头原碱(μg/ml) | 0.1888 | 0.3777 | 1.1330 | 1.8883 | 3.7766 | 9.4416 |
峰面积 | 4214 | 8880 | 27309 | 45998 | 92736 | 232163 |
响应因子 | 22316 | 23513 | 24104 | 24359 | 24555 | 24589 |
苯甲酰次乌头原碱(μg/ml) | 0.1969 | 0.3939 | 1.1816 | 1.9694 | 3.9387 | 9.8468 |
峰面积 | 5878 | 10748 | 32773 | 53533 | 107572 | 261057 |
响应因子 | 29847 | 27288 | 27736 | 27183 | 27312 | 26512 |
项目 | 1 | 2 | 3 | 4 | 5 | 6 | RSD |
苯甲酰新乌头原碱(μg/g) | 347.33 | 355.60 | 354.54 | 361.14 | 350.89 | 351.57 | 1.35% |
苯甲酰乌头原碱(μg/g) | 39.78 | 39.75 | 40.27 | 39.73 | 40.03 | 40.28 | 0.65% |
苯甲酰次乌头原碱(μg/g) | 53.14 | 53.80 | 54.06 | 53.49 | 53.98 | 54.95 | 1.15% |
总含量(μg/g) | 440.26 | 449.15 | 448.87 | 454.36 | 444.90 | 446.81 | 1.06% |
时间 | 0h | 8h | 20h | RSD |
单酯型生物碱峰面积 | 547081 | 546677 | 535693 | 1.19% |
品牌 | 型号 | 填充剂 | 规格 | 含量(μg/g) |
Welch | Ultimate Phenyl-Ether | 极性乙醚连接苯基键合硅胶 | 250×4.6mm,5μm | 449.43 |
Agela | Venusil XBP Polar-Phenyl | 极性乙醚连接苯基键合硅胶 | 250×4.6mm,5μm | 449.11 |
Agela | Venusil XBP Polar-Phenyl | 极性乙醚连接苯基键合硅胶 | 250×4.6mm,5μm | 453.44 |
项目 | 过柱前面积 | 过柱后面积 | 比值 |
苯甲酰新乌头原碱 | 306918 | 301539 | 0.982 |
苯甲酰乌头原碱 | 524040 | 508326 | 0.970 |
苯甲酰次乌头原碱 | 607307 | 601008 | 0.989 |
项目 | 过柱前面积 | 过柱后面积 | 比值 |
苯甲酰新乌头原碱 | 31064 | 30194 | 0.972 |
苯甲酰乌头原碱 | 50357 | 49551 | 0.984 |
苯甲酰次乌头原碱 | 62641 | 61889 | 0.988 |
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CN110794079A (zh) * | 2019-11-20 | 2020-02-14 | 刘圣梅 | 一种麻附辛制剂的鉴别方法 |
CN112763606B (zh) * | 2020-12-24 | 2022-07-08 | 成都中医药大学 | 一种附子理中制剂差异化合物的质量分析方法 |
CN115541739A (zh) * | 2021-09-03 | 2022-12-30 | 成都中医药大学 | 一种附子强心作用的快速评价方法 |
CN114813985A (zh) * | 2022-01-19 | 2022-07-29 | 长春英平药业有限公司 | 一种寒热痹胶囊hplc指纹图谱的构建方法 |
CN114910576B (zh) * | 2022-04-07 | 2023-07-25 | 国药集团广东环球制药有限公司 | 一种桂枝芍药知母汤中附子单酯型生物碱成分的检测方法 |
CN115372497B (zh) * | 2022-07-06 | 2024-01-26 | 河北省药品医疗器械检验研究院(河北省化妆品检验研究中心) | 一种小活络丸中6种生物碱成分的含量测定方法 |
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