CN106635415A - Fly-repelling vegetable essential oil and preparation method and application thereof - Google Patents
Fly-repelling vegetable essential oil and preparation method and application thereof Download PDFInfo
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- CN106635415A CN106635415A CN201610916666.0A CN201610916666A CN106635415A CN 106635415 A CN106635415 A CN 106635415A CN 201610916666 A CN201610916666 A CN 201610916666A CN 106635415 A CN106635415 A CN 106635415A
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- essential oil
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- eucalyptus
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Animal Behavior & Ethology (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- General Chemical & Material Sciences (AREA)
- Dermatology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
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Abstract
The invention discloses fly-repelling vegetable essential oil, prepared from, by weight, 1-3 parts of mint, 2-5 parts of eucalyptus, 2-4 parts of Lantana camara, 1-3 parts of geranium, 1-3 parts of Murraya paniculata, and 2-4 parts of Chinese mugwort. A preparation method comprises the steps of washing the picked mint, eucalyptus, Lantana camara, geranium, Murraya paniculata and Chinese mugwort, and washing to obtain raw materials; air-drying the washed materials, and mixing the materials according to a weight ratio; adding distilled water as heavy as the materials into the mixed materials, adding to a fractionator, and fractionally extracting at 60-85 DEG C to obtain extract; adding sodium chloride as heavy as the extract into the extract, extracting, filtering, and collecting an upper oil layer to obtain the finished vegetable essential oil. The fly-repelling vegetable essential oil may be sprayed to the surface of human and livestock, is nontoxic and harmless to human and livestock, is free of residue, is capable of effectively repelling flies and avoiding disturbance and bite, and is convenient to use and effective to use.
Description
Technical field
The present invention relates to plants essential oil applied technical field, specially a kind of repellent mosquitos and flies plants essential oil and preparation method thereof
And application.
Background technology
The normal life and work of mosquitos and flies harassing and wrecking people and animals, repellent or the product of killing mosquitos and flies in the market are mostly chemical industry
Synthesis, there is certain toxicity, notably safe when using, and prolonged application all has an impact to environment and human and livestock health, safely and effectively, nothing
Any toxic and side effect.
Common fly eradication, mosquito eradication product are mainly divided to two classes：One class is the equipment such as fly-killing lamp, Mosquito killer lamp, because needing fixed installation
It is little for people and animals' effect of outside work life and the mechanism of action is passive, is mostly used for interior.Another kind of is hygienic biocide
Agent, is mainly used in environment dissipation, can control mosquitos and flies overall quantity in certain area, harasses and bites for causing with people and animals
Mosquitos and flies poor effect, cure the symptoms, not the disease.
Hygienic insecticide has certain residual life, if being applied to the fields such as food notably safety, residual may cause
Face the problem of food security.
The usual main component of hygienic insecticide is chemical composition, there is certain toxicity, and Long-Time Service affects environment and people and animals strong
Health, for this purpose, a kind of it is proposed that repellent mosquitos and flies plants essential oil and its preparation method and application.
The content of the invention
The technical problem to be solved in the present invention is to overcome existing defect, there is provided a kind of repellent mosquitos and flies plants essential oil and its system
Preparation Method and application, can be sprayed on people and animals' body surface, harmless, noresidue nontoxic to people and animals itself, while effectively repellent mosquitos and flies,
Avoid harassing and bite, can be with the problem in effectively solving background technology.
For achieving the above object, the present invention provides following technical scheme：A kind of repellent mosquitos and flies plants essential oil, the repellent mosquitos and flies
Plants essential oil raw material according to mass parts meter, including following components：Peppermint 1-3 parts, eucalyptus 2-5 parts, fly expelling plum 2-4 parts, India
Certain herbaceous plants with big flowers 1-3 parts, moon tangerine 1-3 parts and wormwood 2-4 parts.
A kind of preparation method of repellent mosquitos and flies plants essential oil, comprises the steps：
1) peppermint plucked, eucalyptus, fly expelling plum, fish pelargonium, moon tangerine and wormwood are cleaned, as raw material；
2) each raw material after cleaning is dried in the air to drying, then according to quality parts ratio mixing；
3) the quality distilled water such as addition and raw material in mixed raw material, is then put in fractionating device, at 60-85 DEG C
Under the conditions of carry out fractionation extraction, obtain extract；
4) extracted to the sodium chloride for obtaining the quality such as addition in extract, then filtered to take top oil reservoir, obtained final product into
Product plants essential oil.
Used as a preferred technical solution of the present invention, in its raw material, peppermint, fish pelargonium, the mass ratio of moon tangerine are 6:2:
1—2:1:Between 1.
Used as a preferred technical solution of the present invention, in its raw material, fly expelling plum, the mass ratio of wormwood are 1:2—2：1 it
Between.
Used as a preferred technical solution of the present invention, in its raw material, peppermint, eucalyptus mass ratio are 1:1—1：Between 2
As a preferred technical solution of the present invention, in its raw material, peppermint, eucalyptus, fly expelling plum, fish pelargonium, moon tangerine and
Wormwood is plucked before the flowers are in blossom.
As a preferred technical solution of the present invention, the peppermint, eucalyptus, fly expelling plum, fish pelargonium, moon tangerine and Chinese mugwort after cleaning
Grass dries in the air when being dried, and keeps air humidity between 2.5% -5%, while the speed that maintains the circulation of air is in 0.2m/s -0.5m/
Between s.
Compared with prior art, the invention has the beneficial effects as follows：Plants essential oil set peppermint, eucalyptus, fly expelling plum, the India
Certain herbaceous plants with big flowers, moon tangerine, the advantage of six kinds of natural materials of wormwood, according to specific ratio, by fractionation mode plant essence, recovery rate are extracted
It is higher, up to 1.8-3.2%.Peppermint, eucalyptus, fly expelling plum and moon tangerine all have functions that to expel mosquitos and flies, fish pelargonium and wormwood have
There is expelling parasite.Several essential oils are combined together, energy repellent mosquitos and flies, reduce the harassing and wrecking to people and animals and bite, and safety has
Effect, it is without any side effects.Additionally, the input cost of the technology of the present invention is low, it is simple easily operated, and this repellent mosquitos and flies plant
Essential oil and its preparation method and application has the benefit that：
(1) the plants essential oil formula is invented, is had no irritating odor, it is safe efficient, have no side effect；
(2) invent the plants essential oil formula to prepare simply, it is easy to use；
(3) raw material of invention plants essential oil is cheap and easy to get, is easy to large-scale production, and reduces the cost for producing；
(4) invent the plants essential oil performance formula to stablize, can harass and bite people and animals from mosquitos and flies is solved the problems, such as at all.
Specific embodiment
Technical scheme is clearly and completely described below in conjunction with the embodiment of the present invention, it is clear that retouched
The embodiment stated is only a part of embodiment of the invention, rather than the embodiment of whole.Based on the embodiment in the present invention, this
The every other embodiment that field those of ordinary skill is obtained under the premise of creative work is not made, belongs to the present invention
The scope of protection.
Embodiment one：
A kind of repellent mosquitos and flies plants essential oil, the plants essential oil raw material of the repellent mosquitos and flies according to mass parts meter, including with the following group
Point：2 parts of 2 parts of peppermint, 4 parts of eucalyptus, 1 part of fly expelling plum, 1 part of 2 part, month tangerine of fish pelargonium and wormwood.Concrete preparation method includes following
Step：
1) peppermint, eucalyptus, fly expelling plum, fish pelargonium, moon tangerine, wormwood were gathered into Hua Heye before it is bloomed, is cleaned up
As raw material；
2) clean each raw material is dried in the air to drying, each raw material after cleaning dries in the air when being dried, keeps air humidity to exist
Between 2.5% -5%, while speed is maintained the circulation of air between 0.2m/s -0.5m/s, then according to the mass ratio is mixed
Close；
3) the quality distilled water such as addition and raw material in mixed raw material, is then put in fractionating device, at 60-85 DEG C
Under the conditions of carry out fractionation extraction, obtain extract；
4) to obtain in extract add etc. quality sodium chloride extracted, then filter to take top oil reservoir, get product
Plants essential oil, and final oil yield is 1.8%.
In embodiment one：In its raw material, peppermint, fish pelargonium, the mass ratio of moon tangerine are 1:1:0.5, in its raw material, by fly
Plum, the mass ratio of wormwood are 1:2, in its raw material, peppermint, the mass ratio of eucalyptus are 1:2.
Embodiment two：
A kind of repellent mosquitos and flies plants essential oil, the plants essential oil raw material of the repellent mosquitos and flies according to mass parts meter, including with the following group
Point：2 parts of 3 parts of peppermint, 5 parts of eucalyptus, 2 parts of fly expelling plum, 2 parts of 1 part, month tangerine of fish pelargonium and wormwood.Concrete preparation method includes following
Step：
1) peppermint, eucalyptus, fly expelling plum, fish pelargonium, moon tangerine, wormwood were gathered into Hua Heye before it is bloomed, is cleaned up
As raw material；
2) clean each raw material is dried in the air to drying, each raw material after cleaning dries in the air when being dried, keeps air humidity to exist
Between 2.5% -5%, while speed is maintained the circulation of air between 0.2m/s -0.5m/s, then according to the mass ratio is mixed
Close；
3) the quality distilled water such as addition and raw material in mixed raw material, is then put in fractionating device, at 60-85 DEG C
Under the conditions of carry out fractionation extraction, obtain extract；
4) to obtain in extract add etc. quality sodium chloride extracted, then filter to take top oil reservoir, get product
Plants essential oil, and final oil yield is 3.2%.
In embodiment two：In its raw material, peppermint, fish pelargonium, the mass ratio of moon tangerine are 3:1:2, in its raw material, by fly
Plum, the mass ratio of wormwood are 1:1, in its raw material, peppermint, the mass ratio of eucalyptus are 3:5.
Embodiment three：
A kind of repellent mosquitos and flies plants essential oil, the plants essential oil raw material of the repellent mosquitos and flies according to mass parts meter, including with the following group
Point：1.5 parts of 2 parts of peppermint, 4 parts of eucalyptus, 1.5 parts of fly expelling plum, 1 part of 3 part, month tangerine of fish pelargonium and wormwood.Concrete preparation method includes
Following steps：
1) peppermint, eucalyptus, fly expelling plum, fish pelargonium, moon tangerine, wormwood were gathered into Hua Heye before it is bloomed, is cleaned up
As raw material；
2) clean each raw material is dried in the air to drying, each raw material after cleaning dries in the air when being dried, keeps air humidity to exist
Between 2.5% -5%, while speed is maintained the circulation of air between 0.2m/s -0.5m/s, then according to the mass ratio is mixed
Close；
3) the quality distilled water such as addition and raw material in mixed raw material, is then put in fractionating device, at 60-85 DEG C
Under the conditions of carry out fractionation extraction, obtain extract；
4) to obtain in extract add etc. quality sodium chloride extracted, then filter to take top oil reservoir, get product
Plants essential oil, and final oil yield is 2.8%.
In implementing three：In its raw material, peppermint, fish pelargonium, the mass ratio of moon tangerine are 2:3:1, in its raw material, by fly
Plum, the mass ratio of wormwood are 1:1, in its raw material, peppermint, the mass ratio of eucalyptus are 1:2.
Example IV：
A kind of repellent mosquitos and flies plants essential oil, the plants essential oil raw material of the repellent mosquitos and flies according to mass parts meter, including with the following group
Point：2 parts of 2 parts of peppermint, 2 parts of eucalyptus, 3 parts of fly expelling plum, 2 parts of 1.5 part, month tangerine of fish pelargonium and wormwood.Concrete preparation method include with
Lower step：
1) peppermint, eucalyptus, fly expelling plum, fish pelargonium, moon tangerine, wormwood were gathered into Hua Heye before it is bloomed, is cleaned up
As raw material；
2) clean each raw material is dried in the air to drying, each raw material after cleaning dries in the air when being dried, keeps air humidity to exist
Between 2.5% -5%, while speed is maintained the circulation of air between 0.2m/s -0.5m/s, then according to the mass ratio is mixed
Close；
3) the quality distilled water such as addition and raw material in mixed raw material, is then put in fractionating device, at 60-85 DEG C
Under the conditions of carry out fractionation extraction, obtain extract；
4) to obtain in extract add etc. quality sodium chloride extracted, then filter to take top oil reservoir, get product
Plants essential oil, and final oil yield is 2.5%.
In example IV：In its raw material, peppermint, fish pelargonium, the mass ratio of moon tangerine are 4:3:4, in its raw material, by fly
Plum, the mass ratio of wormwood are 3:2, in its raw material, peppermint, the mass ratio of eucalyptus are 1:1.
Contain peppermint oil, menthol, menthones in peppermint, peppermint oil, menthol, menthones easily dissipate, to a certain extent can
Drive away mosquito and be pharmaceutically widely used in wind dispelling, anti-corrosion, anti-inflammatory, analgesia, antipruritic, stomach invigorating etc. including fly.
Eucalyptus, also known as You Jiali trees, is the general designation of Myrtaceae eucalyptus plant.Leaf contains aromatic oil, has sterilized mosquito repellent to make
With.
Fly expelling plum, belongs to Verenaceae shrub, the sensitive smell of mosquitos and flies is volatilized in its branches and leaves and flower, with very strong
Expulsion mosquitos and flies effect.
Fish pelargonium, originates in Africa south, containing active ingredients such as citronellol, citrals, there is the effects such as sterilization, expelling parasite.
Month tangerine has functions that mosquito repellent fly containing medicinal ingredients such as linalools.
Wormwood, composite family artemisia, with a kind of special fragrance, this special fragrance has functions that mosquito dispersing.
Application experiment：
The principle and feature of the present invention are described below, example is served only for explaining the present invention, is not intended to limit
Determine the scope of the present invention.
1.1 are local capture for examination insect and culex；
1.2 trial target：The plants essential oil 1.2g that aforementioned four embodiment is extracted；
1.3 animal protection test：
18-22g healthy mices 4 (male and female half and half) are selected, the four-footed of small white mouse is fixed on little three-ply board, cut abdomen
Portion's fine hair, is then uniformly coated with tried essential oil on the circle of diameter 20mm, then respectively small white mouse is put into into 500mm*
In the culex cage of 500mm*500mm, there is female mosquito 50 per cage, park 3min, and observed and recorded small white mouse belly bite by mosquitos number,
And set control group.
1.4 human bodies bite observation
In 2 circles that 2 diameter 2cm delimited by test arm, and plants essential oil (non-painting essential oil position use is smeared in circle
Cloth is protected) arm is parked into 3min in cage, observe and record by bite by mosquitos number, if control group.
Result of the test：Two essential oils experiment in example 1 and example 2, each essential oil is tested by five repetitions, smeared
, without biting, control group is all by bite by mosquitos for the small white mouse of essential oil and test arm.
The invention provides a kind of plants essential oil, the plants essential oil set peppermint, eucalyptus, fly expelling plum, fish pelargonium, moon tangerine,
The advantage of six kinds of natural materials of wormwood, according to specific ratio, by fractionation mode plant essence is extracted, and recovery rate is higher, can
Up to 1.8-3.2%.Peppermint, eucalyptus, fly expelling plum and moon tangerine all have functions that to expel mosquitos and flies, fish pelargonium and wormwood have expelling parasite
Effect.Several essential oils are combined together, energy repellent mosquitos and flies, reduce the harassing and wrecking to people and animals and bite, and safely and effectively, nothing is appointed
What toxic and side effect.Additionally, the input cost of the technology of the present invention is low, it is simple easily operated.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding can carry out various changes, modification, replacement to these embodiments without departing from the principles and spirit of the present invention
And modification, the scope of the present invention be defined by the appended.
Claims (7)
1. a kind of repellent mosquitos and flies plants essential oil, it is characterised in that：The plants essential oil raw material of the repellent mosquitos and flies is according to mass parts meter, bag
Include following components：Peppermint 1-3 parts, eucalyptus 2-5 parts, fly expelling plum 2-4 parts, fish pelargonium 1-3 parts, moon tangerine 1-3 parts and wormwood 2-4 parts.
2. a kind of preparation method of repellent mosquitos and flies plants essential oil according to claim 1, comprises the steps：
1) peppermint plucked, eucalyptus, fly expelling plum, fish pelargonium, moon tangerine and wormwood are cleaned, as raw material；
2) each raw material after cleaning is dried in the air to drying, then according to quality parts ratio mixing；
3) the quality distilled water such as addition and raw material in mixed raw material, is then put in fractionating device, in 60-85 DEG C of bar
Fractionation extraction is carried out under part, extract is obtained；
4) extracted to the sodium chloride for obtaining the quality such as addition in extract, then filtered to take top oil reservoir, got product plant
Thing essential oil.
3. a kind of repellent mosquitos and flies plants essential oil according to claim 1, it is characterised in that：In its raw material, peppermint, India
Certain herbaceous plants with big flowers, the mass ratio of moon tangerine are 6:2:1—2:1:Between 1.
4. a kind of repellent mosquitos and flies plants essential oil according to claim 1, it is characterised in that：In its raw material, fly expelling plum, wormwood
Mass ratio be 1:2—2：Between 1.
5. a kind of repellent mosquitos and flies plants essential oil according to claim 1, it is characterised in that：In its raw material, peppermint, eucalyptus matter
Amount is than being 1:1—1：Between 2.
6. the preparation method of a kind of repellent mosquitos and flies plants essential oil according to claim 2, it is characterised in that：In its raw material,
Peppermint, eucalyptus, fly expelling plum, fish pelargonium, moon tangerine and wormwood are plucked before the flowers are in blossom.
7. the preparation method of a kind of repellent mosquitos and flies plants essential oil according to claim 2, it is characterised in that：It is thin after cleaning
Lotus, eucalyptus, fly expelling plum, fish pelargonium, moon tangerine and wormwood are dried in the air when being dried, and keep air humidity between 2.5% -5%, while protecting
Air passage rates are held between 0.2m/s -0.5m/s.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610916666.0A CN106635415A (en) | 2016-10-21 | 2016-10-21 | Fly-repelling vegetable essential oil and preparation method and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610916666.0A CN106635415A (en) | 2016-10-21 | 2016-10-21 | Fly-repelling vegetable essential oil and preparation method and application thereof |
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| CN106635415A true CN106635415A (en) | 2017-05-10 |
Family
ID=58855465
Family Applications (1)
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|---|---|---|---|
| CN201610916666.0A Pending CN106635415A (en) | 2016-10-21 | 2016-10-21 | Fly-repelling vegetable essential oil and preparation method and application thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108456594A (en) * | 2018-05-07 | 2018-08-28 | 南召留山岭南艾叶制品有限公司 | A kind of extracting method of high yield wormwood essential oil |
| CN111296507A (en) * | 2020-03-19 | 2020-06-19 | 江苏瑞丰科技实业有限公司 | Efficient spray for killing mosquitoes and flies |
| CN112680280A (en) * | 2020-12-28 | 2021-04-20 | 江苏天晟药业股份有限公司 | Preparation method of sedative composite volatile oil |
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|---|---|---|---|---|
| US6337071B1 (en) * | 1996-06-21 | 2002-01-08 | William Mitchell Molyneux | Mosquito and/or flea control |
| CN105230685A (en) * | 2015-11-06 | 2016-01-13 | 西南大学 | Herbaceous plant essential oil composition with mosquito repelling effect |
| CN105687426A (en) * | 2016-03-18 | 2016-06-22 | 覃淑兰 | Tranquilizing plant essential oil and preparation method and application thereof |
-
2016
- 2016-10-21 CN CN201610916666.0A patent/CN106635415A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6337071B1 (en) * | 1996-06-21 | 2002-01-08 | William Mitchell Molyneux | Mosquito and/or flea control |
| CN105230685A (en) * | 2015-11-06 | 2016-01-13 | 西南大学 | Herbaceous plant essential oil composition with mosquito repelling effect |
| CN105687426A (en) * | 2016-03-18 | 2016-06-22 | 覃淑兰 | Tranquilizing plant essential oil and preparation method and application thereof |
Non-Patent Citations (2)
| Title |
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| 杨继彰: "《药剂学-基本原理及操作》", 30 April 1959, 上海科学技术出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108456594A (en) * | 2018-05-07 | 2018-08-28 | 南召留山岭南艾叶制品有限公司 | A kind of extracting method of high yield wormwood essential oil |
| CN111296507A (en) * | 2020-03-19 | 2020-06-19 | 江苏瑞丰科技实业有限公司 | Efficient spray for killing mosquitoes and flies |
| CN112680280A (en) * | 2020-12-28 | 2021-04-20 | 江苏天晟药业股份有限公司 | Preparation method of sedative composite volatile oil |
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