CN105769711B - A kind of natural anti-dandruff shampoo and preparation method thereof - Google Patents
A kind of natural anti-dandruff shampoo and preparation method thereof Download PDFInfo
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- CN105769711B CN105769711B CN201610329962.0A CN201610329962A CN105769711B CN 105769711 B CN105769711 B CN 105769711B CN 201610329962 A CN201610329962 A CN 201610329962A CN 105769711 B CN105769711 B CN 105769711B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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Abstract
The invention discloses a kind of natural anti-dandruff shampoos and preparation method thereof, are prepared by the raw material of following parts by weight：Chinaroot greenbrier leaf extract, 25~35 parts；Lauryl sodium sulfate, 12~16 parts；Lanolin, 4~6 parts；Coconut oil diethanol amide, 6~8 parts；Glycine betaine, 3~5 parts；Sodium lauroyl glutamate, 2~4 parts；Disodium ethylene diamine tetraacetate, 0.4~0.8 part；Deionized water, 45~55 parts；The weight ratio of synergist vitamin E and totally 0.7~0.9 part of andrographolide, vitamin E and andrographolide is 6~8:1.The anti-dandruff effect of shampoo provided by the invention is good, and this effect may be related with the weight ratio of vitamin E in raw material and andrographolide, and the weight part ratio of vitamin E and andrographolide is 6~8:When 1, anti-dandruff effect is best.
Description
Technical field
The invention belongs to cosmetic fields, and in particular to a kind of natural anti-dandruff shampoo and preparation method thereof.
Background technique
With the continuous improvement of living standards, people also increasingly pay attention to the image construction of itself, and hair just becomes it
In an important ring.The healthy hair of health, if seeing that the dandruff of a vast expanse of whiteness is interspersed wherein, can be very very to beautiful bonus point
Landscape.No matter men and women, dandruff is mostly all the problem of giving offence, and 59% women and 63% male are constantly subjected to this
Kind puzzlement selects correct selection and seems using dandruff control shampoo containing to be even more important for huge " dandruff worry race ".Mesh
Before, the growth of fungi in Drug inhibition scalp is usually used in most of dandruff control shampoo containings in the market, to control dandruff
Generation.And such anti-dandruff component that arrives is mostly artificial compound, there is safety due to having toxicity in certain use scope
Hidden danger, and being used for a long time can promote fungi to generate resistance bacterial strain rapidly, to resist drug, this kind of anti-dandruff product can not be fundamentally
Control and treatment of dandruff, therefore before the exploitation of the dandruff control shampoo containing containing natural anti-dandruff component has realistic meaning and market
Scape.
Summary of the invention
The purpose of the present invention is to provide a kind of natural anti-dandruff shampoos and preparation method thereof.
Above-mentioned purpose of the invention is achieved by following technical solution：
A kind of natural anti-dandruff shampoo, is prepared by the raw material of following parts by weight：Chinaroot greenbrier leaf extract, 25~35
Part；Lauryl sodium sulfate, 12~16 parts；Lanolin, 4~6 parts；Coconut oil diethanol amide, 6~8 parts；Glycine betaine, 3~5
Part；Sodium lauroyl glutamate, 2~4 parts；Disodium ethylene diamine tetraacetate, 0.4~0.8 part；Deionized water, 45~55 parts；Synergy
The weight ratio of agent vitamin E and totally 0.7~0.9 part of andrographolide, vitamin E and andrographolide is 6~8:1；
The preparation method of the chinaroot greenbrier leaf extract is：(a) dry chinaroot greenbrier leaf is crushed, is returned with 70% ethanol solution heat
Stream extracts, merging filtrate, is concentrated into no alcohol taste and obtains ethyl alcohol extraction concentrate；(b) ethyl alcohol obtained by step (a) is extracted into concentrate
It is diluted with water, successively uses petroleum ether, ethyl acetate and water saturated extracting n-butyl alcohol, be concentrated under reduced pressure, respectively obtain petroleum ether extraction
Take object, acetic acid ethyl ester extract and n-butyl alcohol extract；(c) n-butyl alcohol extract is dissolved with water, filtering, and filtrate is big with AB-8 type
Hole resin concentration active constituent first rinses 6 column volumes with 20% ethyl alcohol and removes big polar components, then with 75% ethanol elution 12
A column volume collects 75% ethanol eluate, is concentrated under reduced pressure, is spray-dried to obtain the final product.
Further, the natural anti-dandruff shampoo is prepared by the raw material of following parts by weight：Chinaroot greenbrier leaf extracts
Object, 30 parts；Lauryl sodium sulfate, 14 parts；Lanolin, 5 parts；Coconut oil diethanol amide, 7 parts；Glycine betaine, 4 parts；Lauroyl
Base sodium glutamate, 3 parts；Disodium ethylene diamine tetraacetate, 0.6 part；Deionized water, 50 parts；Synergist vitamin E and andrographolide
Totally 0.8 part, the weight ratio of vitamin E and andrographolide is 7:1.
Further, the natural anti-dandruff shampoo is prepared by the raw material of following parts by weight：Chinaroot greenbrier leaf extracts
Object, 25 parts；Lauryl sodium sulfate, 12 parts；Lanolin, 4 parts；Coconut oil diethanol amide, 6 parts；Glycine betaine, 3 parts；Lauroyl
Base sodium glutamate, 2 parts；Disodium ethylene diamine tetraacetate, 0.4 part；Deionized water, 45 parts；Synergist vitamin E and andrographolide
Totally 0.7 part, the weight ratio of vitamin E and andrographolide is 6:1.
Further, the natural anti-dandruff shampoo is prepared by the raw material of following parts by weight：Chinaroot greenbrier leaf extracts
Object, 35 parts；Lauryl sodium sulfate, 16 parts；Lanolin, 6 parts；Coconut oil diethanol amide, 8 parts；Glycine betaine, 5 parts；Lauroyl
Base sodium glutamate, 4 parts；Disodium ethylene diamine tetraacetate, 0.8 part；Deionized water, 55 parts；Synergist vitamin E and andrographolide
Totally 0.9 part, the weight ratio of vitamin E and andrographolide is 8:1.
The preparation method of above-mentioned natural anti-dandruff shampoo, includes the following steps：
Lauryl sodium sulfate is dissolved in a small amount of deionized water by step S1, adds lanolin and coconut oil diethanol
Amide stirs evenly；
Step S2 obtains that glycine betaine, sodium lauroyl glutamate and ethylenediamine tetra-acetic acid two are added in solution in step S1
It is heated to 70~80 DEG C after sodium, stirs evenly；
Chinaroot greenbrier leaf extract, vitamin E and andrographolide is added in step S3 in the solution that step S2 is obtained, and is added
It stirs evenly, cool down after remaining deionized water, dispensed after defoaming cooling, obtain the natural anti-dandruff shampoo.
Advantages of the present invention：
The anti-dandruff effect of shampoo provided by the invention is good, and this effect may be with vitamin E in raw material and andrographolide
Weight ratio it is related, the weight ratio of vitamin E and andrographolide is 6~8:When 1, anti-dandruff effect is best.
Specific embodiment
Essentiality content of the invention is further illustrated below with reference to embodiment, but present invention protection model is not limited with this
It encloses.Although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should understand that, it can be right
Technical solution of the present invention is modified or replaced equivalently, without departing from the spirit and scope of technical solution of the present invention.
In the present invention, the preparation method of chinaroot greenbrier leaf extract is：(a) dry chinaroot greenbrier leaf is crushed, it is molten with 70% ethyl alcohol
Liquid circumfluence distillation, merging filtrate are concentrated into no alcohol taste and obtain ethyl alcohol extraction concentrate；(b) ethyl alcohol obtained by step (a) is extracted
Concentrate is diluted with water, and successively uses petroleum ether, ethyl acetate and water saturated extracting n-butyl alcohol, is concentrated under reduced pressure, respectively obtains stone
Oily ether extract, acetic acid ethyl ester extract and n-butyl alcohol extract；(c) n-butyl alcohol extract is dissolved with water, and filtering, filtrate is used
AB-8 type macroporous resin enrichment active constituent first rinses 6 column volumes with 20% ethyl alcohol and removes big polar components, then with 75% second
Alcohol elutes 12 column volumes, collects 75% ethanol eluate, is concentrated under reduced pressure, is spray-dried to obtain the final product.
Embodiment 1：The preparation of natural anti-dandruff shampoo
Parts by weight of raw materials ratio：
Chinaroot greenbrier leaf extract, 30 parts；Lauryl sodium sulfate, 14 parts；Lanolin, 5 parts；Coconut oil diethanol amide, 7
Part；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodium ethylene diamine tetraacetate, 0.6 part；Deionized water, 50 parts；Synergy
The weight ratio of agent vitamin E and totally 0.8 part of andrographolide, vitamin E and andrographolide is 7:1.
Preparation method：
Lauryl sodium sulfate is dissolved in a small amount of deionized water by step S1, adds lanolin and coconut oil diethanol
Amide stirs evenly；
Step S2 obtains that glycine betaine, sodium lauroyl glutamate and ethylenediamine tetra-acetic acid two are added in solution in step S1
It is heated to 70~80 DEG C after sodium, stirs evenly；
Chinaroot greenbrier leaf extract, vitamin E and andrographolide is added in step S3 in the solution that step S2 is obtained, and is added
It stirs evenly, cool down after remaining deionized water, dispensed after defoaming cooling, obtain the natural anti-dandruff shampoo.
Embodiment 2：The preparation of natural anti-dandruff shampoo
Parts by weight of raw materials ratio：
Chinaroot greenbrier leaf extract, 25 parts；Lauryl sodium sulfate, 12 parts；Lanolin, 4 parts；Coconut oil diethanol amide, 6
Part；Glycine betaine, 3 parts；Sodium lauroyl glutamate, 2 parts；Disodium ethylene diamine tetraacetate, 0.4 part；Deionized water, 45 parts；Synergy
The weight ratio of agent vitamin E and totally 0.7 part of andrographolide, vitamin E and andrographolide is 6:1.
Preparation method：
Lauryl sodium sulfate is dissolved in a small amount of deionized water by step S1, adds lanolin and coconut oil diethanol
Amide stirs evenly；
Step S2 obtains that glycine betaine, sodium lauroyl glutamate and ethylenediamine tetra-acetic acid two are added in solution in step S1
It is heated to 70~80 DEG C after sodium, stirs evenly；
Chinaroot greenbrier leaf extract, vitamin E and andrographolide is added in step S3 in the solution that step S2 is obtained, and is added
It stirs evenly, cool down after remaining deionized water, dispensed after defoaming cooling, obtain the natural anti-dandruff shampoo.
Embodiment 3：The preparation of natural anti-dandruff shampoo
Parts by weight of raw materials ratio：
Chinaroot greenbrier leaf extract, 35 parts；Lauryl sodium sulfate, 16 parts；Lanolin, 6 parts；Coconut oil diethanol amide, 8
Part；Glycine betaine, 5 parts；Sodium lauroyl glutamate, 4 parts；Disodium ethylene diamine tetraacetate, 0.8 part；Deionized water, 55 parts；Synergy
The weight ratio of agent vitamin E and totally 0.9 part of andrographolide, vitamin E and andrographolide is 8:1.
Preparation method：
Lauryl sodium sulfate is dissolved in a small amount of deionized water by step S1, adds lanolin and coconut oil diethanol
Amide stirs evenly；
Step S2 obtains that glycine betaine, sodium lauroyl glutamate and ethylenediamine tetra-acetic acid two are added in solution in step S1
It is heated to 70~80 DEG C after sodium, stirs evenly；
Chinaroot greenbrier leaf extract, vitamin E and andrographolide is added in step S3 in the solution that step S2 is obtained, and is added
It stirs evenly, cool down after remaining deionized water, dispensed after defoaming cooling, obtain the natural anti-dandruff shampoo.
Embodiment 4：The preparation of natural anti-dandruff shampoo
Parts by weight of raw materials ratio：
Chinaroot greenbrier leaf extract, 30 parts；Lauryl sodium sulfate, 14 parts；Lanolin, 5 parts；Coconut oil diethanol amide, 7
Part；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodium ethylene diamine tetraacetate, 0.6 part；Deionized water, 50 parts；Synergy
The weight ratio of agent vitamin E and totally 0.8 part of andrographolide, vitamin E and andrographolide is 6:1.
Preparation method：
Lauryl sodium sulfate is dissolved in a small amount of deionized water by step S1, adds lanolin and coconut oil diethanol
Amide stirs evenly；
Step S2 obtains that glycine betaine, sodium lauroyl glutamate and ethylenediamine tetra-acetic acid two are added in solution in step S1
It is heated to 70~80 DEG C after sodium, stirs evenly；
Chinaroot greenbrier leaf extract, vitamin E and andrographolide is added in step S3 in the solution that step S2 is obtained, and is added
It stirs evenly, cool down after remaining deionized water, dispensed after defoaming cooling, obtain the natural anti-dandruff shampoo.
Embodiment 5：The preparation of natural anti-dandruff shampoo
Parts by weight of raw materials ratio：
Chinaroot greenbrier leaf extract, 30 parts；Lauryl sodium sulfate, 14 parts；Lanolin, 5 parts；Coconut oil diethanol amide, 7
Part；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodium ethylene diamine tetraacetate, 0.6 part；Deionized water, 50 parts；Synergy
The weight ratio of agent vitamin E and totally 0.8 part of andrographolide, vitamin E and andrographolide is 8:1.
Preparation method：
Lauryl sodium sulfate is dissolved in a small amount of deionized water by step S1, adds lanolin and coconut oil diethanol
Amide stirs evenly；
Step S2 obtains that glycine betaine, sodium lauroyl glutamate and ethylenediamine tetra-acetic acid two are added in solution in step S1
It is heated to 70~80 DEG C after sodium, stirs evenly；
Chinaroot greenbrier leaf extract, vitamin E and andrographolide is added in step S3 in the solution that step S2 is obtained, and is added
It stirs evenly, cool down after remaining deionized water, dispensed after defoaming cooling, obtain the natural anti-dandruff shampoo.
Embodiment 6：The weight ratio of comparative example, vitamin E and andrographolide is 5:1
Parts by weight of raw materials ratio：
Chinaroot greenbrier leaf extract, 30 parts；Lauryl sodium sulfate, 14 parts；Lanolin, 5 parts；Coconut oil diethanol amide, 7
Part；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodium ethylene diamine tetraacetate, 0.6 part；Deionized water, 50 parts；Synergy
The weight ratio of agent vitamin E and totally 0.8 part of andrographolide, vitamin E and andrographolide is 5:1.
Preparation method：
Lauryl sodium sulfate is dissolved in a small amount of deionized water by step S1, adds lanolin and coconut oil diethanol
Amide stirs evenly；
Step S2 obtains that glycine betaine, sodium lauroyl glutamate and ethylenediamine tetra-acetic acid two are added in solution in step S1
It is heated to 70~80 DEG C after sodium, stirs evenly；
Chinaroot greenbrier leaf extract, vitamin E and andrographolide is added in step S3 in the solution that step S2 is obtained, and is added
It stirs evenly, cool down after remaining deionized water, dispensed after defoaming cooling, obtain the natural anti-dandruff shampoo.
Embodiment 7：The weight ratio of comparative example, vitamin E and andrographolide is 9:1
Parts by weight of raw materials ratio：
Chinaroot greenbrier leaf extract, 30 parts；Lauryl sodium sulfate, 14 parts；Lanolin, 5 parts；Coconut oil diethanol amide, 7
Part；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Disodium ethylene diamine tetraacetate, 0.6 part；Deionized water, 50 parts；Synergy
The weight ratio of agent vitamin E and totally 0.8 part of andrographolide, vitamin E and andrographolide is 9:1.
Preparation method：
Lauryl sodium sulfate is dissolved in a small amount of deionized water by step S1, adds lanolin and coconut oil diethanol
Amide stirs evenly；
Step S2 obtains that glycine betaine, sodium lauroyl glutamate and ethylenediamine tetra-acetic acid two are added in solution in step S1
It is heated to 70~80 DEG C after sodium, stirs evenly；
Chinaroot greenbrier leaf extract, vitamin E and andrographolide is added in step S3 in the solution that step S2 is obtained, and is added
It stirs evenly, cool down after remaining deionized water, dispensed after defoaming cooling, obtain the natural anti-dandruff shampoo.
Embodiment 8：Effect example
70 dandruff patients are tested.7 groups are divided into, every group of 10 people test Examples 1 to 7.Make
It is with method：It is washed hair using shampoo prepared by Examples 1 to 7, washes within two days primary, continuous use 30 days, observation dandruff
Therapeutic effect, commented with complete treated effect (there is no the percentages that dandruff number accounts for this group of total number of persons after use)
Estimate, test result see the table below.
| Complete treated effect (%) | |
| Embodiment 1 | 100 |
| Embodiment 4 | 100 |
| Embodiment 5 | 100 |
| Embodiment 6 | 60 |
| Embodiment 7 | 50 |
Embodiment 2,3 effects and embodiment 4,5 are consistent.
The result shows that the anti-dandruff effect of shampoo provided by the invention is good, this effect may with vitamin E in raw material and wear
The weight ratio of heart lotus lactone is related, and the weight ratio of vitamin E and andrographolide is 6~8:When 1, anti-dandruff effect is most
It is good.
The effect of above-described embodiment indicates that essentiality content of the invention, but protection of the invention is not limited with this
Range.Those skilled in the art should understand that can with modification or equivalent replacement of the technical solution of the present invention are made,
Without departing from the essence and protection scope of technical solution of the present invention.
Claims (1)
1. a kind of preparation method of natural anti-dandruff shampoo, it is characterised in that：
The shampoo is prepared by the raw material of following parts by weight：Chinaroot greenbrier leaf extract, 30 parts；Lauryl sodium sulfate, 14 parts；
Lanolin, 5 parts；Coconut oil diethanol amide, 7 parts；Glycine betaine, 4 parts；Sodium lauroyl glutamate, 3 parts；Ethylenediamine tetra-acetic acid
Disodium, 0.6 part；Deionized water, 50 parts；Synergist vitamin E and totally 0.8 part of andrographolide, vitamin E and andrographolide
Weight ratio be 7:1；
Or the shampoo is prepared by the raw material of following parts by weight：Chinaroot greenbrier leaf extract, 25 parts；Lauryl sodium sulfate, 12
Part；Lanolin, 4 parts；Coconut oil diethanol amide, 6 parts；Glycine betaine, 3 parts；Sodium lauroyl glutamate, 2 parts；Ethylenediamine tetrem
Acid disodium, 0.4 part；Deionized water, 45 parts；Synergist vitamin E and totally 0.7 part of andrographolide, in vitamin E and Herba Andrographitis
The weight ratio of ester is 6:1；
Or the shampoo is prepared by the raw material of following parts by weight：Chinaroot greenbrier leaf extract, 35 parts；Lauryl sodium sulfate, 16
Part；Lanolin, 6 parts；Coconut oil diethanol amide, 8 parts；Glycine betaine, 5 parts；Sodium lauroyl glutamate, 4 parts；Ethylenediamine tetrem
Acid disodium, 0.8 part；Deionized water, 55 parts；Synergist vitamin E and totally 0.9 part of andrographolide, in vitamin E and Herba Andrographitis
The weight ratio of ester is 8:1；
The preparation method of the chinaroot greenbrier leaf extract is：(a) dry chinaroot greenbrier leaf is crushed, is mentioned with the reflux of 70% ethanol solution heat
It takes, merging filtrate, is concentrated into no alcohol taste and obtains ethyl alcohol extraction concentrate；(b) ethyl alcohol obtained by step (a) is extracted into concentrate water
Dilution, successively use petroleum ether, ethyl acetate and water saturated extracting n-butyl alcohol, be concentrated under reduced pressure, respectively obtain petroleum ether extract,
Acetic acid ethyl ester extract and n-butyl alcohol extract；(c) n-butyl alcohol extract is dissolved with water, and filtering, filtrate is with AB-8 type macropore tree
Rouge deposition activity ingredient first rinses 6 column volumes with 20% ethyl alcohol and removes big polar components, then with 75% ethanol elution, 12 columns
Volume collects 75% ethanol eluate, is concentrated under reduced pressure, is spray-dried to obtain the final product；
The preparation method of shampoo includes the following steps：
Lauryl sodium sulfate is dissolved in a small amount of deionized water, adds lanolin and coconut oil diethanol amide by step S1,
It stirs evenly；Step S2 obtains that glycine betaine, sodium lauroyl glutamate and ethylenediamine tetra-acetic acid two are added in solution in step S1
It is heated to 70~80 DEG C after sodium, stirs evenly；Chinaroot greenbrier leaf extract, dimension life is added in step S3 in the solution that step S2 is obtained
Plain E and andrographolide are added after remaining deionized water and stir evenly, cool down, and dispense after defoaming cooling, obtain the day
Right dandruff control shampoo containing.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102716045A (en) * | 2012-06-11 | 2012-10-10 | 广东拉芳日化有限公司 | Shampoo composition containing double anti-dandruff agents |
| CN104382760A (en) * | 2014-12-10 | 2015-03-04 | 唯美度科技（北京）有限公司 | Natural anti-dandruff shampoo and preparation method thereof |
| CN105053174A (en) * | 2015-09-17 | 2015-11-18 | 邯郸学院 | Preparation method and application of plant source complex preservative |
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2016
- 2016-05-18 CN CN201610329962.0A patent/CN105769711B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102716045A (en) * | 2012-06-11 | 2012-10-10 | 广东拉芳日化有限公司 | Shampoo composition containing double anti-dandruff agents |
| CN104382760A (en) * | 2014-12-10 | 2015-03-04 | 唯美度科技（北京）有限公司 | Natural anti-dandruff shampoo and preparation method thereof |
| CN105053174A (en) * | 2015-09-17 | 2015-11-18 | 邯郸学院 | Preparation method and application of plant source complex preservative |
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