CN104383516A - Shaoyang cold treatment granules and preparation method for same - Google Patents
Shaoyang cold treatment granules and preparation method for same Download PDFInfo
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- CN104383516A CN104383516A CN201410760589.5A CN201410760589A CN104383516A CN 104383516 A CN104383516 A CN 104383516A CN 201410760589 A CN201410760589 A CN 201410760589A CN 104383516 A CN104383516 A CN 104383516A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/25—Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
- A61K36/258—Panax (ginseng)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/282—Artemisia, e.g. wormwood or sagebrush
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/539—Scutellaria (skullcap)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/66—Papaveraceae (Poppy family), e.g. bloodroot
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/72—Rhamnaceae (Buckthorn family), e.g. buckthorn, chewstick or umbrella-tree
- A61K36/725—Ziziphus, e.g. jujube
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/888—Araceae (Arum family), e.g. caladium, calla lily or skunk cabbage
- A61K36/8888—Pinellia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8962—Allium, e.g. garden onion, leek, garlic or chives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/906—Zingiberaceae (Ginger family)
- A61K36/9068—Zingiber, e.g. garden ginger
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
- A61K9/1605—Excipients; Inactive ingredients
- A61K9/1629—Organic macromolecular compounds
- A61K9/1652—Polysaccharides, e.g. alginate, cellulose derivatives; Cyclodextrin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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Abstract
The invention discloses Shaoyang cold treatment granules and a preparation method for the same. The preparation method is characterized by comprising the following steps: crushing 80 grams of allium macrostemon, 28 grams of corydalis decumbentis, 206 grams of scutellaria baicalensis, 206 grams of pinellia ternata, 138 grams of dried ginger, 138 grams of jujubes, 69 grams of ginseng and 206 grams of sweet wormwood herb into coarse powder, loading the coarse powder in a circular ultrasonic extractor, adding water, germanium powder and tween 60, performing ultrasonic extraction and jet spray drying to prepare nanometer powdery extract, and adding lactose and dextrin to prepare the Shaoyang cold treatment granules. The Shaoyang cold treatment granules are used for treating acute upper respiratory tract infection, and has remarkable curative effects better than those of commercially available Shaoyang cold treatment granules, and the effects are good.
Description
Technical field
The present invention relates to the field of Chinese medicines, be specifically related to a kind of few positive cold granules and preparation method thereof.
Background technology
Few positive cold granules is strengthened body resistance and relieveeed exterior syndrome, heat clearing away and in.Be applicable to acute upper respiratory tract infection, alternate attack of chill and fever, bitter taste in the mouth and dry throat, have a dizzy spell, loss of appetite, vexed nauseating.Commercially available few positive cold granules is due to prescription and technological reason, and curative effect is not satisfactory, and preparation adopts traditional handicraft preparation, there is the shortcoming that curative effect is low.
Summary of the invention
The present invention for overcoming above-mentioned deficiency, few positive cold granules providing a kind of curative effect high and preparation method thereof.
Invention embodiment is as follows:
Get Bulbus Allii Macrostemonis 80g, Rhizoma Corydalis Decumbentis 28g, Radix Scutellariae 206g, the Rhizoma Pinelliae 206, Rhizoma Zingiberis 138, Fructus Jujubae 138, Radix Ginseng 69g, Herba Artemisiae Annuae 206g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 10710g water, 4 ~ 6g germanium powder, 6 ~ 8g polysorbate60, select supersonic frequency 50 ~ 60KHz, pressure 0.3 ~ 0.5 Mpa extracts 30 minutes, use 80 mesh screen, obtain extracting solution; Getting extracting solution puts in jet spray dryer, and control inlet temperature 40 ~ 50 DEG C, pressure 0.02 ~ 0.04 Mpa, 400 ~ 600 meters per second of flow velocity, obtains nanometer extract powder; Get extract powder and add lactose 400g, dextrin 100g, use water wet granulation, 60 DEG C of dryings, granulate, adds Pulvis Talci 15g, mixing, obtained few positive cold granules.
The raw material standards that above-mentioned embodiment is mentioned is as follows:
Bulbus Allii Macrostemonis: China's coastal port one ministerial standard.This product is the dry bulb of liliaceous plant Allium macrostemon Allium macrostemon Bge. or Chinese onion Allium chinensis G.Don.Summer, Qiu Erji dig, and clean, removing fibrous root, steam thoroughly or put in boiling water and scald thoroughly, dry.
Rhizoma Corydalis Decumbentis: China's coastal port one ministerial standard.This product is bloodroot Hotseason grow Corxdalis decumbens(Thunb.) dry tuber of Pers..The spring or early summer is excavated after emerging, removing stem, leaf and fibrous root, cleaning, drying.
Radix Scutellariae: China's coastal port one ministerial standard.This product is the dry root of labiate Radix Scutellariae Scutellaria baicalensis Georgi.Spring, Qiu Erji excavate, and removing fibrous root and silt, hit rough bark after solarization, dry.
The Rhizoma Pinelliae: China's coastal port one ministerial standard.This product is aroid Rhizoma Pinelliae Pinellia ternata(Thunb.) dry tuber of Breit..Summer, Qiu Erji excavate, and clean, and removing crust and fibrous root, dry.
Rhizoma Zingiberis: China's coastal port one ministerial standard.This product is the dry rhizome of zingiber Zingiber o.officinale Rose..Winter excavates, and removing fibrous root and silt, dry or cold drying.Take advantage of fresh slices to dry or cold drying person is called " dried ginger slice ".
Fructus Jujubae: China's coastal port one ministerial standard.This product is the dry mature fruit of Rhamnaceae plant Fructus Jujubae ZiziPhus jujuba Mill..Gather during fruit maturation in autumn, dry.
Radix Ginseng: China's coastal port one ministerial standard.This product is the dry root and rhizome of Araliaceae Radix Ginseng Panax ginseng C.A.Mey..Excavate more than autumn, clean through drying or drying.Cultivation also known as " Park Ginseng "; Sowing under mountain forest wild state self-sow also known as " Panax Ginseng ", practise and claim " seed sea ".
Herba Artemisiae Annuae: China's coastal port one ministerial standard.This product is the dry aerial parts of feverfew Herba Artemisiae annuae Artemisia annua L..Tap when autumn is spent in full bloom, remove old stem, dry in the shade.
Germanium powder: germanium dioxide: No. CAS: 1310-53-8: industry standard: lark prestige Science and Technology Ltd.;
Polysorbate60: Chinese Pharmacopoeia version two ministerial standard in 2010;
Lactose: Chinese Pharmacopoeia version two ministerial standard in 2010;
Dextrin: Chinese Pharmacopoeia version two ministerial standard in 2010;
Pulvis Talci: Chinese Pharmacopoeia version one ministerial standard in 2010;
More than few raw material used by positive cold granules all can be bought from pharmaceuticals and obtain, and is not limited to typical production producer, all can be used to implement the present invention program as long as meet quality standard.
The key equipment that foregoing invention embodiment is mentioned is as follows:
Circulating ultrasonic machine: supersonic frequency 20 ~ 100KHz,
(typical production producer: Beijing Hongxianglong Biotechnology Development Co., Ltd)
Jet spray dryer: inlet temperature scope 30 ~ 70 DEG C, 300 ~ 900 meters per second of effluxvelocity scope;
(typical production producer: Nai Nuo bio tech ltd, Beijing)
More than few raw material used by positive cold granules all can be bought from pharmaceuticals and obtain, and all can be used to implement the present invention program as long as meet national standard.
In foregoing invention scheme, term used is pharmacy proprietary term, as " decompression " etc. all defers to Chinese Pharmacopoeia regulation and pharmaceutical practice of being correlated with.
Unit g in the present invention also can be other weight portion, does not affect the enforcement of the present invention program.
Equipment Market described in the present invention program all has sale, is not limited to typical production producer, as long as technical specification can reach requirement, all can be used to realize the present invention.
Detailed description of the invention
Specific embodiments of the invention 1
Get Bulbus Allii Macrostemonis 80g, Rhizoma Corydalis Decumbentis 28g, Radix Scutellariae 206g, the Rhizoma Pinelliae 206, Rhizoma Zingiberis 138, Fructus Jujubae 138, Radix Ginseng 69g, Herba Artemisiae Annuae 206g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 10710g water, 4g germanium powder, 6g polysorbate60, select supersonic frequency 50KHz, pressure 0.3Mpa extracts 30 minutes, use 80 mesh screen, obtain extracting solution; Getting extracting solution puts in jet spray dryer, and control inlet temperature 40 DEG C, pressure 0.02Mpa, 400 meters per second of flow velocity, obtains nanometer extract powder; Get extract powder and add lactose 400g, dextrin 100g, use water wet granulation, 60 DEG C of dryings, granulate, adds Pulvis Talci 15g, mixing, obtained few positive cold granules.
Specific embodiments of the invention 2
Get Bulbus Allii Macrostemonis 80g, Rhizoma Corydalis Decumbentis 28g, Radix Scutellariae 206g, the Rhizoma Pinelliae 206, Rhizoma Zingiberis 138, Fructus Jujubae 138, Radix Ginseng 69g, Herba Artemisiae Annuae 206g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 10710g water, 6g germanium powder, 8g polysorbate60, select supersonic frequency 60KHz, pressure 0.5 Mpa extracts 30 minutes, use 80 mesh screen, obtain extracting solution; Getting extracting solution puts in jet spray dryer, and control inlet temperature 50 DEG C, pressure 0.04 Mpa, 600 meters per second of flow velocity, obtains nanometer extract powder; Get extract powder and add lactose 400g, dextrin 100g, use water wet granulation, 60 DEG C of dryings, granulate, adds Pulvis Talci 15g, mixing, obtained few positive cold granules.
Specific embodiments of the invention 3
Get Bulbus Allii Macrostemonis 80g, Rhizoma Corydalis Decumbentis 28g, Radix Scutellariae 206g, the Rhizoma Pinelliae 206, Rhizoma Zingiberis 138, Fructus Jujubae 138, Radix Ginseng 69g, Herba Artemisiae Annuae 206g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 10710g water, 5g germanium powder, 7g polysorbate60, select supersonic frequency 55KHz, pressure 0.4Mpa extracts 30 minutes, use 80 mesh screen, obtain extracting solution; Getting extracting solution puts in jet spray dryer, and control inlet temperature 45 DEG C, pressure 0.03Mpa, 500 meters per second of flow velocity, obtains nanometer extract powder; Get extract powder and add lactose 400g, dextrin 100g, use water wet granulation, 60 DEG C of dryings, granulate, adds Pulvis Talci 15g, mixing, obtained few positive cold granules.
Above embodiment illustrates, adopts the extreme condition of embodiment of the present invention and optimal conditions all can make few positive cold granules.Actual effect of the present invention is investigated below with the few positive cold granules that embodiment 3 is obtained:
(1) the few positive cold granules of embodiment 3 and commercially available few positive cold granules treat acute upper respiratory tract infection Disease Clinical observation of curative effect
1 case scenario
Statistics outpatient service and inpatient, observe acute upper respiratory tract infection case 104 example, 30 years old mean age altogether.Patient is divided into two groups, test group takes the few positive cold granules of embodiment 3, and matched group takes the few positive cold granules of tradition.
2 efficacy assessment standards
According to new Chinese medicine guideline of clinical investigations tcm syndrome curative effect determinate standard:
Cure: tcm clinical practice symptom, sign disappear or substantially disappear, syndrome integral reduces >=95%.
Effective: tcm clinical practice symptom, sign are obviously improved, syndrome integral reduces >=70%.
Effective: tcm clinical practice symptom, sign all take a favorable turn, syndrome integral reduces >=30%.
Invalid: tcm clinical practice symptom, sign are all not improved or increase the weight of, syndrome integral reduces < 30%.
Computing formula: [before (before treatment the rear integration of integration-treatment) ÷ treatment integration] × 100%.
3 clinical observation result
The few positive cold granules of table 1 embodiment 3 and commercially available few positive cold granules clinical efficacy contrast
Above-mentioned clinical observation on the therapeutic effect result shows, few positive cold granules prepared by the present invention is when treating acute upper respiratory tract infection, evident in efficacy higher than commercially available few positive cold granules, p < 0.05.
Claims (3)
1. treat a Chinese medicine for acute upper respiratory tract infection, it is characterized in that getting Bulbus Allii Macrostemonis 80g, Rhizoma Corydalis Decumbentis 28g, Radix Scutellariae 206g, the Rhizoma Pinelliae 206, Rhizoma Zingiberis 138, Fructus Jujubae 138, Radix Ginseng 69g, Herba Artemisiae Annuae 206g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 10710g water, 4 ~ 6g germanium powder, 6 ~ 8g polysorbate60, selects supersonic frequency 50 ~ 60KHz, pressure 0.3 ~ 0.5 Mpa extracts 30 minutes, uses 80 mesh screen, obtains extracting solution; Getting extracting solution puts in jet spray dryer, and control inlet temperature 40 ~ 50 DEG C, pressure 0.02 ~ 0.04 Mpa, 400 ~ 600 meters per second of flow velocity, obtains nanometer extract powder; Get extract powder and add lactose 400g, dextrin 100g, use water wet granulation, 60 DEG C of dryings, granulate, adds Pulvis Talci 15g, mixing, obtained few positive cold granules.
2. the preparation method of Chinese medicine according to claim 1, is characterized in that getting Bulbus Allii Macrostemonis 80g, Rhizoma Corydalis Decumbentis 28g, Radix Scutellariae 206g, the Rhizoma Pinelliae 206, Rhizoma Zingiberis 138, Fructus Jujubae 138, Radix Ginseng 69g, Herba Artemisiae Annuae 206g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 10710g water, 4 ~ 6g germanium powder, 6 ~ 8g polysorbate60, selects supersonic frequency 50 ~ 60KHz, pressure 0.3 ~ 0.5 Mpa extracts 30 minutes, uses 80 mesh screen, obtains extracting solution; Getting extracting solution puts in jet spray dryer, and control inlet temperature 40 ~ 50 DEG C, pressure 0.02 ~ 0.04 Mpa, 400 ~ 600 meters per second of flow velocity, obtains nanometer extract powder; Get extract powder and add lactose 400g, dextrin 100g, use water wet granulation, 60 DEG C of dryings, granulate, adds Pulvis Talci 15g, mixing, obtained few positive cold granules.
3. the preparation method of Chinese medicine according to claim 1, is characterized in that getting Bulbus Allii Macrostemonis 80g, Rhizoma Corydalis Decumbentis 28g, Radix Scutellariae 206g, the Rhizoma Pinelliae 206, Rhizoma Zingiberis 138, Fructus Jujubae 138, Radix Ginseng 69g, Herba Artemisiae Annuae 206g, be ground into 40 order coarse powder, put in circulating ultrasonic extractor, add 10710g water, 5g germanium powder, 7g polysorbate60, selects supersonic frequency 55KHz, pressure 0.4Mpa extracts 30 minutes, uses 80 mesh screen, obtains extracting solution; Getting extracting solution puts in jet spray dryer, and control inlet temperature 45 DEG C, pressure 0.03Mpa, 500 meters per second of flow velocity, obtains nanometer extract powder; Get extract powder and add lactose 400g, dextrin 100g, use water wet granulation, 60 DEG C of dryings, granulate, adds Pulvis Talci 15g, mixing, obtained few positive cold granules.
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| CN201410760589.5A CN104383516A (en) | 2014-12-13 | 2014-12-13 | Shaoyang cold treatment granules and preparation method for same |
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| CN201410760589.5A CN104383516A (en) | 2014-12-13 | 2014-12-13 | Shaoyang cold treatment granules and preparation method for same |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107711917A (en) * | 2017-10-20 | 2018-02-23 | 杨广旦 | The method of plant material extraction organic agricultural chemicals and the organic agricultural chemicals extracted |
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2014
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107711917A (en) * | 2017-10-20 | 2018-02-23 | 杨广旦 | The method of plant material extraction organic agricultural chemicals and the organic agricultural chemicals extracted |
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Application publication date: 20150304 |