CN104250510A - Solvent-free epoxy self-leveling roller coating floor paint and preparation and use method thereof - Google Patents
Solvent-free epoxy self-leveling roller coating floor paint and preparation and use method thereof Download PDFInfo
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Abstract
The invention relates to a solvent-free epoxy self-leveling roller coating floor paint and a preparation and use method thereof. The paint comprises a low-viscosity epoxy resin compound, an active diluent, an inactive diluent, a defoamer, a leveling agent, a wetting dispersant, a thixotropic additive, a solvent-free phthalocyanine blue pulp, a solvent-free lemon yellow pulp, a solvent-free titanium white pulp, a solvent-free carbon black pulp, quartz powder, precipitated barium sulfate and a modified alicyclic amine curing agent. The preparation and use method comprises the following steps: preparation of various solvent-free individual color pulps, preparation of a component A and use manner; the low-viscosity epoxy resin compound is a compound of bisphenol-A epoxy resin and bisphenol-F epoxy resin, the viscosity of the compounding system is greatly reduced under the condition of no solvents, the viscosity of the solvent-free system is improved, the amount of the active diluents and the inactive diluents is reduced, the physical mechanical performances of coatings are guaranteed and the paint is endowed with excellent levelability, so that the paint disclosed by the invention has roller coating self levelability and excellent construction performance.
Description
Technical field
The invention belongs to environment-friendly type terrace technical field of coatings, refer more particularly to a kind of solvent-free epoxy self-leveling roller coat terrace paint and preparation using method.
Background technology
Terrace paint just started to apply gradually in the nineties in last century, but terrace paint industry development is rapid, substantially all modern plants all bring into use terrace paint at present, within 2011, the terrace paint output value is more than 18,000,000,000 yuan, developing rapidly particularly along with modern industrial technology and production, the production environment of owner to factory building, workshop proposes more and more higher requirement, require that terrace paint is corrosion-resistant, clean and wear-resisting, room air dustiness is low, operating efficiency is high, this is not only the demand of improving working conditions, especially the guarantee of modern product quality.
Epoxy flooring coating dominate in industry ground slab, in epoxy flooring coating, about 80% is solvent-borne type, and solvent based coating can discharge a large amount of volatile organic matter VOC in production, construction and solidification process, volatile organic matter not only affects the healthy of people, and can cause environmental pollution.
Solventless Epoxy Self-Leveling Floor Coatings viscosity is comparatively large, levelling property is not good, and the sawtooth trowel trowel painting mode that adopts is constructed more, and easily cause trowel trace, and will reach Self-leveling effect, coated designs thickness is large, and industrial application cost is high.
All merely disclose a kind of non-solvent epoxy floor paint and manufacture method thereof in Chinese patent CN103409042A and CN103555145A, the consumption of this floor paint and form of construction work are not described.
No-solvent type epoxy self-leveling floor coating and preparation method thereof and using method disclosed in Chinese patent CN103525249A, this no-solvent type epoxy self-leveling floor coating finish paint adopts trowel to be coated with mode and constructs, film forming thickness reaches 2 ~ 3mm, and theoretical usage quantity reaches 3.2 ~ 4.8kg/m
2, not only construction doses is wasted, and one film forming thickness is large, and great paint film force of cohesion likely destroys the concrete structure of substrate, causes terrace to destroy.
To sum up, there is easy construction, solvent-free terrace paint widely applicable, with low cost yet there are no relevant report.
Summary of the invention
For solving the problem, the invention provides a kind of solvent-free epoxy self-leveling roller coat terrace paint and preparation using method, easy construction, widely applicable, with low cost, the solvent-free epoxy self-leveling roller coat terrace finish paint of workability, mechanical property and antiseptic property excellence.
Object of the present invention is achieved through the following technical solutions:
A kind of solvent-free epoxy self-leveling roller coat terrace paint, first component in this terrace paint contains low viscosity epoxy resin mixture, reactive thinner, non-activated thinner, defoamer, flow agent, wetting dispersing agent, thixotropic agents, silica powder and process white, second component in this terrace paint is modification aliphatic cyclic amine solidifying agent, and feature of the present invention is as follows:
Also containing solvent-free phthalocyanine blue slurry, solvent-free lemon yellow slurry, solvent-free titanium dioxide slurry and solvent-free carbon black in described first component.
Described first component proportioning all is by weight as follows:
Low viscosity epoxy resin mixture 120 ~ 160 parts, reactive thinner 10 ~ 15 parts, non-activated thinner 10 ~ 15 parts, defoamer 0.3 ~ 2.4 part, flow agent 3 ~ 6 parts, wetting dispersing agent 1.0 ~ 2.0 parts, thixotropic agents 1.3 ~ 1.8 parts, solvent-free 0.032 ~ 0.06 part, phthalocyanine blue slurry, solvent-free 0.032 ~ 1.92 part, lemon yellow slurry, solvent-free titanium dioxide slurry 32.8 ~ 39.6 parts, solvent-free carbon black 0.44 ~ 0.9 part, silica powder 50 ~ 80 parts, process white 50 ~ 80 parts.
Blend in process actual, the addition of solvent-free phthalocyanine blue slurry, solvent-free lemon yellow slurry, solvent-free titanium dioxide slurry and solvent-free carbon black can be added and subtracted in right amount according to mixed colours demand, and said ratio is the reference value under a kind of particular case.
Above-mentioned low viscosity epoxy resin mixture is the mixture of bisphenol A type epoxy resin and bisphenol f type epoxy resin, bisphenol A type epoxy resin: bisphenol f type epoxy resin=10:{2 ~ 6}, and this ratio by mass part is counted.
Further, bisphenol A type epoxy resin is CYD-128E, and bisphenol f type epoxy resin is GEFR170, and CYD-128E is by Ba Ling petrochemical iy produced in suggestion, and suggestion GEFR170 is produced by Guangdong Hong Chang
.
Above-mentioned reactive thinner is any one in 10 two to tetradecyl glycidyl ether AGE and n-butyl glycidyl ether BGE, or its two kinds of compositions.
Above-mentioned non-activated thinner is phenylcarbinol.
Above-mentioned defoamer be BYK-A530,6800 and Foamex N in any one, BYK-A530 is by Bi Ke chemical production in suggestion, and suggestion 6800 is produced by moral modest (Shanghai) Chemical Co., Ltd., and suggestion Foamex N is produced by Ying Chuan Specialty Chemical company limited.
Above-mentioned flow agent is any one in BYK-354 and BYK-358N, or its two kinds of compositions, BYK-354 and BYK-358N is by Bi Ke chemical production in suggestion.
Above-mentioned wetting dispersing agent is any one in BYK-220s and BYK-P104s, BYK-220s and BYK-P104s is by Bi Ke chemical production in suggestion.
Above-mentioned thixotropic agent is organobentonite
bP-881, suggestion BP-881 is produced by Taiyuan Mei Te Xiang.
Above-mentioned solvent-free phthalocyanine blue slurry proportioning all is by weight as follows:
The GEFR170 resin of 100 parts, the reactive thinner AGE of 10 parts, the phthalocyanine blue pigment of 10 parts, the wetting dispersing agent BYK-9076 of 5 parts, the silica powder of 100 parts.
Above-mentioned solvent-free lemon yellow slurry proportioning all is by weight as follows:
The GEFR170 resin of 100 parts, the reactive thinner AGE of 10 parts, the lemon yellow pigment of 100 parts, the wetting dispersing agent BYK-110 of 4 parts.
Above-mentioned solvent-free titanium dioxide slurry proportioning all is by weight as follows:
The GEFR170 resin of 100 parts, the reactive thinner AGE of 10 parts, the anatase thpe white powder of 100 parts, the wetting dispersing agent BYK-110 of 4 parts.
Above-mentioned solvent-free carbon black proportioning all is by weight as follows:
The GEFR170 resin of 100 parts, the reactive thinner AGE of 10 parts, the charcoal blacks of 10 parts, the wetting dispersing agent BYK-110 of 1 part, the silica powder of 100 parts.
Above-mentioned wetting dispersing agent BYK-9076 and BYK-110 advises by Bi Ke chemical production.
Above-mentioned silica powder need sieve through 600 orders.
Above-mentioned process white need sieve through 800 orders.
Above-mentioned modification aliphatic cyclic amine solidifying agent is H-3368 solidifying agent, and suggestion H-3368 solidifying agent is produced by Shenzhen Ye Xu Industrial Co., Ltd.
.
Described first component: described component B={ 4 ~ 6}:1, this ratio by mass part is counted.
A preparation using method for solvent-free epoxy self-leveling roller coat terrace paint, this prepare using method comprise various solvent-free monochrome slurry preparation, the preparation of first component, use-pattern three steps, each step is described below:
The preparation of I various solvent-free monochrome slurry
Various solvent-free monochrome slurry comprises solvent-free phthalocyanine blue slurry, solvent-free lemon yellow slurry, solvent-free titanium dioxide slurry and solvent-free carbon black.
The preparation of solvent-free phthalocyanine blue slurry: by the phthalocyanine blue pigment of the wetting dispersing agent of the reactive thinner AGE of the GEFR170 of 100 weight parts, 10 weight parts, 5 weight parts, 10 weight parts, 100 weight parts to add successively in dispersator through the silica powder that 600 orders sieve and stir 10 minutes under rotating speed at 400 ~ 600r/min, with the dispersion of sand mill sand milling after stirring, when fineness reaches 20 um, prepare solvent-free phthalocyanine blue slurry for subsequent use.
The preparation of solvent-free lemon yellow slurry: the lemon yellow pigment of the reactive thinner AGE of the GEFR170 resin of 100 weight parts, 10 weight parts, 100 weight parts, the wetting dispersing agent BYK-110 of 4 weight parts to be added successively in dispersator and to stir 10 minutes under the rotating speed of 400 ~ 600r/min, with the dispersion of sand mill sand milling after stirring, when fineness reaches 20 um, prepare solvent-free lemon yellow slurry for subsequent use.
The preparation of solvent-free titanium dioxide slurry: the anatase thpe white powder of the reactive thinner AGE of the GEFR170 resin of 100 weight parts, 10 weight parts, 100 weight parts, the wetting dispersing agent BYK-110 of 4 weight parts to be added successively in dispersator and to stir 10 minutes under the rotating speed of 400 ~ 600r/min, with the dispersion of sand mill sand milling after stirring, when fineness reaches 20 um, prepare solvent-free titanium dioxide slurry for subsequent use.
The preparation of solvent-free carbon black: by the wetting dispersing agent BYK-110 of the charcoal blacks of the reactive thinner AGE of the GEFR170 resin of 100 weight parts, 10 weight parts, 10 weight parts, 1 weight part, 100 weight parts to add successively in dispersator through the silica powder that 600 orders sieve and stir 10 minutes under rotating speed at 400 ~ 600r/min, with the dispersion of sand mill sand milling after stirring, when fineness reaches 20 um, prepare solvent-free carbon black for subsequent use.
The preparation of II first component
First component comprises low viscosity epoxy resin mixture, reactive thinner, non-activated thinner, defoamer, flow agent, wetting dispersing agent, thixotropic agents, solvent-free phthalocyanine blue slurry, solvent-free lemon yellow slurry, solvent-free titanium dioxide slurry and solvent-free carbon black, silica powder and process white, be wherein the mixture of bisphenol A type epoxy resin and bisphenol f type epoxy resin, described mixture allocation ratio is by weight: bisphenol A type epoxy resin: bisphenol f type epoxy resin=10:{2 ~ 6}.
First the described mixture of 120 ~ 160 weight parts is added in dispersing stirrer, respectively by the reactive thinner of 10 ~ 15 weight parts under the rotating speed of 400 ~ 600r/min, the thixotropic agents of 1.3 ~ 1.8 weight parts, the wetting dispersing agent of 1.0 ~ 2.0 weight parts adds in dispersing stirrer and stirs 10 ~ 20 minutes, to be mixed evenly after the rotating speed of dispersing stirrer is increased to the non-activated thinner that 1000 ~ 1500r/min adds 10 ~ 15 weight parts more successively, the flow agent of 3 ~ 6 weight parts, the defoamer of 0.3 ~ 2.4 weight part, the solvent-free phthalocyanine blue slurry of 0.032 ~ 0.06 weight part, the solvent-free lemon yellow slurry of 0.032 ~ 1.92 weight part, the solvent-free titanium dioxide slurry of 32.8 ~ 39.6 weight parts, the solvent-free carbon black of 0.44 ~ 0.9 weight part, 50 ~ 80 weight parts the silica powder sieved through 600 orders, 50 ~ 80 weight parts the process white sieved through 800 orders, high speed dispersion was filtered through 60 eye mesh screens after 15 ~ 25 minutes, prepare first component.
III use-pattern
In first component, component B is added when scene is blent, second component is modification aliphatic cyclic amine solidifying agent, first component and the component B ratio of blending by weight is: first component: component B={ 4 ~ 6}:1 blends standing 5 minutes froth breakings after stirring and prepares solvent-free epoxy self-leveling roller coat terrace paint.
In adopting during use, hair roller carries out roller coat application with roll coating model in the substrate carrying out screed-coat, and the gauge control of single track film is at 300 ~ 500 um, and theoretical amount controls at 0.4 ~ 0.6kg/m
2, after ambient cure 24h, namely complete coating decoration.
In preparation using method, the concrete title of each raw material is identical with above-mentioned solvent-free epoxy self-leveling roller coat terrace paint, does not separately repeat.
Owing to adopting technical scheme described above, the present invention produces following beneficial effect:
1, the present invention adopts the compound system of bisphenol A type epoxy resin and bisphenol f type epoxy resin, the viscosity of this compound system is greatly reduced when not adding solvent, improve the viscosity of solvent-free system, decrease use that is active and non-activated thinner, while ensureing film physical and mechanical properties, give coating good levelling property, thus making coating of the present invention possess roller coat self-leveling, workability is excellent.
2, the present invention adopts various solvent-free monochrome slurry to mix colours, the preparation process of coating is without the need to sand milling, and preparation technology is simple, improves production efficiency, and the toning of various solvent-free monochrome slurry can reduce the floating phenomenon in coating application process, gives coating better apparent state.
3, coating of the present invention can adopt roller application, and single track film thickness can reach 300 ~ 500 um, and theoretical amount is only 0.4 ~ 0.6kg/m
2; Although application consumption is less, film physical and mechanical properties is excellent, and preservative property are strong, and coating good leveling property, and the apparent full color of film is homogeneous, and painting effect is good.
Embodiment
Below in conjunction with embodiment, further detailed description is done to the present invention, but embodiments of the present invention are not limited thereto.
Following table is the proportioning raw materials of embodiment 1-3:
The preparation using method of solvent-free epoxy self-leveling roller coat terrace paint, see technical scheme of the present invention, does not separately repeat.
Establishing criteria GBT 22374-2008 " terrace coating material " and HGT 3829-2006 " terrace paint " correlated performance to embodiment 1-3 are tested, under its test result is shown in
table:
Upper table absolutely proves:
1, the solvent-free epoxy self-leveling roller coat terrace paint that the present invention prepares has the feature such as physical and mechanical properties and antiseptic property excellence, this is that what to adopt due to resin system of the present invention is dihydroxyphenyl propane and bisphenol F resin compound system, to arrange in pairs or groups appropriate thinner, system viscosity is little, good leveling property, therefore can adopt roll coating model, single track scumbling can realize Self-leveling effect.
2, the solvent-free epoxy self-leveling roller coat terrace paint that the present invention prepares has easy construction, and painting cost is low, and terrace full color is homogeneous, and levelling property is good, smooth, without floating phenomenon, has good mirror effect.
3, do not contain solvent in coating of the present invention, adopt the color coordinate of various solvent-free monochrome slurry, it is good that various solvent-free monochrome slurry has dispersion effect, and therefore without floating phenomenon, film full color, has good mirror effect.
4, owing to have employed modification aliphatic cyclic amine solidifying agent H-3368 of good performance, can be good with composite curable epoxy resin, impart physical and mechanical properties and the antiseptic property of paint film excellence.
Above-mentioned three embodiments are the present invention's preferably embodiments; but embodiments of the present invention are not restricted to the described embodiments; other is any do not deviate from spirit of the present invention and principle under do change, modification, substitute, combine, simplify; all should be the substitute mode of equivalence, be all included within protection scope of the present invention.
Claims (2)
1. a solvent-free epoxy self-leveling roller coat terrace paint, first component in this terrace paint contains low viscosity epoxy resin mixture, reactive thinner, non-activated thinner, defoamer, flow agent, wetting dispersing agent, thixotropic agents, silica powder and process white, second component in this terrace paint is modification aliphatic cyclic amine solidifying agent, it is characterized in that:
Also containing solvent-free phthalocyanine blue slurry, solvent-free lemon yellow slurry, solvent-free titanium dioxide slurry and solvent-free carbon black in described first component;
Described first component proportioning all is by weight as follows:
Low viscosity epoxy resin mixture 120 ~ 160 parts, reactive thinner 10 ~ 15 parts, non-activated thinner 10 ~ 15 parts, defoamer 0.3 ~ 2.4 part, flow agent 3 ~ 6 parts, wetting dispersing agent 1.0 ~ 2.0 parts, thixotropic agents 1.3 ~ 1.8 parts, solvent-free 0.032 ~ 0.06 part, phthalocyanine blue slurry, solvent-free 0.032 ~ 1.92 part, lemon yellow slurry, solvent-free titanium dioxide slurry 32.8 ~ 39.6 parts, solvent-free carbon black 0.44 ~ 0.9 part, silica powder 50 ~ 80 parts, process white 50 ~ 80 parts;
Above-mentioned low viscosity epoxy resin mixture is the mixture of bisphenol A type epoxy resin and bisphenol f type epoxy resin, bisphenol A type epoxy resin: bisphenol f type epoxy resin=10:{2 ~ 6}, and this ratio by mass part is counted;
Further, bisphenol A type epoxy resin is CYD-128E, and bisphenol f type epoxy resin is GEFR170
;
Above-mentioned reactive thinner is any one in 10 two to tetradecyl glycidyl ether AGE and n-butyl glycidyl ether BGE, or its two kinds of compositions;
Above-mentioned non-activated thinner is phenylcarbinol;
Above-mentioned defoamer be BYK-A530,6800 and Foamex N in any one;
Above-mentioned flow agent is any one in BYK-354 and BYK-358N, or its two kinds of compositions;
Above-mentioned wetting dispersing agent is any one in BYK-220s and BYK-P104s;
Above-mentioned thixotropic agent is organobentonite
bP-881;
Above-mentioned solvent-free phthalocyanine blue slurry proportioning all is by weight as follows:
The GEFR170 resin of 100 parts, the reactive thinner AGE of 10 parts, the phthalocyanine blue pigment of 10 parts, the wetting dispersing agent BYK-9076 of 5 parts, the silica powder of 100 parts;
Above-mentioned solvent-free lemon yellow slurry proportioning all is by weight as follows:
The GEFR170 resin of 100 parts, the reactive thinner AGE of 10 parts, the lemon yellow pigment of 100 parts, the wetting dispersing agent BYK-110 of 4 parts;
Above-mentioned solvent-free titanium dioxide slurry proportioning all is by weight as follows:
The GEFR170 resin of 100 parts, the reactive thinner AGE of 10 parts, the anatase thpe white powder of 100 parts, the wetting dispersing agent BYK-110 of 4 parts;
Above-mentioned solvent-free carbon black proportioning all is by weight as follows:
The GEFR170 resin of 100 parts, the reactive thinner AGE of 10 parts, the charcoal blacks of 10 parts, the wetting dispersing agent BYK-110 of 1 part, the silica powder of 100 parts;
Above-mentioned silica powder need sieve through 600 orders;
Above-mentioned process white need sieve through 800 orders;
Above-mentioned modification aliphatic cyclic amine solidifying agent is H-3368 solidifying agent
;
Described first component: described component B={ 4 ~ 6}:1, this ratio by mass part is counted.
2. a preparation using method for solvent-free epoxy self-leveling roller coat terrace paint, this prepare using method comprise various solvent-free monochrome slurry preparation, the preparation of first component, use-pattern three steps, it is characterized in that:
The preparation of I various solvent-free monochrome slurry
Various solvent-free monochrome slurry comprises solvent-free phthalocyanine blue slurry, solvent-free lemon yellow slurry, solvent-free titanium dioxide slurry and solvent-free carbon black;
The preparation of solvent-free phthalocyanine blue slurry: by the phthalocyanine blue pigment of the wetting dispersing agent of the reactive thinner AGE of the GEFR170 of 100 weight parts, 10 weight parts, 5 weight parts, 10 weight parts, 100 weight parts to add successively in dispersator through the silica powder that 600 orders sieve and stir 10 minutes under rotating speed at 400 ~ 600r/min, with the dispersion of sand mill sand milling after stirring, when fineness reaches 20 um, prepare solvent-free phthalocyanine blue slurry for subsequent use;
The preparation of solvent-free lemon yellow slurry: the lemon yellow pigment of the reactive thinner AGE of the GEFR170 resin of 100 weight parts, 10 weight parts, 100 weight parts, the wetting dispersing agent BYK-110 of 4 weight parts to be added successively in dispersator and to stir 10 minutes under the rotating speed of 400 ~ 600r/min, with the dispersion of sand mill sand milling after stirring, when fineness reaches 20 um, prepare solvent-free lemon yellow slurry for subsequent use;
The preparation of solvent-free titanium dioxide slurry: the anatase thpe white powder of the reactive thinner AGE of the GEFR170 resin of 100 weight parts, 10 weight parts, 100 weight parts, the wetting dispersing agent BYK-110 of 4 weight parts to be added successively in dispersator and to stir 10 minutes under the rotating speed of 400 ~ 600r/min, with the dispersion of sand mill sand milling after stirring, when fineness reaches 20 um, prepare solvent-free titanium dioxide slurry for subsequent use;
The preparation of solvent-free carbon black: by the wetting dispersing agent BYK-110 of the charcoal blacks of the reactive thinner AGE of the GEFR170 resin of 100 weight parts, 10 weight parts, 10 weight parts, 1 weight part, 100 weight parts to add successively in dispersator through the silica powder that 600 orders sieve and stir 10 minutes under rotating speed at 400 ~ 600r/min, with the dispersion of sand mill sand milling after stirring, when fineness reaches 20 um, prepare solvent-free carbon black for subsequent use;
The preparation of II first component
First component comprises low viscosity epoxy resin mixture, reactive thinner, non-activated thinner, defoamer, flow agent, wetting dispersing agent, thixotropic agents, solvent-free phthalocyanine blue slurry, solvent-free lemon yellow slurry, solvent-free titanium dioxide slurry and solvent-free carbon black, silica powder and process white, be wherein the mixture of bisphenol A type epoxy resin and bisphenol f type epoxy resin, described mixture allocation ratio is by weight: bisphenol A type epoxy resin: bisphenol f type epoxy resin=10:{2 ~ 6};
First the described mixture of 120 ~ 160 weight parts is added in dispersing stirrer, respectively by the reactive thinner of 10 ~ 15 weight parts under the rotating speed of 400 ~ 600r/min, the thixotropic agents of 1.3 ~ 1.8 weight parts, the wetting dispersing agent of 1.0 ~ 2.0 weight parts adds in dispersing stirrer and stirs 10 ~ 20 minutes, to be mixed evenly after the rotating speed of dispersing stirrer is increased to the non-activated thinner that 1000 ~ 1500r/min adds 10 ~ 15 weight parts more successively, the flow agent of 3 ~ 6 weight parts, the defoamer of 0.3 ~ 2.4 weight part, the solvent-free phthalocyanine blue slurry of 0.032 ~ 0.06 weight part, the solvent-free lemon yellow slurry of 0.032 ~ 1.92 weight part, the solvent-free titanium dioxide slurry of 32.8 ~ 39.6 weight parts, the solvent-free carbon black of 0.44 ~ 0.9 weight part, 50 ~ 80 weight parts the silica powder sieved through 600 orders, 50 ~ 80 weight parts the process white sieved through 800 orders, high speed dispersion was filtered through 60 eye mesh screens after 15 ~ 25 minutes, prepare first component,
III use-pattern
In first component, component B is added when scene is blent, second component is modification aliphatic cyclic amine solidifying agent, first component and the component B ratio of blending by weight is: first component: component B={ 4 ~ 6}:1, blends standing 5 minutes froth breakings after stirring and prepare solvent-free epoxy self-leveling roller coat terrace paint;
In adopting during use, hair roller carries out roller coat application with roll coating model in the substrate carrying out screed-coat, and the gauge control of single track film is at 300 ~ 500 um, and theoretical amount controls at 0.4 ~ 0.6kg/m
2, after ambient cure 24h, namely complete coating decoration.
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