CN104547066A - Cold-fever-treating granules and preparation method thereof - Google Patents
Cold-fever-treating granules and preparation method thereof Download PDFInfo
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Abstract
The invention discloses cold-fever-treating granules and a preparation method thereof. The preparation method comprises the following steps: finishing and preparing 30-40% of folium isatidis, 30-40% of isatis root, 10-20% of fructus forsythiae and 10-20% of bistort rhizome, then adding water and decocting for twice while controlling the temperature, pressure, time, adding amount, solution discharge amount and times of the decoction, and then concentrating the decoction while controlling the temperature, pressure and solution charge amount during the concentration; then continuing to precipitate with ethanol, concentrating, precipitating with water, and concentrating into a paste with a weight which is not less than 12.5% of a raw medicine amount; crushing and sieving, drying, straightening and mixing, sub-packaging and packaging. The cold-fever-treating granules and the preparation method thereof disclosed by the invention have the following advantages: the prepared granules are sweet in taste, slightly bitter (without saccharose) and uniform, are capable of clearing away heat and toxic materials, and dispelling wind and relieving exterior syndrome, and are used for upper respiratory infection, acute tonsillitis, sphagitis, extrapelvic wind-heat, heat-toxin obstruction, fever and swollen sore throat; the production process is simple and easy to control, and only needs four medicinal materials.
Description
Technical field
The invention belongs to pharmaceutical technology sectors, be specifically related to a kind of heat-clearing and toxic substances removing, GANMAO TUIRE KELI of dispelling wind to relieve the exterior syndrome and preparation method thereof.
Background technology
Anemopyretic cold is common flu type, caused by anemopyretic cold is the evil criminal table of wind heat, lung qi is become estranged.Symptoms is heating weight, micro evil wind, distending pain in the head, have antiperspirant, red swelling and pain of throat, cough, expectorant are sticky or yellow, yellow thick nasal discharge of having a stuffy nose, thirst and liking drink, the tip of the tongue limit are red, the micro-Huang of white and thin fur.Cause of disease diseases caused by exogenous pathogenic factor six climate exopathogens, time row virus, defend outer miopragia at human body, when can not regulating strain, from fur, mouth and nose invasion, evil lung of violating is defended, and defends table discord and causes a disease.In general, flu seldom has the situation of the change of disease occurs, the short and being easy to recover of the course of disease.But time sense serious symptom, old man, baby children, weak patients, sometimes also variable sick he.In addition, flu has certain infectiousness, very high at infection seasons sickness rate, produces often bring greater impact people ' s health and work, therefore must actively control.
From traditional medicine theory: flu is the common exogenous diseases that a kind of ailment said due to cold or exposure of catching a cold causes.Method for the treatment of should based on relieving the exterior syndrome with drugs of pungent in flavor and cool in nature.Namely have recognized that as far back as Huangdi's Internal Classics and catch a cold mainly caused by diseases caused by exogenous pathogenic factor ailment said due to cold or exposure." a Plain Questions bone empty talk section " cloud: " wind enters from outward, makes us cold with shivering, and sweating is had a headache, heavy sensation of the body aversion to cold ".Ancient doctor also has what call to be " time row sick ", Qingxu spirit tire " medical science source and course opinion cold refractory opinion " cloud: " ordinary person feels wind and cold, has a headache and fever, and tears of coughing go out, the cold of common saying meaning, and when being, the random thoughts of row also ".As for the name of flu, then get instant result in the Northern Song Dynasty " all wind of Renzhai Zhi Zhi Fang, Effective Recipes from Renzhai House ", in its cold side opinion, introduction shensu drink is controlled " flu ailment said due to cold or exposure, have a headache and fever, cough low voice speaking, tears saliva is sticky ".
At present, the treatment of doctor trained in Western medicine has one-sidedness, and side effect is large, has anaphylactoid patient that shock may be caused lethal.Use Chinese herbal treatment flu to be the work always studied, but current curative effect of medication can not be satisfactory.Chinese patent CN200610111509.9 discloses a kind of compound medicine for the treatment of anemopyretic cold, its raw material medicines in portions by weight proportioning is: Fructus Arctii 280 ~ 380 parts, Flos Lonicerae 780 ~ 880 parts, Fructus Forsythiae 450 ~ 550 parts, Herba Menthae 280 ~ 380 parts, Herba Schizonepetae 280 ~ 380 parts, Radix Isatidis 450 ~ 550 parts, Rhizoma Et Radix Notopterygii 280 ~ 380 parts, Folium Isatidis 450 ~ 550 parts, Radix Glycyrrhizae 110-210 part.
Summary of the invention
The object of the invention is to provide a kind of Be very effective, GANMAO TUIRE KELI of having no side effect and preparation method thereof.
In order to realize object of the present invention, the technical scheme of employing is:
A kind of GANMAO TUIRE KELI, is characterized in that, by weight mark meter, comprising:
As preferred technical scheme: the content of described Folium Isatidis, Radix Isatidis, Fructus Forsythiae and Rhizoma Bistortae is than being 2:2:1:1.
A preparation method for GANMAO TUIRE KELI, is characterized in that, comprises step:
1., arrange concocting process: Folium Isatidis is picked decontamination, slightly washes, be cut into≤the wide sheet of 10cm, dry, moisture is no more than 13%; Radix Isatidis is picked decontamination, drenches Xian, run through, be cut into≤the section of 1.5cm, 65 DEG C of dryings, moisture is no more than 15%; Fructus Forsythiae is picked decontamination, and moisture is no more than 10%; Rhizoma Bistortae is picked decontamination, and the clean silt of wash quickly, runs through, and be cut into≤the section of 1.5cm, 65 DEG C of dryings, moisture is no more than 15%;
2., decoct: by described step 1. in four kinds of medical materials mixing of handling well, add 6 ~ 10 times amount soak by water secondaries; Each 1.5 ~ 3 hours, the temperature 95 ~ 100 DEG C that control decocts, pressure 0.15 ~ 0.3MPa, liquid outlet quantity were 4 ~ 5 times of medical material total amount, and collecting decoction filters, proceeds to basin;
The weight of what wherein 6 ~ 10 times of water gagings referred to the is water added is 6 ~ 10 times of four kinds of medical material gross weights.Liquid outlet quantity refers to the amount of releasing decocting liquid.
3., proceed in Three-effect concentration device by decoction liquor gradation in storage tank, being concentrated into relative density is 1.08 ~ 1.1 (90 ~ 95 DEG C), leaves standstill, and cooling, proceeds in settling tank; Temperature 60 ~ 70 DEG C is controlled well, pressure 0.15MPa ~ 0.25MPa time concentrated,
4., alcohol settling: add 95% ethanol with concentrated solution equivalent in settling tank, limit edged stirs, and leaves standstill and makes precipitation in 24 hours;
5., concentrated: to get the supernatant after alcohol settling, proceed to reclaim ethanol in decompression concentrator after in Three-effect concentration device and be concentrated into the clear paste that relative density is 1.18 ~ 1.20 (60 DEG C), proceed in clean container;
6., water precipitation: get concentrated clear paste, add the water with clear paste equivalent, stir, leave standstill 8 hours;
7., concentrated receipts cream: the supernatant of water intaking precipitation proceeds in concentrator and is condensed into the thick paste that relative density is 1.38 ~ 1.40 (60 DEG C), loads clean container;
8., pulverize and sieve: get sucrose and pulverized 80 mesh sieves, 120 mesh sieves crossed by dextrin, be respectively charged in clean container, get thick paste 1 part, cane sugar powder 3 parts, 1 part, dextrin, is respectively charged in clean container, add thick paste after being mixed homogeneously with dextrin trough type mixing machine by the cane sugar powder of ormal weight to mix, add ethanol and make soft material;
With oscillating granulator, soft material is made full uniform wet granular by 12 eye mesh screens;
9., dry: be evenly laid in by wet granular in clean basin, be no more than 2 ~ 3cm thick, send into baking oven, aeration-drying 6 hours, temperature controls at 70 ± 5 DEG C, timely stirring in dry run, and record;
Granulate with mix: cross 10 mesh sieve granulate, the granule after granulate cross No. one sieve and No. four sieves, the granule mixed is contained in clean container;
Subpackage and packaging.
As preferred technical scheme, described step 7. middle cream weight of receiving is more than or equal to 12.5% of four kinds of medical material total amounts.
Folium Isatidis: this product is the dried leaves of cruciferae isatis Isatis indigotica Fort..In the summer, divide in season in autumn two and gather for 2 ~ 3 times, removing impurity, dries.Character, discriminating, assay etc. should meet " the regulation under Chinese Pharmacopoeia 2005 version one 16 pages " Folium Isatidis " items.
Radix Isatidis: this product is the dry root of cruciferae isatis Isatis indigotica Fort..Autumn excavates, and removing silt, dries.Character, discriminating, inspection, extractum etc. should meet " the regulation under Chinese Pharmacopoeia 2005 version one 163 pages " Radix Isatidis " items.
Fructus Forsythiae: this product is the dry fruit of Oleaceae plants Fructus Forsythiae Forsythia suspensa (Thunb.) Vahl.Gather during fruit in autumn first ripe still band green, removing impurity, cooks, dries, and practises title " green grass or young crops sticks up "; Gather when fruit is well-done, dry, removing impurity, practises and claims " always sticking up ".Character, discriminating, inspection, extractum, assay etc. should meet " the regulation under Chinese Pharmacopoeia 2005 version one 117 pages " Fructus Forsythiae " items
Rhizoma Bistortae: this product is the dry rhizome of polygonaceae plant Rhizoma Bistortae Polygonum bistorta L..When germinateing at the beginning of the spring or autumn stem and leaf excavate time withered, removing silt, dry, remove fibrous root.Character, discriminating, inspection etc. should meet " the regulation under Chinese Pharmacopoeia 2005 version one 202 pages " Rhizoma Bistortae " items.
Sucrose: this product is beta-D-fructofuranose base α-D-pyranglucoside.Character, discriminating, inspection etc. should meet " the regulation under Chinese Pharmacopoeia 2005 version two 922 pages " sucrose " items.
Dextrin: have regulation under character, discriminating, inspection etc. should meet " Chinese Pharmacopoeia " 2000 editions two 1038 pages " dextrin " items.
Extractum: this product is that the paste of brown color is semi-solid.
Wherein sieve 10 orders, No. four sieve 65 orders, No. five sieve 80 orders.
The beneficial effect that the present invention has:
This product is the granule of brown color, is of moderate size, evenly, dry wet, thickness, uniform color are consistent.Wherein moisture is less than or equal to 5%, is not no more than 13.0% by No. 1 sieve with by No. 5 granules sieved and powder summation.
Taste is sweet, micro-hardship (without sucrose), heat-clearing and toxic substances removing, dispelling wind to relieve the exterior syndrome.Stop up sense card for upper respiratory tract infection, acute tonsillitis, pharyngolaryngitis, the outer broad-mouthed receptacle for holding liquid wind heat of genus, pyretic toxicity, card is shown in heating, laryngopharynx swelling and pain.
Processing technology is simple and easy to control, only needs four kinds of medical materials.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described, but protection scope of the present invention is not only confined to embodiment.
Embodiment 1
A kind of preparation process of GANMAO TUIRE KELI is as follows:
1., arrange concocting process: 400g Folium Isatidis is picked decontamination, slightly washes, be cut into the wide sheet of 8 ~ 10cm, dry, moisture is no more than 13%; 400g Radix Isatidis is picked decontamination, and drench Xian, run through, be cut into the section of 1.3 ~ 1.5cm, 65 DEG C of dryings, moisture is no more than 15%; 200g Fructus Forsythiae is picked decontamination, and moisture is no more than 10%; 200g Rhizoma Bistortae is picked decontamination, and the clean silt of wash quickly, runs through, and is cut into the section of 1.3 ~ 1.5cm, 65 DEG C of dryings, and moisture is no more than 15%;
2., decoct: by described step 1. in four kinds of medical materials mixing of handling well, add 10 times amount soak by water secondaries, each 3 hours, the temperature 95 ~ 100 DEG C that control decocts, pressure 0.15 ~ 0.2MPa, liquid outlet quantity are 4 ~ 4.5 times of medical material total amount, collecting decoction, filters, proceeds to basin;
3., proceed in Three-effect concentration device by decoction liquor gradation in storage tank, being concentrated into relative density is 1.08 (90 ~ 95 DEG C), leaves standstill, and cooling, proceeds in settling tank; Temperature 65 ~ 70 DEG C is controlled well, pressure 0.15MPa ~ 0.2MPa time concentrated,
4., alcohol settling: add 95% ethanol with concentrated solution equivalent in settling tank, limit edged stirs, and leaves standstill and makes precipitation in 24 hours;
5., concentrated: to get the supernatant after alcohol settling, proceed to reclaim ethanol in decompression concentrator after in Three-effect concentration device and be concentrated into the clear paste that relative density is 1.20 (60 DEG C), proceed in clean container;
6., water precipitation: get concentrated clear paste, add the water with clear paste equivalent, stir, leave standstill 8 hours;
7., concentrated receipts cream: the supernatant of water intaking precipitation proceeds in concentrator and is condensed into the thick paste that relative density is 1.40 (60 DEG C), loads clean container, and receiving cream weight is 180g, is 15% of raw medicinal herbs total amount;
8., pulverize and sieve: get sucrose and pulverized 80 mesh sieves, 120 mesh sieves crossed by dextrin, be respectively charged in clean container, get thick paste 1 part, cane sugar powder 3 parts, 1 part, dextrin, is respectively charged in clean container, add thick paste after being mixed homogeneously with dextrin trough type mixing machine by the cane sugar powder of ormal weight to mix, add ethanol and make soft material;
With oscillating granulator, soft material is made full uniform wet granular by 12 eye mesh screens;
9., dry: be evenly laid in by wet granular in clean basin, be no more than 2 ~ 3cm thick, send into baking oven, aeration-drying 6 hours, temperature controls at 70 ± 5 DEG C, timely stirring in dry run, and record;
Granulate with mix: cross 10 mesh sieve granulate, the granule after granulate cross No. one sieve and No. four sieves, the granule mixed is contained in clean container;
Subpackage and packaging.
Embodiment 2
A kind of preparation process of GANMAO TUIRE KELI is as follows:
1., arrange concocting process: 300g Folium Isatidis is picked decontamination, slightly washes, be cut into the wide sheet of 7 ~ 9cm, dry, moisture is no more than 13%; 300g Radix Isatidis is picked decontamination, and drench Xian, run through, be cut into the section of 1.1 ~ 1.3cm, 65 DEG C of dryings, moisture is no more than 15%; 120g Fructus Forsythiae is picked decontamination, and moisture is no more than 10%; 100g Rhizoma Bistortae is picked decontamination, and the clean silt of wash quickly, runs through, and is cut into the section of 1.2 ~ 1.5cm, 65 DEG C of dryings, and moisture is no more than 15%;
2., decoct: by described step 1. in four kinds of medical materials mixing of handling well, add 6 times amount soak by water secondaries, each 2 hours, the temperature 95 ~ 100 DEG C that control decocts, pressure 0.2 ~ 0.3MPa, liquid outlet quantity are 4 ~ 5 times of medical material total amount, collecting decoction, filters, proceeds to basin;
3., proceed in Three-effect concentration device by decoction liquor gradation in storage tank, being concentrated into relative density is 1.1 (90 ~ 95 DEG C), leaves standstill, and cooling, proceeds in settling tank; Temperature 60 ~ 65 DEG C is controlled well, pressure 0.2MPa ~ 0.25MPa time concentrated,
4., alcohol settling: add 95% ethanol with concentrated solution equivalent in settling tank, limit edged stirs, and leaves standstill and makes precipitation in 24 hours;
5., concentrated: to get the supernatant after alcohol settling, proceed to reclaim ethanol in decompression concentrator after in Three-effect concentration device and be concentrated into the clear paste that relative density is 1.19 (60 DEG C), proceed in clean container;
6., water precipitation: get concentrated clear paste, add the water with clear paste equivalent, stir, leave standstill 8 hours;
7., concentrated receipts cream: the supernatant of water intaking precipitation proceeds in concentrator and is condensed into the thick paste that relative density is 1.38 (60 DEG C), loads clean container, and receiving cream weight 110g, is 13.5% of raw medicinal herbs total amount;
Subsequent step is with embodiment 1.
Embodiment 3
A kind of preparation process of GANMAO TUIRE KELI is as follows:
1., arrange concocting process: 330g Folium Isatidis is picked decontamination, slightly washes, be cut into the wide sheet of 7 ~ 10cm, dry, moisture is no more than 13%; 350g Radix Isatidis is picked decontamination, and drench Xian, run through, be cut into the section of 1.2 ~ 1.5cm, 65 DEG C of dryings, moisture is no more than 15%; 140g Fructus Forsythiae is picked decontamination, and moisture is no more than 10%; 160g Rhizoma Bistortae is picked decontamination, and the clean silt of wash quickly, runs through, and is cut into the section of 1.1 ~ 1.4cm, 65 DEG C of dryings, and moisture is no more than 15%;
2., decoct: by described step 1. in four kinds of medical materials mixing of handling well, add 8 times amount soak by water secondaries, each 1.5 hours, the temperature 95 ~ 100 DEG C that control decocts, pressure 0.15 ~ 0.25MPa, liquid outlet quantity are 4 ~ 5 times of medical material total amount, collecting decoction, filters, proceeds to basin;
3., proceed in Three-effect concentration device by decoction liquor gradation in storage tank, being concentrated into relative density is 1.09 (90 ~ 95 DEG C), leaves standstill, and cooling, proceeds in settling tank; Temperature 60 ~ 70 DEG C is controlled well, pressure 0.15MPa ~ 0.25MPa time concentrated,
4., alcohol settling: add 95% ethanol with concentrated solution equivalent in settling tank, limit edged stirs, and leaves standstill and makes precipitation in 24 hours;
5., concentrated: to get the supernatant after alcohol settling, proceed to reclaim ethanol in decompression concentrator after in Three-effect concentration device and be concentrated into the clear paste that relative density is 1.18 (60 DEG C), proceed in clean container;
6., water precipitation: get concentrated clear paste, add the water with clear paste equivalent, stir, leave standstill 8 hours;
7., concentrated receipts cream: the supernatant of water intaking precipitation proceeds in concentrator and is condensed into the thick paste that relative density is 1.39 (60 DEG C), loads clean container, and receiving cream weight 127g, is 13% of raw medicinal herbs total amount;
Subsequent step is with embodiment 1.
Differentiate:
(1) get the obtained finished product 3g of the present embodiment 50ml that adds water and make dissolving, filter, filtrate is extracted 2 times (40ml, 30ml) with ether jolting, merges ether solution, is concentrated into about 0.5ml, as need testing solution.
(2) get indirubin reference substance, add diethyl ether and make the solution of every 1ml containing 0.05mg, product solution in contrast.
(3) with reference to " Chinese Pharmacopoeia " annex VI B, according to the test of book layer chromatography, draw each 15 μ l of above-mentioned two kinds of solution, put respectively on same silica gel g thin-layer plate, with benzene-acetone (4: 1) for developing solvent, launch to take out, dry.
Water content detection: according to aquametry (annex IXH) first method (oven drying method).
The inspection of particle size uniformity: get the finished product 30g that various embodiments of the present invention are obtained, weighed weight, puts in regulation medicine sieve, sieve maintenance level is sieved, and left and right comes and goes, and sieves while tapping 3 minutes, the granule and powder summation M that do not sieve by No. 1 and sieve by No. 5, calculate percent.
Melting checks: get granule 18g, heating water (70 ~ 80 DEG C) 200ml, stir 5 minutes, observe immediately, granule should all dissolve, and has allowed slight haze, must not have the foreign bodies such as breeze.
Identification result is as shown in table 1 below:
Table 1 each GANMAO TUIRE KELI differential test result
As shown in Table 1, the GANMAO TUIRE KELI that various embodiments of the present invention are obtained, meets national standard.
Last it is noted that above embodiment only in order to illustrate the present invention and and unrestricted technical scheme described in the invention; Therefore, although this description with reference to each above-mentioned embodiment to present invention has been detailed description, those of ordinary skill in the art should be appreciated that and still can modify to the present invention or equivalent to replace; And all do not depart from technical scheme and the improvement thereof of the spirit and scope of the present invention, it all should be encompassed in right of the present invention.
Claims (4)
1. a GANMAO TUIRE KELI, is characterized in that, by weight mark meter, comprising:
2. a kind of GANMAO TUIRE KELI according to claim 1, is characterized in that: the content of described Folium Isatidis, Radix Isatidis, Fructus Forsythiae and Rhizoma Bistortae is than being 2:2:1:1.
3. a preparation method for GANMAO TUIRE KELI, is characterized in that, comprises step:
1., arrange concocting process: Folium Isatidis is picked decontamination, slightly washes, be cut into≤the wide sheet of 10cm, dry, moisture is no more than 13%; Radix Isatidis is picked decontamination, drenches Xian, run through, be cut into≤the section of 1.5cm, 65 DEG C of dryings, moisture is no more than 15%; Fructus Forsythiae is picked decontamination, and moisture is no more than 10%; Rhizoma Bistortae is picked decontamination, and the clean silt of wash quickly, runs through, and be cut into≤the section of 1.5cm, 65 DEG C of dryings, moisture is no more than 15%;
2., decoct: by described step 1. in four kinds of medical materials mixing of handling well, add 6 ~ 10 times amount soak by water secondaries; Each 1.5 ~ 3 hours, the temperature 95 ~ 100 DEG C that control decocts, pressure 0.15 ~ 0.3MPa, liquid outlet quantity were 4 ~ 5 times of medical material total amount, and collecting decoction filters, proceeds to basin;
3., proceed in Three-effect concentration device by decoction liquor gradation in storage tank, being concentrated into relative density is 1.08 ~ 1.1 (90 ~ 95 DEG C), leaves standstill, and cooling, proceeds in settling tank; Temperature 60 ~ 70 DEG C is controlled well, pressure 0.15MPa ~ 0.25MPa time concentrated,
4., alcohol settling: add 95% ethanol with concentrated solution equivalent in settling tank, limit edged stirs, and leaves standstill and makes precipitation in 24 hours;
5., concentrated: to get the supernatant after alcohol settling, proceed to reclaim ethanol in decompression concentrator after in Three-effect concentration device and be concentrated into the clear paste that relative density is 1.18 ~ 1.20 (60 DEG C), proceed in clean container;
6., water precipitation: get concentrated clear paste, add the water with clear paste equivalent, stir, leave standstill 8 hours;
7., concentrated receipts cream: the supernatant of water intaking precipitation proceeds in concentrator and is condensed into the thick paste that relative density is 1.38 ~ 1.40 (60 DEG C), loads clean container;
8., pulverize and sieve: get sucrose and pulverized 80 mesh sieves, 120 mesh sieves crossed by dextrin, be respectively charged in clean container, get thick paste 1 part, cane sugar powder 3 parts, 1 part, dextrin, is respectively charged in clean container, add thick paste after being mixed homogeneously with dextrin trough type mixing machine by the cane sugar powder of ormal weight to mix, add ethanol and make soft material;
With oscillating granulator, soft material is made full uniform wet granular by 12 eye mesh screens;
9., dry: be evenly laid in by wet granular in clean basin, be no more than 2 ~ 3cm thick, send into baking oven, aeration-drying 6 hours, temperature controls at 70 ± 5 DEG C, timely stirring in dry run, and record;
Granulate with mix: cross 10 mesh sieve granulate, the granule after granulate cross No. one sieve and No. four sieves, the granule mixed is contained in clean container;
Subpackage and packaging.
4. the preparation method of a kind of GANMAO TUIRE KELI according to claim 3, is characterized in that, described step 7. middle cream weight of receiving is more than or equal to 12.5% of four kinds of medical material total amounts.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107125678A (en) * | 2017-05-24 | 2017-09-05 | 湖北盛通药业有限公司 | A kind of pyrus nivalis clear cream extraction process |
| CN109288930A (en) * | 2018-11-26 | 2019-02-01 | 河南百年康鑫药业有限公司 | A kind of preparation method of GANMAO TUIRE KELI |
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| CN107125678A (en) * | 2017-05-24 | 2017-09-05 | 湖北盛通药业有限公司 | A kind of pyrus nivalis clear cream extraction process |
| CN109288930A (en) * | 2018-11-26 | 2019-02-01 | 河南百年康鑫药业有限公司 | A kind of preparation method of GANMAO TUIRE KELI |
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Application publication date: 20150429 |