CN101422419A - Toilet water and manufacture method thereof - Google Patents
Toilet water and manufacture method thereof Download PDFInfo
- Publication number
- CN101422419A CN101422419A CNA2008102201565A CN200810220156A CN101422419A CN 101422419 A CN101422419 A CN 101422419A CN A2008102201565 A CNA2008102201565 A CN A2008102201565A CN 200810220156 A CN200810220156 A CN 200810220156A CN 101422419 A CN101422419 A CN 101422419A
- Authority
- CN
- China
- Prior art keywords
- extraction
- flos
- extractum
- water
- floral water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention relates to toilet water and a manufacture method thereof, in particular to toilet water which has the antiphlogistic and antibacterial functions and heat clearing and detoxifying. The invention discloses a substrate which contains 5 to 10 percent of a compound antimicrobial agent of the wild chrysanthemum concrete, honeysuckle concrete and frangipani concrete extracted by supercritical carbon dioxide and the phellodendron extract and the aloe extract extracted by an alcohol extraction method as well as contains the substance of toilet water accounting for the rest percent. The manufacture method is as follows: the oil-soluble material of the concrete compound is added into 20 percent of water, then water-soluble extraction liquid and pigments are added, fully mixed, aged, frozen and filtered; then a humectant and 85 percent of water are added, thus obtaining the finished product. In the invention, a plurality of plant extracts with the antiphlogistic and antibacterial functions as well as heat-clearing and detoxifying are adopted; moreover, the plant extracts mutually function and have remarkable effects; the effective components of the plants are completely and safely extracted; and the technique is effective and saves time.
Description
Technical field
The floral water that the present invention relates to use in the daily life specifically has certain antiphlogistic antibacterial, the floral water of effects for removing toxic heat.
Background technology
Floral water is a kind of aqueous solution that contains essence, can be used for being sprinkled upon on the clothes fragrant, also can be sprinkled upon places such as toilet and cover abnormal smells from the patient.There was the people constantly to discover afterwards, and in floral water, added some material and can have a certain specific function respectively, and added in the floral water such as material that can repel mosquitoes or chemical products and can make mosquito-repellent perfume; But itching relieving material or chemical and medicine industry product added in the floral water can make antipruritus toilet water.Present additive component can be divided into two big classes, and a class is the extracting solution of plant, and another kind of is chemical pharmaceutical substance.With regard to present plant extraction liquid is to adopt traditional processing technology, adopts basically and all raw materials is mixed mutually ageing then, freezing and filtering.This traditional handicraft method can cause the destruction to the effective ingredient of wherein certain plants, also causes organic solvent residual simultaneously.And chemical pharmaceutical substance, common disadvantage is not anti-anti-, the pharmaceutical quantities deficiency that slow release comes out, cause the drug-fast generation of microorganism simultaneously, the chemical substance short-term is used all right, but life-time service can cause skin allergy, and essence is the compositions of one kind of multiple class chemical substances, and also having other chemical substances to exist in the floral water, this all can reduce, the effect of the organic antibacterial agent of degrading.So people trend towards the additive of natural botanical extraction liquid now, but all wish to overcome the deficiency of making because of traditional handicraft,, yet there is not a kind of additive that adopts the antibacterial of natural plants simultaneously with regard in each kind of present floral water.
Summary of the invention
The purpose of this invention is to provide a kind of floral water, the sterilizing function additive of this floral water is the extract of plant, and has that broad-spectrum presses down, biocidal efficacies.
Another purpose of the present invention provides the manufacture method of floral water, and the extraction effective ingredients in plant of its energy safe and complete is when technology efficiently saves.
Technical solution of the present invention is:
One, a kind of floral water
1, a kind of floral water is counted by weight percentage: comprise the Flocdrysanthemi by supercritical carbon dioxide extraction, Flos Lonicerae extractum, Flos Plumeriae Acutifoliae extractum, the content of the compositions antibacterial of Aloe extraction solution and Cortex Phellodendri extracting solution is 5%～10%, all the other are the substrate of floral water.
In the above antibacterial, Flocdrysanthemi 1%～3%, Flos Lonicerae extractum 1%～2%, Flos Plumeriae Acutifoliae extractum 1%～2%, Aloe extraction solution 1%～2%, Cortex Phellodendri extracting solution 1%～2%.
Floral water substrate of the present invention is counted by weight percentage, and includes edible ethanol 30%～50%, essence 2%～5%, and the wetting agent 2%～5% of sorbitol, glycerol or propylene glycol, solubilizing agent 1%～2%, pigment is an amount of, the Purified Water surplus.
Two, a kind of manufacture method of floral water:
A, that Flos Chrysanthemi Indici, Flos Lonicerae or Herba Portulacae Grandiflorae are carried out supercritical carbon dioxide method for extracting respectively is as follows: drop into the dry thing of a certain amount of Flos Chrysanthemi Indici, Flos Lonicerae or Herba Portulacae Grandiflorae in the extraction kettle respectively, extraction kettle, extraction-container I, extraction-container II, detached dowel, basin are heated respectively, when reaching selected temperature, open CO
2Bottle pressurizes to system by high-pressure pump, as extraction kettle, extraction-container I, extraction-container II, when detached dowel pressure reaches the pressure that sets respectively, close CO
2Bottle, the beginning cycling extraction adds a certain amount of entrainer simultaneously, and regulates CO
2Flow to a certain amount of, keep constant temperature and pressure, after reaching selected extraction time,, obtain the crude product of active matter from extraction-container II discharge hole for discharge, sucking filtration or centrifugal and washing is refining is drying to obtain Flocdrysanthemi, Flos Lonicerae extractum, Flos Plumeriae Acutifoliae extractum,
B, respectively according to the following steps: fragmentation with Cortex Phellodendri, aloe raw material
Weigh
Extract
Purification
Filter
Finished product.
(1) earlier raw material is broken for sample powder about 30 orders;
(2) extract with 70% ethanol then;
(3) method of reuse macroporous resin adsorption is carried out purification;
(4) will can obtain Cortex Phellodendri, Aloe extraction solution after the solution filtration.
C, with Flocdrysanthemi, Flos Lonicerae extractum, Flos Plumeriae Acutifoliae extractum, essence, ethanol, 20% water mixed dissolution is complete, stand-by;
D, with above dissolving completely solution add Aloe extraction solution, mix homogeneously behind the Cortex Phellodendri extracting solution, ageing adds the water of wetting agent and 80% again behind the freezing and filtering, promptly get floral water of the present invention.
Extractum of the present invention is Flocdrysanthemi, Flos Lonicerae extractum, Flos Plumeriae Acutifoliae extractum.Its basic index is as follows:
Flocdrysanthemi
| Project | Index |
| Outward appearance and organoleptic attribute | This product is yellow to the yellowish-brown paste, has the Flos Chrysanthemi Indici characteristic odor. |
| Differentiate | This product ethanol extract is observed down at ultra-violet lamp (365nm), shows yellow-green fluorescence. |
| Flos Chrysanthemi glycosides content (μ g/ml) | 80 |
| Moisture, % | ≤ 10.0 |
| Acid number, mgKOH/g | ≤ 25 |
| Dissolvent residual | Must not detect |
Flos Lonicerae extractum
| Project | Index |
| Outward appearance and organoleptic attribute | This product is yellow to the yellowish-brown paste, has characteristic odor. |
| Chlorogenic acid content (μ g/ml) | 20 |
| Moisture, % | ≤ 10.0 |
| Acid number, mgKOH/g | ≤ 40 |
| Dissolvent residual | Must not detect |
Flos Plumeriae Acutifoliae extractum
| Project | Index |
| Outward appearance and organoleptic attribute | This product is yellow to the yellowish-brown paste, has characteristic odor. |
| Plumieride content (μ g/ml) | 30 |
| Plumieric acid content (μ g/ml) | 20 |
| Moisture, % | ≤ 10.0 |
| Acid number, mgKOH/g | ≤ 60 |
| Dissolvent residual | Must not detect |
Extracting solution of the present invention is Cortex Phellodendri extracting solution, Aloe extraction solution, and its basic index is as follows:
Aloe extraction solution
1, abnormal smells from the patient: clear Aloe is newly counted flavor, free from extraneous odour
2, proportion (g/ml): 0.86-0.92
3、PH：4—6
4, barbaloin content (μ g/ml): 〉=2
5, total number of bacteria :≤100/ml
The Cortex Phellodendri extracting solution
1, abnormal smells from the patient: have characteristic odor
2, proportion (g/ml): 0.85-0.90
3、PH：4—6
4, total alkaloid content (μ g/ml): 〉=20
5, total number of bacteria :≤100/ml
Wetting agent of the present invention: glycerol can absorb in the air 37% moisture, than sorbitol and propylene glycol stronger water absorbing properties is arranged, but the skin sense is more sticky, and by contrast, propylene glycol is between sorbitol and glycerol, so use relatively extensively in the floral water prescription.The edible ethanol consumption: the ethanol of high consumption brings more the algefacient sensation to skin, but simultaneously the zest of skin is also increased thereupon, is applicable to that generally the adult uses.And the child then requires to lower the ethanol consumption for less stimulation to skin.
Antibacterial of the present invention:
Flocdrysanthemi: Flos Chrysanthemi Indici is the head inflorescence of feverfew Herba Dendranthematis indici Dendranthema indicum (L.) Des Moul..Belong to perennial herb, be born in by patana, shrubbery, river bank meadow bog, beach salt lick and the field wing.Be widely distributed in northeast, North China and southwest.Flos Chrysanthemi Indici bitter in the mouth, cold nature are gone into lung, Liver Channel.The tool heat-clearing and toxic substances removing, the effect of dispelling wind suppressing the hyperactive liver.
For the merit of the wind and heat dispersing of Flos Chrysanthemi Indici, how on the books China's this agrostology monograph at all times is.Put down in writing in the Compendium of Material Medica: Flos Chrysanthemi Indici " bitter, hot, warm, it is swollen to control pain, treats poison, scrofula, eye Xi ".Record in " book on Chinese herbal medicine converge with speech ": Flos Chrysanthemi Indici " the gas cold, removing blood stasis is soothing the liver, separate treat the poison that looses medicine also, stagnated blood in housewife people's abdomen, the capable fire-toxin pellet of Xie Tian furuncle is smash juice and living wine is obeyed it; Or get Zi Fu An and also imitate.Boil soup and wash the skin ulcer scabies, can remove the wind parasite killing again." " book on Chinese herbal medicine just " claim that also Flos Chrysanthemi Indici can " fire that looses loose gas, eliminating carbuncle poison, swollen, the scrofula of furuncle, eyes burning pain "." Sichuan Chinese medicinal herbal " nineteen eighty-two version is also carried: Flos Chrysanthemi Indici " dispelling wind, heat clearing away, detoxifcation.Be used for flu, skin ulcer pain toxic swelling, laryngopharynx swelling and pain, wind-fire acute conjunctivitis, jaundice due to damp-heat, liver-heat type hypertension ".The Pharmacopoeia of the People's Republic of China is stated its heat-clearing and toxic substances removing also with its income, returns the effect of liver, heart channel.
The effects for removing toxic heat of Flos Chrysanthemi Indici excellence, by wide clinical application in section's diseases such as inside and outside, the woman of medical science, youngsters.Utilize these drug effects of Flos Chrysanthemi Indici to be applied to other field, as the daily-use chemical industry industry, especially skin nursing aspect has positive effect, we by to the extracting method of Flos Chrysanthemi Indici, pharmacology, antibacterial, product is used, the research of clinic trial, particularly uses supercritical CO
2Extracting process extracts the Flos Chrysanthemi Indici elite, explores the modern extraction method of traditional Chinese herbal medicine, and Flos Chrysanthemi Indici extract is applied to skin nursing products---on the floral water,, traditional Chinese herbal medicine provides scientific basis for being applied to modern oral health-care product.Consumption is generally: 1-3%.
Flos Lonicerae extractum: Flos Lonicerae is traditional Chinese herbal medicine, belongs to medical flower, and the another name Flos Lonicerae is because the alabastrum of its to be Caprifoliaceae perennial half evergreen voluble shrub Radix Ophiopogonis is Flos Lonicerae again.Pure white when just opening, change yellow after a couple of days.Flos Lonicerae is a heat and toxic materials clearing away medicine, and nature and flavor are sweet, cold, goes into lung, stomach, heart channel, mainly treats the pyretic toxicity carbuncle sore, symptoms such as child's furuncle, miliaria, clearing away heat and cooling blood simultaneously, can also swell clearly make eye bright, expelling wind and cold.
The analysis and research of modern pharmacology find that Flos Lonicerae contains biochemical components such as cyclohexanhexanol, wooden slippers straw colour element, inositol, Saponin, tannic acid, also contain and go back protogene in a large number.Excretory toxin such as staphylococcus, Hemolytic streptococcus, typhoid fever, tuberculosis, streptococcus pneumoniae there is stronger inhibitory action.So Flos Lonicerae has been put into antibacterials, belong to antibiotic series.Also be used for the treatment of appendicitis, bacillary dysentery etc. clinically, receive certain curative effect.Also can be made into beverage, have diffusing summer-heat heat clearing away for tea-drinking summer, during appetizing is multiple, the wind that the looses effect that makes eye bright.Consumption is generally 1-2%
Egg egg flower concrete: spending usually of Herba Portulacae Grandiflorae is open in the sun, and early morning, dusk or cloudy day are just closed, so another name is called heronsbill.Thereby the implied meaning of bright ＂, the ardent ＂ of ＂ of ＂ arranged.In the rural area, people call out its Herba Portulacae Grandiflorae again.Because it is always in full bloom in the period of the day from 11 a.m. to 1 p.m, close again in the afternoon, on Plant Taxonomy, belong to portulacaceous Herba Portulacae Grandiflorae, also often be called as Portulaca grandilora.
Herba Portulacae Grandiflorae contains multiple antibacterial disease-resistant composition, can suppress multiple bacillus.Stem, leaf can be used as medicine, and bitter in the mouth cold in nature has the effect of heat-clearing and toxic substances removing.Carry according to " Nanning City's medicine will ": the ＂ Herba Portulacae Grandiflorae has effects such as anticancer detoxifcation, reducing swelling and alleviating pain, blood circulation promoting and blood stasis dispelling.＂ can treat diseases such as laryngopharynx swelling and pain, traumatic injury, scald, eczema.As mashing deposited affected part in right amount, can treat diseases such as infantile eczema, damp and hot bark rot skin ulcer, traumatic injury, furuncle toxic swelling with bright stem, leaf.Smash juice in right amount with the bright stem and leaf of Herba Portulacae Grandiflorae, add the borax powder a little, frequent rinsing the mouth can be treated laryngopharynx swelling and pain.Consumption is generally 1-2%.
Aloe extraction solution: the heat clearing away bath is wet, and pathogenic fire purging removes steams, and detoxifcation is treated skin ulcer and is used for sore swollen toxin, eczema symptom such as scratch where it itches.Consumption is generally 2%
The Cortex Phellodendri extracting solution: the dispel effect of poison of antiinflammatory is arranged, the external moss that wets, consumption is generally 1-2%.
Mentholum is the extract that large Chinese crude drug Herba Menthae or the bright product of tame Herba Menthae are planted by Labiatae man.Mentholum is a Chinese medicine, and acrid in the mouth is cool in nature, has effects such as dispelling wind, heat clearing away, detoxifcation, is mainly used in diseases such as treatment headache conjunctival congestion, affection due to external wind and heat, pharynx tooth swell and ache, skin pruritus due to wind pathogen.Consumption is generally 1-2%.
Solubilising is meant oil soluble material under the effect of surfactant, increases dissolubility and form the process of solution in water.Consumption is generally 1-2%.
Flocdrysanthemi of the present invention, Flos Lonicerae extractum, Flos Plumeriae Acutifoliae extractum, Aloe extraction solution and blended pharmacological action of Cortex Phellodendri extracting solution and application direction:
1.1 pharmacological research
1.1.1 antibacterial action
Above-mentioned five kinds of mixture can suppress general pathogenic bacterium such as golden Portugal bacterium, escherichia coli, dysentery bacterium, also can suppress the growth of streptococcus, lactobacillus etc.
1.1.2 Detoxication
By family being exempted to carry out the research of refrigeration function, show that the said extracted thing has the good thermal effect of separating.
1.1.3 enhancing human body immunity effect
Annotate the 0.2ml Flos Chrysanthemi indici injection to white mice, that gets that its peritoneal fluid calculates macrophage engulfs the chicken red blood cell number, compares with matched group, finds that Flos Chrysanthemi indici injection can obviously strengthen cytophagous phagocytic function.
1.1.4 anticoagulant effect
Flocdrysanthemi, Flos Lonicerae extractum, Flos Plumeriae Acutifoliae extractum all have the obvious suppression effect to golden Portugal bacterium and collagen-induced rat platelet aggregation in vitro.
1.1.5 toxic action
(1) acute toxicity testing: mouse vein injects Flos Chrysanthemi Indici, Flos Lonicerae, Flos Plumeriae Acutifoliae injection (every ml contains biological 1g approximately), LD respectively
50Be 10.47g/kg, show that its toxicity is very little.
(2) inferior anxious, property toxicity test chamber: every day, lumbar injection 0.2g/kg Flos Chrysanthemi Indici, Flos Lonicerae, Flos Plumeriae Acutifoliae injection were 1 time, continuous one month, contrasted with normal saline, two groups of weight of mice indifferences are put to death after the drug withdrawal, dissect, perusal does not see that histiocyte is unusual.
2.2 application direction
The function of Flos Chrysanthemi Indici, Flos Lonicerae, Flos Plumeriae Acutifoliae heat-clearing and toxic substances removing, anti-inflammation is widely used in clinical medicine, to be decocted in water for oral dose or to make modes such as extractum, suppository, injection, tablet, the clean injection of pyretic toxicity, be used for the treatment of furuncle, pyretic toxicity eczema, summertime furuncle, hot conjunctival congestion with ophthalmalgia, anti-curing cold, influenza, meningitis and treat acute urinary system infection, acute mastitis, liver-heat type hypertension etc.Application medically is for Flos Chrysanthemi Indici, Flos Lonicerae, Flos Plumeriae Acutifoliae provide scientific basis in the daily chemical products application.The application on floral water of Flos Chrysanthemi Indici, Flos Lonicerae, Flos Plumeriae Acutifoliae extract will further promote the function of daily chemical products.
3. Flos Chrysanthemi Indici, Flos Lonicerae, Flos Plumeriae Acutifoliae extract are at the application test of floral water
3.1 the bacteriostasis property of Lotus flower dew test
The Lotus flower dew sample of getting 3.1 preparations carries out the bacteriostasis property test.
3.2.1 laboratory sample: some of Lotus flower dew
3.2.2 experimental strain: Streptococcus mutans, streptococcus thermophilus, lactobacillus, staphylococcus aureus, escherichia coli.
3.2.3 experimental technique
(1) test tube method: contain 0.1 milliliter of test of inoculation bacterium liquid in the variable concentrations at 10 milliliters of BHI culture fluid.A, get 0.1 milliliter respectively be added on 2 MS flat boards from every pipe, the coating inoculation is carried out colony counting to each flat board, calculates its average.The floral water concentration of not having bacterial growth in the plate count fully is minimum bacteria concentration: the floral water concentration that the bacterium number that falls is equal to or less than 0.1% initial inoculation bacterium amount is minimal inhibitory concentration.B, get 0.1 milliliter be switched in 10 milliliters of BHI culture fluid from every pipe, observing in vitro liquid, limpid not have minimum floral water concentration muddy or the precipitation growth be minimal inhibitory concentration.
(2) dull and stereotyped method of testing: with reference to State Standard of the People's Republic of China GB15979-1995 " disposable use hygienic article standard " appendix B " product antibacterial and bactericidal property and stability test method ".
3.2.4 bacteriostasis property test
Conventional bacteriostatic experiment: by flat band method Lotus flower dew is carried out staphylococcus aureus and colibacillary bacteriostatic test, it the results are shown in following table
The conventional bacteriostatic experiment result of floral water of the present invention
Above-mentioned test data shows that floral water of the present invention has the obvious sterilization effect, meets the sterilised products standard-required.
4. result and discussion
4.1 Flos Chrysanthemi Indici, Flos Lonicerae, Flos Plumeriae Acutifoliae are a heat-clearing and detoxifying herb commonly used, wide material sources, and cheap, clinical efficacy is definite, and its extraction is applied to daily chemical products, especially having a extensive future on juvenile product.
4.2 employing supercritical CO
2The Flos Chrysanthemi Indici of abstraction technique separation and Extraction, Flos Lonicerae, Flos Plumeriae Acutifoliae working substance have the technology advanced person, and the content height does not destroy advantages such as original chemical analysis, extracting solution color and luster be more shallow, through chromatography, does not have destroyed with this method extract active ingredient.
4.3 Flos Chrysanthemi Indici, Flos Lonicerae, Flos Plumeriae Acutifoliae extract pharmacology mechanism are clear and definite, add in the floral water as additive, have the effect of heat-clearing and toxic substances removing equally, so floral water of the present invention have the effect of tangible inhibiting bacteria and diminishing inflammation.
4.4 floral water of the present invention is obvious as a kind of novel antiphlogistic antibacterial, heat-clearing and toxic substances removing product effect, steady quality.
The invention has the beneficial effects as follows that the present invention is the floral water of a kind of antiphlogistic antibacterial, heat-clearing and toxic substances removing, adopt the pure plant extracts and the mutual synergism of multiple energy antiphlogistic antibacterial, heat-clearing and toxic substances removing, effect is remarkable, and the effective ingredients in plant complete safety is extracted, when technology efficiently saves.
The specific embodiment
Floral water of the present invention, its composition are (calculating by weight percentage)
Embodiment one
Flocdrysanthemi 3%, Flos Lonicerae extractum 1%, Flos Plumeriae Acutifoliae extractum 2%, Aloe extraction solution 1%, Cortex Phellodendri extracting solution 2%, edible ethanol 50%, essence 5%, sorbitol 2%, solubilizing agent castor oil hydrogenated 2%, pigment is an amount of, the Purified Water surplus.
Embodiment two
Flocdrysanthemi 2%, Flos Lonicerae extractum 2%, Flos Plumeriae Acutifoliae extractum 1%, Aloe extraction solution 2%, Cortex Phellodendri extracting solution 2%, edible ethanol 40%, essence 3%, glycerol 5%, solubilizing agent castor oil hydrogenated 2%, pigment is an amount of, the Purified Water surplus.
Embodiment three
Flocdrysanthemi 1%, Flos Lonicerae extractum 2%, Flos Plumeriae Acutifoliae extractum 2%, Aloe extraction solution 2%, Cortex Phellodendri extracting solution 2%, edible ethanol 30%, essence 2%, propylene glycol 3%, solubilizing agent castor oil hydrogenated 2%, pigment is an amount of, the Purified Water surplus.
The manufacture method of floral water of the present invention: A, the Flos Chrysanthemi Indici with indication of the present invention, Flos Lonicerae, the dry thing of Herba Portulacae Grandiflorae extract respectively, and extraction process is that with the above monotaste plant input extraction kettle, the extraction time is 100min; Extraction temperature is 40 ℃; Extracting pressure is 15Mpa; Thereafter blood pressure lowering, heating up enters separating still, CO
2Flow velocity is 12kg/kgh; Separating pressure is: detached dowel is 6MPa, and parsing I is that 10Mpa, temperature are 44 ℃, and parsing II is that 5.6MPa, temperature are 25 ℃; The entrainer that adopts is an ethanol.After reaching selected extraction time, from resolving the II discharge hole for discharge, obtain the crude product of active matter, sucking filtration or the centrifugal and refining extractum product that is drying to obtain of washing.
A, respectively according to the following steps: fragmentation with Cortex Phellodendri, aloe raw material
Weigh
Extract
Purification
Filter
Finished product.
(1) earlier raw material is broken for sample powder about 30 orders;
(2) extract with 70% ethanol then;
(3) method of reuse macroporous resin adsorption is carried out purification;
(4) will can obtain Cortex Phellodendri, Aloe extraction solution after the solution filtration.
B, with Flocdrysanthemi, Flos Lonicerae extractum, Flos Plumeriae Acutifoliae extractum, essence, ethanol, 20% water mixed dissolution is complete, stand-by;
Stirred 10～20 minutes behind C, dissolving solution adding completely Aloe extraction solution, Cortex Phellodendri extracting solution and the pigment B; behind all material mix homogeneously, shut down ageing, freezing and filtering; add the water of wetting agent propylene glycol and 80% after the filtration again, promptly get floral water of the present invention.
Floral water of the present invention can also add Mentholum, and making to be applied to increases refrigerant sense behind the skin, and addition is for should be 2%.
Claims (4)
1, a kind of floral water, it is characterized in that percentage by weight calculates: comprise Flocdrysanthemi, Flos Lonicerae extractum, Flos Plumeriae Acutifoliae extractum by supercritical carbon dioxide extraction, the content of the compositions antibacterial of Aloe extraction solution and Cortex Phellodendri extracting solution is 5%～10%, and all the other are the substrate of floral water.
2, a kind of floral water according to claim 1 is characterized in that in the antibacterial, Flocdrysanthemi 1%～3%, Flos Lonicerae extractum 1%～2%, Flos Plumeriae Acutifoliae extractum 1%～2%, Aloe extraction solution 1%～2%, Cortex Phellodendri extracting solution 1%～2%.
3, a kind of floral water according to claim 1, it is characterized in that floral water substrate counts by weight percentage, include edible ethanol 30%～50%, essence 2%～5%, the wetting agent 2%～5% of sorbitol, glycerol or propylene glycol, solubilizing agent 1%～2%, pigment is an amount of, the Purified Water surplus.
4, according to the manufacture method of the described a kind of floral water of claim 1 to 3, it is characterized in that
A, that Flos Chrysanthemi Indici, Flos Lonicerae, Herba Portulacae Grandiflorae are carried out supercritical carbon dioxide method for extracting respectively is as follows: drop into a certain amount of Flos Chrysanthemi Indici, Flos Lonicerae, the dry thing of Herba Portulacae Grandiflorae in the extraction kettle respectively, extraction kettle, extraction-container I, extraction-container II, detached dowel, basin are heated respectively, when reaching selected temperature, open CO
2Bottle pressurizes to system by high-pressure pump, as extraction kettle, extraction-container I, extraction-container II, when detached dowel pressure reaches the pressure that sets respectively, close CO
2Bottle, the beginning cycling extraction adds a certain amount of entrainer simultaneously, and regulates CO
2Flow to a certain amount of, keep constant temperature and pressure, after reaching selected extraction time,, obtain the crude product of active matter from extraction-container II discharge hole for discharge, sucking filtration or centrifugal and washing is refining is drying to obtain Flocdrysanthemi, Flos Lonicerae extractum, Flos Plumeriae Acutifoliae extractum,
B, respectively according to the following steps with Cortex Phellodendri, aloe raw material: broken, weigh, promptly be finished product after the extraction, purification, filtration,
(1) earlier raw material is broken for sample powder about 30 orders;
(2) extract with 70% ethanol then;
(3) method of reuse macroporous resin adsorption is carried out purification;
(4) will can obtain Cortex Phellodendri, Aloe extraction solution after the solution filtration,
C, with Flocdrysanthemi, Flos Lonicerae extractum, Flos Plumeriae Acutifoliae extractum, essence, ethanol, 20% water mixed dissolution is complete, stand-by;
With above dissolving completely solution add Aloe extraction solution, mix homogeneously behind Cortex Phellodendri extracting solution, the pigment, ageing adds the water of wetting agent and 80% again behind the freezing and filtering, promptly get floral water of the present invention.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008102201565A CN101422419B (en) | 2008-12-19 | 2008-12-19 | Toilet water and manufacture method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008102201565A CN101422419B (en) | 2008-12-19 | 2008-12-19 | Toilet water and manufacture method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101422419A true CN101422419A (en) | 2009-05-06 |
| CN101422419B CN101422419B (en) | 2010-12-22 |
Family
ID=40613448
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008102201565A Active CN101422419B (en) | 2008-12-19 | 2008-12-19 | Toilet water and manufacture method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101422419B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103735465A (en) * | 2014-01-15 | 2014-04-23 | 张一文 | Child floral water and preparation method thereof |
| CN104721095A (en) * | 2015-04-10 | 2015-06-24 | 唐山职业技术学院 | Caryopteris clandonensis mosquito repelling liquid and preparation method thereof |
| CN105997767A (en) * | 2016-07-28 | 2016-10-12 | 扬中市锦丰工业设计有限公司 | Aloe floral water |
| CN108685774A (en) * | 2018-07-09 | 2018-10-23 | 福建省海乐威生物工程有限公司 | A kind of mosquito-repellent water of the jasmin containing thermal water |
| CN113069519A (en) * | 2021-04-14 | 2021-07-06 | 河南中医药大学 | Anti-inflammatory itching-relieving hair washing formula and preparation method and using method thereof |
-
2008
- 2008-12-19 CN CN2008102201565A patent/CN101422419B/en active Active
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103735465A (en) * | 2014-01-15 | 2014-04-23 | 张一文 | Child floral water and preparation method thereof |
| CN104721095A (en) * | 2015-04-10 | 2015-06-24 | 唐山职业技术学院 | Caryopteris clandonensis mosquito repelling liquid and preparation method thereof |
| CN105997767A (en) * | 2016-07-28 | 2016-10-12 | 扬中市锦丰工业设计有限公司 | Aloe floral water |
| CN108685774A (en) * | 2018-07-09 | 2018-10-23 | 福建省海乐威生物工程有限公司 | A kind of mosquito-repellent water of the jasmin containing thermal water |
| CN113069519A (en) * | 2021-04-14 | 2021-07-06 | 河南中医药大学 | Anti-inflammatory itching-relieving hair washing formula and preparation method and using method thereof |
| CN113069519B (en) * | 2021-04-14 | 2022-02-25 | 河南中医药大学 | Anti-inflammatory itching-relieving hair washing formula and preparation method and using method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101422419B (en) | 2010-12-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102440266B (en) | Traditional Chinese medicine preparation for antibiosis, bactriostasis and sterilization and preparation method thereof | |
| Daniyan et al. | Evaluation of the antimicrobial activities and phytochemical properties of extracts of Tamaridus indica against some diseases causing bacteria | |
| CN101347395B (en) | Chinese medicine floral water for preventing and treating bite by mosquitos | |
| CN105920977A (en) | Pure vegetal air disinfection purifying agent and preparing method thereof | |
| CN105055244A (en) | Organic natural plant preservative | |
| CN101422419B (en) | Toilet water and manufacture method thereof | |
| CN104127779B (en) | A kind of Chinese herb compound washing lotion of anti-inflammation and preparation method thereof | |
| CN103585074A (en) | Rabdosia rubescens aqueous extract, use of rabdosia rubescens aqueous extract, rabdosia rubescens extract, skin care product and preparation methods of rabdosia rubescens aqueous extract and skin care product | |
| CN103416718A (en) | Rosemary health-protection soy sauce and preparation method thereof | |
| CN103622865A (en) | Medical liquid soap containing plant extracted essential oil and preparation method of medical liquid soap | |
| CN103830404A (en) | Traditional Chinese medicine composition for treating Chicken colibacillosis, preparation method of traditional Chinese medicine mixture and traditional Chinese medicine mixture | |
| CN103504437B (en) | Forsythia leaf beverage | |
| CN101181208B (en) | Gargle containing natural antibiotics and preparation method thereof | |
| CN110025691A (en) | A kind of compound houttuynia cordata preparation and preparation method and application | |
| CN106719955A (en) | A kind of plant disinfectant | |
| KR20170130690A (en) | Natural detergent composition and preparation method thereof | |
| CN101972025B (en) | Bamboo vinegar health care beverage and preparation method thereof | |
| CN107320758B (en) | Air purifying agent for efficiently removing bacteria in livestock and poultry breeding environment | |
| CN104208294A (en) | Traditional Chinese medicine composition for treating piglet yellow-white dysentery and preparation method thereof | |
| CN111053937A (en) | Plant-extracted household deodorizing and deodorizing disinfection composition and preparation method thereof | |
| CN103520287B (en) | Forsythia suspense leaves refreshing sugar | |
| CN110402969A (en) | A kind of environmental type plant source thimerosal | |
| CN108553572A (en) | A kind of functional incense and preparation method thereof | |
| CN1977894A (en) | Medicinal composition with anti-inflammation effect and its preparing method | |
| CN101297857B (en) | Chinese medicine preparation for treating recessive mastitis of cow and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20190909 Address after: 510000 First Floor B1 of Baishuitang 1-2, Huangpu Industrial Avenue, Tianhe District, Guangzhou City, Guangdong Province Patentee after: Dr. Kang Daihua Group Co., Ltd. Address before: 510130 Guangdong city of Guangzhou province Liwan District Sand Street South No. 48 Patentee before: Meichen Group Co., Ltd. |