CN104278575A - Preparation method of functional biodegradable polyester fiber patterned woollen blanket - Google Patents
Preparation method of functional biodegradable polyester fiber patterned woollen blanket Download PDFInfo
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- CN104278575A CN104278575A CN201410513462.3A CN201410513462A CN104278575A CN 104278575 A CN104278575 A CN 104278575A CN 201410513462 A CN201410513462 A CN 201410513462A CN 104278575 A CN104278575 A CN 104278575A
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Abstract
The invention provides a preparation method of a functional biodegradable polyester fiber patterned woollen blanket. The preparation method of the functional biodegradable polyester fiber patterned woollen blanket is characterized by specifically comprising the following steps: step one, weaving; step two, carrying out natural lustre finishing; step three, shaping; step four, patterning; step five, carrying out steaming fixation; step six, carrying out functional finishing; step seven, washing with water; step eight, drying; step nine, scalding pattern blanks; and step ten, finishing and packing. According to the preparation method of the functional biodegradable polyester fiber patterned woollen blanket, a warp knitting and weaving technology is adopted, the natural lustre finishing temperature is properly increased, the cloth roller speed is reduced and the fiber is fully stretched; due to the adoption of an enhanced steaming process, the softness, smoothness and fluffiness of the wool surface can be ensured; a nano organic-inorganic complex antimicrobial self-cleaning finishing agent is prepared, and a one-bath-method-based functional finishing technology is adopted, so that the durable antibacterial and warmth retention effects can be achieved; a three-tank washing process is adopted, and a complex soft finishing agent is prepared, so that the touch comfort of the wool surface is ensured; the patterned woollen blanket is soft in hand feel, good in elastic resilience and bright in color, and has antibacterial and warmth retention functions.
Description
Technical field
The present invention relates to the preparation method of the functional printing woollen blanket of biodegradable polyester fiber, belong to textile material technical field.
Background technology
Polyester fiber becomes the textile fabric of maximum application because excellent combination property, cost are low, but polyester fiber is petroleum base synthetic fiber, along with its output of minimizing of petroleum resources will be restricted; In addition, polyester fiber can not be degraded, and the environmental pollution that its discarded object causes is on the rise.Biodegradable polyester fiber is as a kind of aliphatic/aromatic copolyester fiber, in flexibility, elastic recovery, anti-crease property, DIMENSIONAL STABILITY, weather fastness and easy dyeing etc., all there is outstanding advantage, and there is good degradability, more and more cause the concern of people.Compared with conventional polyester fiber, elongation at break and the elastic recovery rate of biodegradable polyester fiber significantly improve, and dyeability significantly improves, thus the functional printing woollen blanket preparation method of existing polyester fiber be not suitable for biodegradable polyester fiber.
Summary of the invention
The object of this invention is to provide the preparation method of the functional printing woollen blanket of biodegradable polyester fiber, make biodegradable polyester fiber can be used in preparing new type functional printing woollen blanket.
In order to achieve the above object, the invention provides the preparation method of the functional printing woollen blanket of a kind of biodegradable polyester fiber, it is characterized in that, concrete steps comprise:
The first step: weave: adopt, through braiding technology for making, biodegradable polyester fiber yarn weaving is become woollen blanket, weaving tension is 7 ~ 10g;
Second step: hot light: woollen blanket is carried out hot light, hot light temperature is 180 ~ 200 DEG C, cloth rewinder roll speed 10 ~ 15m/min;
3rd step: sizing: shaped by the woollen blanket after hot light, setting temperature is 110 ~ 130 DEG C, and cloth rewinder roll speed is 16 ~ 20m/min;
4th step: stamp: the woollen blanket after sizing is carried out stamp, printing temperature is 70 ~ 80 DEG C, concentrator contains low temperature disperse dye, emulsion thickening, softener, shrink-resistant agent, diffusant and dyeing assistant, wherein low temperature disperse dye concentration is 2.3 ~ 2.6%, emulsion thickening concentration is 550 ~ 650g/L, and softer consistency is 5 ~ 6g/L, and shiinkproof finish agent concentration is 18 ~ 22g/L, diffusant concentration is 1 ~ 1.5g/L, and dyeing assistant concentration is 8 ~ 12g/L;
5th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, described steam temperature is 120 ~ 140 DEG C, and it is 55 ~ 70min that gas steams the time;
6th step: functional treatment: preparation organo-mineral complexing antibiotic self-cleaning finishing agent, described organo-mineral complexing antibiotic self-cleaning finishing agent contains antiseptic, modified nano-titanium dioxide, dispersant and finishing auxiliaries, wherein, antimicrobial agent concentration is 40 ~ 50g/L, modified nano-titanium dioxide concentration is 0.7 ~ 0.9%, dispersant concentration is 9 ~ 12g/L, finishing auxiliaries concentration is 9 ~ 12g/L, woollen blanket just after vapour steaming colour fixing immerses above-mentioned organo-mineral complexing antibiotic self-cleaning finishing agent and adopts single bath process to carry out functional treatment, bath raio is 1: 8 ~ 1: 10, arranging temperature is 40 ~ 50 DEG C,
7th step: washing: the woollen blanket after arranging is washed through three road rinsing bowls successively, 1st rinsing bowl temperature is 40 DEG C ~ 50 DEG C, 2nd rinsing bowl temperature is 50 DEG C ~ 60 DEG C, 3rd rinsing bowl temperature is 40 DEG C ~ 50 DEG C, and be added with composite soft finishing agent in the 2nd described rinsing bowl, described composite soft finishing agent contains softener, smooth agent and antistatic additive, wherein, softer consistency is 5 ~ 6g/L, and smooth agent concentration is 10 ~ 15g/L, and antistatic additive concentration is 8 ~ 12g/L;
8th step: dry: dried by the woollen blanket after washing, bake out temperature is 80 ~ 90 DEG C, and cloth rewinder roll speed is 6 ~ 10m/min;
9th step: flower base scalds to be cut: the woollen blanket after drying is carried out hot light and scald cutting, and hot light temperature is 160 ~ 180 DEG C, scalds that to cut temperature be 150 ~ 170 DEG C, and cloth rewinder roll speed is all 6 ~ 10m/min;
Tenth step: arrange packing.
Preferably, the low temperature disperse dye in the 4th described step is Disperse Red 3B.
Preferably, the emulsion thickening in the 4th described step is emulsion thickening EL-80.
Preferably, the softener in the 4th described step is softener Hans LSE.
Preferably, the shrink-resistant agent in the 4th described step is shrink-resistant agent BF-588.
Preferably, the diffusant in the 4th described step is polyoxyethylene ether is main emulsion.
Preferably, the dyeing assistant in the 4th described step is dyeing assistant Goon701.
Preferably, the antiseptic in the 6th described step is antiseptic SHT-108.
Preferably, the dispersant in the 6th described step is dispersant DM-2480.
Preferably, the finishing auxiliaries in the 6th described step is fatty alcohol and ethylene oxide condensate.
Preferably, the softener in the 7th described step is softener Goon1201.
Preferably, the smooth agent in the 7th described step is two amido functional group organic silicon emulsions.
Preferably, described antistatic additive is antistatic additive TK-155.
Compared with prior art, the invention has the beneficial effects as follows:
The present invention has the features such as good flexibility, elastic recovery and dyeability according to biodegradable polyester fiber, adopts through braiding technology for making, suitably improves hot light temperature, reduces cloth rewinder roll speed, fiber is fully stretched; Adopt strengthening Steaming, ensure a softer and smoother touch and bulkiness of matte; Preparation of nano organo-mineral complexing antibiotic self-cleaning finishing agent, adopts single bath process functional treatment technology, reaches the effect that Durable antibacterial is warming; Adopt 3 groove washing process, and prepare composite flexible finishing agent, to ensure the sense of touch comfortableness of matte.Exploitation have soft, elastic recovery good, bright in colour and have the printing woollen blanket of antibacterial thermal insulating function concurrently.The successful exploitation of this product and applying, to reduce petroleum base synthetic fiber use amount and protection of the environment, promote sustainable development all significant.
Detailed description of the invention
Below in conjunction with specific embodiment, set forth the present invention further.Should be understood that these embodiments are only not used in for illustration of the present invention to limit the scope of the invention.In addition should be understood that those skilled in the art can make various changes or modifications the present invention, and these equivalent form of values fall within the application's appended claims limited range equally after the content of having read the present invention's instruction.
Embodiment 1
A preparation method for the functional printing woollen blanket of biodegradable polyester fiber, concrete steps are:
The first step: weave: adopt, through braiding technology for making, biodegradable polyester fiber yarn weaving is become woollen blanket, weaving tension is 9g; Described biodegradable polyester fiber yarn is produced by Jiangsu Heshili New Material Co., Ltd., and model is PBST;
Second step: hot light: woollen blanket is carried out hot light, hot light temperature is 190 DEG C, cloth rewinder roll speed 8m/min;
3rd step: sizing: shaped by the woollen blanket after hot light, setting temperature is 120 DEG C, and cloth rewinder roll speed is 18m/min;
4th step: stamp: the woollen blanket after sizing is carried out stamp, printing temperature is 70 DEG C, concentrator forms by by low temperature disperse dye, emulsion thickening, softener, shrink-resistant agent, diffusant, dyeing assistant and water, wherein low temperature disperse dye concentration is 2.5%, emulsion thickening concentration is 600g/L, and softer consistency is 5g/L, and shiinkproof finish agent concentration is 20g/L, diffusant concentration is 1g/L, and dyeing assistant concentration is 10g/L, described low temperature disperse dye is produced by Hangzhou Le Cai Chemical Co., Ltd., model is Disperse Red 3B, emulsion thickening is produced by Fine Chemical Works federal in Guangdong, model is EL-80, softener is by Changzhou Mei Sheng biomaterial Co., Ltd, model is Hans LSE, shrink-resistant agent by Dongyang City make the country prosperous Chemical Co., Ltd. produce, model is BF-588, diffusant is extraordinary polyoxyethylene ether is main emulsion, buy from Changzhou Xu Jie textile material Co., Ltd, model is DR, dyeing assistant is produced by Dongguan Jiahong Silicone Technology Co., Ltd., model is Goon701.
5th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, described steam temperature is 130 DEG C, and it is 60min that gas steams the time;
6th step: functional treatment: preparation organo-mineral complexing antibiotic self-cleaning finishing agent, described organo-mineral complexing antibiotic self-cleaning finishing agent is made up of antiseptic, modified nano-titanium dioxide, dispersant, finishing auxiliaries and water, wherein, antimicrobial agent concentration is 40g/L, modified nano-titanium dioxide concentration is 0.8%, dispersant concentration is 10g/L, finishing auxiliaries concentration is 10g/L, woollen blanket just after vapour steaming colour fixing immerses above-mentioned organo-mineral complexing antibiotic self-cleaning finishing agent and adopts single bath process to carry out functional treatment; bath raio is 1: 10, and arranging temperature is 40 DEG C; Described antiseptic is produced by Haining City Haitai Fine Chemical Co., Ltd, model is SHT-108 type, dispersant is produced by Guangdong Demei Fine Chemical Co., Ltd., model is DM-2480, and finishing auxiliaries is fatty alcohol and ethylene oxide condensate, and Nantong Chen Run Chemical Co., Ltd. produces, model is IW, modified nano-titanium dioxide is produced by Haitai Nano Material Co., Ltd., Nanjing, and model is HTTi03-F, and average grain diameter is 20nm.
7th step: washing: the woollen blanket after arranging is washed through three road rinsing bowls successively, 1st rinsing bowl temperature is 45 DEG C, 2nd rinsing bowl temperature is 55 DEG C, 3rd rinsing bowl temperature is 45 DEG C, be water in the 1st described rinsing bowl and the 3rd rinsing bowl, rinsing solution in the 2nd described rinsing bowl is that water adds composite soft finishing agent and obtains, described composite soft finishing agent is made up of softener, smooth agent and antistatic additive, wherein, softer consistency is 5g/L, smooth agent concentration is 12g/L, and antistatic additive concentration is 10g/L; Described softener is produced by Dongguan Jiahong Silicone Technology Co., Ltd., model is Goon1201, and smooth agent is two amido functional group organic silicon emulsions, is produced by upper Haikang Pei Er Industrial Co., Ltd., antistatic additive is produced by Wujiang gold Tyke auxiliary chemicals Co., Ltd, and model is TK-155.
8th step: dry: dried by the woollen blanket after washing, bake out temperature is 85 DEG C, and cloth rewinder roll speed is 8m/min;
9th step: flower base scalds to be cut: the woollen blanket after drying is carried out hot light and scald cutting, and hot light temperature is 170 DEG C, scalds that to cut temperature be 160 DEG C, and cloth rewinder roll speed is all 8m/min;
Tenth step: arrange packing.
The performance test of the biodegradable polyester fiber antibacterial thermal insulating printing woollen blanket of embodiment 1 is as follows:
Ultimate strength (GB/T3923.1-1997): 297N;
Colour fastness to rubbing (GB/T 3920-1997): resistance to dry, wet friction COLOR FASTNESS is 5 grades;
Colour fasteness to sunlight (GB/T 8427-1998): 4-5 level;
Water-fastness COLOR FASTNESS (GB/T 12490-1990): 4-5 level;
Bacteriostasis rate (GB/T 20944.3-2008): 99%;
Warming rate (GB/T 11048-89): 86%.
Embodiment 2
A preparation method for the functional printing woollen blanket of biodegradable polyester fiber, concrete steps are:
The first step: weave: adopt, through braiding technology for making, biodegradable polyester fiber yarn weaving is become woollen blanket, weaving tension is 9g; Described biodegradable polyester fiber yarn is produced by Jiangsu Heshili New Material Co., Ltd., and model is PBST;
Second step: hot light: woollen blanket is carried out hot light, hot light temperature is 180 DEG C, cloth rewinder roll speed 10m/min;
3rd step: sizing: shaped by the woollen blanket after hot light, setting temperature is 110 DEG C, and cloth rewinder roll speed is 20m/min;
4th step: stamp: the woollen blanket after sizing is carried out stamp, printing temperature is 75 DEG C, concentrator forms by by low temperature disperse dye, emulsion thickening, softener, shrink-resistant agent, diffusant, dyeing assistant and water, wherein low temperature disperse dye concentration is 2.4%, emulsion thickening concentration is 620g/L, and softer consistency is 5g/L, and shiinkproof finish agent concentration is 22g/L, diffusant concentration is 1.2g/L, and dyeing assistant concentration is 10g/L, described low temperature disperse dye is produced by Hangzhou Le Cai Chemical Co., Ltd., model is Disperse Red 3B, emulsion thickening is produced by Fine Chemical Works federal in Guangdong, model is EL-80, softener is by Changzhou Mei Sheng biomaterial Co., Ltd, model is Hans LSE, shrink-resistant agent by Dongyang City make the country prosperous Chemical Co., Ltd. produce, model is BF-588, diffusant is extraordinary polyoxyethylene ether is main emulsion, buy from Changzhou Xu Jie textile material Co., Ltd, model is DR, dyeing assistant is produced by Dongguan Jiahong Silicone Technology Co., Ltd., model is Goon701.
5th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, described steam temperature is 120 DEG C, and it is 70min that gas steams the time;
6th step: functional treatment: preparation organo-mineral complexing antibiotic self-cleaning finishing agent, described organo-mineral complexing antibiotic self-cleaning finishing agent is made up of antiseptic, modified nano-titanium dioxide, dispersant, finishing auxiliaries and water, wherein, antimicrobial agent concentration is 45g/L, modified nano-titanium dioxide concentration is 0.9%, dispersant concentration is 12g/L, finishing auxiliaries concentration is 12g/L, woollen blanket just after vapour steaming colour fixing immerses above-mentioned organo-mineral complexing antibiotic self-cleaning finishing agent and adopts single bath process to carry out functional treatment; bath raio is 1: 8, and arranging temperature is 45 DEG C; Described antiseptic is produced by Haining City Haitai Fine Chemical Co., Ltd, model is SHT-108 type, dispersant is produced by Guangdong Demei Fine Chemical Co., Ltd., model is DM-2480, and finishing auxiliaries is fatty alcohol and ethylene oxide condensate, and Nantong Chen Run Chemical Co., Ltd. produces, model is IW, modified nano-titanium dioxide is produced by Haitai Nano Material Co., Ltd., Nanjing, and model is HTTi03-F, and average grain diameter is 20nm.
7th step: washing: the woollen blanket after arranging is washed through three road rinsing bowls successively, 1st rinsing bowl temperature is 40 DEG C, 2nd rinsing bowl temperature is 50 DEG C, 3rd rinsing bowl temperature is 40 DEG C, be water in the 1st described rinsing bowl and the 3rd rinsing bowl, rinsing solution in the 2nd described rinsing bowl is that water adds composite soft finishing agent and obtains, described composite soft finishing agent is made up of softener, smooth agent and antistatic additive, wherein, softer consistency is 6g/L, smooth agent concentration is 15g/L, and antistatic additive concentration is 12g/L; Described softener is produced by Dongguan Jiahong Silicone Technology Co., Ltd., model is Goon1201, and smooth agent is two amido functional group organic silicon emulsions, is produced by upper Haikang Pei Er Industrial Co., Ltd., antistatic additive is produced by Wujiang gold Tyke auxiliary chemicals Co., Ltd, and model is TK-155.
8th step: dry: dried by the woollen blanket after washing, bake out temperature is 90 DEG C, and cloth rewinder roll speed is 6m/min;
9th step: flower base scalds to be cut: the woollen blanket after drying is carried out hot light and scald cutting, and hot light temperature is 160 DEG C, scalds that to cut temperature be 150 DEG C, and cloth rewinder roll speed is all 6m/min;
Tenth step: arrange packing.
The performance test of the biodegradable polyester fiber antibacterial thermal insulating printing woollen blanket of embodiment 2 is as follows:
Ultimate strength (GB/T3923.1-1997): 326N;
Colour fastness to rubbing (GB/T 3920-1997): resistance to dry, wet friction COLOR FASTNESS is 5 grades;
Colour fasteness to sunlight (GB/T 8427-1998): 4-5 level;
Water-fastness COLOR FASTNESS (GB/T 12490-1990): 4-5 level;
Bacteriostasis rate (GB/T 20944.3-2008): 99%; Warming rate (GB/T 11048-89): 86%.
Above-mentioned adopted formula of size, functional treatment agents useful for same formula, composite soft finish agent prescription, working process parameter etc. are only preferred embodiment of the present invention, are not used for limiting practical range of the present invention.Namely all equivalences done according to the content of the present patent application the scope of the claims change and modify, and all should be technology category of the present invention.
Claims (10)
1. a preparation method for the functional printing woollen blanket of biodegradable polyester fiber, it is characterized in that, concrete steps comprise:
The first step: weave: adopt, through braiding technology for making, biodegradable polyester fiber yarn weaving is become woollen blanket, weaving tension is 7 ~ 10g;
Second step: hot light: woollen blanket is carried out hot light, hot light temperature is 180 ~ 200 DEG C, cloth rewinder roll speed 10 ~ 15m/min;
3rd step: sizing: shaped by the woollen blanket after hot light, setting temperature is 110 ~ 130 DEG C, and cloth rewinder roll speed is 16 ~ 20m/min;
4th step: stamp: the woollen blanket after sizing is carried out stamp, printing temperature is 70 ~ 80 DEG C, concentrator contains low temperature disperse dye, emulsion thickening, softener, shrink-resistant agent, diffusant and dyeing assistant, wherein low temperature disperse dye concentration is 2.3 ~ 2.6%, emulsion thickening concentration is 550 ~ 650g/L, and softer consistency is 5 ~ 6g/L, and shiinkproof finish agent concentration is 18 ~ 22g/L, diffusant concentration is 1 ~ 1.5g/L, and dyeing assistant concentration is 8 ~ 12g/L;
5th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, described steam temperature is 120 ~ 140 DEG C, and it is 55 ~ 70min that gas steams the time;
6th step: functional treatment: preparation organo-mineral complexing antibiotic self-cleaning finishing agent, described organo-mineral complexing antibiotic self-cleaning finishing agent contains antiseptic, modified nano-titanium dioxide, dispersant and finishing auxiliaries, wherein, antimicrobial agent concentration is 40 ~ 50g/L, modified nano-titanium dioxide concentration is 0.7 ~ 0.9%, dispersant concentration is 9 ~ 12g/L, finishing auxiliaries concentration is 9 ~ 12g/L, woollen blanket just after vapour steaming colour fixing immerses above-mentioned organo-mineral complexing antibiotic self-cleaning finishing agent and adopts single bath process to carry out functional treatment, bath raio is 1: 8 ~ 1: 10, arranging temperature is 40 ~ 50 DEG C,
7th step: washing: the woollen blanket after arranging is washed through three road rinsing bowls successively, 1st rinsing bowl temperature is 40 DEG C ~ 50 DEG C, 2nd rinsing bowl temperature is 50 DEG C ~ 60 DEG C, 3rd rinsing bowl temperature is 40 DEG C ~ 50 DEG C, and be added with composite soft finishing agent in the 2nd described rinsing bowl, described composite soft finishing agent contains softener, smooth agent and antistatic additive, wherein, softer consistency is 5 ~ 6g/L, and smooth agent concentration is 10 ~ 15g/L, and antistatic additive concentration is 8 ~ 12g/L;
8th step: dry: dried by the woollen blanket after washing, bake out temperature is 80 ~ 90 DEG C, and cloth rewinder roll speed is 6 ~ 10m/min;
9th step: flower base scalds to be cut: the woollen blanket after drying is carried out hot light and scald cutting, and hot light temperature is 160 ~ 180 DEG C, scalds that to cut temperature be 150 ~ 170 DEG C, and cloth rewinder roll speed is all 6 ~ 10m/min;
Tenth step: arrange packing.
2. the preparation method of the functional printing woollen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterized in that, the emulsion thickening in the 4th described step is emulsion thickening EL-80.
3. the preparation method of the functional printing woollen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterized in that, the softener in the 4th described step is softener Hans LSE.
4. the preparation method of the functional printing woollen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterized in that, the shrink-resistant agent in the 4th described step is shrink-resistant agent BF-588.
5. the preparation method of the functional printing woollen blanket of biodegradable polyester fiber as claimed in claim 1, is characterized in that, the diffusant in the 4th described step is polyoxyethylene ether is main emulsion.
6. the preparation method of the functional printing woollen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterized in that, the dyeing assistant in the 4th described step is dyeing assistant Goon701.
7. the preparation method of the functional printing woollen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterized in that, the antiseptic in the 6th described step is antiseptic SHT-108.
8. the preparation method of the functional printing woollen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterized in that, the dispersant in the 6th described step is dispersant DM-2480.
9. the preparation method of the functional printing woollen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterized in that, the finishing auxiliaries in the 6th described step is fatty alcohol and ethylene oxide condensate.
10. the preparation method of the functional printing woollen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterized in that, the softener in the 7th described step is softener Goon1201.
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| CN106592087A (en) * | 2017-02-27 | 2017-04-26 | 山东中奥毯业有限公司 | Preparation method of polyester blanket |
| CN110735336A (en) * | 2019-11-04 | 2020-01-31 | 上海德高服饰有限公司 | Thermal transfer printing process for terylene |
| CN112030420A (en) * | 2020-08-27 | 2020-12-04 | 江苏金太阳纺织科技股份有限公司 | Preparation method of heat-storage antibacterial flannel |
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| CN104278575B (en) | 2016-06-08 |
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