CN105769711A - Natural anti-dandruff shampoo and preparation method - Google Patents
Natural anti-dandruff shampoo and preparation method Download PDFInfo
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- CN105769711A CN105769711A CN201610329962.0A CN201610329962A CN105769711A CN 105769711 A CN105769711 A CN 105769711A CN 201610329962 A CN201610329962 A CN 201610329962A CN 105769711 A CN105769711 A CN 105769711A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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Abstract
The invention discloses a natural anti-dandruff shampoo and a preparation method. The natural anti-dandruff shampoo is prepared from the following raw materials in parts by weight: 25-35 parts of china root greenbrier leaf extract, 12-16 parts of sodium lauryl sulfate, 4-6 parts of lanolin, 6-8 parts of coconut oil diethanol amide, 3-5 parts of betaine, 2-4 parts of sodium lauroylglutamate, 0.4-0.8 part of ethylenediamine tetraacetic acid disodium, 45-55 parts of deionized water and 0.7-0.9 part of synergist vitamin E and andrographolide, wherein the ratio of the vitamin E to the andrographolide in parts by weight is (6-8) to 1. The natural anti-dandruff shampoo is good in anti-dandruff effect; the effect can be relevant to the ratio of the parts by weight of the vitamin E and the andrographolide in the raw materials; and the anti-dandruff effect is the best when the ratio of the vitamin E to the andrographolide in parts by weight is (6-8) to 1.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of natural anti-dandruff shampoo and preparation method thereof.
Background technology
Along with improving constantly of living standard, people also increasingly pay attention to the image construction of self, and hair just becomes a wherein important ring.Healthy healthy hair can give beautiful bonus point, if seeing that the dandruff of a vast expanse of whiteness interts wherein, is very unpleasant.No matter men and women, the dandruff is many is all a problem given offence, and the women of 59% and 63% male be constantly subjected to this puzzlement, for huge " dandruff worry race ", select selecting properly and use dandruff control shampoo containing to seem to be even more important.At present, the most of dandruff control shampoo containings on market, it is usually and adopts the growth of fungus in Drug inhibition scalp, thus controlling the generation of the dandruff.And this type of anti-dandruff component that arrives mostly is artificial compound, potential safety hazard is there is owing to there is toxicity within the scope of certain use, and life-time service can promote fungus to produce rapidly to resist bacterial strain, resist medicine, this kind of anti-dandruff product cannot fundamentally control and treatment of dandruff, and the exploitation therefore containing the dandruff control shampoo containing of natural anti-dandruff component has realistic meaning and market prospect.
Summary of the invention
It is an object of the invention to provide a kind of natural anti-dandruff shampoo and preparation method thereof.
The above-mentioned purpose of the present invention is achieved by the techniques below scheme:
A kind of natural anti-dandruff shampoo, is prepared from by the raw material of following weight portion: Folium smilacis chinensis extract, 25～35 parts；Sodium lauryl sulphate, 12～16 parts；Lanoline, 4～6 parts；Coconut oil diethanol amide, 6～8 parts；Glycine betaine, 3～5 parts；Sodium lauroyl glutamate, 2～4 parts；Disodiumedetate, 0.4～0.8 part；Deionized water, 45～55 parts；Synergist vitamin E and andrographolide totally 0.7～0.9 part, the weight ratio of vitamin E and andrographolide is 6～8:1；
The preparation method of described Folium smilacis chinensis extract is: dry Folium smilacis chinensis is pulverized by (a), with 70% alcoholic solution circumfluence distillation, merging filtrate, is concentrated into and obtains ethanol extraction concentrated solution without alcohol taste；B (), by step (a) gained ethanol extraction concentrated solution dilute with water, successively with petroleum ether, ethyl acetate and water saturated n-butanol extraction, concentrating under reduced pressure, respectively obtains petroleum ether extract, acetic acid ethyl ester extract and n-butyl alcohol extract；C () n-butyl alcohol extract water dissolution, filters, filtrate is with AB-8 type macroporous resin enrichment active component, first remove big polar component with 6 column volumes of 20% alcohol flushing, then with 12 column volumes of 75% ethanol elution, collect 75% ethanol elution, concentrating under reduced pressure, spray drying and get final product.
Further, described natural anti-dandruff shampoo is prepared from by the raw material of following weight portion: Folium smilacis chinensis extract, 30 parts；Sodium lauryl sulphate, 14 parts；Lanoline, 5 parts；Coconut oil diethanol amide, 7 parts；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodiumedetate, 0.6 part；Deionized water, 50 parts；Synergist vitamin E and andrographolide totally 0.8 part, the weight ratio of vitamin E and andrographolide is 7:1.
Further, described natural anti-dandruff shampoo is prepared from by the raw material of following weight portion: Folium smilacis chinensis extract, 25 parts；Sodium lauryl sulphate, 12 parts；Lanoline, 4 parts；Coconut oil diethanol amide, 6 parts；Glycine betaine, 3 parts；Sodium lauroyl glutamate, 2 parts；Disodiumedetate, 0.4 part；Deionized water, 45 parts；Synergist vitamin E and andrographolide totally 0.7 part, the weight ratio of vitamin E and andrographolide is 6:1.
Further, described natural anti-dandruff shampoo is prepared from by the raw material of following weight portion: Folium smilacis chinensis extract, 35 parts；Sodium lauryl sulphate, 16 parts；Lanoline, 6 parts；Coconut oil diethanol amide, 8 parts；Glycine betaine, 5 parts；Sodium lauroyl glutamate, 4 parts；Disodiumedetate, 0.8 part；Deionized water, 55 parts；Synergist vitamin E and andrographolide totally 0.9 part, the weight ratio of vitamin E and andrographolide is 8:1.
The preparation method of above-mentioned natural anti-dandruff shampoo, comprises the steps:
Step S1, is dissolved in sodium lauryl sulphate in a small amount of deionized water, adds lanoline and coconut oil diethanol amide, stirs；
Step S2, obtains adding glycine betaine, sodium lauroyl glutamate and disodiumedetate post-heating in solution to 70～80 DEG C in step S1, stirs；
Step S3, adds Folium smilacis chinensis extract, vitamin E and andrographolide in the step S2 solution obtained, stirs, lowers the temperature after adding remaining deionized water, and subpackage after froth breaking is lowered the temperature obtains described natural anti-dandruff shampoo.
Advantages of the present invention:
Shampoo provided by the invention is anti-dandruff effective, and this effect is likely to relevant with the weight ratio of vitamin E in raw material and andrographolide, and when the weight ratio of vitamin E and andrographolide is 6～8:1, anti-dandruff effect is best.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit scope with this.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, it is possible to technical scheme is modified or equivalent replacement, without deviating from the spirit and scope of technical solution of the present invention.
In the present invention, the preparation method of Folium smilacis chinensis extract is: dry Folium smilacis chinensis is pulverized by (a), with 70% alcoholic solution circumfluence distillation, merging filtrate, is concentrated into and obtains ethanol extraction concentrated solution without alcohol taste；B (), by step (a) gained ethanol extraction concentrated solution dilute with water, successively with petroleum ether, ethyl acetate and water saturated n-butanol extraction, concentrating under reduced pressure, respectively obtains petroleum ether extract, acetic acid ethyl ester extract and n-butyl alcohol extract；C () n-butyl alcohol extract water dissolution, filters, filtrate is with AB-8 type macroporous resin enrichment active component, first remove big polar component with 6 column volumes of 20% alcohol flushing, then with 12 column volumes of 75% ethanol elution, collect 75% ethanol elution, concentrating under reduced pressure, spray drying and get final product.
Embodiment 1: the preparation of natural anti-dandruff shampoo
Parts by weight of raw materials compares:
Folium smilacis chinensis extract, 30 parts；Sodium lauryl sulphate, 14 parts；Lanoline, 5 parts；Coconut oil diethanol amide, 7 parts；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodiumedetate, 0.6 part；Deionized water, 50 parts；Synergist vitamin E and andrographolide totally 0.8 part, the weight ratio of vitamin E and andrographolide is 7:1.
Preparation method:
Step S1, is dissolved in sodium lauryl sulphate in a small amount of deionized water, adds lanoline and coconut oil diethanol amide, stirs；
Step S2, obtains adding glycine betaine, sodium lauroyl glutamate and disodiumedetate post-heating in solution to 70～80 DEG C in step S1, stirs；
Step S3, adds Folium smilacis chinensis extract, vitamin E and andrographolide in the step S2 solution obtained, stirs, lowers the temperature after adding remaining deionized water, and subpackage after froth breaking is lowered the temperature obtains described natural anti-dandruff shampoo.
Embodiment 2: the preparation of natural anti-dandruff shampoo
Parts by weight of raw materials compares:
Folium smilacis chinensis extract, 25 parts；Sodium lauryl sulphate, 12 parts；Lanoline, 4 parts；Coconut oil diethanol amide, 6 parts；Glycine betaine, 3 parts；Sodium lauroyl glutamate, 2 parts；Disodiumedetate, 0.4 part；Deionized water, 45 parts；Synergist vitamin E and andrographolide totally 0.7 part, the weight ratio of vitamin E and andrographolide is 6:1.
Preparation method:
Step S1, is dissolved in sodium lauryl sulphate in a small amount of deionized water, adds lanoline and coconut oil diethanol amide, stirs；
Step S2, obtains adding glycine betaine, sodium lauroyl glutamate and disodiumedetate post-heating in solution to 70～80 DEG C in step S1, stirs；
Step S3, adds Folium smilacis chinensis extract, vitamin E and andrographolide in the step S2 solution obtained, stirs, lowers the temperature after adding remaining deionized water, and subpackage after froth breaking is lowered the temperature obtains described natural anti-dandruff shampoo.
Embodiment 3: the preparation of natural anti-dandruff shampoo
Parts by weight of raw materials compares:
Folium smilacis chinensis extract, 35 parts；Sodium lauryl sulphate, 16 parts；Lanoline, 6 parts；Coconut oil diethanol amide, 8 parts；Glycine betaine, 5 parts；Sodium lauroyl glutamate, 4 parts；Disodiumedetate, 0.8 part；Deionized water, 55 parts；Synergist vitamin E and andrographolide totally 0.9 part, the weight ratio of vitamin E and andrographolide is 8:1.
Preparation method:
Step S1, is dissolved in sodium lauryl sulphate in a small amount of deionized water, adds lanoline and coconut oil diethanol amide, stirs；
Step S2, obtains adding glycine betaine, sodium lauroyl glutamate and disodiumedetate post-heating in solution to 70～80 DEG C in step S1, stirs；
Step S3, adds Folium smilacis chinensis extract, vitamin E and andrographolide in the step S2 solution obtained, stirs, lowers the temperature after adding remaining deionized water, and subpackage after froth breaking is lowered the temperature obtains described natural anti-dandruff shampoo.
Embodiment 4: the preparation of natural anti-dandruff shampoo
Parts by weight of raw materials compares:
Folium smilacis chinensis extract, 30 parts；Sodium lauryl sulphate, 14 parts；Lanoline, 5 parts；Coconut oil diethanol amide, 7 parts；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodiumedetate, 0.6 part；Deionized water, 50 parts；Synergist vitamin E and andrographolide totally 0.8 part, the weight ratio of vitamin E and andrographolide is 6:1.
Preparation method:
Step S1, is dissolved in sodium lauryl sulphate in a small amount of deionized water, adds lanoline and coconut oil diethanol amide, stirs；
Step S2, obtains adding glycine betaine, sodium lauroyl glutamate and disodiumedetate post-heating in solution to 70～80 DEG C in step S1, stirs；
Step S3, adds Folium smilacis chinensis extract, vitamin E and andrographolide in the step S2 solution obtained, stirs, lowers the temperature after adding remaining deionized water, and subpackage after froth breaking is lowered the temperature obtains described natural anti-dandruff shampoo.
Embodiment 5: the preparation of natural anti-dandruff shampoo
Parts by weight of raw materials compares:
Folium smilacis chinensis extract, 30 parts；Sodium lauryl sulphate, 14 parts；Lanoline, 5 parts；Coconut oil diethanol amide, 7 parts；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodiumedetate, 0.6 part；Deionized water, 50 parts；Synergist vitamin E and andrographolide totally 0.8 part, the weight ratio of vitamin E and andrographolide is 8:1.
Preparation method:
Step S1, is dissolved in sodium lauryl sulphate in a small amount of deionized water, adds lanoline and coconut oil diethanol amide, stirs；
Step S2, obtains adding glycine betaine, sodium lauroyl glutamate and disodiumedetate post-heating in solution to 70～80 DEG C in step S1, stirs；
Step S3, adds Folium smilacis chinensis extract, vitamin E and andrographolide in the step S2 solution obtained, stirs, lowers the temperature after adding remaining deionized water, and subpackage after froth breaking is lowered the temperature obtains described natural anti-dandruff shampoo.
The weight ratio of embodiment 6: comparative example, vitamin E and andrographolide is 5:1
Parts by weight of raw materials compares:
Folium smilacis chinensis extract, 30 parts；Sodium lauryl sulphate, 14 parts；Lanoline, 5 parts；Coconut oil diethanol amide, 7 parts；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodiumedetate, 0.6 part；Deionized water, 50 parts；Synergist vitamin E and andrographolide totally 0.8 part, the weight ratio of vitamin E and andrographolide is 5:1.
Preparation method:
Step S1, is dissolved in sodium lauryl sulphate in a small amount of deionized water, adds lanoline and coconut oil diethanol amide, stirs；
Step S2, obtains adding glycine betaine, sodium lauroyl glutamate and disodiumedetate post-heating in solution to 70～80 DEG C in step S1, stirs；
Step S3, adds Folium smilacis chinensis extract, vitamin E and andrographolide in the step S2 solution obtained, stirs, lowers the temperature after adding remaining deionized water, and subpackage after froth breaking is lowered the temperature obtains described natural anti-dandruff shampoo.
The weight ratio of embodiment 7: comparative example, vitamin E and andrographolide is 9:1
Parts by weight of raw materials compares:
Folium smilacis chinensis extract, 30 parts；Sodium lauryl sulphate, 14 parts；Lanoline, 5 parts；Coconut oil diethanol amide, 7 parts；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodiumedetate, 0.6 part；Deionized water, 50 parts；Synergist vitamin E and andrographolide totally 0.8 part, the weight ratio of vitamin E and andrographolide is 9:1.
Preparation method:
Step S1, is dissolved in sodium lauryl sulphate in a small amount of deionized water, adds lanoline and coconut oil diethanol amide, stirs；
Step S2, obtains adding glycine betaine, sodium lauroyl glutamate and disodiumedetate post-heating in solution to 70～80 DEG C in step S1, stirs；
Step S3, adds Folium smilacis chinensis extract, vitamin E and andrographolide in the step S2 solution obtained, stirs, lowers the temperature after adding remaining deionized water, and subpackage after froth breaking is lowered the temperature obtains described natural anti-dandruff shampoo.
Embodiment 8: effect example
70 dandruff patients are tested.It is divided into 7 groups, often organizes 10 people, embodiment 1～7 is tested.Using method is: use the shampoo hair washing of embodiment 1～7 preparation, within two days, wash once, use 30 days continuously, observe the therapeutic effect of dandruff, being estimated with complete treated effect (no longer having dandruff number to account for the percentage ratio of this group total number of persons after use), result of the test is shown in following table.
| Complete treated effect (%) | |
| Embodiment 1 | 100 |
| Embodiment 4 | 100 |
| Embodiment 5 | 100 |
| Embodiment 6 | 60 |
| Embodiment 7 | 50 |
Embodiment 2,3 effect is consistent with embodiment 4,5.
It is shown that shampoo provided by the invention is anti-dandruff effective, this effect is likely to relevant with the weight ratio of vitamin E in raw material and andrographolide, and when the weight ratio of vitamin E and andrographolide is 6～8:1, anti-dandruff effect is best.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit protection scope of the present invention with this.It will be understood by those within the art that, it is possible to technical scheme is modified or equivalent replacement, without deviating from essence and the protection domain of technical solution of the present invention.
Claims (5)
1. a natural anti-dandruff shampoo, it is characterised in that be prepared from by the raw material of following weight portion: Folium smilacis chinensis extract, 25～35 parts；Sodium lauryl sulphate, 12～16 parts；Lanoline, 4～6 parts；Coconut oil diethanol amide, 6～8 parts；Glycine betaine, 3～5 parts；Sodium lauroyl glutamate, 2～4 parts；Disodiumedetate, 0.4～0.8 part；Deionized water, 45～55 parts；Synergist vitamin E and andrographolide totally 0.7～0.9 part, the weight ratio of vitamin E and andrographolide is 6～8:1；
The preparation method of described Folium smilacis chinensis extract is: dry Folium smilacis chinensis is pulverized by (a), with 70% alcoholic solution circumfluence distillation, merging filtrate, is concentrated into and obtains ethanol extraction concentrated solution without alcohol taste；B (), by step (a) gained ethanol extraction concentrated solution dilute with water, successively with petroleum ether, ethyl acetate and water saturated n-butanol extraction, concentrating under reduced pressure, respectively obtains petroleum ether extract, acetic acid ethyl ester extract and n-butyl alcohol extract；C () n-butyl alcohol extract water dissolution, filters, filtrate is with AB-8 type macroporous resin enrichment active component, first remove big polar component with 6 column volumes of 20% alcohol flushing, then with 12 column volumes of 75% ethanol elution, collect 75% ethanol elution, concentrating under reduced pressure, spray drying and get final product.
2. natural anti-dandruff shampoo according to claim 1, it is characterised in that be prepared from by the raw material of following weight portion: Folium smilacis chinensis extract, 30 parts；Sodium lauryl sulphate, 14 parts；Lanoline, 5 parts；Coconut oil diethanol amide, 7 parts；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodiumedetate, 0.6 part；Deionized water, 50 parts；Synergist vitamin E and andrographolide totally 0.8 part, the weight ratio of vitamin E and andrographolide is 7:1.
3. natural anti-dandruff shampoo according to claim 1, it is characterised in that be prepared from by the raw material of following weight portion: Folium smilacis chinensis extract, 25 parts；Sodium lauryl sulphate, 12 parts；Lanoline, 4 parts；Coconut oil diethanol amide, 6 parts；Glycine betaine, 3 parts；Sodium lauroyl glutamate, 2 parts；Disodiumedetate, 0.4 part；Deionized water, 45 parts；Synergist vitamin E and andrographolide totally 0.7 part, the weight ratio of vitamin E and andrographolide is 6:1.
4. natural anti-dandruff shampoo according to claim 1, it is characterised in that be prepared from by the raw material of following weight portion: Folium smilacis chinensis extract, 35 parts；Sodium lauryl sulphate, 16 parts；Lanoline, 6 parts；Coconut oil diethanol amide, 8 parts；Glycine betaine, 5 parts；Sodium lauroyl glutamate, 4 parts；Disodiumedetate, 0.8 part；Deionized water, 55 parts；Synergist vitamin E and andrographolide totally 0.9 part, the weight ratio of vitamin E and andrographolide is 8:1.
5. the preparation method of the arbitrary described natural anti-dandruff shampoo of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, is dissolved in sodium lauryl sulphate in a small amount of deionized water, adds lanoline and coconut oil diethanol amide, stirs；
Step S2, obtains adding glycine betaine, sodium lauroyl glutamate and disodiumedetate post-heating in solution to 70～80 DEG C in step S1, stirs；
Step S3, adds Folium smilacis chinensis extract, vitamin E and andrographolide in the step S2 solution obtained, stirs, lowers the temperature after adding remaining deionized water, and subpackage after froth breaking is lowered the temperature obtains described natural anti-dandruff shampoo.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102716045A (en) * | 2012-06-11 | 2012-10-10 | 广东拉芳日化有限公司 | Shampoo composition containing double anti-dandruff agents |
| CN104382760A (en) * | 2014-12-10 | 2015-03-04 | 唯美度科技（北京）有限公司 | Natural anti-dandruff shampoo and preparation method thereof |
| CN105053174A (en) * | 2015-09-17 | 2015-11-18 | 邯郸学院 | Preparation method and application of plant source complex preservative |
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2016
- 2016-05-18 CN CN201610329962.0A patent/CN105769711B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102716045A (en) * | 2012-06-11 | 2012-10-10 | 广东拉芳日化有限公司 | Shampoo composition containing double anti-dandruff agents |
| CN104382760A (en) * | 2014-12-10 | 2015-03-04 | 唯美度科技（北京）有限公司 | Natural anti-dandruff shampoo and preparation method thereof |
| CN105053174A (en) * | 2015-09-17 | 2015-11-18 | 邯郸学院 | Preparation method and application of plant source complex preservative |
Non-Patent Citations (3)
| Title |
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| 国家食品药品监督管理总局执业药师资格认证中心: "《中药学专业知识》", 31 January 2016, 中国医药科技出版社 * |
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| 詹益兴: "《绿色精细化工—天然产品制造法（第1集）》", 31 May 2005, 科学技术文献出版社 * |
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