CN104721095A - Caryopteris clandonensis mosquito repelling liquid and preparation method thereof - Google Patents
Caryopteris clandonensis mosquito repelling liquid and preparation method thereof Download PDFInfo
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Abstract
The invention relates to caryopteris clandonensis mosquito repelling liquid and a preparation method thereof and belongs to the technical field of natural plant extract mosquito repelling. According to the technical scheme, the method includes: natural rose flower extract, chamomile extract or aloe extract is added into the extract of natural caryopteris clandonensis flowers and leaves to prepare the caryopteris clandonensis mosquito repelling liquid. The caryopteris clandonensis mosquito repelling liquid has the advantages that the caryopteris clandonensis mosquito repelling liquid is prepared by using plant extract as raw material and through steam distillation; the flowers and leaves of caryopteris clandonensis, the rose flower extract, the chamomile extract and the aloe extract which serve as the main ingredient are pure natural plant ingredients, so that the prepared mosquito repelling liquid is good in mosquito repelling effect, safe and environmental friendly to use, and especially good in use safety for children and elder people, and can relieve itching, diminish inflammation and inhibit bacteria; the caryopteris clandonensis mosquito repelling liquid uses natural plants, does not contain chemical mosquito repelling ingredients, and is free of skin stimulation and widely applicable.
Description
Technical field
The present invention relates to a kind of Caryopteris clandonensis mosquito-driving liquid and preparation method thereof, belong to natural botanical extraction liquid mosquito dispersing technical field.
Background technology
Mosquito can suck human blood, spread disease.According to the study, insect-borne diseases reaches kind more than 80, about has 700,000,000 people to be infected various disease by mosquito every year, and serious harm humans is healthy.For this reason, people have used a variety of method in the hope of reaching the object of mosquito control.At present, main use chemical insecticide and mosquito-repellent on market, its main component is synthetic chemicals diethyltoluamide (DEET), belong to pesticide chemical reagent, chemosynthesis repellant has problems, has certain toxic and side effects to human body, also causes certain pollution to environment; How using natural repellant to carry out anophelifuge, is this area technical problem urgently to be resolved hurrily.
Summary of the invention
The object of the invention is to provide a kind of Caryopteris clandonensis mosquito-driving liquid and preparation method thereof, with the mosquito-driving liquid that natural plants Caryopteris clandonensis extracting solution is made, can not only mosquito dispersing simultaneously can also itch stopping and diminish inflammation antibacterial, harmless to human body, can not environmental pollution be caused, the inflammation brought to skin after solving mosquito bite cannot give effective the suppression and the problem for the treatment of.
Technical scheme of the present invention is:
A kind of Caryopteris clandonensis mosquito-driving liquid, is utilize natural plants Caryopteris clandonensis flower and leaf to be raw-material extracting solution, adds natural rose liquid distilled from honeysuckle flowers or lotus leaves, be prepared from; Mass percent is: Caryopteris clandonensis extracting solution 95%, natural rose liquid distilled from honeysuckle flowers or lotus leaves 5%.
A kind of Caryopteris clandonensis mosquito-driving liquid, is utilize natural plants Caryopteris clandonensis flower and leaf to be raw-material extracting solution, adds Flos Matricariae chamomillae extracting solution, be prepared from; Mass percent is: Caryopteris clandonensis extracting solution 95%, Flos Matricariae chamomillae extracting solution 5%.
A kind of Caryopteris clandonensis mosquito-driving liquid, is utilize natural plants Caryopteris clandonensis flower and leaf to be raw-material extracting solution, adds Aloe extraction solution, be prepared from; Mass percent is: Caryopteris clandonensis extracting solution 95%, Aloe extraction solution 5%.
The present invention is natural flower aroma mosquito-driving liquid, not only harmless to human body, can not environmental pollution be caused, and there is good mosquito-repelling effect, and can itch stopping and diminish inflammation antibacterial, use safety, environmental protection.
A kind of Caryopteris clandonensis mosquito-driving liquid preparation method, comprises following steps:
raw material choose; Be raw material by the flower of natural plants Caryopteris clandonensis and the blade of Caryopteris clandonensis, mass percent is: Caryopteris clandonensis spend 80%, the blade 20% of Caryopteris clandonensis;
2. the preparation of Caryopteris clandonensis extracting solution;
(1) be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, the mass ratio of water and raw material is 1:1 ratio, namely adds 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate Caryopteris clandonensis extracting solution; Weight to Caryopteris clandonensis extracting solution is 100 jin and stops;
3. natural rose liquid distilled from honeysuckle flowers or lotus leaves is prepared:
(1) with natural rose flower for raw material, be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, water and raw-material mass ratio are 1:1 ratio, namely add 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate natural rose liquid distilled from honeysuckle flowers or lotus leaves; Weight to natural rose liquid distilled from honeysuckle flowers or lotus leaves is 100 jin and stops;
4. Caryopteris clandonensis mosquito-driving liquid is prepared:
Mixed homogeneously with natural rose liquid distilled from honeysuckle flowers or lotus leaves by the Caryopteris clandonensis extracting solution prepared and be Caryopteris clandonensis mosquito-driving liquid, mass percent is: Caryopteris clandonensis extracting solution 95%, natural rose liquid distilled from honeysuckle flowers or lotus leaves 5%.
A kind of Caryopteris clandonensis mosquito-driving liquid preparation method, comprises following steps:
raw material choose; Be raw material by the flower of natural plants Caryopteris clandonensis and the blade of Caryopteris clandonensis, mass percent is: Caryopteris clandonensis spend 80%, the blade 20% of Caryopteris clandonensis;
2. the preparation of Caryopteris clandonensis extracting solution;
(1) be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, the mass ratio of water and raw material is 1:1 ratio, namely adds 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate Caryopteris clandonensis extracting solution; Weight to Caryopteris clandonensis extracting solution is 100 jin and stops;
3. Flos Matricariae chamomillae extracting solution is prepared:
(1) with natural anthemidis flos for raw material, be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, water and raw-material mass ratio are 1:1 ratio, namely add 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate Flos Matricariae chamomillae extracting solution; Weight to Flos Matricariae chamomillae extracting solution is 100 jin and stops;
4. Caryopteris clandonensis mosquito-driving liquid is prepared:
Mixed homogeneously with Flos Matricariae chamomillae extracting solution by the Caryopteris clandonensis extracting solution prepared and be Caryopteris clandonensis mosquito-driving liquid, mass percent is: Caryopteris clandonensis extracting solution 95%, Flos Matricariae chamomillae extracting solution 5%.
A kind of Caryopteris clandonensis mosquito-driving liquid preparation method, comprises following steps:
raw material choose; Be raw material by the flower of natural plants Caryopteris clandonensis and the blade of Caryopteris clandonensis, mass percent is: Caryopteris clandonensis spend 80%, the blade 20% of Caryopteris clandonensis;
2. the preparation of Caryopteris clandonensis extracting solution;
(1) be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, the mass ratio of water and raw material is 1:1 ratio, namely adds 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate Caryopteris clandonensis extracting solution; Weight to Caryopteris clandonensis extracting solution is 100 jin and stops;
3. Aloe extraction solution is prepared:
The aloe leaf of fresh harvesting is cleaned peeling, pulping is ground in mortar, pour test tube into, extract under room temperature 20 DEG C of conditions with 50% ethanol, Aloe slurry and ethanol than 1:15, quiescent time 60min, be centrifugal 10min under the condition of 6000r/min at rotating speed, filter paper filtering, filtrate is centrifugal more under the same conditions to be refiltered, and obtains extracting solution and is Aloe extraction solution;
4. Caryopteris clandonensis mosquito-driving liquid is prepared:
Mixed homogeneously with Aloe extraction solution by the Caryopteris clandonensis extracting solution prepared and be Caryopteris clandonensis mosquito-driving liquid, mass percent is: Caryopteris clandonensis extracting solution 95%, Aloe extraction solution 5%.
After preparing Caryopteris clandonensis extracting solution, alembic carries out drainage, slag discharge, reclaims residual water in the pot in alembic, use as when distilling next time again with container; Pour out residue; Rinse the pot in alembic, distill next time.
Caryopteris clandonensis (
caryopteris × dandonensis1worcester Gold) for Verenaceae Herba caryopteridis nepetaefoliae belongs to, machaka, plants then and blooms then.Caryopteris clandonensis in growth distributes a kind of abnormal smells from the patient of delicate fragrance, this abnormal smells from the patient can play the effect of anophelifuge, 12 kinds of compounds are identified from the plant of Caryopteris clandonensis, be mainly the compound of volatile oil, terpenoid, flavonoid and other types, there is the effects such as anti-inflammation detumescence, antipruritic, antioxidation, antibacterial, promoting blood circulation and stopping pain.
Beneficial effect of the present invention: be that raw water steam distillation method is made with plant extract, because of its main component be the flower of Caryopteris clandonensis, blade and rose flower water, Aloe extraction solution, Flos Matricariae chamomillae extracting solution be all pure natural plant ingredients, the mosquito-driving liquid made has good mosquito-repelling effect, and energy itch stopping and diminish inflammation is antibacterial, use safety, environmental protection are especially good to child, old people's safety in utilization.
Advantage of the present invention:
1, Caryopteris clandonensis mosquito-driving liquid is the Caryopteris clandonensis dew with mosquito repellent function extracted from natural plants Caryopteris clandonensis, and therefore this kind of mosquito-driving liquid has the feature of safety, environmental protection.Rose flower water makes from the distillation of natural plants Flos Rosae Rugosae, and have pure and fresh pleasant fragrance, therefore this kind of mosquito-driving liquid is more easily esthetically acceptable to the consumers.Flos Matricariae chamomillae extracting solution has antiinflammatory, the effect such as antipruritic, antibacterial.Aloe extraction solution is nutritious moisturizing not only, anti-sunlight function, can also treat scytitis;
2, Caryopteris clandonensis mosquito-driving liquid adopts natural plants, not containing chemical mosquito component, to skin without any stimulation, has wide range of applications;
3, Caryopteris clandonensis also has promoting blood circulation and stopping pain, antibacterial, the good action such as antioxidation, itch stopping and diminish inflammation.
Detailed description of the invention
The present invention will be further described by the following examples
Embodiment one:
Caryopteris clandonensis extracting solution: the Caryopteris clandonensis flower of (1) fresh harvesting and blade constitutive material, in raw material, flower mass percent accounts for 80%, and leaf quality percentage ratio accounts for 20%, is that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, the raw-material weight ratio in water and step (1) is 1:1 ratio, namely adds 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and material and aqueous mixtures are heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to material and aqueous mixtures; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, make entering containing quintessence oil steam in step (4) that the condenser organizing condensing tubes is housed more, oil mixing with water steam is condensed into liquid; (6) liquid be condensed enters in the condenser that many group cooling water pipes are housed, and oil mixing with water liquid cools; (7) through process for cooling, utilize temp-difference condensing to become liquid condition, thus isolate hydrosol water, be Caryopteris clandonensis extracting solution, the weight to Caryopteris clandonensis extracting solution is 100 jin and stops; (8) drainage, slag discharge: by the residual water in pot in container recycling can, uses as during lower tank distillation again; Pour out residue; Rinse the pot in alembic, distill next time.
Get the extracting solution percentage by weight 95% prepared, rose flower water percentage by weight 5%, the two mix homogeneously both obtained Caryopteris clandonensis mosquito-driving liquid, lucifuge preservation.
Rose flower water is natural plants fresh rose flower water vapour material, and be a kind of hydrosol, its fragrance is pleasant, and being used for increases fragrance, plays the effect of fresh air.
The extracting method of rose flower water: weight for raw material, is that the raw material of 100 jin drops in the pot in alembic with the Flos Rosae Rugosae of fresh harvesting by (1); Step (2)-(7) are with the step method of Caryopteris clandonensis extracting solution (2)-(7).
Embodiment two:
Get the Caryopteris clandonensis extracting solution percentage by weight 95% prepared, Flos Matricariae chamomillae extracting solution percentage by weight 5%, the two mix homogeneously both obtained Caryopteris clandonensis mosquito-driving liquid.
Flos Matricariae chamomillae extracting solution has antiinflammatory, the effect such as antipruritic, antibacterial.
raw material choose; Be raw material by the flower of natural plants Caryopteris clandonensis and the blade of Caryopteris clandonensis, mass percent is: Caryopteris clandonensis spend 80%, the blade 20% of Caryopteris clandonensis;
2. the preparation of Caryopteris clandonensis extracting solution;
(1) be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, the mass ratio of water and raw material is 1:1 ratio, namely adds 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate Caryopteris clandonensis extracting solution; Weight to Caryopteris clandonensis extracting solution is 100 jin and stops;
3. Flos Matricariae chamomillae extracting solution is prepared:
(1) with natural anthemidis flos for raw material, be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, water and raw-material mass ratio are 1:1 ratio, namely add 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate Flos Matricariae chamomillae extracting solution; Weight to Flos Matricariae chamomillae extracting solution is 100 jin and stops;
4. Caryopteris clandonensis mosquito-driving liquid is prepared:
Mixed homogeneously with Flos Matricariae chamomillae extracting solution by the Caryopteris clandonensis extracting solution prepared and be Caryopteris clandonensis mosquito-driving liquid, mass percent is: Caryopteris clandonensis extracting solution 95%, Flos Matricariae chamomillae extracting solution 5%.
Embodiment three:
Get the Caryopteris clandonensis extracting solution percentage by weight 95% prepared, Aloe extraction solution percentage by weight 5%, the two mix homogeneously both obtained Caryopteris clandonensis mosquito-driving liquid.
Aloe extraction solution is nutritious moisturizing not only, anti-sunlight function, can also treat scytitis.
raw material choose; Be raw material by the flower of natural plants Caryopteris clandonensis and the blade of Caryopteris clandonensis, mass percent is: Caryopteris clandonensis spend 80%, the blade 20% of Caryopteris clandonensis;
2. the preparation of Caryopteris clandonensis extracting solution;
(1) be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, the mass ratio of water and raw material is 1:1 ratio, namely adds 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate Caryopteris clandonensis extracting solution; Weight to Caryopteris clandonensis extracting solution is 100 jin and stops;
3. Aloe extraction solution is prepared:
The aloe leaf of fresh harvesting is cleaned peeling, pulping is ground in mortar, pour test tube into, extract under room temperature 20 DEG C of conditions with 50% ethanol, Aloe slurry and ethanol than 1:15, quiescent time 60min, be centrifugal 10min under the condition of 6000r/min at rotating speed, filter paper filtering, filtrate is centrifugal more under the same conditions to be refiltered, and obtains extracting solution and is Aloe extraction solution;
4. Caryopteris clandonensis mosquito-driving liquid is prepared:
Mixed homogeneously with Aloe extraction solution by the Caryopteris clandonensis extracting solution prepared and be Caryopteris clandonensis mosquito-driving liquid, mass percent is: Caryopteris clandonensis extracting solution 95%, Aloe extraction solution 5%.
Using method of the present invention and effect:
Mosquito-driving liquid of the present invention is evenly applied to the outside baring skins such as arm, all can effective expelling mosquito biting human body at indoor environment and outdoor environment.In indoor storage the present invention, also can expelling mosquito, reach good mosquito-repelling effect.
In addition, Caryopteris clandonensis mosquito-driving liquid main component of the present invention is pure natural plant ingredients, therefore has the feature of no side effects, has no stimulation to human body, safety and environmental protection, and have good mosquito-repelling effect, is particularly suitable for child and old people's use.
The mosquito-driving liquid of embodiment one, two, three is done anophelifuge experiment, process is as follows:
Laboratory test: in 7-8 month, by embodiment one mosquito-driving liquid, be sprayed at the bottom of four corners of certain multidimensional aquaculture company limited planting base crew quarter, bed and doorway with cosmetic watering can respectively, dormitory size is about 10m
2two single beds in dormitory, often open a people on bed, totally 6 dormitories, tester men and women half and half, sprinkling every night 7, each sprinkling about 2ml, 9 .-10 rests in workman's evening, arm, lower limb and face all expose in atmosphere in bed, get up in the morning about 6, not by mosquito bite phenomenon in two months of test.
The mosquito-driving liquid of embodiment two, three, carry out same experiment, effect is identical.
Outdoor experiment: in the 7-8 month, by the mosquito-driving liquid of embodiment one, two, three, according to people like abnormal smells from the patient in the afternoon 6 be sprayed at respectively will arrive outdoor enjoy the cool child, adult and old man's body exposure position, comprise arm, lower limb and neck position, testing location is in the village in certain district, test crowd enjoys the cool outdoor, evening, 8-9 point was gone home, test in 2 months, test more than 55 years old crowd 100 person-times altogether, 15 years old to 55 years old crowd 160 person-times, less than 15 years old child 200 person-times, what result display was crossed by mosquito bite only has 5 person-times.
Like abnormal smells from the patient according to people, select the mosquito-driving liquid of embodiment one, two, three respectively, effect is identical.
Claims (6)
1. a Caryopteris clandonensis mosquito-driving liquid, is characterized in that: utilize natural plants Caryopteris clandonensis flower and leaf to be raw-material extracting solution, add natural rose liquid distilled from honeysuckle flowers or lotus leaves, be prepared from; Mass percent is: Caryopteris clandonensis extracting solution 95%, natural rose liquid distilled from honeysuckle flowers or lotus leaves 5%.
2. a Caryopteris clandonensis mosquito-driving liquid, is characterized in that: utilize natural plants Caryopteris clandonensis flower and leaf to be raw-material extracting solution, add Flos Matricariae chamomillae extracting solution, be prepared from; Mass percent is: Caryopteris clandonensis extracting solution 95%, Flos Matricariae chamomillae extracting solution 5%.
3. a Caryopteris clandonensis mosquito-driving liquid, is characterized in that: utilize natural plants Caryopteris clandonensis flower and leaf to be raw-material extracting solution, add Aloe extraction solution, be prepared from; Mass percent is: Caryopteris clandonensis extracting solution 95%, Aloe extraction solution 5%.
4. a Caryopteris clandonensis mosquito-driving liquid preparation method, is characterized in that: comprise following steps:
raw material choose; Be raw material by the flower of natural plants Caryopteris clandonensis and the blade of Caryopteris clandonensis, mass percent is: Caryopteris clandonensis spend 80%, the blade 20% of Caryopteris clandonensis;
2. the preparation of Caryopteris clandonensis extracting solution;
(1) be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, the mass ratio of water and raw material is 1:1 ratio, namely adds 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate Caryopteris clandonensis extracting solution; Weight to Caryopteris clandonensis extracting solution is 100 jin and stops;
3. natural rose liquid distilled from honeysuckle flowers or lotus leaves is prepared:
(1) with natural rose flower for raw material, be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, water and raw-material mass ratio are 1:1 ratio, namely add 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate natural rose liquid distilled from honeysuckle flowers or lotus leaves; Weight to natural rose liquid distilled from honeysuckle flowers or lotus leaves is 100 jin and stops;
4. Caryopteris clandonensis mosquito-driving liquid is prepared:
Mixed homogeneously with natural rose liquid distilled from honeysuckle flowers or lotus leaves by the Caryopteris clandonensis extracting solution prepared and be Caryopteris clandonensis mosquito-driving liquid, mass percent is: Caryopteris clandonensis extracting solution 95%, natural rose liquid distilled from honeysuckle flowers or lotus leaves 5%.
5. a Caryopteris clandonensis mosquito-driving liquid preparation method, is characterized in that: comprise following steps:
raw material choose; Be raw material by the flower of natural plants Caryopteris clandonensis and the blade of Caryopteris clandonensis, mass percent is: Caryopteris clandonensis spend 80%, the blade 20% of Caryopteris clandonensis;
2. the preparation of Caryopteris clandonensis extracting solution;
(1) be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, the mass ratio of water and raw material is 1:1 ratio, namely adds 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate Caryopteris clandonensis extracting solution; Weight to Caryopteris clandonensis extracting solution is 100 jin and stops;
3. Flos Matricariae chamomillae extracting solution is prepared:
(1) with natural anthemidis flos for raw material, be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, water and raw-material mass ratio are 1:1 ratio, namely add 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate Flos Matricariae chamomillae extracting solution; Weight to Flos Matricariae chamomillae extracting solution is 100 jin and stops;
4. Caryopteris clandonensis mosquito-driving liquid is prepared:
Mixed homogeneously with Flos Matricariae chamomillae extracting solution by the Caryopteris clandonensis extracting solution prepared and be Caryopteris clandonensis mosquito-driving liquid, mass percent is: Caryopteris clandonensis extracting solution 95%, Flos Matricariae chamomillae extracting solution 5%.
6. a Caryopteris clandonensis mosquito-driving liquid preparation method, is characterized in that:
raw material choose; Be raw material by the flower of natural plants Caryopteris clandonensis and the blade of Caryopteris clandonensis, mass percent is: Caryopteris clandonensis spend 80%, the blade 20% of Caryopteris clandonensis;
2. the preparation of Caryopteris clandonensis extracting solution;
(1) be that the raw material of 100 jin drops in the pot in alembic by weight; (2) in the pot in alembic, clear water is added; By weight, the mass ratio of water and raw material is 1:1 ratio, namely adds 100 jin, clear water; (3) heat alembic, pressure is transferred between 0.3-0.5 MPa, and the mixture of raw material and water is heated to 100 DEG C; (4) be depressurized to 0.1 MPa, at this pressure distill repeatedly 4h carried out to the mixture of raw material and water; Utilize steam to carry out by the stronger plant fragrance quintessence oil of volatilization, make it to form the vapor phase containing quintessence oil; (5) open condenser, the steam containing quintessence oil is entered the condenser organizing condensing tube is housed more, the steam containing quintessence oil is condensed into liquid; (6) liquid be condensed enters in the cooler that many group cooling water pipes are housed, and cools; (7) after supercooling, utilize difference variation to be condensed into liquid condition, isolate Caryopteris clandonensis extracting solution; Weight to Caryopteris clandonensis extracting solution is 100 jin and stops;
3. Aloe extraction solution is prepared:
The aloe leaf of fresh harvesting is cleaned peeling, pulping is ground in mortar, pour test tube into, extract under room temperature 20 DEG C of conditions with 50% ethanol, Aloe slurry and ethanol than 1:15, quiescent time 60min, be centrifugal 10min under the condition of 6000r/min at rotating speed, filter paper filtering, filtrate is centrifugal more under the same conditions to be refiltered, and obtains extracting solution and is Aloe extraction solution;
4. Caryopteris clandonensis mosquito-driving liquid is prepared:
Mixed homogeneously with Aloe extraction solution by the Caryopteris clandonensis extracting solution prepared and be Caryopteris clandonensis mosquito-driving liquid, mass percent is: Caryopteris clandonensis extracting solution 95%, Aloe extraction solution 5%.
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Citations (4)
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| CN101422419A (en) * | 2008-12-19 | 2009-05-06 | 美晨集团股份有限公司 | Toilet water and manufacture method thereof |
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| CN101906353A (en) * | 2010-08-03 | 2010-12-08 | 河北科技大学 | Extraction method and application of chestnut flower essential oil |
| CN102429840A (en) * | 2011-09-22 | 2012-05-02 | 黄馨莹 | Mosquito repellent liquid and preparation method thereof |
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| CN101422419A (en) * | 2008-12-19 | 2009-05-06 | 美晨集团股份有限公司 | Toilet water and manufacture method thereof |
| CN101691522A (en) * | 2009-09-30 | 2010-04-07 | 云南省农业科学院药用植物研究所 | Method for extracting rose damascana and rose flower water from roses |
| CN101906353A (en) * | 2010-08-03 | 2010-12-08 | 河北科技大学 | Extraction method and application of chestnut flower essential oil |
| CN102429840A (en) * | 2011-09-22 | 2012-05-02 | 黄馨莹 | Mosquito repellent liquid and preparation method thereof |
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| EK BLYTHE等: ""Composition of the essential oil of Pink Chablis bluebeard (Caryopteris ×clandonensis"Durio") and its biological activity against the yellow fever mosquito Aedes aegypti"", 《NATURAL VOLATILES & ESSENTIAL OILS》 * |
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