CN104449141B - 纳米复合冷镀锌涂料及其制备方法 - Google Patents
纳米复合冷镀锌涂料及其制备方法 Download PDFInfo
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- CN104449141B CN104449141B CN201410727047.8A CN201410727047A CN104449141B CN 104449141 B CN104449141 B CN 104449141B CN 201410727047 A CN201410727047 A CN 201410727047A CN 104449141 B CN104449141 B CN 104449141B
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- zinc powder
- coating
- cold galvanizing
- nano combined
- powder
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- 239000011248 coating agent Substances 0.000 title claims abstract description 91
- 238000000576 coating method Methods 0.000 title claims abstract description 91
- 238000005246 galvanizing Methods 0.000 title claims abstract description 49
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims abstract description 127
- 239000000843 powder Substances 0.000 claims abstract description 32
- 239000002904 solvent Substances 0.000 claims abstract description 22
- ABTOQLMXBSRXSM-UHFFFAOYSA-N silicon tetrafluoride Chemical compound F[Si](F)(F)F ABTOQLMXBSRXSM-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 16
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 16
- 239000007822 coupling agent Substances 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000203 mixture Substances 0.000 claims abstract description 11
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 6
- 238000012545 processing Methods 0.000 claims abstract description 5
- 238000001914 filtration Methods 0.000 claims description 13
- 239000000376 reactant Substances 0.000 claims description 9
- 238000005119 centrifugation Methods 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 7
- QQQSFSZALRVCSZ-UHFFFAOYSA-N triethoxysilane Chemical compound CCO[SiH](OCC)OCC QQQSFSZALRVCSZ-UHFFFAOYSA-N 0.000 claims description 6
- -1 trifluoro octyl group trimethoxy silanes Chemical class 0.000 claims description 5
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 4
- 229910000077 silane Inorganic materials 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 2
- CWAFVXWRGIEBPL-UHFFFAOYSA-N ethoxysilane Chemical compound CCO[SiH3] CWAFVXWRGIEBPL-UHFFFAOYSA-N 0.000 claims 1
- 239000011701 zinc Substances 0.000 abstract description 30
- 229910052725 zinc Inorganic materials 0.000 abstract description 30
- 238000005260 corrosion Methods 0.000 abstract description 10
- 239000003973 paint Substances 0.000 abstract description 10
- 229910000831 Steel Inorganic materials 0.000 abstract description 9
- 230000007797 corrosion Effects 0.000 abstract description 9
- 239000010959 steel Substances 0.000 abstract description 9
- 238000007598 dipping method Methods 0.000 abstract description 5
- 239000011347 resin Substances 0.000 abstract description 4
- 229920005989 resin Polymers 0.000 abstract description 4
- 238000012423 maintenance Methods 0.000 abstract description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 52
- 239000003795 chemical substances by application Substances 0.000 description 27
- 239000002270 dispersing agent Substances 0.000 description 13
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 12
- PWSZACWUDDFZMQ-UHFFFAOYSA-N 2,4-Diphenyl-1-butene Chemical compound C=1C=CC=CC=1C(=C)CCC1=CC=CC=C1 PWSZACWUDDFZMQ-UHFFFAOYSA-N 0.000 description 11
- 239000013530 defoamer Substances 0.000 description 11
- 239000008096 xylene Substances 0.000 description 10
- 239000000463 material Substances 0.000 description 8
- 238000012360 testing method Methods 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- 230000010148 water-pollination Effects 0.000 description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000002209 hydrophobic effect Effects 0.000 description 3
- 240000002853 Nelumbo nucifera Species 0.000 description 2
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 2
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 2
- 229920000180 alkyd Polymers 0.000 description 2
- 239000004411 aluminium Substances 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 2
- 230000033228 biological regulation Effects 0.000 description 2
- 229920001971 elastomer Polymers 0.000 description 2
- 239000000806 elastomer Substances 0.000 description 2
- 229920006334 epoxy coating Polymers 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical group [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 239000011527 polyurethane coating Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000009736 wetting Methods 0.000 description 2
- QTRSWYWKHYAKEO-UHFFFAOYSA-N 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-henicosafluorodecyl-tris(1,1,2,2,2-pentafluoroethoxy)silane Chemical compound FC(F)(F)C(F)(F)O[Si](OC(F)(F)C(F)(F)F)(OC(F)(F)C(F)(F)F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F QTRSWYWKHYAKEO-UHFFFAOYSA-N 0.000 description 1
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 description 1
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 1
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 1
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 229910000635 Spelter Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000003916 acid precipitation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 description 1
- 238000004210 cathodic protection Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 125000002704 decyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- BAAAEEDPKUHLID-UHFFFAOYSA-N decyl(triethoxy)silane Chemical compound CCCCCCCCCC[Si](OCC)(OCC)OCC BAAAEEDPKUHLID-UHFFFAOYSA-N 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- ZOMNIUBKTOKEHS-UHFFFAOYSA-L dimercury dichloride Chemical group Cl[Hg][Hg]Cl ZOMNIUBKTOKEHS-UHFFFAOYSA-L 0.000 description 1
- 238000000840 electrochemical analysis Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 238000011900 installation process Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 1
- ARYZCSRUUPFYMY-UHFFFAOYSA-N methoxysilane Chemical compound CO[SiH3] ARYZCSRUUPFYMY-UHFFFAOYSA-N 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 230000010287 polarization Effects 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000009991 scouring Methods 0.000 description 1
- 230000008771 sex reversal Effects 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000010301 surface-oxidation reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- YUYCVXFAYWRXLS-UHFFFAOYSA-N trimethoxysilane Chemical compound CO[SiH](OC)OC YUYCVXFAYWRXLS-UHFFFAOYSA-N 0.000 description 1
- 239000002966 varnish Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
- C08K9/06—Ingredients treated with organic substances with silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
- C09D5/10—Anti-corrosive paints containing metal dust
- C09D5/106—Anti-corrosive paints containing metal dust containing Zn
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0893—Zinc
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Laminated Bodies (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Paints Or Removers (AREA)
Abstract
Description
纳米锌粉占总锌粉量,% | 水接触角,° | 电流密度,A/cm2 | 附着力,级 | 耐冲击性,cm | |
比较例1 | 2 | 125 | 2.1E-05 | 1 | 5 |
比较例2 | 25 | 127 | 3.2E-06 | 2 | 5 |
比较例3 | 50 | 128 | 2.6E-06 | 3 | 5 |
比较例4 | 75 | 132 | 1.8E-06 | 4 | 5 |
比较例5 | 98 | 135 | 9.6E-7 | 4 | 5 |
实施例1 | 2 | 135 | 1.1E-05 | 1 | 50 |
实施例2 | 25 | 138 | 1.5E-06 | 2 | 30 |
实施例3 | 50 | 139 | 1.1E-06 | 3 | 20 |
实施例4 | 75 | 141 | 3.4E-08 | 4 | 10 |
实施例5 | 98 | 145 | 7.5E-10 | 4 | 10 |
Claims (2)
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CN201410727047.8A CN104449141B (zh) | 2014-12-04 | 2014-12-04 | 纳米复合冷镀锌涂料及其制备方法 |
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CN201410727047.8A CN104449141B (zh) | 2014-12-04 | 2014-12-04 | 纳米复合冷镀锌涂料及其制备方法 |
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CN104449141A CN104449141A (zh) | 2015-03-25 |
CN104449141B true CN104449141B (zh) | 2017-07-18 |
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Families Citing this family (14)
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CN106479353B (zh) * | 2015-09-02 | 2019-05-21 | 佛山市高明区(中国科学院)新材料专业中心 | 一种疏水无铬达克罗涂料 |
CN111234621B (zh) * | 2018-11-29 | 2021-09-24 | 中国科学院金属研究所 | 可修复超疏水纳米金属导电涂层及其制备方法 |
CN109390499A (zh) * | 2018-11-30 | 2019-02-26 | 云谷(固安)科技有限公司 | 一种显示面板及移动终端 |
CN109632576B (zh) * | 2018-12-04 | 2021-04-23 | 浙江理工大学 | 材料腐蚀速率与壁面润湿特性测试系统 |
CN110204934A (zh) * | 2019-06-13 | 2019-09-06 | 贵州电网有限责任公司 | 一种纳米稀土冷镀锌涂料及在输电杆塔中的应用方法 |
CN110317478B (zh) * | 2019-06-19 | 2021-07-23 | 中国科学院金属研究所 | 一种聚噻吩改性冷涂锌涂料及其制备方法 |
CN112302838B (zh) * | 2019-08-02 | 2022-04-01 | 广州汽车集团股份有限公司 | Egr废气再循环系统及汽车 |
CN110467861A (zh) * | 2019-08-20 | 2019-11-19 | 广东恒宝缘新材料有限公司 | 一种冷涂锌涂料及其制备方法 |
CN112080182B (zh) * | 2020-09-24 | 2022-02-08 | 西北永新涂料有限公司 | 一种高致密性能的冷涂锌涂料及其制备方法 |
CN112694804A (zh) * | 2021-01-08 | 2021-04-23 | 湖南翰坤实业有限公司 | 一种抗污渍镀锌涂料及其制备方法 |
CN112961559A (zh) * | 2021-03-24 | 2021-06-15 | 中国科学院金属研究所 | 一种氯烃基硅烷偶联剂改性冷涂锌涂料及其制备方法 |
CN112980274A (zh) * | 2021-03-24 | 2021-06-18 | 广东腐蚀科学与技术创新研究院 | 一种巯基硅烷偶联剂改性冷涂锌涂料及其制备方法 |
CN115368806B (zh) * | 2022-10-09 | 2023-05-05 | 青岛海洋新材料科技有限公司 | 一种应用于石油管道的防腐涂料及其制备方法 |
CN116535924B (zh) * | 2023-06-07 | 2023-10-17 | 南京中金润恒金属科技股份有限公司 | 一种复合冷镀锌涂料及其制备方法 |
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CN101104764B (zh) * | 2007-07-17 | 2010-11-24 | 深圳市明远氟涂料有限公司 | 一种钢铁用重防腐涂料及其制备方法 |
CN101760056A (zh) * | 2009-11-10 | 2010-06-30 | 南通飞拓生物科技有限公司 | 一种高效防腐自喷型银富锌涂料 |
KR20130094093A (ko) * | 2012-02-15 | 2013-08-23 | 한국건설기술연구원 | 상하수 관거의 방수 및 오염 방지를 위한 코팅 조성물 및 그의 제조 방법 |
CN103881494A (zh) * | 2012-12-24 | 2014-06-25 | 深圳市嘉达高科产业发展有限公司 | 一种金属防腐防污涂料 |
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