CN104382760A - Natural anti-dandruff shampoo and preparation method thereof - Google Patents
Natural anti-dandruff shampoo and preparation method thereof Download PDFInfo
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Abstract
The invention discloses natural anti-dandruff shampoo and a preparation method thereof. Based on the total amounts of 100 parts, the natural anti-dandruff shampoo is prepared from the following components in parts by weight: 0.03 to 3 parts of natural anti-dandruff components, 2 to 10 parts of sodium dodecyl sulfate, 0.3 to 2 parts of lanolin, 0.5 to 2 parts of coconut diethanol amide, 0.23 to 3 parts of betaine, 0.3 to 3 parts of sodium N-lauroylglutamate, 0.05 to 0.1 part of pearl powder, 0.2 to 3 parts of ethylenediamine tetraacetic acid and the balance of de-ionized water. According to the natural anti-dandruff shampoo and the preparation method for the natural anti-dandruff shampoo, surfactants (sodium dodecyl sulfate, lanolin, coconut diethanol amide, sodium N-lauroylglutamate and the like) are combined with the natural anti-dandruff components in the shampoo, so that the dissolution and release of active ingredients can be promoted, and effects can be better achieved when the shampoo is used.
Description
Technical field
The present invention relates to article of everyday use, be specifically related to a kind of natural anti-dandruff shampoo, also relate to the preparation method of this shampoo.
Background technology
Along with improving constantly of living standard, people also more and more pay attention to self image construction, and hair just becomes a wherein important ring.Healthy healthy hair can give beautiful bonus point, if see that the dandruff of a vast expanse of whiteness interts wherein, is very unpleasant.No matter men and women, the dandruff is many is all a problem given offence, and the women of 59% and 63% male be subject to this puzzlement always, for huge " the worried race of dandruff ", select selecting properly and use dandruff control shampoo containing to seem to be even more important.At present, the most of dandruff control shampoo containings on market are generally the growths adopting fungus in Drug inhibition scalp, thus the generation of control head scurf.And this type of anti-dandruff component that arrives mostly is artificial compound, potential safety hazard is there is owing to there is toxicity in certain scope of application, and life-time service can impel fungus to produce rapidly resistance bacterial strain, resist medicine, this kind of anti-dandruff product cannot fundamentally control and treatment of dandruff, and the exploitation of the dandruff control shampoo containing therefore containing natural anti-dandruff component has realistic meaning and market prospect.
Summary of the invention
The first object of the present invention is to provide a kind of natural anti-dandruff shampoo.
Natural anti-dandruff shampoo of the present invention; be prepared from by following each component by weight: natural anti-dandruff component 0.03-3 part; sodium lauryl sulphate 2-10 part; lanoline 0.3-2 part, coconut oil diethanol amide 0.5-2 part, betanin 0.23-3 part; sodium lauroyl glutamate 0.3-3 part; pearl essence 0.05-0.1 part, ethylenediaminetetraacetic acid 0.2-3 part, deionized water adds to 100 parts.
Wherein, described natural anti-dandruff component is cecropin, emodin, baicalin, berberine, magnolol, at least two kinds in honokiol and diosgenin.
Described natural anti-dandruff component is preferably cecropin and emodin mixture, and both weight ratios are 1-2:1.
As preferred scheme, described natural anti-dandruff shampoo, be prepared from by following each component by weight: natural anti-dandruff component 0.03-1 part, sodium lauryl sulphate 2-5 part, lanoline 0.3-1.5 part, coconut oil diethanol amide 0.5-1 part, betanin 0.23-1 part, sodium lauroyl glutamate 0.3-1 part, pearl essence 0.05-0.09 part, ethylenediaminetetraacetic acid 0.2-0.4 part, deionized water adds to 100 parts; Described natural anti-dandruff component is cecropin and emodin mixture, and both weight ratios are 1-2:1.
Described natural anti-dandruff component is preferably cecropin, emodin, baicalin, berberine, magnolol, the mixture of honokiol and diosgenin, and the weight ratio of seven is 1.5-2:2.5-3:4.5-5:1.5-2:6-7:2-3:7-8.
Cecropin described in the present invention (such as cecropin A etc.) is known substance, by commercially available buy or known method obtain.
As preferred scheme, described natural anti-dandruff shampoo, be prepared from by following each component by weight: natural anti-dandruff component 2.5-3 part, sodium lauryl sulphate 9-10 part, lanoline 1.8-2 part, coconut oil diethanol amide 1.8-2 part, betanin 2.5-3 part, sodium lauroyl glutamate 2.5-3 part, pearl essence 0.09-0.1 part, ethylenediaminetetraacetic acid 1.5-3 part, deionized water adds to 100 parts; Described natural anti-dandruff component is cecropin, emodin, baicalin, berberine, magnolol, the mixture of honokiol and diosgenin, and the weight ratio of seven is 1.5-2:2.5-3:4.5-5:1.5-2:6-7:2-3:7-8.
Described natural anti-dandruff component is preferably berberine, the mixture of magnolol and honokiol, and three's weight ratio is 6-8:3-5:9-11.
As preferred scheme, described natural anti-dandruff shampoo, be prepared from by following each component by weight: natural anti-dandruff component 2-2.5 part, sodium lauryl sulphate 7-9 part, lanoline 1.8-2 part, coconut oil diethanol amide 1.4-1.7 part, betanin 1.5-2.5 part, sodium lauroyl glutamate 1.5-2.5 part, pearl essence 0.05-0.09 part, ethylenediaminetetraacetic acid 0.5-1.5 part, deionized water adds to 100 parts; Described natural anti-dandruff component is the mixture of berberine, magnolol and honokiol, and three's weight ratio is 6-8:3-5:9-11.
As preferred scheme, described natural anti-dandruff shampoo, be prepared from by following each component by weight: natural anti-dandruff component 2.1 parts, sodium lauryl sulphate 8 parts, lanoline 1.9 parts, coconut oil diethanol amide 1.5 parts, betanin 2 parts, sodium lauroyl glutamate 2 parts, pearl essence 0.08 part, ethylenediaminetetraacetic acid 1 part, deionized water adds to 100 parts; Described natural anti-dandruff component is the mixture of berberine, magnolol and honokiol, and three's weight ratio is 7:4:10.
Another object of the present invention is to provide the preparation method of described natural anti-dandruff shampoo, comprises following steps:
(1) sodium lauryl sulphate is dissolved in a small amount of deionized water, then adds lanoline and coconut oil diethanol amide, stir;
(2) obtain adding betanin, sodium lauroyl glutamate and ethylenediaminetetraacetic acid post-heating in solution to 70-80 DEG C in step (1), stir simultaneously;
(3) add natural anti-dandruff component and pearl essence in the solution obtained in step (2), stir, lower the temperature after adding remaining deionized water, subpackage after froth breaking cooling, obtains described natural anti-dandruff shampoo.
The preparation method of natural anti-dandruff shampoo of the present invention, use deionized water to be a small amount of in step (1), concrete consumption is for just to dissolve sodium lauryl sulphate.
Compared with prior art; natural anti-dandruff shampoo prepared by the present invention has the following advantages: the present invention can promote dissolubility and the release of effective ingredient by the surfactant (sodium lauryl sulphate, lanoline, coconut oil diethanol amide, sodium lauroyl glutamate etc.) in shampoo and the compatibility of natural anti-dandruff component, can ensure that it can better play a role when shampoo uses.Natural anti-dandruff component cecropin in natural anti-dandruff shampoo of the present invention, emodin, baicalin, berberine, magnolol, honokiol, diosgenin is natural bacteriostatic composition, can suppress and kill the growth of the chlosma producing dandruff, natural anti-dandruff shampoo of the present invention, use safety, natural non-stimulated, gentle to moisten, there is good anti-dandruff effect, use that rear dandruff obviously reduces, hair gloss, not short-tempered, nutritional sufficiency.
Detailed description of the invention
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
Embodiment 1: natural anti-dandruff shampoo
Natural anti-dandruff shampoo in the present embodiment; the each component following by weight is prepared from: berberine 0.7g, magnolol 0.4g, honokiol 1g; sodium lauryl sulphate 8g; lanoline 1.9g, coconut oil diethanol amide 1.5g, betanin 2g; sodium lauroyl glutamate 2g; pearl essence 0.08g, ethylenediaminetetraacetic acid 1g, deionized water adds to 100g.
The preparation method of natural anti-dandruff shampoo in the present embodiment, comprises following steps:
(1) sodium lauryl sulphate is dissolved in a small amount of deionized water, then adds lanoline and coconut oil diethanol amide, stir;
(2) obtain adding betanin, sodium lauroyl glutamate and ethylenediaminetetraacetic acid post-heating in solution to 70-80 DEG C in step (1), stir simultaneously;
(3) add natural anti-dandruff component and pearl essence in the solution obtained in step (2), stir, lower the temperature after adding remaining deionized water, subpackage after froth breaking cooling, obtains described natural anti-dandruff shampoo.
Embodiment 2: natural anti-dandruff shampoo
Natural anti-dandruff shampoo in the present embodiment; the each component following by weight is prepared from: berberine 0.67g, magnolol 0.33g, honokiol 1g; sodium lauryl sulphate 7g; lanoline 1.8g, coconut oil diethanol amide 1.4g, betanin 1.5g; sodium lauroyl glutamate 1.5g; pearl essence 0.05g, ethylenediaminetetraacetic acid 0.5g, deionized water adds to 100g.
In the present embodiment, the preparation method of natural anti-dandruff shampoo is with embodiment 1.
Embodiment 3: natural anti-dandruff shampoo
Natural anti-dandruff shampoo in the present embodiment; the each component following by weight is prepared from: berberine 0.83g, magnolol 0.52g, honokiol 1.15g; sodium lauryl sulphate 9g; lanoline 2g, coconut oil diethanol amide 1.7g, betanin 2.5g; sodium lauroyl glutamate 2.5g; pearl essence 0.09g, ethylenediaminetetraacetic acid 1.5g, deionized water adds to 100g.
In the present embodiment, the preparation method of natural anti-dandruff shampoo is with embodiment 1.
Embodiment 4: natural anti-dandruff shampoo
Natural anti-dandruff shampoo in the present embodiment; the each component following by weight is prepared from: cecropin 0.02g; emodin 0.01g, sodium dialkyl sulfate 2g, lanoline 0.3g; coconut oil diethanol amide 0.5g; betanin 0.23g, sodium lauroyl glutamate 0.3g, pearl essence 0.05g; ethylenediaminetetraacetic acid 0.2g, deionized water adds to 100g.
In the present embodiment, the preparation method of natural anti-dandruff shampoo is with embodiment 1.
Embodiment 5: natural anti-dandruff shampoo
Natural anti-dandruff shampoo in the present embodiment, each component following by weight is prepared from: cecropin 0.2g, emodin 0.3g; baicalin 0.5g, berberine 0.2g, magnolol 0.7g; honokiol 0.3g, diosgenin 0.8g, sodium lauryl sulphate 10g; lanoline 2g, coconut oil diethanol amide 2g, betanin 3g; sodium lauroyl glutamate 3g; pearl essence 0.1g, ethylenediaminetetraacetic acid 3g, deionized water adds to 100g.
In the present embodiment, the preparation method of natural anti-dandruff shampoo is with embodiment 1.
Embodiment 6: natural anti-dandruff shampoo
Natural anti-dandruff shampoo in the present embodiment; the each component following by weight is prepared from: cecropin 0.5g; emodin 0.5g, sodium lauryl sulphate 5g, lanoline 1.5g; coconut oil diethanol amide 1g; betanin 1g, sodium lauroyl glutamate 1g, pearl essence 0.09g; ethylenediaminetetraacetic acid 0.4g, deionized water adds to 100g.
In the present embodiment, the preparation method of natural anti-dandruff shampoo is with embodiment 1.
Embodiment 7: natural anti-dandruff shampoo
Natural anti-dandruff shampoo in the present embodiment, each component following by weight is prepared from: cecropin 0.15g, emodin 0.25g; baicalin 0.45g, berberine 0.15g, magnolol 0.6g; honokiol 0.2g, diosgenin 0.7g, sodium lauryl sulphate 9g; lanoline 1.8g, coconut oil diethanol amide 1.8g, betanin 2.5g; sodium lauroyl glutamate 2.5g; pearl essence 0.09g, ethylenediaminetetraacetic acid 1.5g, deionized water adds to 100g.
In the present embodiment, the preparation method of natural anti-dandruff shampoo is with embodiment 1.
For verifying the excellent properties of shampoo of the present invention further, inventor expands the test of a large amount of Performance Detection further to it, and length limit, and only exemplifies the part test of part most cogency herein.
Experimental example 1: the anti-dandruff evaluation of shampoo
1, laboratory sample
Sample 1-5: the sample prepared by embodiment of the present invention 1-5.
Reference substance 1-3: the composition of reference example 3 and preparation method, wherein:
Reference substance 1: delete berberine honokiol, adjustment honokiol is 2.5g, all the other components and proportioning constant;
Reference substance 2: delete berberine and honokiol, adjustment magnolol is 2.5g, all the other components and proportioning constant;
Reference substance 3: delete magnolol and honokiol, adjustment berberine is 2.5g, all the other components and proportioning constant;
Reference substance 4: the shampoo using embodiment 1 in CN102600052A.
2, experimental technique
The dandruff is the mild seborrheic dermatitis of hair, its formed to divide with epidermis cell accelerate, epidermal area come off accelerate relevant, pityrosporum furfur is cause epidermis cell to divide the one of the main reasons accelerated in the transition hypertrophy of scalp, therefore selects measure and evaluate anti-dandruff effect to pityrosporum furfur with or without inhibitory action and action intensity more in vitro.
(1) sample 1-5 and reference substance 1-4 sterile distilled water are mixed with 10mg/mL.
(2) strain: be separated Pityrosporum oval with containing in rapeseed oil culture medium culturing from the beginning seborrheic dermatitis patient dandruff.
(3) evaluation of result
Bactericidal test criterion: antibacterial circle diameter is greater than 20mm: extremely quick; 15 ~ 20mm: Gao Min; 10 ~ 15mm: in quick; 7 ~ 10mm: hypoallergenic; Be less than 7mm: insensitive.
3, experimental result
Extracorporeal bacteria inhibitor test 3 experiments record average inhibition zone, in table 1.
Table 1: the average inhibition zone of extracorporeal bacteria inhibitor test (mm)
Known according to table 1, compared with reference substance 1-4, the good antimicrobial effect of sample 1-5, sample 1-3 is better, and sample 1 is best.Therefore, the fungistatic effect of shampoo of the present invention is remarkable, and the anti-dandruff effect of the shampoo of embodiment 1 is best.
Experimental example 2: foaming power and foaming stability test
1, test specimen: with experimental example 1.
2, test method:
Get 3mL testing sample and be placed in 50mL tool plug graduated cylinder, adding distil water is diluted to 15mL, adds a cover, concuss 10 times, and immediate record foam volume (mL), records foam volume after 10min again.
3, result of the test
Foaming power and foaming stability test result, in table 2.
Table 2: foaming power and foam stability result (ml)
As shown in Table 2, compared with reference substance 1-4, sample 1-5 produces foaming abundancy, good stability, and sample 1-3 effect is better, and sample 1 is best.Therefore good, the good stability of the foaming effect of shampoo of the present invention, the effect of the shampoo of embodiment 1 is best.
Experimental example 3: histamine phosphate causes test of itching
1, test specimen: with experimental example 1.
2, test method:
Body weight is 350 ~ 450g healthy guinea pig random packet, tests and each group of right back dorsal portion of Cavia porcellus is shaved hair, coating in first 1 day.50min after experiment administration on the same day, hair place is shaved with No. 0 sand paper scratch right back back of Cavia porcellus, and with wound surface Chu Di 0.01% histamine phosphate 0.05mL/ only, after this 0.01%, 0.02%, 0.03%, 0.04% is complied with every 3min ... increasing concen-trations, only be 0.05mL/, till Cavia porcellus occurs later licking right back foot at every turn.With Cavia porcellus occur later licking right back sufficient time histamine phosphate's total amount of giving for itch-threshold, record the itch-threshold of relatively more each group.
3, experimental result
Histamine phosphate causes result of the test of itching, in table 3.
Table 3: histamine phosphate causes result of the test of itching
Known according to table 3, relative with reference substance 1-4, the causing of sample 1-5 is itched effective, and sample 1-3 is better, and sample 1 is best.Therefore, having of shampoo of the present invention causes effect of itching significantly, and the effect of embodiment 1 is best.
Experimental example 4: trial effect
1, test specimen: with embodiment 1.
2, trial method
Use population ages 17 ~ 60 years old.Hair perplexs: dandruff, head pruritus, scalp pomade.
Number on probation: 144 people, wherein each 72 people of men and women, are divided into 9 experimental grouies at random.
Each experimental group uses a kind of sample on probation.Hair washing cycles: 3 days once; Service time: 30 days.Shampooing process: use a shampoo, massages 10 minutes afterflush.
3, result on trial
Shampoo result on trial, in table 4.
Table 4: result on trial (%)
Known according to table 4, compared with reference substance 1-4, the satisfaction of sample 1-5 is high, and the satisfaction of sample 1-3 is higher, and sample 1 is best.Therefore, the user satisfaction of shampoo of the present invention is very high, and the result of use of embodiment 1 is best.
Although above the present invention is described in detail with a general description of the specific embodiments, on basis of the present invention, can make some modifications or improvements it, this will be apparent to those skilled in the art.Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, all belong to the scope of protection of present invention.
Claims (10)
1. a natural anti-dandruff shampoo; it is characterized in that: be prepared from by following each component by weight: natural anti-dandruff component 0.03-3 part; sodium lauryl sulphate 2-10 part; lanoline 0.3-2 part, coconut oil diethanol amide 0.5-2 part, betanin 0.23-3 part; sodium lauroyl glutamate 0.3-3 part; pearl essence 0.05-0.1 part, ethylenediaminetetraacetic acid 0.2-3 part, deionized water adds to 100 parts.
2. natural anti-dandruff shampoo according to claim 1, is characterized in that: described natural anti-dandruff component is cecropin, emodin, baicalin, berberine, magnolol, at least two kinds in honokiol and diosgenin.
3. natural anti-dandruff shampoo according to claim 2, is characterized in that: described natural anti-dandruff component is cecropin and emodin mixture, and both weight ratios are 1-2:1.
4. natural anti-dandruff shampoo according to claim 3, it is characterized in that: be prepared from by following each component by weight: natural anti-dandruff component 0.03-1 part, sodium lauryl sulphate 2-5 part, lanoline 0.3-1.5 part, coconut oil diethanol amide 0.5-1 part, betanin 0.23-1 part, sodium lauroyl glutamate 0.3-1 part, pearl essence 0.05-0.09 part, ethylenediaminetetraacetic acid 0.2-0.4 part, deionized water adds to 100 parts;
Described natural anti-dandruff component is cecropin and emodin mixture, and both weight ratios are 1-2:1.
5. natural anti-dandruff shampoo according to claim 2, it is characterized in that: described natural anti-dandruff component is cecropin, emodin, baicalin, berberine, magnolol, the mixture of honokiol and diosgenin, the weight ratio of seven is 1.5-2:2.5-3:4.5-5:1.5-2:6-7:2-3:7-8.
6. natural anti-dandruff shampoo according to claim 5, it is characterized in that: be prepared from by following each component by weight: natural anti-dandruff component 2.5-3 part, sodium lauryl sulphate 9-10 part, lanoline 1.8-2 part, coconut oil diethanol amide 1.8-2 part, betanin 2.5-3 part, sodium lauroyl glutamate 2.5-3 part, pearl essence 0.09-0.1 part, ethylenediaminetetraacetic acid 1.5-3 part, deionized water adds to 100 parts;
Described natural anti-dandruff component is cecropin, emodin, baicalin, berberine, magnolol, the mixture of honokiol and diosgenin, and the weight ratio of seven is 1.5-2:2.5-3:4.5-5:1.5-2:6-7:2-3:7-8.
7. natural anti-dandruff shampoo according to claim 2, is characterized in that: described natural anti-dandruff component is the mixture of berberine, magnolol and honokiol, and three's weight ratio is 6-8:3-5:9-11.
8. natural anti-dandruff shampoo according to claim 7, it is characterized in that: be prepared from by following each component by weight: natural anti-dandruff component 2-2.5 part, sodium lauryl sulphate 7-9 part, lanoline 1.8-2 part, coconut oil diethanol amide 1.4-1.7 part, betanin 1.5-2.5 part, sodium lauroyl glutamate 1.5-2.5 part, pearl essence 0.05-0.09 part, ethylenediaminetetraacetic acid 0.5-1.5 part, deionized water adds to 100 parts;
Described natural anti-dandruff component is the mixture of berberine, magnolol and honokiol, and three's weight ratio is 6-8:3-5:9-11.
9. natural anti-dandruff shampoo according to claim 8, it is characterized in that: be prepared from by following each component by weight: natural anti-dandruff component 2.1 parts, sodium lauryl sulphate 8 parts, lanoline 1.9 parts, coconut oil diethanol amide 1.5 parts, betanin 2 parts, sodium lauroyl glutamate 2 parts, pearl essence 0.08 part, ethylenediaminetetraacetic acid 1 part, deionized water adds to 100 parts;
Described natural anti-dandruff component is the mixture of berberine, magnolol and honokiol, and three's weight ratio is 7:4:10.
10. the preparation method of natural anti-dandruff shampoo according to any one of claim 1 to 9, is characterized in that: comprise following steps:
(1) sodium lauryl sulphate is dissolved in a small amount of deionized water, then adds lanoline and coconut oil diethanol amide, stir;
(2) obtain adding betanin, sodium lauroyl glutamate and ethylenediaminetetraacetic acid post-heating in solution to 70-80 DEG C in step (1), stir simultaneously;
(3) add natural anti-dandruff component and pearl essence in the solution obtained in step (2), stir, lower the temperature after adding remaining deionized water, subpackage after froth breaking cooling, obtains described natural anti-dandruff shampoo.
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CN105769711B (en) * | 2016-05-18 | 2018-11-16 | 佛山市安安美容保健品有限公司 | A kind of natural anti-dandruff shampoo and preparation method thereof |
CN109646447A (en) * | 2018-12-29 | 2019-04-19 | 昆明医科大学第附属医院 | Application of the chonglou saponin in anti-Malassezia furfur and candida albicans bacterium product |
CN109646447B (en) * | 2018-12-29 | 2021-04-27 | 昆明医科大学第一附属医院 | Application of rhizoma paridis saponin in resisting malassezia furfur and candida albicans products |
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