CN104524488A - Extract essence pill and preparation method thereof - Google Patents
Extract essence pill and preparation method thereof Download PDFInfo
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- CN104524488A CN104524488A CN201410731931.9A CN201410731931A CN104524488A CN 104524488 A CN104524488 A CN 104524488A CN 201410731931 A CN201410731931 A CN 201410731931A CN 104524488 A CN104524488 A CN 104524488A
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Abstract
The invention discloses an extract essence pill and a preparation method thereof. The method comprises the following steps: taking 50g of ginger, 50g of Herba Moslae, 80g of Citron Fruit, 20g of Chinese magnoliavine, 20g of Rubus idaeus, 40g of Polygonum multiflorum, 30g of Malaytea Scurfpea Fruit, 20g of walnut kernel, 20g of Poria cocos, 10g of ginseng, 40g of wolfberry fruit, 30g of (stir-fried) lotus seed, 30g of oyster, 10g of Corn Cervi Pantotrichum, 40g of (stir-fried) Semen Euryales, 30g of Chinese yam and 30g of Fructus Rosae Laevigatae, crushing to form coarse powder, putting the coarse powder in a circulating ultrasonic extraction device, adding water, germanium powder and tween60, carrying out ultrasonic extraction, carrying out jet spray drying to prepare nanometer extraction powder, and carrying out honey processing to prepare the extract essence pill. The extract essence pill is used for treating kidney deficiency, essence damage, impotence, premature ejaculation, weak body, hypodynamia and soreness of loins and knees, has substantial curative effects than extract essence pills in the market, and has a good effect.
Description
Technical field
The present invention relates to the field of Chinese medicines, be specifically related to celestial ball of a kind of extraction and preparation method thereof.
Background technology
Extract celestial ball tonifying the kidney to consolidate the essence, replenishing QI to invigorate the spleen, for deficiency of kidney essence, impotence and premature ejaculation, weak weak, soreness of the waist and knees.The celestial ball of commercially available extraction is due to prescription and technological reason, and curative effect is not satisfactory, and preparation adopts traditional handicraft preparation, there is the shortcoming that curative effect is low.
Summary of the invention
The present invention for overcoming above-mentioned deficiency, celestial ball of the extraction that provides a kind of curative effect high and preparation method thereof.
Invention embodiment is as follows:
Get Rhizoma Zingiberis Recens 50g, Herba Moslae 50g, Fructus Citri 80g, Fructus Schisandrae Chinensis 20g, Fructus Rubi 20g, Radix Polygoni Multiflori 40g, Fructus Psoraleae 30g, Semen Juglandis 20g, Poria 20g, Radix Ginseng 10g, Fructus Lycii 40g, Semen Nelumbinis (stir-fry) 30g, Concha Ostreae 30g, Cornu Cervi Pantotrichum 10g, Semen Euryales (stir-fry) 40g, Rhizoma Dioscoreae 30g, Fructus Rosae Laevigatae 30g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 5400g water, 4 ~ 6g germanium powder, 6 ~ 8g polysorbate60, select supersonic frequency 50 ~ 60KHz, pressure 0.3 ~ 0.5 Mpa extracts 30 minutes, uses 80 mesh screen, obtains extracting solution; Getting extracting solution puts in jet spray dryer, and control inlet temperature 40 ~ 50 DEG C, pressure 0.02 ~ 0.04 Mpa, 400 ~ 600 meters per second of flow velocity, obtains nanometer extract powder; Every 100g nanometer extract powder refined honey 20-30g adds appropriate water pill, dry, makes water-honeyed pill, the celestial ball of obtained extraction.
The raw material standards that above-mentioned embodiment is mentioned is as follows:
Rhizoma Zingiberis Recens: China's coastal port one ministerial standard.This product is the fresh rhizome of zingiber Zingiber officinale Rosc..Autumn, season in winter two excavate, removing fibrous root and silt.
Herba Moslae: China's coastal port one ministerial standard.This product is the ten dry aerial partss of labiate Mosla chinensis Maxim. Misla chinensis Maxim. or Mosla chinensis Maxim.cv.Jiangxiangru Mosla chinensis ' Jiangxiangru '.The former practises title " Chinese mosla ", and the latter practises title " Mosla chinensis Maxim.cv.Jiangxiangru ".Luxuriant, the colored flower of stem and leaf in summer is selected fine day and is tapped, and removing impurity, dries in the shade.
Fructus Citri: China's coastal port one ministerial standard.This product is the dry mature fruit of rutaceae structure rafter Citrus medica L. or fragrant circle Citruswilsonii Tanaka.Gather during fruit maturation in autumn, take advantage of fresh slices, dry or cold drying.Fragrant circle also can be whole or to after cuing open two halves, dries or cold drying.
Fructus Schisandrae Chinensis: China's coastal port one ministerial standard.This product is magnoliaceae schisandra Schisandra chfnensis(Turcz.) dry mature fruit of Baill., practise and claim " Radix Schisandrae Bicoloris ".Pluck during fruit maturation in autumn, dry or dry after steaming, removing carpopodium and impurity.
Fructus Rubi: China's coastal port one ministerial standard.This product is the dry fruit of rosaceous plant rubus chingii Hu Rubus chingii Hu.Gather when early summer fruit is greenish-yellow by green change, except destemming, leaf, put in boiling water and slightly scald or slightly steam, take out, dry.
Radix Polygoni Multiflori: China's coastal port one ministerial standard.This product is the dried root of polygonum multiflorum thunb Polygonum multiflorumThunb.Autumn, winter two excavate when season, leaf was withered, two ends of pruning. clean, individual greatly be cut into block, dry.
Fructus Psoraleae: China's coastal port one ministerial standard.This product is the dry mature fruit of legumes psoraleae Psoralea corylifolia L..To gather during fruit maturation in autumn infructescence, dry, rub fruit, removing impurity.
Semen Juglandis: China's coastal port one ministerial standard.This product is the dry mature seed of juglandaceae plant Semen Juglandis Juglans regia L..Gather during fruit maturation in autumn, removing meat peel, dries, then removes nucleocapsid and wooden barrier film.
Poria: China's coastal port one ministerial standard.This product is On Polyporaceae Poria Poria cocos(Schw.) dry sclerotia of Wolf.Excavate more than the 7-9 month, dig out rear removing silt, bank up after " diaphoresis ", spread out and dry in the air to dry tack free, then " diaphoresis ", after extremely now scatter and disappear in wrinkle, the large portion of internal moisture for several times repeatedly, dry in the shade, be called " Poria "; Or fresh Poria is pressed different parts cutting, cloudy in, be called " Cortex Sclerotii Poriae " and " Poria block ".
Radix Ginseng: China's coastal port one ministerial standard.This product is the dry root and rhizome of Araliaceae Radix Ginseng Panax ginseng C.A.Mey..Excavate more than autumn, clean through drying or drying.Cultivation also known as " Park Ginseng "; Sowing under mountain forest wild state self-sow also known as " Panax Ginseng ", practise and claim " seed sea ".
Fructus Lycii: China's coastal port one ministerial standard.This product is the dry mature fruit of plant of Solanaceae lycium barbarum Lycium barbarum L..Summer, autumn two gather when season, fruit took on a red color, hot-air seasoning, removing carpopodium, or dry in the air to rhicnosis, dry, removing carpopodium.
Semen Nelumbinis (stir-fry): China's coastal port one ministerial standard.This product is the dry mature seed of nymphaeaceae plant lotus Nelumbo nucifera Gaertn..Tap Receptaculum Nelumbinis during fruit maturation in autumn, take out fruit, removing peel, dry.
Concha Ostreae: China's coastal port one ministerial standard.This product is the shell of Ostreidae animal long Concha Ostreae Ostrea gigas Thunberg, Dalian Bay Concha Ostreae Ostrea talienwhanensis Crosse or Crassostrea rivularis Ostrear riv-ularis Gould.The whole year all can gather, fleshing, cleans, dries.
Cornu Cervi Pantotrichum: China's coastal port one ministerial standard.This product is the young horn of the unossified close raw fine hair of stag of animal in deer family Cervus nippon Temminck Cervus nippon Temminck or Cervus elaphus linnaeus Cervus elaphus Linnaeus.The former practises title " pilose antler of sika ", and the latter practises title " cervus elaphus linnaeus ".Cornu Cervi Pantotrichum got by summer, Qiu Erji saw, after processing, dries in the shade or dries.
Semen Euryales (stir-fry): China's coastal port one ministerial standard.This product is the dry mature kernal of nymphaeaceae plant Gorgon euryale Euryale ferox Salisb..Time of the year when autumn changes into winter gathers mature fruit, and removing peel, takes out seed, cleans, then removes duricrust (episperm), dry.
Rhizoma Dioscoreae: China's coastal port one ministerial standard.This product is the dry rhizome of Dioscoreaceae plant Rhizoma Dioscoreae Dioscorea opposita Thunb..Winter, stem and leaf was excavated after withering, and cut macroradical head, cleaned, and removing crust and fibrous root are dry; Also have and select loose straight dry Rhizoma Dioscoreae, put in clear water, be dipped into without the dry heart, vexed, trim two ends, be twisted into plank cylindric, dry, polishing, practise and claim " light yam ".
Fructus Rosae Laevigatae: China's coastal port one ministerial standard.This product is the dry mature fruit of rosaceous plant Fructus Rosae Laevigatae Rosa laevigata Michx..Gather when the 10-11 month, fruit maturation reddened, dry. except deburring.
Germanium powder: germanium dioxide: No. CAS: 1310-53-8: industry standard: lark prestige Science and Technology Ltd.;
Polysorbate60: Chinese Pharmacopoeia version two ministerial standard in 2010;
The raw material more than extracted used by celestial ball all can be bought from pharmaceuticals and obtain, and is not limited to typical production producer, all can be used to implement the present invention program as long as meet quality standard.
The key equipment that foregoing invention embodiment is mentioned is as follows:
Circulating ultrasonic machine: supersonic frequency 20 ~ 100KHz,
(typical production producer: Beijing Hongxianglong Biotechnology Development Co., Ltd)
Jet spray dryer: inlet temperature scope 30 ~ 70 DEG C, 300 ~ 900 meters per second of effluxvelocity scope;
(typical production producer: Nai Nuo bio tech ltd, Beijing)
The raw material more than extracted used by celestial ball all can be bought from pharmaceuticals and obtain, and all can be used to implement the present invention program as long as meet national standard.
In foregoing invention scheme, term used is pharmacy proprietary term, as " decompression " etc. all defers to Chinese Pharmacopoeia regulation and pharmaceutical practice of being correlated with.
Unit g in the present invention also can be other weight portion, does not affect the enforcement of the present invention program.
Equipment Market described in the present invention program all has sale, is not limited to typical production producer, as long as technical specification can reach requirement, all can be used to realize the present invention.
Detailed description of the invention
Specific embodiments of the invention 1
Get Rhizoma Zingiberis Recens 50g, Herba Moslae 50g, Fructus Citri 80g, Fructus Schisandrae Chinensis 20g, Fructus Rubi 20g, Radix Polygoni Multiflori 40g, Fructus Psoraleae 30g, Semen Juglandis 20g, Poria 20g, Radix Ginseng 10g, Fructus Lycii 40g, Semen Nelumbinis (stir-fry) 30g, Concha Ostreae 30g, Cornu Cervi Pantotrichum 10g, Semen Euryales (stir-fry) 40g, Rhizoma Dioscoreae 30g, Fructus Rosae Laevigatae 30g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 5400g water, 4g germanium powder, 6g polysorbate60, select supersonic frequency 50KHz, pressure 0.3Mpa extracts 30 minutes, uses 80 mesh screen, obtains extracting solution; Getting extracting solution puts in jet spray dryer, and control inlet temperature 40 DEG C, pressure 0.02Mpa, 400 meters per second of flow velocity, obtains nanometer extract powder; Every 100g nanometer extract powder refined honey 20g adds appropriate water pill, dry, makes water-honeyed pill, the celestial ball of obtained extraction.
Specific embodiments of the invention 2
Get Rhizoma Zingiberis Recens 50g, Herba Moslae 50g, Fructus Citri 80g, Fructus Schisandrae Chinensis 20g, Fructus Rubi 20g, Radix Polygoni Multiflori 40g, Fructus Psoraleae 30g, Semen Juglandis 20g, Poria 20g, Radix Ginseng 10g, Fructus Lycii 40g, Semen Nelumbinis (stir-fry) 30g, Concha Ostreae 30g, Cornu Cervi Pantotrichum 10g, Semen Euryales (stir-fry) 40g, Rhizoma Dioscoreae 30g, Fructus Rosae Laevigatae 30g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 5400g water, 6g germanium powder, 8g polysorbate60, select supersonic frequency 60KHz, pressure 0.5 Mpa extracts 30 minutes, uses 80 mesh screen, obtains extracting solution; Getting extracting solution puts in jet spray dryer, and control inlet temperature 50 DEG C, pressure 0.04 Mpa, 600 meters per second of flow velocity, obtains nanometer extract powder; Every 100g nanometer extract powder refined honey 30g adds appropriate water pill, dry, makes water-honeyed pill, the celestial ball of obtained extraction.
Specific embodiments of the invention 3
Get Rhizoma Zingiberis Recens 50g, Herba Moslae 50g, Fructus Citri 80g, Fructus Schisandrae Chinensis 20g, Fructus Rubi 20g, Radix Polygoni Multiflori 40g, Fructus Psoraleae 30g, Semen Juglandis 20g, Poria 20g, Radix Ginseng 10g, Fructus Lycii 40g, Semen Nelumbinis (stir-fry) 30g, Concha Ostreae 30g, Cornu Cervi Pantotrichum 10g, Semen Euryales (stir-fry) 40g, Rhizoma Dioscoreae 30g, Fructus Rosae Laevigatae 30g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 5400g water, 5g germanium powder, 7g polysorbate60, select supersonic frequency 55KHz, pressure 0.4Mpa extracts 30 minutes, uses 80 mesh screen, obtains extracting solution; Getting extracting solution puts in jet spray dryer, and control inlet temperature 45 DEG C, pressure 0.03Mpa, 500 meters per second of flow velocity, obtains nanometer extract powder; Every 100g nanometer extract powder refined honey 25g adds appropriate water pill, dry, makes water-honeyed pill, the celestial ball of obtained extraction.
Above embodiment illustrates, adopts the extreme condition of embodiment of the present invention and optimal conditions all can make the celestial ball of extraction.Actual effect of the present invention is investigated below with the celestial ball of the extraction that embodiment 3 is obtained:
(1) embodiment 3 extracts celestial ball and the celestial pill for curing deficiency of kidney essence of commercially available extraction, and impotence and premature ejaculation is weak weak, soreness of the waist and knees clinical observation on the therapeutic effect
1 case scenario
Statistics outpatient service and inpatient, observe deficiency of kidney essence, impotence and premature ejaculation altogether, weak weak, soreness of the waist and knees case 104 example, 47 years old mean age.Patient is divided into two groups, test group is taken embodiment 3 and is extracted celestial ball, and matched group takes the celestial ball of tradition extraction.
2 efficacy assessment standards
According to new Chinese medicine guideline of clinical investigations tcm syndrome curative effect determinate standard:
Cure: tcm clinical practice symptom, sign disappear or substantially disappear, syndrome integral reduces >=95%.
Effective: tcm clinical practice symptom, sign are obviously improved, syndrome integral reduces >=70%.
Effective: tcm clinical practice symptom, sign all take a favorable turn, syndrome integral reduces >=30%.
Invalid: tcm clinical practice symptom, sign are all not improved or increase the weight of, syndrome integral reduces < 30%.
Computing formula: [before (before treatment the rear integration of integration-treatment) ÷ treatment integration] × 100%.
3 clinical observation result
Table 1 embodiment 3 extracts celestial ball and the celestial ball clinical efficacy contrast of commercially available extraction
Above-mentioned clinical observation on the therapeutic effect result shows, the celestial ball of extraction prepared by the present invention is treating deficiency of kidney essence, impotence and premature ejaculation, weak weak, during soreness of the waist and knees, evident in efficacy higher than the celestial ball of commercially available extraction, p < 0.05.
Claims (3)
1. kind for the treatment of deficiency of kidney essence, impotence and premature ejaculation, weak weak, the Chinese medicine of soreness of the waist and knees disease, it is characterized in that getting Rhizoma Zingiberis Recens 50g, Herba Moslae 50g, Fructus Citri 80g, Fructus Schisandrae Chinensis 20g, Fructus Rubi 20g, Radix Polygoni Multiflori 40g, Fructus Psoraleae 30g, Semen Juglandis 20g, Poria 20g, Radix Ginseng 10g, Fructus Lycii 40g, Semen Nelumbinis (stir-fry) 30g, Concha Ostreae 30g, Cornu Cervi Pantotrichum 10g, Semen Euryales (stir-fry) 40g, Rhizoma Dioscoreae 30g, Fructus Rosae Laevigatae 30g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 5400g water, 4 ~ 6g germanium powder, 6 ~ 8g polysorbate60, select supersonic frequency 50 ~ 60KHz, pressure 0.3 ~ 0.5 Mpa extracts 30 minutes, use 80 mesh screen, obtain extracting solution, getting extracting solution puts in jet spray dryer, and control inlet temperature 40 ~ 50 DEG C, pressure 0.02 ~ 0.04 Mpa, 400 ~ 600 meters per second of flow velocity, obtains nanometer extract powder, every 100g nanometer extract powder refined honey 20-30g adds appropriate water pill, dry, makes water-honeyed pill, the celestial ball of obtained extraction.
2. the preparation method of Chinese medicine according to claim 1, it is characterized in that getting Rhizoma Zingiberis Recens 50g, Herba Moslae 50g, Fructus Citri 80g, Fructus Schisandrae Chinensis 20g, Fructus Rubi 20g, Radix Polygoni Multiflori 40g, Fructus Psoraleae 30g, Semen Juglandis 20g, Poria 20g, Radix Ginseng 10g, Fructus Lycii 40g, Semen Nelumbinis (stir-fry) 30g, Concha Ostreae 30g, Cornu Cervi Pantotrichum 10g, Semen Euryales (stir-fry) 40g, Rhizoma Dioscoreae 30g, Fructus Rosae Laevigatae 30g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 5400g water, 4 ~ 6g germanium powder, 6 ~ 8g polysorbate60, select supersonic frequency 50 ~ 60KHz, pressure 0.3 ~ 0.5 Mpa extracts 30 minutes, use 80 mesh screen, obtain extracting solution, getting extracting solution puts in jet spray dryer, and control inlet temperature 40 ~ 50 DEG C, pressure 0.02 ~ 0.04 Mpa, 400 ~ 600 meters per second of flow velocity, obtains nanometer extract powder, every 100g nanometer extract powder refined honey 20-30g adds appropriate water pill, dry, makes water-honeyed pill, the celestial ball of obtained extraction.
3. the preparation method of Chinese medicine according to claim 1, it is characterized in that getting Rhizoma Zingiberis Recens 50g, Herba Moslae 50g, Fructus Citri 80g, Fructus Schisandrae Chinensis 20g, Fructus Rubi 20g, Radix Polygoni Multiflori 40g, Fructus Psoraleae 30g, Semen Juglandis 20g, Poria 20g, Radix Ginseng 10g, Fructus Lycii 40g, Semen Nelumbinis (stir-fry) 30g, Concha Ostreae 30g, Cornu Cervi Pantotrichum 10g, Semen Euryales (stir-fry) 40g, Rhizoma Dioscoreae 30g, Fructus Rosae Laevigatae 30g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 5400g water, 5g germanium powder, 7g polysorbate60, select supersonic frequency 55KHz, pressure 0.4Mpa extracts 30 minutes, use 80 mesh screen, obtain extracting solution, getting extracting solution puts in jet spray dryer, and control inlet temperature 45 DEG C, pressure 0.03Mpa, 500 meters per second of flow velocity, obtains nanometer extract powder, every 100g nanometer extract powder refined honey 25g adds appropriate water pill, dry, makes water-honeyed pill, the celestial ball of obtained extraction.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410731931.9A CN104524488A (en) | 2014-12-06 | 2014-12-06 | Extract essence pill and preparation method thereof |
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| CN201410731931.9A CN104524488A (en) | 2014-12-06 | 2014-12-06 | Extract essence pill and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107496648A (en) * | 2017-08-31 | 2017-12-22 | 北京摇太阳生物科技有限公司 | A kind of function of male that strengthens improves the antifatigue diet therapy formula of fecundity relieving alcoholism and protecting liver |
| CN108283701A (en) * | 2018-04-12 | 2018-07-17 | 李军 | A kind of drug and preparation method thereof for promoting male's sexual and treating impotence |
-
2014
- 2014-12-06 CN CN201410731931.9A patent/CN104524488A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107496648A (en) * | 2017-08-31 | 2017-12-22 | 北京摇太阳生物科技有限公司 | A kind of function of male that strengthens improves the antifatigue diet therapy formula of fecundity relieving alcoholism and protecting liver |
| CN108283701A (en) * | 2018-04-12 | 2018-07-17 | 李军 | A kind of drug and preparation method thereof for promoting male's sexual and treating impotence |
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Application publication date: 20150422 |
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| WW01 | Invention patent application withdrawn after publication |