CN104278575B - A kind of preparation method of the functional printed woolen blanket of biodegradable polyester fiber - Google Patents
A kind of preparation method of the functional printed woolen blanket of biodegradable polyester fiber Download PDFInfo
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- CN104278575B CN104278575B CN201410513462.3A CN201410513462A CN104278575B CN 104278575 B CN104278575 B CN 104278575B CN 201410513462 A CN201410513462 A CN 201410513462A CN 104278575 B CN104278575 B CN 104278575B
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Abstract
The preparation method that the invention provides the functional printed woolen blanket of a kind of biodegradable polyester fiber, it is characterised in that concrete steps include: the first step: weaving; Second step: hot light; 3rd step: sizing; 4th step: stamp; 5th step: vapour steaming colour fixing; 6th step: functional treatment; 7th step: washing; 8th step: dry; 9th step: flower base scalds to be cut; Tenth step: arrange packing. The present invention adopts woven technology for making, properly increases hot light temperature, reduces cloth rewinder roll speed so that fiber fully stretches; Adopt strengthening Steaming, it is ensured that a softer and smoother touch and bulkiness of matte; Preparation of nano organo-mineral complexing antibiotic self-cleaning finishing agent, adopts single bath process functional treatment technology, reaches the effect that Durable antibacterial is warming; Adopt 3 groove washing process, and prepare composite flexible finishing agent, to ensure the sense of touch comfortableness of matte. The printed woolen blanket of gained have soft, elastic recovery good, bright in colour and have antibacterial thermal insulating function concurrently.
Description
Technical field
The preparation method that the present invention relates to the functional printed woolen blanket of biodegradable polyester fiber, belongs to textile material technical field.
Background technology
Polyester fiber is because excellent combination property, cost are low and become the textile fabric of maximum application, but polyester fiber is petroleum base synthetic fibers, along with its yield of minimizing of petroleum resources is limited; It addition, polyester fiber can not be degraded, the environmental pollution that its garbage causes is on the rise. Biodegradable polyester fiber is as a kind of aliphatic/aromatic copolyester fiber, it is respectively provided with prominent advantage in flexibility, elastic recovery, anti-crease property, dimensional stability, against weather and easy dyeing etc., and there is good degradability, increasingly cause the concern of people. Compared with conventional polyester fiber, elongation at break and the elastic recovery rate of biodegradable polyester fiber significantly improve, and dyeability significantly improves, thus the functional printed woolen blanket preparation method of existing polyester fiber is not particularly suited for biodegradable polyester fiber.
Summary of the invention
The preparation method that it is an object of the invention to provide the functional printed woolen blanket of biodegradable polyester fiber so that biodegradable polyester fiber can be used in preparing new type functional printed woolen blanket.
In order to achieve the above object, the preparation method that the invention provides the functional printed woolen blanket of a kind of biodegradable polyester fiber, it is characterised in that concrete steps include:
The first step: weaving: adopting woven technology for making that biodegradable polyester fiber yarn weaving is become woollen blanket, weaving tension is 7��10g;
Second step: hot light: woollen blanket is carried out hot light, hot light temperature is 180��200 DEG C, cloth rewinder roll speed 10��15m/min;
3rd step: sizing: being shaped by the woollen blanket after hot light, setting temperature is 110��130 DEG C, and cloth rewinder roll speed is 16��20m/min;
4th step: stamp: the woollen blanket after sizing is carried out stamp, printing temperature is 70��80 DEG C, concentrator contains low temperature disperse dye, emulsion thickening, softening agent, shrink-resistant agent, diffusant and dyeing assistant, wherein low temperature disperse dye concentration is 2.3��2.6%, emulsion thickening concentration is 550��650g/L, and softer consistency is 5��6g/L, and shiinkproof finish agent concentration is 18��22g/L, diffusant concentration is 1��1.5g/L, and dyeing assistant concentration is 8��12g/L;
5th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, described steam temperature is 120��140 DEG C, and the gas steaming time is 55��70min;
6th step: functional treatment: prepare organic inorganic composite antimicrobial self-cleaning finishing agent, described organo-mineral complexing antibiotic self-cleaning finishing agent contains antibacterial, modified nano-titanium dioxide, dispersant and finishing auxiliaries, wherein, antimicrobial agent concentration is 40��50g/L, modified nano-titanium dioxide concentration is 0.7��0.9%, dispersant concentration is 9��12g/L, finishing auxiliaries concentration is 9��12g/L, just woollen blanket after vapour steaming colour fixing immerses above-mentioned organo-mineral complexing antibiotic self-cleaning finishing agent and adopts single bath process to carry out functional treatment, bath raio is 1: 8��1: 10, arranging temperature is 40��50 DEG C,
7th step: washing: the woollen blanket after arrangement is sequentially passed through three road rinsing bowls and washes, 1st rinsing bowl temperature is 40 DEG C��50 DEG C, 2nd rinsing bowl temperature is 50 DEG C��60 DEG C, 3rd rinsing bowl temperature is 40 DEG C��50 DEG C, and added with composite soft finishing agent in the 2nd described rinsing bowl, described composite soft finishing agent contains softening agent, smooth agent and antistatic additive, wherein, softer consistency is 5��6g/L, and smooth agent concentration is 10��15g/L, and antistatic additive concentration is 8��12g/L;
8th step: dry: the woollen blanket after washing is dried, drying temperature is 80��90 DEG C, and cloth rewinder roll speed is 6��10m/min;
9th step: flower base scalds to be cut: the woollen blanket after drying carrying out hot light and scalding and cuts, hot light temperature is 160��180 DEG C, scalds that to cut temperature be 150��170 DEG C, and cloth rewinder roll speed is all 6��10m/min;
Tenth step: arrange packing.
Preferably, the described low temperature disperse dye in the 4th step is Disperse Red 3B.
Preferably, the described emulsion thickening in the 4th step is emulsion thickening EL-80.
Preferably, the described softening agent in the 4th step is softening agent HansLSE.
Preferably, the described shrink-resistant agent in the 4th step is shrink-resistant agent BF-588.
Preferably, the described diffusant in the 4th step is polyoxyethylene ether is the emulsion led.
Preferably, the described dyeing assistant in the 4th step is dyeing assistant Goon701.
Preferably, the described antibacterial in the 6th step is antibacterial SHT-108.
Preferably, the described dispersant in the 6th step is dispersant DM-2480.
Preferably, the described finishing auxiliaries in the 6th step is fatty alcohol and ethylene oxide condensate.
Preferably, the described softening agent in the 7th step is softening agent Goon1201.
Preferably, the described smooth agent in the 7th step is double; two amido functional group organic silicon emulsions.
Preferably, described antistatic additive is antistatic additive TK-155.
Compared with prior art, the invention has the beneficial effects as follows:
The present invention has the features such as good flexibility, elastic recovery and dyeability according to biodegradable polyester fiber, adopts woven technology for making, properly increases hot light temperature, reduces cloth rewinder roll speed so that fiber fully stretches;Adopt strengthening Steaming, it is ensured that a softer and smoother touch and bulkiness of matte; Preparation of nano organo-mineral complexing antibiotic self-cleaning finishing agent, adopts single bath process functional treatment technology, reaches the effect that Durable antibacterial is warming; Adopt 3 groove washing process, and prepare composite flexible finishing agent, to ensure the sense of touch comfortableness of matte. Exploitation have soft, elastic recovery good, bright in colour and have the printed woolen blanket of antibacterial thermal insulating function concurrently. The successful exploitation of this product and popularization and application, to reduce petroleum base synthetic fibers make consumption and protection environment, promoting sustainable development is respectively provided with significance.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is expanded on further. Should be understood that these embodiments are merely to illustrate the present invention rather than restriction the scope of the present invention. In addition, it is to be understood that after having read the content that the present invention lectures, the present invention can be made various changes or modifications by those skilled in the art, and these equivalent form of values fall within the application appended claims limited range equally.
Embodiment 1
The preparation method of the functional printed woolen blanket of a kind of biodegradable polyester fiber, concretely comprises the following steps:
The first step: weaving: adopting woven technology for making that biodegradable polyester fiber yarn weaving is become woollen blanket, weaving tension is 9g; Described biodegradable polyester fiber yarn is produced by Jiangsu Heshili New Material Co., Ltd., and model is PBST;
Second step: hot light: woollen blanket is carried out hot light, hot light temperature is 190 DEG C, cloth rewinder roll speed 8m/min;
3rd step: sizing: being shaped by the woollen blanket after hot light, setting temperature is 120 DEG C, and cloth rewinder roll speed is 18m/min;
4th step: stamp: the woollen blanket after sizing is carried out stamp, printing temperature is 70 DEG C, concentrator is formed by by low temperature disperse dye, emulsion thickening, softening agent, shrink-resistant agent, diffusant, dyeing assistant and water, wherein low temperature disperse dye concentration is 2.5%, emulsion thickening concentration is 600g/L, and softer consistency is 5g/L, and shiinkproof finish agent concentration is 20g/L, diffusant concentration is 1g/L, and dyeing assistant concentration is 10g/L, described low temperature disperse dye is produced by Hangzhou Le Cai Chemical Co., Ltd., model is Disperse Red 3B, emulsion thickening is produced by Fine Chemical Works federal in Guangdong, model is EL-80, softening agent is by Changzhou Mei Sheng biomaterial company limited, model is HansLSE, shrink-resistant agent by Dongyang City make the country prosperous Chemical Co., Ltd. produce, model is BF-588, diffusant is extraordinary polyoxyethylene ether is main emulsion, buy from Changzhou Xu Jie textile material company limited, model is DR, dyeing assistant is produced by Dongguan Jiahong Silicone Technology Co., Ltd., model is Goon701.
5th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, described steam temperature is 130 DEG C, and the gas steaming time is 60min;
6th step: functional treatment: prepare organic inorganic composite antimicrobial self-cleaning finishing agent, described organo-mineral complexing antibiotic self-cleaning finishing agent is made up of antibacterial, modified nano-titanium dioxide, dispersant, finishing auxiliaries and water, wherein, antimicrobial agent concentration is 40g/L, modified nano-titanium dioxide concentration is 0.8%, dispersant concentration is 10g/L, finishing auxiliaries concentration is 10g/L, just woollen blanket after vapour steaming colour fixing immerses above-mentioned organo-mineral complexing antibiotic self-cleaning finishing agent and adopts single bath process to carry out functional treatment; bath raio is 1: 10, and arranging temperature is 40 DEG C;Described antibacterial is produced by Haining City Haitai Fine Chemical Co., Ltd, model is SHT-108 type, dispersant is produced by Guangdong Demei Fine Chemical Co., Ltd., model is DM-2480, and finishing auxiliaries is fatty alcohol and ethylene oxide condensate, and Nantong Chen Run Chemical Co., Ltd. produces, model is IW, modified nano-titanium dioxide is produced by Haitai Nano Material Co., Ltd., Nanjing, and model is HTTi03-F, and mean diameter is 20nm.
7th step: washing: the woollen blanket after arrangement is sequentially passed through three road rinsing bowls and washes, 1st rinsing bowl temperature is 45 DEG C, 2nd rinsing bowl temperature is 55 DEG C, 3rd rinsing bowl temperature is 45 DEG C, the 1st described rinsing bowl and the 3rd rinsing bowl are water, the described rinsing solution in the 2nd rinsing bowl is that the water composite soft finishing agent of interpolation obtains, described composite soft finishing agent is made up of softening agent, smooth agent and antistatic additive, wherein, softer consistency is 5g/L, smooth agent concentration is 12g/L, and antistatic additive concentration is 10g/L; Described softening agent is produced by Dongguan Jiahong Silicone Technology Co., Ltd., model is Goon1201, and smooth agent is double; two amido functional group organic silicon emulsions, upper Haikang Pei Er Industrial Co., Ltd. produce, antistatic additive is produced by gold Tyke, Wujiang auxiliary chemicals company limited, and model is TK-155.
8th step: dry: the woollen blanket after washing is dried, drying temperature is 85 DEG C, and cloth rewinder roll speed is 8m/min;
9th step: flower base scalds to be cut: the woollen blanket after drying carrying out hot light and scalding and cuts, hot light temperature is 170 DEG C, scalds that to cut temperature be 160 DEG C, and cloth rewinder roll speed is all 8m/min;
Tenth step: arrange packing.
The performance test of the biodegradable polyester fiber antibacterial thermal insulating printed woolen blanket of embodiment 1 is as follows:
Ultimate strength (GB/T3923.1-1997): 297N;
Colour fastness to rubbing (GB/T3920-1997): resistance to dry, wet friction color fastness is 5 grades;
Colour fasteness to sunlight (GB/T8427-1998): 4-5 level;
Water-fastness color fastness (GB/T12490-1990): 4-5 level;
Bacteriostasis rate (GB/T20944.3-2008): 99%;
Warming rate (GB/T11048-89): 86%.
Embodiment 2
The preparation method of the functional printed woolen blanket of a kind of biodegradable polyester fiber, concretely comprises the following steps:
The first step: weaving: adopting woven technology for making that biodegradable polyester fiber yarn weaving is become woollen blanket, weaving tension is 9g; Described biodegradable polyester fiber yarn is produced by Jiangsu Heshili New Material Co., Ltd., and model is PBST;
Second step: hot light: woollen blanket is carried out hot light, hot light temperature is 180 DEG C, cloth rewinder roll speed 10m/min;
3rd step: sizing: being shaped by the woollen blanket after hot light, setting temperature is 110 DEG C, and cloth rewinder roll speed is 20m/min;
4th step: stamp: the woollen blanket after sizing is carried out stamp, printing temperature is 75 DEG C, concentrator is formed by by low temperature disperse dye, emulsion thickening, softening agent, shrink-resistant agent, diffusant, dyeing assistant and water, wherein low temperature disperse dye concentration is 2.4%, emulsion thickening concentration is 620g/L, and softer consistency is 5g/L, and shiinkproof finish agent concentration is 22g/L, diffusant concentration is 1.2g/L, and dyeing assistant concentration is 10g/L, described low temperature disperse dye is produced by Hangzhou Le Cai Chemical Co., Ltd., model is Disperse Red 3B, emulsion thickening is produced by Fine Chemical Works federal in Guangdong, model is EL-80, softening agent is by Changzhou Mei Sheng biomaterial company limited, model is HansLSE, shrink-resistant agent by Dongyang City make the country prosperous Chemical Co., Ltd. produce, model is BF-588, diffusant is extraordinary polyoxyethylene ether is main emulsion, buy from Changzhou Xu Jie textile material company limited, model is DR, dyeing assistant is produced by Dongguan Jiahong Silicone Technology Co., Ltd., model is Goon701.
5th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, described steam temperature is 120 DEG C, and the gas steaming time is 70min;
6th step: functional treatment: prepare organic inorganic composite antimicrobial self-cleaning finishing agent, described organo-mineral complexing antibiotic self-cleaning finishing agent is made up of antibacterial, modified nano-titanium dioxide, dispersant, finishing auxiliaries and water, wherein, antimicrobial agent concentration is 45g/L, modified nano-titanium dioxide concentration is 0.9%, dispersant concentration is 12g/L, finishing auxiliaries concentration is 12g/L, just woollen blanket after vapour steaming colour fixing immerses above-mentioned organo-mineral complexing antibiotic self-cleaning finishing agent and adopts single bath process to carry out functional treatment; bath raio is 1: 8, and arranging temperature is 45 DEG C; Described antibacterial is produced by Haining City Haitai Fine Chemical Co., Ltd, model is SHT-108 type, dispersant is produced by Guangdong Demei Fine Chemical Co., Ltd., model is DM-2480, and finishing auxiliaries is fatty alcohol and ethylene oxide condensate, and Nantong Chen Run Chemical Co., Ltd. produces, model is IW, modified nano-titanium dioxide is produced by Haitai Nano Material Co., Ltd., Nanjing, and model is HTTi03-F, and mean diameter is 20nm.
7th step: washing: the woollen blanket after arrangement is sequentially passed through three road rinsing bowls and washes, 1st rinsing bowl temperature is 40 DEG C, 2nd rinsing bowl temperature is 50 DEG C, 3rd rinsing bowl temperature is 40 DEG C, the 1st described rinsing bowl and the 3rd rinsing bowl are water, the described rinsing solution in the 2nd rinsing bowl is that the water composite soft finishing agent of interpolation obtains, described composite soft finishing agent is made up of softening agent, smooth agent and antistatic additive, wherein, softer consistency is 6g/L, smooth agent concentration is 15g/L, and antistatic additive concentration is 12g/L; Described softening agent is produced by Dongguan Jiahong Silicone Technology Co., Ltd., model is Goon1201, and smooth agent is double; two amido functional group organic silicon emulsions, upper Haikang Pei Er Industrial Co., Ltd. produce, antistatic additive is produced by gold Tyke, Wujiang auxiliary chemicals company limited, and model is TK-155.
8th step: dry: the woollen blanket after washing is dried, drying temperature is 90 DEG C, and cloth rewinder roll speed is 6m/min;
9th step: flower base scalds to be cut: the woollen blanket after drying carrying out hot light and scalding and cuts, hot light temperature is 160 DEG C, scalds that to cut temperature be 150 DEG C, and cloth rewinder roll speed is all 6m/min;
Tenth step: arrange packing.
The performance test of the biodegradable polyester fiber antibacterial thermal insulating printed woolen blanket of embodiment 2 is as follows:
Ultimate strength (GB/T3923.1-1997): 326N;
Colour fastness to rubbing (GB/T3920-1997): resistance to dry, wet friction color fastness is 5 grades;
Colour fasteness to sunlight (GB/T8427-1998): 4-5 level;
Water-fastness color fastness (GB/T12490-1990): 4-5 level;
Bacteriostasis rate (GB/T20944.3-2008): 99%; Warming rate (GB/T11048-89): 86%.
Above-mentioned adopted formula of size, functional treatment agents useful for same formula, composite soft finish agent prescription, working process parameter etc. are only presently preferred embodiments of the present invention, are not used for limiting the practical range of the present invention. Namely all equivalences made according to the content of the present patent application the scope of the claims change and modify, and all should be the technology category of the present invention.
Claims (10)
1. the preparation method of the functional printed woolen blanket of biodegradable polyester fiber, it is characterised in that concrete steps include:
The first step: weaving: adopting woven technology for making that biodegradable polyester fiber yarn weaving is become woollen blanket, weaving tension is 7 ~ 10g;
Second step: hot light: woollen blanket is carried out hot light, hot light temperature is 180 ~ 200 DEG C, cloth rewinder roll speed 10 ~ 15m/min;
3rd step: sizing: being shaped by the woollen blanket after hot light, setting temperature is 110 ~ 130 DEG C, and cloth rewinder roll speed is 16 ~ 20m/min;
4th step: stamp: the woollen blanket after sizing is carried out stamp, printing temperature is 70 ~ 80 DEG C, concentrator contains low temperature disperse dye, emulsion thickening, softening agent, shrink-resistant agent, diffusant and dyeing assistant, wherein low temperature disperse dye concentration is 2.3 ~ 2.6%, emulsion thickening concentration is 550 ~ 650g/L, and softer consistency is 5 ~ 6g/L, and shiinkproof finish agent concentration is 18 ~ 22g/L, diffusant concentration is 1 ~ 1.5g/L, and dyeing assistant concentration is 8 ~ 12g/L;
5th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, described steam temperature is 120 ~ 140 DEG C, and steaming time is 55 ~ 70min;
6th step: functional treatment: prepare organic inorganic composite antimicrobial self-cleaning finishing agent, described organo-mineral complexing antibiotic self-cleaning finishing agent contains antibacterial, modified nano-titanium dioxide, dispersant and finishing auxiliaries, wherein, antimicrobial agent concentration is 40 ~ 50g/L, modified nano-titanium dioxide concentration is 0.7 ~ 0.9%, dispersant concentration is 9 ~ 12g/L, finishing auxiliaries concentration is 9 ~ 12g/L, woollen blanket after vapour steaming colour fixing immerses above-mentioned organo-mineral complexing antibiotic self-cleaning finishing agent adopts single bath process to carry out functional treatment, bath raio is 1:8 ~ 1:10, arranging temperature is 40 ~ 50 DEG C,
7th step: washing: the woollen blanket after arrangement is sequentially passed through three road rinsing bowls and washes, 1st rinsing bowl temperature is 40 DEG C ~ 50 DEG C, 2nd rinsing bowl temperature is 50 DEG C ~ 60 DEG C, 3rd rinsing bowl temperature is 40 DEG C ~ 50 DEG C, and added with composite soft finishing agent in the 2nd described rinsing bowl, described composite soft finishing agent contains softening agent, smooth agent and antistatic additive, wherein, softer consistency is 5 ~ 6g/L, and smooth agent concentration is 10 ~ 15g/L, and antistatic additive concentration is 8 ~ 12g/L;
8th step: dry: the woollen blanket after washing is dried, drying temperature is 80 ~ 90 DEG C, and cloth rewinder roll speed is 6 ~ 10m/min;
9th step: flower base scalds to be cut: the woollen blanket after drying carrying out hot light and scalding and cuts, hot light temperature is 160 ~ 180 DEG C, scalds that to cut temperature be 150 ~ 170 DEG C, and cloth rewinder roll speed is all 6 ~ 10m/min;
Tenth step: arrange packing.
2. the preparation method of the functional printed woolen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterised in that the described emulsion thickening in the 4th step is emulsion thickening EL-80.
3. the preparation method of the functional printed woolen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterised in that the described softening agent in the 4th step is softening agent HansLSE.
4. the preparation method of the functional printed woolen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterised in that the described shrink-resistant agent in the 4th step is shrink-resistant agent BF-588.
5. the preparation method of the functional printed woolen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterised in that the described diffusant in the 4th step is polyoxyethylene ether is the emulsion led.
6. the preparation method of the functional printed woolen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterised in that the described dyeing assistant in the 4th step is dyeing assistant Goon701.
7. the preparation method of the functional printed woolen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterised in that the described antibacterial in the 6th step is antibacterial SHT-108.
8. the preparation method of the functional printed woolen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterised in that the described dispersant in the 6th step is dispersant DM-2480.
9. the preparation method of the functional printed woolen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterised in that the described finishing auxiliaries in the 6th step is fatty alcohol and ethylene oxide condensate.
10. the preparation method of the functional printed woolen blanket of biodegradable polyester fiber as claimed in claim 1, it is characterised in that the described softening agent in the 7th step is softening agent Goon1201.
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| CN106592087A (en) * | 2017-02-27 | 2017-04-26 | 山东中奥毯业有限公司 | Preparation method of polyester blanket |
| CN110735336A (en) * | 2019-11-04 | 2020-01-31 | 上海德高服饰有限公司 | Thermal transfer printing process for terylene |
| CN112030420A (en) * | 2020-08-27 | 2020-12-04 | 江苏金太阳纺织科技股份有限公司 | Preparation method of heat-storage antibacterial flannel |
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