CN114053195A - Shampoo shower gel and preparation method thereof - Google Patents

Shampoo shower gel and preparation method thereof Download PDF

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CN114053195A
CN114053195A CN202111349077.6A CN202111349077A CN114053195A CN 114053195 A CN114053195 A CN 114053195A CN 202111349077 A CN202111349077 A CN 202111349077A CN 114053195 A CN114053195 A CN 114053195A
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shampoo
surfactant
shower gel
components
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纪黎影
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Xiamen Svert Daily Necessities Co ltd
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Xiamen Svert Daily Necessities Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4993Derivatives containing from 2 to 10 oxyalkylene groups
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/602Glycosides, e.g. rutin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • A61K8/9717Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/596Mixtures of surface active compounds

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Abstract

The invention relates to the technical field of daily chemical articles, and particularly discloses a shampoo and shower gel and a preparation method thereof, wherein the shampoo and shower gel comprises the following components in percentage by weight: 6.5 to 11 percent of first surfactant; 1.4-2.8% of a second surfactant; 6-9.4% of a third surfactant; 1.1 to 1.8 percent of fourth surfactant; 0.6-1% of skin conditioner; 0.2 to 0.6 percent of humectant; 0.11-0.2% of chelating agent; 0.1-0.3% of hair conditioner; 0.08 to 0.12 percent of essence; 0.25 to 0.5 percent of pH regulator; 0.2 to 0.4 percent of preservative; the balance of water; the components of the first surfactant and the weight percentage of each component in the total amount of the shampoo and the shower gel are as follows: 3-5% of cocamidopropyl betaine; 3.5 to 6 percent of water for the first surfactant; the components of the second surfactant and the weight percentage of each component in the total amount of the shampoo and the shower gel are as follows: 1-2% of sorbitan laurate; the second surfactant is 0.4-0.8% of water; the skin conditioner comprises at least one of soapwort extract and Chondrus crispus; the application has the advantages that the irritation of the shampoo and the shower gel to the skin is small.

Description

Shampoo shower gel and preparation method thereof
Technical Field
The invention relates to the technical field of daily chemical articles, in particular to a shampoo and shower gel and a preparation method thereof.
Background
The bath lotion is also called bath foam and bath cream, is a liquid cleanser used during bathing, and has the advantages of no contact with hands, cleanness and the like compared with the traditional solid soap.
Along with the technical development and various requirements of people on the shower gel, the shower gel used for bathing and shampooing gradually appears. At present, the main components of the shampoo and the shower gel are surfactants, and the shampoo and the shower gel also comprise raw materials such as essence, chelating agent, thickening agent and the like. The components such as the surfactant can effectively remove and clean substances such as grease and the like on the surface of the skin and the scalp, and has better cleaning effect.
With the above-mentioned related technologies, various surfactants are currently used, such as alkanolamide and amine oxide surfactants, which have good cleansing effects, but have certain irritation to the skin and scalp, and are liable to damage the skin after long-term use.
Disclosure of Invention
In order to reduce the irritation of the shampoo and the shower gel to the skin, the application provides the shampoo and the shower gel and a preparation method thereof.
In a first aspect, the application provides a shampoo and shower gel, which adopts the following technical scheme:
a shampoo and shower gel comprises the following components in percentage by weight:
6.5 to 11 percent of first surfactant;
1.4-2.8% of a second surfactant;
6-9.4% of a third surfactant;
1.1 to 1.8 percent of fourth surfactant;
0.6-1% of skin conditioner;
0.2 to 0.6 percent of humectant
0.11-0.2% of chelating agent;
0.1-0.3% of hair conditioner;
0.08 to 0.12 percent of essence;
0.25 to 0.5 percent of pH regulator;
0.2 to 0.4 percent of preservative;
the balance of water;
the components of the first surfactant and the weight percentage of each component in the total amount of the shampoo and the shower gel are as follows:
3-5% of cocamidopropyl betaine;
3.5 to 6 percent of water for the first surfactant;
the components of the second surfactant and the weight percentage of each component in the total amount of the shampoo and the shower gel are as follows:
1-2% of sorbitan laurate;
the second surfactant is 0.4-0.8% of water;
the skin conditioner comprises at least one of soapwort extract, Chondrus crispus.
By adopting the technical scheme, the multiple surfactants are matched with each other, so that the skin is effectively cleaned, and the stimulation to the skin is reduced. The soapwort extract and the carrageen are natural substances in the skin conditioner, so that the skin conditioner is nonirritating; on one hand, the two are matched with the surfactant, so that the shampoo has a good cleaning effect, has a promoting effect on the generation of skin collagen, and has a good moisturizing effect, and the moisturizing performance of the shampoo and the shower gel is further improved. The first surfactant is a combination of a zwitterionic surfactant, namely cocamidopropyl betaine and water, and the cocamidopropyl betaine is mainly prepared from coca leaves and betaine, has a cleaning effect and is less irritant to the skin. The second surfactant is a combination of a nonionic surfactant sorbitan laurate and water, and the sorbitan laurate has good emulsifying and penetrating properties and a good cleaning effect. Firstly, respectively and uniformly mixing cocamidopropyl betaine and sorbitan laurate with water so as to carry out effective dispersion; the two different types of surfactants are mixed and compounded with the third surfactant and the fourth surfactant, so that the irritation to the skin and the scalp is further reduced while the cleaning effect of the shampoo and the shower gel is improved.
The moisturizer and the skin conditioner moisturize and moisturize the skin, and the problem of dry skin caused by over-cleaning of the skin by the shower gel is solved. The chelating agent is matched with various surfactants to further enhance the cleaning effect of the shampoo and the shower gel. The hair conditioner is matched with various surfactants to enhance the cleaning capability to scalp and skin; the pH regulator is used for regulating the pH value of the shampoo and shower gel, so that the shampoo and shower gel can better protect the skin and reduce the stimulation to the skin.
In conclusion, at least one of the saponaria officinalis extract and the carrageen crispa is selected as the skin conditioner, and the cocamidopropyl betaine in the first surfactant and the sorbitan laurate in the second surfactant are respectively and uniformly mixed with water, so that the effective dispersion is realized. The post-skin conditioner is compounded with various surfactants, so that the irritation to the skin and the scalp is further reduced while the cleaning effect of the shampoo and the shower gel is improved. The moisturizer, the chelating agent and the pH regulator are added for cooperation, so that the skin cleaning effect of the shampoo and the shower gel is further improved, and the irritation to the skin is reduced.
Preferably, the components of the skin conditioner and the weight percentage of each component in the total amount of the shampoo and the shower gel are as follows:
0.4-0.6% of soapwort extract;
0.2-0.4% of Chondrus crispus.
By adopting the technical scheme, the components of the skin conditioner are preferably selected, and the weight percentage of the components is controlled, so that the moisturizing performance of the shampoo and the shower gel is enhanced, and the irritation is reduced.
Preferably, the components of the third surfactant and the weight percentage of each component in the total amount of the shampoo and shower gel are as follows:
2-3% of sodium lauroamphoacetate;
the third surfactant is water 4-6.4%.
By adopting the technical scheme, firstly, the lauroyl amphoacetate is dispersed by adopting a third surfactant, namely water, and then the third surfactant is added into the shampoo and shower gel to be dissolved with surfactants such as cocamidopropyl betaine, sorbitan laurate and the like, so that the cleaning capability of the shampoo and shower gel is further enhanced. Meanwhile, the sodium lauroamphoacetate has small irritation and is mild, and the irritation of the shampoo and the shower gel can be reduced.
Preferably, the components of the fourth surfactant and the weight percentage of each component in the total amount of the shampoo and shower gel are as follows:
decyl glucoside 0.5-1%;
the fourth surfactant is 0.6-0.8% of water.
By adopting the technical scheme, decyl glucoside is taken as one of novel nonionic surfactants APG, has the characteristics of both nonionic and anionic surfactants, and has relatively low irritation due to extraction from plants. When decyl glucoside is compounded with surfactants such as cocamidopropyl betaine, sorbitan laurate and the like, the irritation of other surfactants is effectively reduced, and the moisturizing effect of the shampoo and the bath cream is enhanced by being matched with a moisturizing agent and a skin conditioner.
Preferably, the components of the moisturizer and the weight percentage of each component in the total amount of the shampoo and the shower gel are as follows:
trehalose 0.1-0.3%;
0.1-0.3% of glyceryl caprylate.
By adopting the technical scheme, the trehalose has higher moisturizing performance and ultraviolet resistance, and is matched with glyceryl caprylate with the moisturizing performance, so that the skin is moisturized while the cleaning capability of the shampoo and the shower gel is ensured, and the problem of dry skin caused by over-cleaning of the shower gel on the skin is solved; meanwhile, the humectant is also matched with the skin conditioner, so that the moisturizing performance of the shampoo and the shower gel is further enhanced.
Preferably, the components of the hair conditioner and the weight percentage of each component in the total amount of the shampoo and the shower gel are as follows:
stearyl dimethyl ammonium hydroxypropyl hydrolyzed fibroin 0.08-0.25%;
0.02-0.05% of the extract of the phyllostachys pubescens.
By adopting the technical scheme, the stearyl dimethyl ammonium hydroxypropyl hydrolyzed fibroin serving as the zwitterionic surfactant of ammonium amino acid salts has excellent dispersing, emulsifying and cleaning capabilities, but has relatively high irritation compared with surfactants such as the first surfactant and the second surfactant. The Phyllostachys Pubescens extract is mainly derived from leaf and stem of Phyllostachys Pubescens, is natural, and has no irritation; the hair washing and bathing liquid has excellent dispersing, emulsifying and cleaning capabilities, reduces irritation to skin and has better hair moistening and caring effects at the same time by combining a hair conditioner consisting of stearyl dimethyl ammonium hydroxypropyl hydrolyzed fibroin and the phyllostachys pubescens with cocamidopropyl betaine, sorbitan laurate, sodium lauroamphoacetate and decyl glucoside.
Preferably, the components of the chelating agent and the weight percentage of each component in the total amount of the shampoo and shower gel are as follows:
0.08 to 0.12 percent of caprylyl hydroximic acid;
0.03-0.08% of EDTA-disodium.
By adopting the technical scheme, the octanoyl hydroximic acid is used as the organic acid, and can carry out efficient and selective chelation capacity on ferrous ions and ferric ions. After the caprylyl hydroximic acid is matched with the EDTA-disodium, the caprylyl hydroximic acid is beneficial to being matched with various surfactants, and the cleaning effect of the shampoo and the shower gel is enhanced. The two are also matched with the preservative, and the preservative is easier to permeate into the bacteria by chelating calcium ions on the bacterial cell membrane, so that better preservative performance is achieved.
Preferably, the pH adjusting agent is citric acid.
By adopting the technical scheme, although various surfactants adopted in the shampoo and shower gel have better cleaning capability, most of the surfactants are alkaline surfactants, and the skin of a human body is weakly acidic, so that the shampoo and shower gel is easy to stimulate the skin after being used for a long time. By preferably adding citric acid, the neutralization is effectively carried out, and the irritation and harm of the alkaline surfactant to the skin are reduced; in addition, citric acid can also accelerate stratum corneum renewal, and has effects of moisturizing skin, etc.
In a second aspect, the application provides a preparation method of a shampoo and shower gel, which adopts the following technical scheme:
a preparation method of the shampoo and the shower gel comprises the following preparation steps:
s1, mixing and stirring a first surfactant, a second surfactant, a third surfactant, a fourth surfactant, a skin conditioner, a humectant, a chelating agent, a hair conditioner, a pH regulator and a preservative water, and uniformly stirring to obtain a first mixture; and S2, adding the essence into the first mixture, mixing and stirring, and filling after stirring uniformly to obtain the shampoo and shower gel.
By adopting the technical scheme, water is heated at first, various surfactants are fully mixed and dissolved, and the coordination effect of various surfactants is promoted. And other substances are added in steps later, so that the problem of partial component effect loss caused by overhigh temperature is solved. And finally, adding a pH regulator to regulate the shampoo and the shower gel, so as to reduce the stimulation to the skin.
Preferably, in the step S1, the stirring speed is 40-50r/min, and the stirring time is 30-40 min; in the step S2, the stirring speed is 40-50r/min, and the stirring time is 4-6 min.
By adopting the technical scheme, various surfactants are better dissolved, the temperature is lower, and the dissolving effect of the surfactants is poorer; the stirring speed is controlled within the range, so that the production efficiency is improved while the intermiscibility is ensured.
In summary, the present application has the following beneficial effects:
1. in the application, a plurality of surfactants are selected and firstly dissolved in water respectively for effective dispersion; the skin conditioner is at least one of soapwort extract and Chondrus crispus, and both are natural substances without irritation; through the matching of the cocamidopropyl betaine, the sorbitan laurate, the third surfactant, the fourth surfactant and the skin conditioner, the cleaning effect of the shampoo and the shower gel is enhanced, the irritation to the skin and the scalp is reduced, and the moisturizing effect is improved.
2. In the application, specific components of the third surfactant and the fourth surfactant are preferably selected, and are better matched with cocamidopropyl betaine and sorbitan laurate, so that the cleaning capability of the shampoo and shower gel is further enhanced, and the irritation is reduced. Specific components of the moisturizing agent, the chelating agent and the pH regulator are preferably selected, so that the skin is effectively cleaned and simultaneously is moisturized, and the irritation of the shampoo and the shower gel to the skin is further reduced.
3. According to the preparation method, various raw materials are added step by step, and meanwhile, the cooling speed of the first mixture is controlled, so that the production efficiency is improved while the intermiscibility is ensured.
Detailed Description
The present application is described in further detail below.
Examples
Example 1A shampoo shower gel comprising the specific components and weights shown in Table 1 was prepared by the following steps: s1, mixing and stirring a first surfactant, a second surfactant, a third surfactant, a fourth surfactant, a skin conditioner, a humectant, a chelating agent, a hair conditioner, a pH regulator and a preservative with water at a stirring speed of 30r/min for 35min to obtain a first mixture;
and S2, adding the essence into the first mixture, mixing and stirring at the speed of 35r/min and 3min, and filling to obtain the shampoo and shower gel.
Examples 2 to 3 a shampoo and body wash differing from example 1 in the specific components and weights included, as shown in table 1.
Examples 4-5A shampoo bath, differing from example 1 in the weight of the specific components of the skin conditioner, the specific components and weights included are as shown in Table 1.
Examples 6 to 7A hair shampoo and shower gel, which is different from example 5 in that the specific components of the third surfactant are different, and the specific components and weights thereof are shown in Table 1.
Examples 8 to 9A hair shampoo and body wash which is different from example 7 in the specific components of the fourth surfactant and the specific components and weights thereof are shown in Table 1.
Examples 10 to 11A hair shampoo and body wash which is different from example 9 in the specific components of the moisturizer, the specific components and weights thereof are shown in Table 1.
TABLE 1 specific Components and weights in examples 1-11
Figure BDA0003355071460000051
Figure BDA0003355071460000061
Examples 12-13A shampoo bath differing from example 11 in the specific components of the hair conditioner, including the specific components and weights shown in Table 2.
Examples 14-15A shampoo bath which differs from example 13 in the specific components of the chelating agent and the specific components and weights included are shown in Table 2.
Examples 16 to 17A shampoo bath which differs from example 15 in that citric acid was used instead of the pH adjuster, and the specific components and weights thereof were as shown in Table 2.
Examples 18 to 19A shampoo bath lotion is different from example 17 in the components and weight, and the specific components and weight are shown in Table 2.
Example 20A shampoo bath cream which is different from example 19 in that in step S1, the stirring speed is 40r/min and the stirring time is 40 min; in the step S2, the stirring speed is 50r/min, and the stirring time is 4 min.
Example 21A shampoo bath cream which is different from example 20 in that in step S1, the stirring speed is 50r/min and the stirring time is 30 min; in the step S2, the stirring speed is 40r/min, and the stirring time is 6 min.
TABLE 2 specific compositions and weights for examples 12-19
Figure BDA0003355071460000071
Comparative example
Comparative example 1 a shampoo bath lotion was distinguished from example 1 in that an equal amount of aloe extract was used instead of soapwort extract.
Comparative example 2 a shampoo bath lotion was distinguished from example 1 in that the same amount of aloe extract was used instead of carrageen crispus.
Comparative example 3 a shampoo bath lotion was distinguished from example 1 in that the extract of aloe vera was used in equal amounts instead of the extract of physalis pubescens and the carrageen crispus.
Comparative example 4 a shampoo bath distinguished from example 1 by the use of an equal amount of propylene glycol oleate instead of sorbitan laurate.
Comparative example 5 a shampoo bath lotion was distinguished from example 1 in that the same amount of propylene glycol oleate was used instead of sorbitan laurate and the same amount of aloe extract was used instead of the primula sikkimensis extract and the carrageen crispus.
Comparative example 6A shampoo shower gel consisting of the following components by weight: 3kg of polyethylene glycol, 4kg of sodium carboxymethylcellulose, 10kg of citric acid, 3kg of sucrose cocoate, 2kg of vitamin E, 3kg of coconut oil, 4kg of lanolin and 70kg of deionized water.
The preparation method comprises the following steps: the components are mixed and stirred uniformly to obtain the shampoo shower gel.
Detection method
Experiment one: irritation test
Experimental samples: examples 1-21 and comparative examples 1-6.
Subject: 54 healthy adult Japanese big-ear rabbits (2.5-3 kg in body weight) were used and divided into 17 groups, corresponding to examples 1-21 and comparative examples 1-6, respectively.
The experimental method comprises the following steps:
the rabbit eyes were checked to be normal, and the next day 0.1mL of a shampoo/10 distilled water dilution was dropped directly into one side of each rabbit, into the conjunctival sac of the eyes, and allowed to passively close for 30 seconds.
Evaluation of irritation: the conjunctiva, cornea and iris of the tested side eye were observed 24 hours after eye dropping to see whether there was any abnormal change.
The scoring criteria were as follows: the score is 1-10, the score is given according to the change degree of the abnormal condition, and the larger the change degree is, the higher the score is, the larger the irritation is; the smaller the degree of change, the lower the score, indicating less irritation. The specified fraction is less than or equal to 3, namely the irritation meets the safety standard.
Experimental results the results of the irritation experiments of examples 1-21 and comparative examples 1-6 are shown in Table 3.
Experiment two: sensory evaluation experimental subjects: in the same area, 81 women in China with healthy lips and 25-35 years old who had no obvious skin wounds and diseases were recruited and divided into 27 experimental groups on average, and the groups were assigned to examples 1-21 and comparative examples 1-6, respectively.
The experimental method comprises the following steps:
grading the cleanliness degree; the subjects used the shampoo and bath according to examples 1-21 and comparative examples 1-6, respectively, with 5ml per shampoo and 6ml per bath. Two weeks of continuous use, the testers scored according to the experience of use.
The scoring criteria were as follows:
the degree of cleanliness: 1-10 points, the better and the fresher the degree of cleaning, the higher the score, the worse the degree of cleaning, the worse the degree of refreshing, and the lower the score.
The hair care effect is as follows: 1-10 points, the better the clean, the fresher the hair, the softer the hair, the higher the score, the worse the clean, the less cool, the softer the hair, the lower the score.
The experimental results are as follows: the experimental results of examples 1 to 21 and comparative examples 1 to 6 are shown in Table 3.
Experiment three: moisture retention test
Experimental samples: examples 1-21 and comparative examples 1-6.
Experimental subjects in the same area, 81 women in China with healthy lips and without obvious skin wounds and diseases in the age of 25-35 years were recruited and divided into 27 experimental groups on average, which correspond to examples 1-21 and comparative examples 1-6, respectively.
An experimental instrument: skin moisture meter Corneometer CM 825.
The experimental method comprises the following steps: the subjects used 6ml of the shampoo and shower gel corresponding to examples 1 to 21 and comparative examples 1 to 6, respectively, for bathing; a skin moisture tester CM 825 is adopted to respectively detect the skin moisture content of the forearm part of the human arm after 1h and 2h of bathing, and the increase rate of the 2h compared with the 1h of the back moisture content is calculated, wherein the calculation formula is (namely the skin moisture content of 2 h-the skin moisture content of 1 h)/the skin moisture content of 1h multiplied by 100%.
Because the moisture of the skin of the human body is not completely dispersed within 1 hour after the human body is bathed, the moisture content is high, and the test accuracy is low. The water after bathing is dissipated after 1h, the effect on the water content of the skin is small, and the influence degree is small, so that 1h after bathing is selected as the starting point for testing the water content of the skin.
The results of the moisturizing performance tests of examples 1-21 and comparative examples 1-6 were obtained using the above test methods, respectively.
The experimental results are as follows: the results of the moisturizing performance tests of examples 1 to 21 and comparative examples 1 to 6 are shown in Table 3
TABLE 3 results of experiments of examples 1 to 21 and comparative examples 1 to 6
Figure BDA0003355071460000091
Figure BDA0003355071460000101
As can be seen from the experimental data in Table 3, the irritation scores of examples 1 to 21 were 0.7 to 2.6, the cleansing degree was 8.1 to 9.4, the hair care effect was 7.7 to 8.8, and the moisture content increase rate was 4.09 to 5.38%; comparative examples 1 to 6 had irritation scores of 3.1 to 5.3, cleansing degrees of 4.5 to 7.3, hair care effects of 5.3 to 7.5, and moisture content growth rates of 1.31 to 3.28%. Examples 1-21 are less irritating and more clean than comparative examples 1-6, while also having better moisturizing properties.
As can be seen from the comparison of example 1 and comparative examples 1 to 3, the combination of soapwort extract and bornel is more effective in moisturizing than the combination of soapwort extract and bornel, while having less irritation and higher cleaning degree than the combination of soapwort extract and bornel. The two have better cooperation effect, and can better enhance the moisturizing performance and the cleaning strength of the shampoo and the shower gel. It can be seen from comparative example 1 and comparative examples 3 to 5 that the second surfactant and the skin conditioner, when added together, provide better moisturizing and cleansing effects and less irritation than the shampoo and body wash obtained by adding them separately.
As can be seen from comparing example 1 with examples 4 to 5, the components and weight of the skin conditioner are preferred, and the moisturizing performance of the shampoo and body wash is improved while the irritation is small; it is demonstrated that the combination of soapwort extract and Chondrus crispus helps to enhance the moisturizing properties of the shampoo compositions.
As can be seen from comparative examples 5-7, a third surfactant component is preferred to help enhance the cleaning benefits of the shampoo compositions, with less irritation. The sodium lauroamphoacetate in the third surfactant can be effectively dispersed and is dissolved with surfactants such as cocamidopropyl betaine, sorbitan laurate and the like, so that the cleaning capability of the shampoo and the shower gel is further enhanced. As is clear from comparative examples 7 to 9, decyl glucoside is preferred as the main component of the fourth surfactant, and the cleansing power of the shampoo and body wash is improved while the irritancy is reduced, and the moisturizing effect is improved; probably, when the surfactants are preferably selected, the first surfactant, the second surfactant, the third surfactant and the fourth surfactant are compounded, so that the irritation to the skin and the scalp is further reduced and the moisturizing effect is improved while the cleaning effect of the shampoo and the shower gel is improved. Comparative examples 9 to 11 show that the moisturizer consisting of trehalose and glyceryl caprylate can enhance the moisturizing performance of the shampoo composition.
As can be seen from comparative examples 11 to 13, the moisturizing performance of the shampoo and body wash was improved by adding the Phyllostachys nigra extract to the hair conditioner, and the hair care effect of the hair was improved by combining the Phyllostachys nigra extract with various surfactants, indicating that the hair care effect of the shampoo and body wash and the moisturizing performance were improved by adding the Phyllostachys nigra extract.
As can be seen from comparative examples 13 to 15, the specific formulation of the chelating agent is preferred to improve the cleansing power of the shampoo composition to some extent. Comparative examples 15 to 17 show that citric acid as a pH adjuster improves the cleansing ability and moisturizing ability of the shampoo and body wash and is less irritating. Probably because the citric acid is acidic, the irritation of the alkaline surfactant to the skin can be effectively reduced, the stratum corneum is accelerated to be renewed, and the moisturizing state of the skin is further enhanced. As is clear from comparative examples 19 to 21, the stirring speed and the stirring time in the production method are preferable, and the irritation of the shampoo and body wash can be reduced.
The present embodiment is only for explaining the present application, and it is not limited to the present application, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present application.

Claims (10)

1. The shampoo and shower gel is characterized by comprising the following components in percentage by weight:
6.5 to 11 percent of first surfactant;
1.4-2.8% of a second surfactant;
6-9.4% of a third surfactant;
1.1 to 1.8 percent of fourth surfactant;
0.6-1% of skin conditioner;
0.2 to 0.6 percent of humectant
0.11-0.2% of chelating agent;
0.1-0.3% of hair conditioner;
0.08 to 0.12 percent of essence;
0.25 to 0.5 percent of pH regulator;
0.2 to 0.4 percent of preservative;
the balance of water;
the components of the first surfactant and the weight percentage of each component in the total amount of the shampoo and the shower gel are as follows:
3-5% of cocamidopropyl betaine;
3.5 to 6 percent of water for the first surfactant;
the components of the second surfactant and the weight percentage of each component in the total amount of the shampoo and the shower gel are as follows:
1-2% of sorbitan laurate;
the second surfactant is 0.4-0.8% of water;
the skin conditioner comprises at least one of soapwort extract, Chondrus crispus.
2. The shampoo and shower gel of claim 1 wherein the components of the skin conditioner and the weight percentages of the components in the total amount of the shampoo and shower gel are:
0.4-0.6% of soapwort extract;
0.2-0.4% of Chondrus crispus.
3. The shampoo and shower gel of claim 1 wherein the components of the third surfactant and the weight percentages of the components in the total amount of the shampoo and shower gel are:
2-3% of sodium lauroamphoacetate;
the third surfactant is water 4-6.4%.
4. The shampoo and shower gel of claim 1 wherein the components of the fourth surfactant and the weight percentages of the components in the total amount of the shampoo and shower gel are:
decyl glucoside 0.5-1%;
the fourth surfactant is 0.6-0.8% of water.
5. The shampoo and shower gel of claim 1 wherein the components of the moisturizer and the weight percentages of the components in the total amount of the shampoo and shower gel are as follows:
trehalose 0.1-0.3%;
0.1-0.3% of glyceryl caprylate.
6. The shampoo and shower gel of claim 1 wherein the components of the hair conditioner and the weight percentages of the components in the total amount of the shampoo and shower gel are as follows:
stearyl dimethyl ammonium hydroxypropyl hydrolyzed fibroin 0.08-0.25%;
0.02-0.05% of the extract of the phyllostachys pubescens.
7. The shampoo and shower gel of claim 1 wherein the components of said chelating agent and the weight percentages of the components in the total amount of the shampoo and shower gel are:
0.08 to 0.12 percent of caprylyl hydroximic acid;
0.03-0.08% of EDTA-disodium.
8. A shampoo bath as claimed in claim 1 characterised in that the pH adjuster is citric acid.
9. A method of preparing a shampoo shower gel as claimed in any one of claims 1 to 8 comprising the steps of:
s1, mixing and stirring a first surfactant, a second surfactant, a third surfactant, a fourth surfactant, a skin conditioner, a humectant, a chelating agent, a hair conditioner, a pH regulator and a preservative water, and uniformly stirring to obtain a first mixture;
and S2, adding the essence into the first mixture, mixing and stirring, and filling after stirring uniformly to obtain the shampoo and shower gel.
10. The method for preparing a hair shampoo and body wash as claimed in claim 9, wherein in the step S1, the stirring speed is 40-50r/min, and the stirring time is 30-40 min; in the step S2, the stirring speed is 40-50r/min, and the stirring time is 4-6 min.
CN202111349077.6A 2021-11-15 2021-11-15 Shampoo shower gel and preparation method thereof Withdrawn CN114053195A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115813820A (en) * 2022-12-14 2023-03-21 福建省梦娇兰日用化学品有限公司 Double-layer shampoo shower gel containing grease and preparation method thereof
CN116236405A (en) * 2023-02-02 2023-06-09 福建省梦娇兰日用化学品有限公司 Shampoo bath lotion containing multiple conditioning agents and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115813820A (en) * 2022-12-14 2023-03-21 福建省梦娇兰日用化学品有限公司 Double-layer shampoo shower gel containing grease and preparation method thereof
CN116236405A (en) * 2023-02-02 2023-06-09 福建省梦娇兰日用化学品有限公司 Shampoo bath lotion containing multiple conditioning agents and preparation method thereof

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